CN109675493B - BB oil emulsifier and preparation method thereof - Google Patents
BB oil emulsifier and preparation method thereof Download PDFInfo
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- CN109675493B CN109675493B CN201811583421.6A CN201811583421A CN109675493B CN 109675493 B CN109675493 B CN 109675493B CN 201811583421 A CN201811583421 A CN 201811583421A CN 109675493 B CN109675493 B CN 109675493B
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- phenol ether
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/017—Mixtures of compounds
- C09K23/018—Mixtures of two or more different organic oxygen-containing compounds
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- Organic Chemistry (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
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Abstract
The invention discloses a BB oil emulsifier which is prepared from the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water, wherein the BB oil emulsifier can completely remove oily stains such as mineral oil and edible oil on the fabric under the specified conditions (the concentration is 0.2%, the temperature is 80 ℃ and the time is 30 minutes) by arranging the components of the phenol ether phosphate, the low-foaming surfactant, the dipropyl dimethyl phenol ether, the potassium oleate, the kerosene and the deionized water.
Description
Technical Field
The invention relates to the technical field of emulsifiers, in particular to a BB oil emulsifier.
Background
BB oil is a skin care product (makeup remover, bean remover, bath, etc.), also known as Baby oil. It is called BB oil because it is mild in nature and fits (is easily absorbed) even on delicate skin like Baby (Baby).
However, the existing BB oil emulsifier has simple components, single function and lack of certain market competitiveness, thereby influencing the application range of the emulsifier.
Disclosure of Invention
1. Technical problem to be solved
The invention aims to solve the problems that in the prior art, a BB oil emulsifier is simple in composition, single in function and lack of certain market competitiveness.
2. Technical scheme
In order to achieve the purpose, the invention adopts the following technical scheme:
the BB oil emulsifier is composed of the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water.
Preferably, the feed is composed of the following raw materials in parts by weight: 5 parts of phenol ether phosphate, 10 parts of low-foaming surfactant, 10 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 20 parts of kerosene and 45 parts of deionized water.
Preferably, the feed is composed of the following raw materials in parts by weight: 3 parts of phenol ether phosphate, 7 parts of low-foaming surfactant, 7 parts of dipropyl dimethyl phenol ether, 27 parts of potassium oleate, 18 parts of kerosene and 40 parts of deionized water.
Preferably, the feed is composed of the following raw materials in parts by weight: the composition comprises the following raw materials in parts by weight: 4 parts of phenol ether phosphate, 8 parts of low-foaming surfactant, 8 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 19 parts of kerosene and 55 parts of deionized water.
Preferably, the phenol ether phosphate is TXP-10 phenol ether phosphate.
Preferably, the low foaming surfactant is a PE6200 low foaming surfactant.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water according to the weight part of the raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min;
step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
3. Advantageous effects
Compared with the prior art, the invention has the advantages that: according to the invention, through the arrangement of the components of the phenol ether phosphate, the low-foaming surfactant, the dipropyl dimethyl phenol ether, the potassium oleate, the kerosene and the deionized water, the BB oil emulsifier can completely remove oily stains such as mineral oil and edible oil on the fabric under specified conditions except normal oil removal, (the concentration is 0.2%, the temperature is 80 ℃, and the time is 30 minutes).
The following are the characteristics or functions of the raw materials of the BB oil emulsifier:
TXP-10 phenol ether phosphate: the water-soluble antistatic emulsion has the advantages of strong alkali resistance, good cleaning capacity in concentrated alkali, high solubility in organic solvents, high solubility in water, high antistatic property, high emulsification property, high smoothness and high softness; as a wash enhancer; is used for preparing dry cleaning agent; used as an emulsifier added in the metal cleaning agent; an emulsifier for emulsion polymerization; emulsifier added in the production of pesticide and cosmetics, and anticorrosive agent and antistatic agent.
PE6200 low foam surfactant: the foam control is very good, defoaming rapidly and suppressing foam generation, independent of the presence of protein, starch or juice.
Dipropylene dimethyl phenol ether: can be dissolved in ethanol, chloroform, diethyl ether, glycerol, etc.; is very soluble in fatty oil and volatile oil; is neutral.
Potassium oleate: has high emulsifying efficiency, but is easy to form calcium soap when meeting hard water. Can also be used as fiber softening agent.
Kerosene: is easy to dissolve in water, and is especially suitable for continuously keeping defoaming and foam inhibition under the conditions of high temperature, strong acid and alkali, high shearing force and high pressure. Better high temperature resistance, acid and alkali resistance and no oil floating, and can be widely used for eliminating foams of various severe systems in a wide temperature range.
Deionized water: it is used for removing impurities (such as silt, colloid and suspended substances), calcium and magnesium in water by plasma.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
The first embodiment is as follows:
the BB oil emulsifier is composed of the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water according to the weight part of the raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min;
step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
Example two:
the BB oil emulsifier provided by the invention comprises the following raw materials in parts by weight: 5 parts of phenol ether phosphate, 10 parts of low-foaming surfactant, 10 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 20 parts of kerosene and 45 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in parts by weight according to the weight ratio of raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min.
