CN109675493A - BB emulsifier and preparation method thereof - Google Patents
BB emulsifier and preparation method thereof Download PDFInfo
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- CN109675493A CN109675493A CN201811583421.6A CN201811583421A CN109675493A CN 109675493 A CN109675493 A CN 109675493A CN 201811583421 A CN201811583421 A CN 201811583421A CN 109675493 A CN109675493 A CN 109675493A
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- parts
- phenolic ether
- kerosene
- weight
- dipropyl
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/017—Mixtures of compounds
- C09K23/018—Mixtures of two or more different organic oxygen-containing compounds
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Colloid Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses BB emulsifiers, it is made of the parts by weight of following raw material: 3-5 parts of phenolic ether phosphate, 6-10 parts of low foaming surfactant, 7-10 parts of dipropyl diformazan phenolic ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene, 40-60 parts of deionized water, pass through the setting of phenolic ether phosphate, low foaming surfactant, dipropyl diformazan phenolic ether, potassium oleate, kerosene and deionized water ingredient in the present invention, make BB emulsifier under the defined conditions and can completely remove the mineral oil on fabric, the oil-dirts such as edible oil (concentration 0.2%, 80 DEG C of temperature, 30 minutes time).
Description
Technical field
The present invention relates to emulsifier technical field more particularly to BB emulsifiers.
Background technique
BB oil is skin-protection product (makeup removing removes beans, shower etc. kind) also known as Baby oil.Because its property is mild, even
Baby(baby) skin delicate like that is suitable for and (is easy to absorb), so being called for BB oil.
But existing BB emulsifier constituent is relatively simple, function is excessively single, lacks certain market competition
Power, to influence the scope of application of emulsifier.
Summary of the invention
1. technical problems to be solved
The purpose of the present invention is to solve BB emulsifier constituent in the prior art is relatively simple, function is excessively single,
The BB emulsifier for lacking certain market competitiveness, and proposing.
2. technical solution
To achieve the goals above, present invention employs following technical solutions:
BB emulsifier is made of the parts by weight of following raw material: 3-5 parts of phenolic ether phosphate, 6-10 parts of low foaming surfactant,
7-10 parts of dipropyl diformazan phenolic ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene, 40-60 parts of deionized water.
Preferably, it is made of the parts by weight of following raw material: 5 parts of phenolic ether phosphate, 10 parts of low foaming surfactant, dipropyl
10 parts of diformazan phenolic ether, 30 parts of potassium oleate, 20 parts of kerosene, 45 parts of deionized water.
Preferably, it is made of the parts by weight of following raw material: 3 parts of phenolic ether phosphate, 7 parts of low foaming surfactant, dipropyl
7 parts of diformazan phenolic ether, 27 parts of potassium oleate, 18 parts of kerosene, 40 parts of deionized water.
Preferably, it is made of the parts by weight of following raw material: being made of the parts by weight of following raw material: phenolic ether phosphate 4
Part, 8 parts of low foaming surfactant, 8 parts of dipropyl diformazan phenolic ether, 30 parts of potassium oleate, 19 parts of kerosene, 55 parts of deionized water.
Preferably, the phenolic ether phosphate is TXP-10 phenolic ether phosphate.
Preferably, the low foaming surfactant is PE6200 low foaming surfactant.
The preparation method of BB emulsifier, comprising the following steps:
Step 1: being matched first, in accordance with parts by weight of raw materials composition by phenolic ether phosphate, low foaming surfactant, dipropyl diformazan
Phenolic ether, potassium oleate are added in the deionized water of the parts by weight, ultrasonic high speed dispersion, and ultrasonic frequency is 30~50KHz, point
4000~5000r/min of speed is dissipated, jitter time is 40~50min；
Step 2: the kerosene of the mass fraction, ultrasonic high speed dispersion is added, ultrasonic frequency is 15~35KHz, rate of dispersion
4700~5100r/min, jitter time are 20~40min, and this product is made after mixing.
3. beneficial effect
Compared with the prior art, the present invention has the advantages that passing through phenolic ether phosphate, low foaming surfactant, two in the present invention
The setting of third diformazan phenolic ether, potassium oleate, kerosene and deionized water ingredient advise BB emulsifier can also in addition to normal oil removing
It can completely remove the mineral oil on fabric under conditions of fixed, the oil-dirts such as edible oil, (concentration 0.2%, 80 DEG C of temperature, the time
30 minutes).
The characteristics of being the raw material of BB emulsifier below or effect:
TXP-10 phenolic ether phosphate: being resistant to highly basic, has good washing ability in concentrated base, is soluble in organic solvent, readily soluble
Yu Shui has stronger antistatic, emulsification, smooth, softness；As washing reinforcing agent；For preparing dry cleaning agent；As gold
Belong to the emulsifier added in cleaning agent；Emulsifier for emulsion polymerization；The emulsifier added in pesticide and Cosmetic Manufacture, Yi Jifang
Corrosive agent and antistatic agent.
PE6200 low foaming surfactant: control foam is very good, quickly defoams and foam is inhibited to generate, not by albumen
Matter, starch or juice are existing to be influenced.
