CN1114345C - Process for preparing insecticide for mosquito, fly and roach - Google Patents
Process for preparing insecticide for mosquito, fly and roach Download PDFInfo
- Publication number
- CN1114345C CN1114345C CN00124870A CN00124870A CN1114345C CN 1114345 C CN1114345 C CN 1114345C CN 00124870 A CN00124870 A CN 00124870A CN 00124870 A CN00124870 A CN 00124870A CN 1114345 C CN1114345 C CN 1114345C
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- China
- Prior art keywords
- insecticide
- grams
- seminal fluid
- flies
- tetramethrin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000002917 insecticide Substances 0.000 title claims abstract description 40
- 241000255925 Diptera Species 0.000 title claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 241000231739 Rutilus rutilus Species 0.000 title 1
- 241001674044 Blattodea Species 0.000 claims abstract description 24
- CXBMCYHAMVGWJQ-CABCVRRESA-N (1,3-dioxo-4,5,6,7-tetrahydroisoindol-2-yl)methyl (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OCN1C(=O)C(CCCC2)=C2C1=O CXBMCYHAMVGWJQ-CABCVRRESA-N 0.000 claims abstract description 13
- 239000005946 Cypermethrin Substances 0.000 claims abstract description 13
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract description 13
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 13
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229960005424 cypermethrin Drugs 0.000 claims abstract description 13
- 229960005199 tetramethrin Drugs 0.000 claims abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 230000001476 alcoholic effect Effects 0.000 claims abstract description 3
- 241000256113 Culicidae Species 0.000 claims description 19
- 241001104043 Syringa Species 0.000 claims description 16
- 235000004338 Syringa vulgaris Nutrition 0.000 claims description 16
- 210000000582 semen Anatomy 0.000 claims description 16
- 241000723346 Cinnamomum camphora Species 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 9
- 239000003380 propellant Substances 0.000 claims description 8
- 241000723353 Chrysanthemum Species 0.000 claims description 7
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 7
- 150000002148 esters Chemical class 0.000 claims description 7
- 239000000443 aerosol Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 241000894006 Bacteria Species 0.000 abstract description 2
- 230000003211 malignant effect Effects 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- VQXSOUPNOZTNAI-UHFFFAOYSA-N Pyrethrin I Natural products CC(=CC1CC1C(=O)OC2CC(=O)C(=C2C)CC=C/C=C)C VQXSOUPNOZTNAI-UHFFFAOYSA-N 0.000 abstract 2
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 abstract 2
- -1 pyrethrin compound Chemical class 0.000 abstract 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 abstract 1
- 229940025250 camphora Drugs 0.000 abstract 1
- 239000010238 camphora Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 238000003912 environmental pollution Methods 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 12
- 239000000047 product Substances 0.000 description 10
- 239000000843 powder Substances 0.000 description 5
- 241000238631 Hexapoda Species 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000001665 lethal effect Effects 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 231100000053 low toxicity Toxicity 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- LNJXZKBHJZAIKQ-UHFFFAOYSA-N 1,1,1,2-tetrachloro-3-(2,3,3,3-tetrachloropropoxy)propane Chemical compound ClC(Cl)(Cl)C(Cl)COCC(Cl)C(Cl)(Cl)Cl LNJXZKBHJZAIKQ-UHFFFAOYSA-N 0.000 description 1
- 235000003826 Artemisia Nutrition 0.000 description 1
- 235000003261 Artemisia vulgaris Nutrition 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- YVGGHNCTFXOJCH-UHFFFAOYSA-N DDT Chemical compound C1=CC(Cl)=CC=C1C(C(Cl)(Cl)Cl)C1=CC=C(Cl)C=C1 YVGGHNCTFXOJCH-UHFFFAOYSA-N 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 241000256626 Pterygota <winged insects> Species 0.000 description 1
- 241000320333 Ptilostemon afer Species 0.000 description 1
- 235000007303 Thymus vulgaris Nutrition 0.000 description 1
- 240000002657 Thymus vulgaris Species 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 244000030166 artemisia Species 0.000 description 1
- 235000009052 artemisia Nutrition 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- OEBRKCOSUFCWJD-UHFFFAOYSA-N dichlorvos Chemical compound COP(=O)(OC)OC=C(Cl)Cl OEBRKCOSUFCWJD-UHFFFAOYSA-N 0.000 description 1
- 229950001327 dichlorvos Drugs 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000077 insect repellent Substances 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 231100000225 lethality Toxicity 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000001585 thymus vulgaris Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to an insecticide for mosquitoes, flies and roaches, which comprises the pure agent prepared from cloves, a pyrethrin compound, camphora, and alcoholic solution, wherein the pyrethrin compound is cypermethrin and tetramethrin. The insecticide has the advantages of effective extermination of indoor malignant bacteria after being sprayed, no oil and no environmental pollution because of alcohol used as solvents, is a good environmental protection insecticide and is suitable for the places such as families, hotels, etc. because of easy use and effective control of mosquitoes, flies and roaches.
