CN109675493B - BB oil emulsifier and preparation method thereof - Google Patents
BB oil emulsifier and preparation method thereof Download PDFInfo
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- CN109675493B CN109675493B CN201811583421.6A CN201811583421A CN109675493B CN 109675493 B CN109675493 B CN 109675493B CN 201811583421 A CN201811583421 A CN 201811583421A CN 109675493 B CN109675493 B CN 109675493B
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- China
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- parts
- phenol ether
- low
- kerosene
- foaming surfactant
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- 239000003995 emulsifying agent Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title description 7
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 27
- LRMHFDNWKCSEQU-UHFFFAOYSA-N ethoxyethane;phenol Chemical compound CCOCC.OC1=CC=CC=C1 LRMHFDNWKCSEQU-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000010452 phosphate Substances 0.000 claims abstract description 27
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 27
- 239000004094 surface-active agent Substances 0.000 claims abstract description 27
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 26
- 238000005187 foaming Methods 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- -1 dipropyl dimethyl phenol Chemical compound 0.000 claims abstract description 24
- 239000008367 deionised water Substances 0.000 claims abstract description 23
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 23
- 239000003350 kerosene Substances 0.000 claims abstract description 23
- 229940096992 potassium oleate Drugs 0.000 claims abstract description 23
- MLICVSDCCDDWMD-KVVVOXFISA-M potassium;(z)-octadec-9-enoate Chemical compound [K+].CCCCCCCC\C=C/CCCCCCCC([O-])=O MLICVSDCCDDWMD-KVVVOXFISA-M 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 21
- 239000006185 dispersion Substances 0.000 claims description 29
- 238000000034 method Methods 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 25
- 239000008157 edible vegetable oil Substances 0.000 abstract description 3
- 239000004744 fabric Substances 0.000 abstract description 3
- 239000002480 mineral oil Substances 0.000 abstract description 3
- 235000010446 mineral oil Nutrition 0.000 abstract description 3
- 239000006260 foam Substances 0.000 description 5
- 239000003513 alkali Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000002216 antistatic agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000005108 dry cleaning Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000007720 emulsion polymerization reaction Methods 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/017—Mixtures of compounds
- C09K23/018—Mixtures of two or more different organic oxygen-containing compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Colloid Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a BB oil emulsifier which is prepared from the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water, wherein the BB oil emulsifier can completely remove oily stains such as mineral oil and edible oil on the fabric under the specified conditions (the concentration is 0.2%, the temperature is 80 ℃ and the time is 30 minutes) by arranging the components of the phenol ether phosphate, the low-foaming surfactant, the dipropyl dimethyl phenol ether, the potassium oleate, the kerosene and the deionized water.
Description
Technical Field
The invention relates to the technical field of emulsifiers, in particular to a BB oil emulsifier.
Background
BB oil is a skin care product (makeup remover, bean remover, bath, etc.), also known as Baby oil. It is called BB oil because it is mild in nature and fits (is easily absorbed) even on delicate skin like Baby (Baby).
However, the existing BB oil emulsifier has simple components, single function and lack of certain market competitiveness, thereby influencing the application range of the emulsifier.
Disclosure of Invention
1. Technical problem to be solved
The invention aims to solve the problems that in the prior art, a BB oil emulsifier is simple in composition, single in function and lack of certain market competitiveness.
2. Technical scheme
In order to achieve the purpose, the invention adopts the following technical scheme:
the BB oil emulsifier is composed of the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water.
Preferably, the feed is composed of the following raw materials in parts by weight: 5 parts of phenol ether phosphate, 10 parts of low-foaming surfactant, 10 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 20 parts of kerosene and 45 parts of deionized water.
Preferably, the feed is composed of the following raw materials in parts by weight: 3 parts of phenol ether phosphate, 7 parts of low-foaming surfactant, 7 parts of dipropyl dimethyl phenol ether, 27 parts of potassium oleate, 18 parts of kerosene and 40 parts of deionized water.
Preferably, the feed is composed of the following raw materials in parts by weight: the composition comprises the following raw materials in parts by weight: 4 parts of phenol ether phosphate, 8 parts of low-foaming surfactant, 8 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 19 parts of kerosene and 55 parts of deionized water.