Dipropyl diformazan phenolic ether: ethyl alcohol, chloroform, ether, glycerol etc. are dissolved in；It is highly soluble in fat oil and volatile oil；In being in
Property.
Potassium oleate: having very high emulsifying power, but meets hard water and easily form calcium soap.Softening agent for fibres can also be made.
Kerosene: being readily soluble in water, under the conditions of being particularly suitable for existing for high temperature, strong acid-base, high shear force, the high pressure, continues
Keep defoaming, foam inhibition.Preferable heat-resisting quantity, resistance to acid and alkali, not floating oil, can be widely used in various within the scope of very wide temperature
The foam of severe system eliminates.
Deionized water: for some impurity (such as silt, colloid, suspended matter) in water, calcium, the removal of magnesium plasma.
Specific embodiment
Combined with specific embodiments below the present invention is made further to explain.
Embodiment one:
BB emulsifier is made of the parts by weight of following raw material: 3-5 parts of phenolic ether phosphate, 6-10 parts of low foaming surfactant,
7-10 parts of dipropyl diformazan phenolic ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene, 40-60 parts of deionized water.
The preparation method of BB emulsifier, comprising the following steps:
Step 1: being matched first, in accordance with parts by weight of raw materials composition by phenolic ether phosphate, low foaming surfactant, dipropyl diformazan
Phenolic ether, potassium oleate are added in the deionized water of the parts by weight, ultrasonic high speed dispersion, and ultrasonic frequency is 30~50KHz, point
4000~5000r/min of speed is dissipated, jitter time is 40~50min；
Step 2: the kerosene of the mass fraction, ultrasonic high speed dispersion is added, ultrasonic frequency is 15~35KHz, rate of dispersion
4700~5100r/min, jitter time are 20~40min, and this product is made after mixing.
Embodiment two:
BB emulsifier proposed by the present invention, is made of the parts by weight of following raw material: 5 parts of phenolic ether phosphate, low bubble surface are living
Property 10 parts of agent, 10 parts of dipropyl diformazan phenolic ether, 30 parts of potassium oleate, 20 parts of kerosene, 45 parts of deionized water.
The preparation method of BB emulsifier, comprising the following steps:
Step 1: being matched first, in accordance with parts by weight of raw materials composition by phenolic ether phosphate, low foaming surfactant, dipropyl diformazan
Phenolic ether, potassium oleate are added in the deionized water of the parts by weight, ultrasonic high speed dispersion, and ultrasonic frequency is 30~50KHz, point
4000~5000r/min of speed is dissipated, jitter time is 40~50min.
Step 2: the kerosene of the mass fraction, ultrasonic high speed dispersion is added, ultrasonic frequency is 15~35KHz, dispersion
4700~5100r/min of speed, jitter time are 20~40min, and this product is made after mixing.
Embodiment three:
BB emulsifier proposed by the present invention, is made of the parts by weight of following raw material: 3 parts of phenolic ether phosphate, low bubble surface are living
Property 7 parts of agent, 7 parts of dipropyl diformazan phenolic ether, 27 parts of potassium oleate, 18 parts of kerosene, 40 parts of deionized water.
The preparation method of BB emulsifier, comprising the following steps:
Step 1: being matched first, in accordance with parts by weight of raw materials composition by phenolic ether phosphate, low foaming surfactant, dipropyl diformazan
Phenolic ether, potassium oleate are added in the deionized water of the parts by weight, ultrasonic high speed dispersion, and ultrasonic frequency is 30~50KHz, point
4000~5000r/min of speed is dissipated, jitter time is 40~50min.
Step 2: the kerosene of the mass fraction, ultrasonic high speed dispersion is added, ultrasonic frequency is 15~35KHz, dispersion
4700~5100r/min of speed, jitter time are 20~40min, and this product is made after mixing.
Example IV:
BB emulsifier proposed by the present invention, is made of the parts by weight of following raw material: 4 parts of phenolic ether phosphate, low bubble surface are living
Property 8 parts of agent, 8 parts of dipropyl diformazan phenolic ether, 30 parts of potassium oleate, 19 parts of kerosene, 55 parts of deionized water.
The preparation method of BB emulsifier, comprising the following steps:
Step 1: being matched first, in accordance with parts by weight of raw materials composition by phenolic ether phosphate, low foaming surfactant, dipropyl diformazan
Phenolic ether, potassium oleate are added in the deionized water of the parts by weight, ultrasonic high speed dispersion, and ultrasonic frequency is 30~50KHz, point
4000~5000r/min of speed is dissipated, jitter time is 40~50min.
Step 2: the kerosene of the mass fraction, ultrasonic high speed dispersion is added, ultrasonic frequency is 15~35KHz, dispersion
4700~5100r/min of speed, jitter time are 20~40min, and this product is made after mixing.
Pass through phenolic ether phosphate, low foaming surfactant, dipropyl diformazan phenolic ether, potassium oleate, kerosene in the present invention and goes
The setting of ion water constituent completely remove BB emulsifier can also on fabric under the defined conditions in addition to normal oil removing
Mineral oil, the oil-dirts such as edible oil, (concentration 0.2%, 80 DEG C of temperature, 30 minutes time).