Description
The present invention is a kind of various winged insect medicaments of killing, and especially goes up a kind of mosquitos and flies and cockroach insecticide and preparation method thereof.
The product of killing mosquitos and flies and cockroach at present is more, and its kind is broadly divided into three kinds: a class is the flammable product of solid, shaped, thereby it drives away and kill mosquitos and flies and cockroach by burning generation smell, and this product mainly is to apply medicament on combustible carrier.As mosquito-repellent incense and the patent No. is that 981048161 the cockroach tablet of killing is exactly to be made up of medicament and combustible support thereof, this series products produces carbonic acid gas on the one hand when burning, unfavorable to indoor environment, it is when burning on the other hand, the diffusion of smell has certain restriction, basically the effect of dispersing can only be played, insects such as mosquitos and flies and cockroach can not be thoroughly killed.One class is the medicinal powder of powdery, as cockroach medicinal powder on the existing market, it be by with the medicinal powder bulk storage in places such as limit, corner that cockroach is come in and gone out, insects such as cockroach kill it when passing its medicinal powder, insecticide efficiency through facts have proved this medicinal powder is lower, and will use the time, needs to apply around indoor to loose, be not easy to sweep on the one hand, be bonded on the food easily on the other hand.The 3rd class is a medicament, the insecticide of most of this respect mainly is merely to adopt chrysanthemum ester class chemicals, as the patent No. is a kind of high effective safety and hygienic insecticide of 971040693, and medicinal plant extract (03～06%) and compound emulsifying agent that it mainly extracts by 2～3 kinds of composite former medicine compositional liquors (02～04%) that form of chrysanthemum ester insecticide, by aromatic planies such as thyme, lavender, wild wormwood artemisias are formed.Though this medicament is different from the insecticides such as dichlorvos, dichlorodiphenyl trichloroethane that health and fowl poultry safety had harm, used product category is more in its medicament, and processing is complicated, thereby its price is higher; This in addition insecticide does not have the cleaning and disinfection effect to indoor environment.
The purpose of this invention is to provide a kind of low toxicity, harmless, and have lasting medicine, the kill ratio of mosquitos and flies and cockroach is reached 100% mosquitos and flies and cockroach insecticide human body and livestock and poultry.And this insecticide has biocidal efficacies.
Another object of the present invention provides a kind of mosquitos and flies and cockroach process for preparing insecticide.
Mosquitos and flies of the present invention and cockroach insecticide mainly include pure dose that is made up of cypermethrin, tetramethrin, camphor tree ice, cloves synergist and an amount of essence and alcohol; This insecticide can be divided into two kinds of aerosol and propellants again according to its preparation method difference.
The present invention by quick-acting chrysanthemum ester type compounds and the Chinese medicinal ingredients of imitating slowly constitute, it has mosquitos and flies and cockroach knocks down and good lethal effect fast, and air is also had disinfective action, non-stimulated, safe in utilization.In addition, it also has following significant advantage: owing to adopt compounds such as cypermethrin, tetramethrin, insects such as mosquitos and flies, cockroach can be killed fast, up hill and dale, its speed kill rate very high and its extremely the rate of dying can reach 100%, and its lasting period was three months; Adopted Chinese medicine camphor tree ice in this insecticide and it is dissolved in the alcohol, strong drug action and long-term low toxicity can keep its drug effect enduringly, after 40 days reentrant mosquitos and flies are also had 100% lethal effect at the spray medicine; Because of having adopted cloves, this insecticide has very strong adhesive force, long-term lethality and becomes to catching up with ability; Because this insecticide adopts alcohol to make solvent, can kill indoor malignant bacteria effectively after the spray, its no oil and environmentally safe is a kind of good environment-friendly pesticide; This insecticide is easy to use, can prevent and treat mosquitos and flies and cockroach effectively, is adapted to places such as family, restaurant.