Preferably, the phenol ether phosphate is TXP-10 phenol ether phosphate.
Preferably, the low foaming surfactant is a PE6200 low foaming surfactant.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water according to the weight part of the raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min;
step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
3. Advantageous effects
Compared with the prior art, the invention has the advantages that: according to the invention, through the arrangement of the components of the phenol ether phosphate, the low-foaming surfactant, the dipropyl dimethyl phenol ether, the potassium oleate, the kerosene and the deionized water, the BB oil emulsifier can completely remove oily stains such as mineral oil and edible oil on the fabric under specified conditions except normal oil removal, (the concentration is 0.2%, the temperature is 80 ℃, and the time is 30 minutes).
The following are the characteristics or functions of the raw materials of the BB oil emulsifier:
TXP-10 phenol ether phosphate: the water-soluble antistatic emulsion has the advantages of strong alkali resistance, good cleaning capacity in concentrated alkali, high solubility in organic solvents, high solubility in water, high antistatic property, high emulsification property, high smoothness and high softness; as a wash enhancer; is used for preparing dry cleaning agent; used as an emulsifier added in the metal cleaning agent; an emulsifier for emulsion polymerization; emulsifier added in the production of pesticide and cosmetics, and anticorrosive agent and antistatic agent.
PE6200 low foam surfactant: the foam control is very good, defoaming rapidly and suppressing foam generation, independent of the presence of protein, starch or juice.
Dipropylene dimethyl phenol ether: can be dissolved in ethanol, chloroform, diethyl ether, glycerol, etc.; is very soluble in fatty oil and volatile oil; is neutral.
Potassium oleate: has high emulsifying efficiency, but is easy to form calcium soap when meeting hard water. Can also be used as fiber softening agent.
Kerosene: is easy to dissolve in water, and is especially suitable for continuously keeping defoaming and foam inhibition under the conditions of high temperature, strong acid and alkali, high shearing force and high pressure. Better high temperature resistance, acid and alkali resistance and no oil floating, and can be widely used for eliminating foams of various severe systems in a wide temperature range.
Deionized water: it is used for removing impurities (such as silt, colloid and suspended substances), calcium and magnesium in water by plasma.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
The first embodiment is as follows:
the BB oil emulsifier is composed of the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water according to the weight part of the raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min;
step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
Example two:
the BB oil emulsifier provided by the invention comprises the following raw materials in parts by weight: 5 parts of phenol ether phosphate, 10 parts of low-foaming surfactant, 10 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 20 parts of kerosene and 45 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in parts by weight according to the weight ratio of raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min.
Step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
Example three:
the BB oil emulsifier provided by the invention comprises the following raw materials in parts by weight: 3 parts of phenol ether phosphate, 7 parts of low-foaming surfactant, 7 parts of dipropyl dimethyl phenol ether, 27 parts of potassium oleate, 18 parts of kerosene and 40 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in parts by weight according to the weight ratio of raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min.
Step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
Example four:
the BB oil emulsifier provided by the invention comprises the following raw materials in parts by weight: 4 parts of phenol ether phosphate, 8 parts of low-foaming surfactant, 8 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 19 parts of kerosene and 55 parts of deionized water.
The preparation method of the BB oil emulsifier comprises the following steps:
step 1: firstly, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in parts by weight according to the weight ratio of raw materials, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min.
Step 2: adding the kerosene in parts by weight, performing ultrasonic high-speed dispersion, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
According to the invention, through the arrangement of the components of the phenol ether phosphate, the low-foaming surfactant, the dipropyl dimethyl phenol ether, the potassium oleate, the kerosene and the deionized water, the BB oil emulsifier can completely remove oily stains such as mineral oil and edible oil on the fabric under specified conditions except normal oil removal, (the concentration is 0.2%, the temperature is 80 ℃, and the time is 30 minutes).
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (5)
- BB oil emulsifier is composed of the following raw materials in parts by weight: 3-5 parts of phenol ether phosphate, 6-10 parts of low-foaming surfactant, 7-10 parts of dipropyl dimethyl phenol ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene and 40-60 parts of deionized water;the phenol ether phosphate is TXP-10 phenol ether phosphate;the low-foaming surfactant is PE6200 low-foaming surfactant.
