CN109674377A - A kind of Antimicrobial sanitation paper and its processing method - Google Patents
A kind of Antimicrobial sanitation paper and its processing method Download PDFInfo
- Publication number
- CN109674377A CN109674377A CN201910054819.9A CN201910054819A CN109674377A CN 109674377 A CN109674377 A CN 109674377A CN 201910054819 A CN201910054819 A CN 201910054819A CN 109674377 A CN109674377 A CN 109674377A
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- China
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- essential oil
- wood pulp
- pulp material
- antibacterial agent
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Classifications
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47K—SANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
- A47K10/00—Body-drying implements; Toilet paper; Holders therefor
- A47K10/16—Paper towels; Toilet paper; Holders therefor
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
- D21F11/00—Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines
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- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of Antimicrobial sanitation paper, the raw material including following parts by weight: 30-40 parts of eucalyptus leaves wood pulp material, 30-40 parts of rhizome of chuanxiong leaf wood pulp material, 20-30 parts of kuh-seng leaf wood pulp material, 5-10 parts of bamboo pulp, 0.5-1.5 parts of softener, 3-7 parts of antibacterial agent；The antibacterial agent is the compound of attapulgite load composite essential oil.Toilet paper of the present invention is environment-protecting and non-poisonous, by the way that eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp is added, so that toilet paper has lesser tear index and degree of holding, by the way that softener is added, so that paper soft comfortable；By the way that the compound of attapulgite load composite essential oil is added as antibacterial agent, the antibacterial agent combines the performance of attapulgite absorption bacterium and the antibacterial activity of essential oil well, so that toilet paper has significant antibacterial effect, 99.9% or more is reached to the antibiotic rate of staphylococcus aureus, Escherichia coli, Candida albicans, salmonella.
Description
Technical field
The present invention relates to paper and its preparation fields, and in particular to a kind of Antimicrobial sanitation paper and its processing method.
Background technique
Toilet paper is one of the most common type paper for daily use, is one of basic supplies necessary to modern humans live, life
Yield and consumption are as the trend increased year by year is presented in the horizontal raising of people's life.Currently, people are commonly hygienic
Paper, although papery is very soft, sanitary index also complies with the standard of toilet paper, and antibacterial this part has no remarkable result, especially
Crissum has the crowd of sufferer, and common toilet paper can not thoroughly remove crissum bacterium, has brought many unnecessary fiber crops
Tired and pain.
Summary of the invention
It is an object of the invention to: a kind of Antimicrobial sanitation paper and its processing method are provided.
To achieve the goals above, the invention provides the following technical scheme:
A kind of Antimicrobial sanitation paper, the raw material including following parts by weight: 30-40 parts of eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material 30-40
Part, 20-30 parts of kuh-seng leaf wood pulp material, 5-10 parts of bamboo pulp, 0.5-1.5 parts of softener, 3-7 parts of antibacterial agent；The antibacterial agent is
The compound of attapulgite load composite essential oil.
Preferably, a kind of Antimicrobial sanitation paper, the raw material including following parts by weight: 36 parts of eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood
35 parts of slurry, 28 parts of kuh-seng leaf wood pulp material, 7 parts of bamboo pulp, 1 part of softener, 5 parts of antibacterial agent；The antibacterial agent is attapulgite
Load the compound of composite essential oil.
Preferably, in the antibacterial agent composite essential oil be by tea tree ethereal oil, galic essential oil, thyme essential oil mixing and
At.
Preferably, tea tree ethereal oil in the composite essential oil, galic essential oil, thyme essential oil mass ratio be 1:0.5-1:
0.5-1。
Preferably, tea tree ethereal oil in the composite essential oil, galic essential oil, thyme essential oil mass ratio be 1:0.8:
0.7。
Preferably, the antibacterial agent is prepared with the following method: by attapulgite in 420-520 DEG C of roasting 0.8-
Attapulgite after roasting is added in deionized water 1.8h, and ultrasonic disperse forms suspension system, and composite essential oil is taken to dissolve Yushan Hill
It in pears alcohol, is then added in attapulgite suspension system, the centrifugation point after 70-78 DEG C of stirring 1.5-2.5h on magnetic stirring apparatus
From being precipitated, ground 300-400 mesh is spare after precipitating drying.
Preferably, any one of the softener in imidazoline quaternary ammonium salt class, ethylene ketone softening agent.