Mosquitos and flies of the present invention and cockroach insecticide mainly contain pure dose that is made up of cloves, chrysanthemum ester type compound, camphor tree ice and alcoholic solution, and described chrysanthemum ester type compound is cypermethrin and tetramethrin, and wherein the prescription of pure dose of each part is as follows: cloves: 10～20 restrain; Alcohol: 100 grams; Cypermethrin 0.05～0.65 gram: tetramethrin: 0.1～0.45 gram; Camphor tree ice 3.2～3.7 grams.
Its specific embodiment 1;
Cloves: 10～15 grams; 95% alcohol: 100 grams;
Cypermethrin 0.05～0.25 gram; Tetramethrin: 0.1～0.45 gram;
Camphor tree ice 3.6 grams.
Its specific embodiment 2:
Cloves: 20 grams; 70% alcohol: 100 grams;
Cypermethrin 0.3～0.6 gram; Tetramethrin: 0.1～0.4 gram;
Camphor tree ice 3.3 grams.
Mosquitos and flies of the present invention and cockroach process for preparing insecticide, by the made insecticide of this method is a kind of aerosol, this insecticide is the making that enters according to following method, and its step is as follows: 1. got in the alcohol that cloves 10～15 grams are dissolved in 100 grams 95% 40 hours, the lilac wine seminal fluid; 2. getting with respect to above-mentioned lilac wine seminal fluid again is 0.05～0.15% (stereometer, below identical) cypermethrin, be 0.1～0.35% tetramethrin with respect to above-mentioned lilac wine seminal fluid, be dissolved in fully in the above-mentioned lilac wine seminal fluid with camphor tree ice 3.6 grams, add synergist again, essence is an amount of, and getting product P H value is 5～6 pure doses; 3. again by pure dose of 0.05～0.15 volume unit of 100 volume units addings, bottling and adding butagas are made propellant behind the dilute with water, promptly get the insecticide of aerosol type.The condensation rate of this aerosol type insecticide is greater than 98%, and product pressure is 1.9～2.6 handkerchiefs, and normal temperature is preserved 2 years constant product quality down.
Above-mentioned described butagas is to add by 30% of toatl proportion.
A kind of mosquitos and flies and cockroach process for preparing insecticide, the prepared insecticide of this method is a kind of propellant, this insecticide is the making that enters according to following method, and its step is as follows: 1. got in the alcohol that cloves 20 grams are dissolved in 100 grams 70% 60 hours, the lilac wine seminal fluid; 2. getting with respect to above-mentioned lilac wine seminal fluid again is 0.3～0.6% (stereometer, below identical) cypermethrin, be 0.1～0.4% tetramethrin with respect to above-mentioned lilac wine seminal fluid, be dissolved in fully in the above-mentioned lilac wine seminal fluid with camphor tree ice 3.3 grams, getting product P H value is 5～6 pure doses; 3. add pure dose of 0.1～0.45 volume unit by 100 volume units again, add synergist behind the dilute with water and add in the sprayer, propellant formula insecticide.This propellant in use, the spray get final product, preserve 2 years constant product quality at normal temperatures.
Synergist described in the said method mainly plays synergistic effect in medicament, select Octachlorodipropyl Ether for use.
Claims (3)
1, a kind of mosquitos and flies and cockroach insecticide mainly contain pure dose that is made up of cloves, chrysanthemum ester type compound, camphor tree ice and alcoholic solution, and it is characterized in that: described chrysanthemum ester type compound is cypermethrin and tetramethrin, and wherein the prescription of pure dose of each part is as follows:
Cloves: 10～20 grams; Alcohol: 100 grams;
Cypermethrin 0.05～0.65 gram; Tetramethrin: 0.1～0.45 gram;
Camphor tree ice 3.2～3.7 grams.