- 2. The BB oil emulsifier of claim 1, which is prepared from the following raw materials in parts by weight: 5 parts of phenol ether phosphate, 10 parts of low-foaming surfactant, 10 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 20 parts of kerosene and 45 parts of deionized water.
- 3. The BB oil emulsifier of claim 1, which is prepared from the following raw materials in parts by weight: 3 parts of phenol ether phosphate, 7 parts of low-foaming surfactant, 7 parts of dipropyl dimethyl phenol ether, 27 parts of potassium oleate, 18 parts of kerosene and 40 parts of deionized water.
- 4. The BB oil emulsifier of claim 1, which is prepared from the following raw materials in parts by weight: 4 parts of phenol ether phosphate, 8 parts of low-foaming surfactant, 8 parts of dipropyl dimethyl phenol ether, 30 parts of potassium oleate, 19 parts of kerosene and 55 parts of deionized water.
- 5. The method of preparing BB oil emulsifier of any one of claims 1-4, comprising the steps of:step 1: firstly, proportioning according to the weight parts of raw materials, adding phenol ether phosphate, a low-foaming surfactant, dipropyl dimethyl phenol ether and potassium oleate into deionized water in corresponding weight parts, and ultrasonically dispersing at a high speed, wherein the ultrasonic frequency is 30-50 KHz, the dispersion speed is 4000-5000 r/min, and the dispersion time is 40-50 min;step 2: adding kerosene with corresponding weight parts, ultrasonically dispersing at high speed, wherein the ultrasonic frequency is 15-35 KHz, the dispersion speed is 4700-5100 r/min, the dispersion time is 20-40 min, and uniformly mixing to obtain the product.
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CN201811583421.6A CN109675493B (en) | 2018-12-24 | 2018-12-24 | BB oil emulsifier and preparation method thereof |
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CN109675493B true CN109675493B (en) | 2021-06-01 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004098021A (en) * | 2002-09-12 | 2004-04-02 | Nikko Kagaku Kenkyusho:Kk | Water drop-in-oil-type emulsion defoaming agent composition |
CN101100507A (en) * | 2006-07-07 | 2008-01-09 | 戈尔德施米特股份公司 | Phosphate ester used as emulsifier and disperser |
CN102491650A (en) * | 2011-12-16 | 2012-06-13 | 上海久安水质稳定剂厂 | Mineral oil composite emulsifier and preparation method thereof |
CN103937628A (en) * | 2014-05-12 | 2014-07-23 | 苏州禾川化学技术服务有限公司 | High-alkalinity non-foaming spraying cleaning agent |
CN106621478A (en) * | 2016-11-23 | 2017-05-10 | 北京麦尔化工科技有限公司 | Light-colored mineral oil de-foaming agent and preparation method thereof |
-
2018
- 2018-12-24 CN CN201811583421.6A patent/CN109675493B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004098021A (en) * | 2002-09-12 | 2004-04-02 | Nikko Kagaku Kenkyusho:Kk | Water drop-in-oil-type emulsion defoaming agent composition |
CN101100507A (en) * | 2006-07-07 | 2008-01-09 | 戈尔德施米特股份公司 | Phosphate ester used as emulsifier and disperser |
CN102491650A (en) * | 2011-12-16 | 2012-06-13 | 上海久安水质稳定剂厂 | Mineral oil composite emulsifier and preparation method thereof |
CN103937628A (en) * | 2014-05-12 | 2014-07-23 | 苏州禾川化学技术服务有限公司 | High-alkalinity non-foaming spraying cleaning agent |
CN106621478A (en) * | 2016-11-23 | 2017-05-10 | 北京麦尔化工科技有限公司 | Light-colored mineral oil de-foaming agent and preparation method thereof |
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Address after: 510000, 1st and 2nd floors, Building A, No. 15 Luogang Raotiantou Road, Junhe Street, Baiyun District, Guangzhou City, Guangdong Province Patentee after: Guangzhou Ligao Biotechnology Co.,Ltd. Country or region after: China Address before: 510000 1st floor, building a, No.15, shatiantou Road, Luogang, JUNHE street, Baiyun District, Guangzhou City, Guangdong Province Patentee before: GUANGZHOU LIGAO WASHING PRODUCTS CO.,LTD. Country or region before: China |