A kind of processing method of Antimicrobial sanitation paper, the specific steps are as follows:
(1) eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp, softener, antibacterial agent are stirred
It is even, manufacture paper with pulp into l Water Paper page；
(2) by l Water Paper page cylinder dried, page moisture content is controlled in 6-10%；
(3) dry page will be completed to carry out scraper corrugation, batch coiled, preservation.
The beneficial effects of the present invention are:
Toilet paper of the present invention is environment-protecting and non-poisonous, by the way that eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp is added,
So that the toilet paper has lesser tear index and degree of holding, by the way that softener is added, so that paper soft comfortable；By adding
Enter the compound of attapulgite load composite essential oil as antibacterial agent, which combines attapulgite absorption bacterium well
Performance and essential oil antibacterial activity so that the toilet paper being prepared have significant antibacterial effect, to Staphylococcus aureus
Bacterium, Escherichia coli, Candida albicans, salmonella antibiotic rate reach 99.9% or more.
Specific embodiment
Embodiment 1
A kind of Antimicrobial sanitation paper, the raw material including following parts by weight: 30 parts of eucalyptus leaves wood pulp material, 30 parts of rhizome of chuanxiong leaf wood pulp material, hardship
Join 20 parts of leaf wood pulp material, 5 parts of bamboo pulp, 0.5 part of ethylene ketone softening agent, 3 parts of antibacterial agent；The antibacterial agent is negative for attapulgite
Carry the compound of composite essential oil.
Wherein, composite essential oil is tea tree ethereal oil, galic essential oil, the thyme for being 1:0.5:0.5 by mass ratio in antibacterial agent
Essential oil mixes.
Antibacterial agent is prepared with the following method: by attapulgite in 420 DEG C of roasting 1.8h, by the concave convex rod after roasting
Stone is added in deionized water, and ultrasonic disperse forms suspension system, takes composite essential oil to be dissolved in sorbierite, is then added to concave convex rod
In stone suspension system, it is centrifugally separating to obtain precipitating after 75 DEG C of stirring 2h on magnetic stirring apparatus, it will be ground after precipitating drying
300-400 mesh is spare.
The processing method of above-mentioned Antimicrobial sanitation paper, the specific steps are as follows:
(1) eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp, softener, antibacterial agent are stirred
It is even, manufacture paper with pulp into l Water Paper page；
(2) by l Water Paper page cylinder dried, page moisture content is controlled in 6-10%；
(3) dry page will be completed to carry out scraper corrugation, batch coiled, preservation.
Embodiment 2
A kind of Antimicrobial sanitation paper, the raw material including following parts by weight: 36 parts of eucalyptus leaves wood pulp material, 35 parts of rhizome of chuanxiong leaf wood pulp material, hardship
Join 28 parts of leaf wood pulp material, 7 parts of bamboo pulp, 1 part of softener, 5 parts of antibacterial agent；The antibacterial agent is attapulgite load composite essential oil
Compound.
Wherein, composite essential oil is tea tree ethereal oil, galic essential oil, the thyme for being 1:0.8:0.7 by mass ratio in antibacterial agent
Essential oil mixes.
Antibacterial agent is prepared with the following method: by attapulgite in 480 DEG C of roasting 1.5h, by the concave convex rod after roasting
Stone is added in deionized water, and ultrasonic disperse forms suspension system, takes composite essential oil to be dissolved in sorbierite, is then added to concave convex rod
In stone suspension system, it is centrifugally separating to obtain precipitating after 75 DEG C of stirring 2h on magnetic stirring apparatus, it will be ground after precipitating drying
300-400 mesh is spare.
The processing method of above-mentioned Antimicrobial sanitation paper, the specific steps are as follows:
(1) eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp, softener, antibacterial agent are stirred
It is even, manufacture paper with pulp into l Water Paper page；
(2) by l Water Paper page cylinder dried, page moisture content is controlled in 6-10%；
(3) dry page will be completed to carry out scraper corrugation, batch coiled, preservation.
Embodiment 3
A kind of Antimicrobial sanitation paper, the raw material including following parts by weight: 40 parts of eucalyptus leaves wood pulp material, 40 parts of rhizome of chuanxiong leaf wood pulp material, hardship
Join 30 parts of leaf wood pulp material, 10 parts of bamboo pulp .5 parts of ethylene ketone softening agent, 7 parts of antibacterial agent；The antibacterial agent is negative for attapulgite
Carry the compound of composite essential oil.
Wherein, composite essential oil is tea tree ethereal oil, galic essential oil, the thyme essential oil for being 1:1:1 by mass ratio in antibacterial agent
It mixes.