2, a kind of mosquitos and flies and cockroach process for preparing insecticide, the prepared insecticide of this method is an aerosol, it is characterized in that this insecticide is the making that enters according to following method, its step is as follows: 1. got in the alcohol that cloves 10～15 grams are dissolved in 100 grams 95% 40 hours, the lilac wine seminal fluid; 2. getting with respect to above-mentioned lilac wine seminal fluid again is 0.05～0.15% (stereometer, below identical) cypermethrin, be 0.1～0.35% tetramethrin with respect to above-mentioned lilac wine seminal fluid, be dissolved in fully in the above-mentioned lilac wine seminal fluid with camphor tree ice 3.6 grams, add synergist again, essence is an amount of, and getting product P H value is 5～6 pure doses; 3. again by pure dose of 0.05～0.15 volume unit of 100 volume units addings, bottling and adding butagas are made propellant behind the dilute with water, promptly get the insecticide of aerosol type.
3, a kind of mosquitos and flies and cockroach process for preparing insecticide, the prepared insecticide of this method is a kind of propellant, it is characterized in that this insecticide is the making that enters according to following method, its step is as follows: 1. got in the alcohol that cloves 20 grams are dissolved in 100 grams 70% 60 hours, the lilac wine seminal fluid; 2. getting with respect to above-mentioned lilac wine seminal fluid again is 0.3～0.6% (stereometer, below identical) cypermethrin, be 0.1～0.4% tetramethrin with respect to above-mentioned lilac wine seminal fluid, be dissolved in fully in the above-mentioned lilac wine seminal fluid with camphor tree ice 3.3 grams, getting product P H value is 5～6 pure doses; 3. add pure dose of 0.1～0.45 volume unit by 100 volume units again, add synergist behind the dilute with water and add in the sprayer, propellant formula insecticide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00124870A CN1114345C (en) | 2000-09-20 | 2000-09-20 | Process for preparing insecticide for mosquito, fly and roach |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00124870A CN1114345C (en) | 2000-09-20 | 2000-09-20 | Process for preparing insecticide for mosquito, fly and roach |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1291434A CN1291434A (en) | 2001-04-18 |
| CN1114345C true CN1114345C (en) | 2003-07-16 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN00124870A Expired - Fee Related CN1114345C (en) | 2000-09-20 | 2000-09-20 | Process for preparing insecticide for mosquito, fly and roach |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1114345C (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1313002C (en) * | 2004-09-17 | 2007-05-02 | 陕西中辉环保有限公司 | Fly killing agent |
| CN101953370A (en) * | 2010-06-02 | 2011-01-26 | 深圳诺普信农化股份有限公司 | Composite containing chlorine fluorine ethofenprox and cypermethrin and application thereof |
| CN103651523A (en) * | 2013-12-06 | 2014-03-26 | 济南凯因生物科技有限公司 | Water dispersible granules containing phthalthrin and application |
| CN105076189A (en) * | 2015-04-28 | 2015-11-25 | 乌鲁木齐市疾病预防控制中心 | Cockroach-killing glue bait |
| CN107568255A (en) * | 2017-10-26 | 2018-01-12 | 桂林大创科技有限公司 | A kind of mosquitos and flies and cockroach insecticide and preparation method thereof |
| CN112602733B (en) * | 2020-12-29 | 2022-01-18 | 福建兴全香业有限公司 | Incense for killing cockroaches and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1997047198A1 (en) * | 1996-06-11 | 1997-12-18 | Attali Jean Claude | Aqueous insecticide and pesticide composition, method of production and use thereof |
-
2000
- 2000-09-20 CN CN00124870A patent/CN1114345C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1997047198A1 (en) * | 1996-06-11 | 1997-12-18 | Attali Jean Claude | Aqueous insecticide and pesticide composition, method of production and use thereof |
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| Publication number | Publication date |
|---|---|
| CN1291434A (en) | 2001-04-18 |
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Effective date of registration: 20031222 Address after: 100088, No. 38 middle third ring road, North Taiping Village, Beijing, Haidian District Patentee after: Beijing Yitong oasis Biological Engineering Technology Co Ltd Address before: Willow Park District 252000 in Shandong province Liaocheng City Fu Dongchang District No. 5 building 303 room Co-patentee before: Yang Jinsong Patentee before: Yang Baoguo |
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