Step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
Example three:
the BB oil emulsifier provided by the invention comprises the following raw materials in parts by weight: 3 parts of phenol ether phosphate, 7 parts of low-foaming surfactant, 7 parts of dipropyl dimethyl phenol ether, 27 parts of potassium oleate, 18 parts of kerosene and 40 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in parts by weight according to the weight ratio of raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min.
Step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
Example four:
the BB oil emulsifier provided by the invention comprises the following raw materials in parts by weight: 4 parts of phenol ether phosphate, 8 parts of low-foaming surfactant, 8 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 19 parts of kerosene and 55 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in parts by weight according to the weight ratio of raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min.
Step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
According to the invention, through the arrangement of the components of the phenol ether phosphate, the low-foaming surfactant, the dipropyl dimethyl phenol ether, the potassium oleate, the kerosene and the deionized water, the BB oil emulsifier can completely remove oily stains such as mineral oil and edible oil on the fabric under specified conditions except normal oil removal, (the concentration is 0.2%, the temperature is 80 ℃, and the time is 30 minutes).
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (5)
- BB oil emulsifier is composed of the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water;the phenol ether phosphate is TXP-10 phenol ether phosphate;the low-foaming surfactant is PE6200 low-foaming surfactant.
- 2. The BB oil emulsifier of claim 1, which is prepared from the following raw materials in parts by weight: 5 parts of phenol ether phosphate, 10 parts of low-foaming surfactant, 10 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 20 parts of kerosene and 45 parts of deionized water.
- 3. The BB oil emulsifier of claim 1, which is prepared from the following raw materials in parts by weight: 3 parts of phenol ether phosphate, 7 parts of low-foaming surfactant, 7 parts of dipropyl dimethyl phenol ether, 27 parts of potassium oleate, 18 parts of kerosene and 40 parts of deionized water.
- 4. The BB oil emulsifier of claim 1, which is prepared from the following raw materials in parts by weight: 4 parts of phenol ether phosphate, 8 parts of low-foaming surfactant, 8 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 19 parts of kerosene and 55 parts of deionized water.
- 5. The method of preparing BB oil emulsifier of any one of claims 1-4, comprising the steps of:step 1: firstly, proportioning according to the weight parts of raw materials, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in corresponding weight parts, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min;step 2: adding kerosene with corresponding weight parts, ultrasonically dispersing at high speed, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
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| CN201811583421.6A CN109675493B (en) | 2018-12-24 | 2018-12-24 | BB oil emulsifier and preparation method thereof |
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| CN201811583421.6A CN109675493B (en) | 2018-12-24 | 2018-12-24 | BB oil emulsifier and preparation method thereof |
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| CN109675493B true CN109675493B (en) | 2021-06-01 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004098021A (en) * | 2002-09-12 | 2004-04-02 | Nikko Kagaku Kenkyusho:Kk | Water drop-in-oil-type emulsion defoaming agent composition |
| CN101100507A (en) * | 2006-07-07 | 2008-01-09 | 戈尔德施米特股份公司 | Phosphate ester used as emulsifier and disperser |
| CN102491650A (en) * | 2011-12-16 | 2012-06-13 | 上海久安水质稳定剂厂 | Mineral oil composite emulsifier and preparation method thereof |
| CN103937628A (en) * | 2014-05-12 | 2014-07-23 | 苏州禾川化学技术服务有限公司 | High-alkalinity non-foaming spraying cleaning agent |
| CN106621478A (en) * | 2016-11-23 | 2017-05-10 | 北京麦尔化工科技有限公司 | Light-colored mineral oil de-foaming agent and preparation method thereof |
-
2018
- 2018-12-24 CN CN201811583421.6A patent/CN109675493B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004098021A (en) * | 2002-09-12 | 2004-04-02 | Nikko Kagaku Kenkyusho:Kk | Water drop-in-oil-type emulsion defoaming agent composition |
| CN101100507A (en) * | 2006-07-07 | 2008-01-09 | 戈尔德施米特股份公司 | Phosphate ester used as emulsifier and disperser |
| CN102491650A (en) * | 2011-12-16 | 2012-06-13 | 上海久安水质稳定剂厂 | Mineral oil composite emulsifier and preparation method thereof |
| CN103937628A (en) * | 2014-05-12 | 2014-07-23 | 苏州禾川化学技术服务有限公司 | High-alkalinity non-foaming spraying cleaning agent |
| CN106621478A (en) * | 2016-11-23 | 2017-05-10 | 北京麦尔化工科技有限公司 | Light-colored mineral oil de-foaming agent and preparation method thereof |
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| CN109675493A (en) | 2019-04-26 |
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