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (7)
1.BB emulsifier is made of the parts by weight of following raw material: 3-5 parts of phenolic ether phosphate, low foaming surfactant 6-10
Part, 7-10 parts of dipropyl diformazan phenolic ether, 26-31 parts of potassium oleate, 17-21 parts of kerosene, 40-60 parts of deionized water.
2. BB emulsifier according to claim 1, which is characterized in that be made of the parts by weight of following raw material: phenolic ether
5 parts of phosphate, 10 parts of low foaming surfactant, 10 parts of dipropyl diformazan phenolic ether, 30 parts of potassium oleate, 20 parts of kerosene, deionized water 45
Part.
3. BB emulsifier according to claim 1, which is characterized in that be made of the parts by weight of following raw material: phenolic ether
3 parts of phosphate, 7 parts of low foaming surfactant, 7 parts of dipropyl diformazan phenolic ether, 27 parts of potassium oleate, 18 parts of kerosene, 40 parts of deionized water.
4. BB emulsifier according to claim 1, which is characterized in that be made of the parts by weight of following raw material: phenolic ether
4 parts of phosphate, 8 parts of low foaming surfactant, 8 parts of dipropyl diformazan phenolic ether, 30 parts of potassium oleate, 19 parts of kerosene, 55 parts of deionized water.
5. BB emulsifier according to claim 1, which is characterized in that the phenolic ether phosphate is TXP-10 phenolic ether phosphoric acid
Ester.
6. BB emulsifier according to claim 1, which is characterized in that the low foaming surfactant is the low bubble of PE6200
Surfactant.
The preparation method of 7.BB emulsifier, which comprises the following steps:
Step 1: being matched first, in accordance with parts by weight of raw materials composition by phenolic ether phosphate, low foaming surfactant, dipropyl diformazan
Phenolic ether, potassium oleate are added in the deionized water of the parts by weight, ultrasonic high speed dispersion, and ultrasonic frequency is 30~50KHz, point
4000~5000r/min of speed is dissipated, jitter time is 40~50min；
Step 2: the kerosene of the mass fraction, ultrasonic high speed dispersion is added, ultrasonic frequency is 15~35KHz, rate of dispersion
4700~5100r/min, jitter time are 20~40min, and this product is made after mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811583421.6A CN109675493B (en) | 2018-12-24 | 2018-12-24 | BB oil emulsifier and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811583421.6A CN109675493B (en) | 2018-12-24 | 2018-12-24 | BB oil emulsifier and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109675493A true CN109675493A (en) | 2019-04-26 |
| CN109675493B CN109675493B (en) | 2021-06-01 |
Family
ID=66189006
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811583421.6A Active CN109675493B (en) | 2018-12-24 | 2018-12-24 | BB oil emulsifier and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004098021A (en) * | 2002-09-12 | 2004-04-02 | Nikko Kagaku Kenkyusho:Kk | Water drop-in-oil-type emulsion defoaming agent composition |
| CN101100507A (en) * | 2006-07-07 | 2008-01-09 | 戈尔德施米特股份公司 | Phosphate ester used as emulsifier and disperser |
| CN102491650A (en) * | 2011-12-16 | 2012-06-13 | 上海久安水质稳定剂厂 | Mineral oil composite emulsifier and preparation method thereof |
| CN103937628A (en) * | 2014-05-12 | 2014-07-23 | 苏州禾川化学技术服务有限公司 | High-alkalinity non-foaming spraying cleaning agent |
| CN106621478A (en) * | 2016-11-23 | 2017-05-10 | 北京麦尔化工科技有限公司 | Light-colored mineral oil de-foaming agent and preparation method thereof |
-
2018
- 2018-12-24 CN CN201811583421.6A patent/CN109675493B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004098021A (en) * | 2002-09-12 | 2004-04-02 | Nikko Kagaku Kenkyusho:Kk | Water drop-in-oil-type emulsion defoaming agent composition |
| CN101100507A (en) * | 2006-07-07 | 2008-01-09 | 戈尔德施米特股份公司 | Phosphate ester used as emulsifier and disperser |
| CN102491650A (en) * | 2011-12-16 | 2012-06-13 | 上海久安水质稳定剂厂 | Mineral oil composite emulsifier and preparation method thereof |
| CN103937628A (en) * | 2014-05-12 | 2014-07-23 | 苏州禾川化学技术服务有限公司 | High-alkalinity non-foaming spraying cleaning agent |
| CN106621478A (en) * | 2016-11-23 | 2017-05-10 | 北京麦尔化工科技有限公司 | Light-colored mineral oil de-foaming agent and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 张晋霞等: "《含锌冶金尘泥分选理论及应用》", 31 July 2017, 冶金工业出版社 * |
| 杨成德: "《涂料开发与试验》", 28 February 2015, 科学技术文献出版社 * |
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| CN109675493B (en) | 2021-06-01 |
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