Antibacterial agent is prepared with the following method: by attapulgite in 520 DEG C of roasting 0.8h, by the concave convex rod after roasting
Stone is added in deionized water, and ultrasonic disperse forms suspension system, takes composite essential oil to be dissolved in sorbierite, is then added to concave convex rod
In stone suspension system, it is centrifugally separating to obtain precipitating after 75 DEG C of stirring 2h on magnetic stirring apparatus, it will be ground after precipitating drying
300-400 mesh is spare.
The processing method of above-mentioned Antimicrobial sanitation paper, the specific steps are as follows:
(1) eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp, softener, antibacterial agent are stirred
It is even, manufacture paper with pulp into l Water Paper page；
(2) by l Water Paper page cylinder dried, page moisture content is controlled in 6-10%；
(3) dry page will be completed to carry out scraper corrugation, batch coiled, preservation.
Embodiment 4 toilet paper of the invention is to staphylococcus aureus, Escherichia coli, Candida albicans, salmonella
The test of antibacterial effect
Pour into agar medium plate；Bacteria suspension is diluted to 105cfu/mL~106cfu/mL as test bacteria suspension；It will
The tested toilet paper sample containing antibacterial effect is made 50mm × 50mm size print and puts down piecewise after 78% ethanol disinfection
Be put in sterile vessel, take 0.1mL test bacteria suspension drop dye in print center, smoothen, make bacterium solution and print edge there are
It is spare to set dry 30min~60min, the antibacterial print as microbiological contamination in 37 DEG C of incubators for the distance of 5mm；By the antibacterial sample of microbiological contamination
Piece has bacterium smooth in sterile letheen planar surface up；With semi-solid agar 3.0mL~5.0mL, uniform fold is in microbiological contamination sample
Piece surface sets culture 18h in 37 DEG C of incubators~for 24 hours, observes result；Test bacteria suspension is separately made into appropriate dilution, makes its concentration
For 1 × 103cfu/mL~2 × 103cfu/mL, its 0.1mL drop dye is taken to smoothen on the toilet paper without antibacterial effect, with examination
It tests after a group print does same processing, with putting in a plate, is covered and cultivated with semi-solid agar, as positive control；It tests simultaneously,
Bacteria suspension is tested as count plate, and the culture for observing the control tested bacterium of print without antibacterial agent counts, test repeats 5
Secondary, obtained antibiotic rate is as shown in the table:
Wherein, the calculating of antibiotic rate: antibiotic rate=[(control average colony number-test average colony number)/control average colony
Number] × 100%.
From the data in above table it can be seen that toilet paper antibacterial effect of the invention is significant, to Staphylococcus aureus
Bacterium, Escherichia coli, Candida albicans, salmonella antibiotic rate reach 99.9% or more.
Claims (8)
1. a kind of Antimicrobial sanitation paper, it is characterised in that: the raw material including following parts by weight: 30-40 parts of eucalyptus leaves wood pulp material, rhizome of chuanxiong
30-40 parts of leaf wood pulp material, 20-30 parts of kuh-seng leaf wood pulp material, 5-10 parts of bamboo pulp, 0.5-1.5 parts of softener, 3-7 parts of antibacterial agent；Institute
The antibacterial agent stated is the compound of attapulgite load composite essential oil.
2. a kind of Antimicrobial sanitation paper according to claim 1, it is characterised in that: the raw material including following parts by weight: eucalyptus
36 parts of leaf wood pulp material, 35 parts of rhizome of chuanxiong leaf wood pulp material, 28 parts of kuh-seng leaf wood pulp material, 7 parts of bamboo pulp, 1 part of softener, 5 parts of antibacterial agent；Institute
The antibacterial agent stated is the compound of attapulgite load composite essential oil.
3. a kind of Antimicrobial sanitation paper according to claim 1, it is characterised in that: in the antibacterial agent composite essential oil be by
Tea tree ethereal oil, galic essential oil, thyme essential oil mix.
4. a kind of Antimicrobial sanitation paper according to claim 3, it is characterised in that: tea tree ethereal oil in the composite essential oil,
Galic essential oil, thyme essential oil mass ratio be 1:0.5-1:0.5-1.
5. a kind of Antimicrobial sanitation paper according to claim 4, it is characterised in that: tea tree ethereal oil in the composite essential oil,
Galic essential oil, thyme essential oil mass ratio be 1:0.8:0.7.
6. a kind of Antimicrobial sanitation paper according to claim 1, it is characterised in that: the antibacterial agent is made with the following method
It is standby to form: by attapulgite in 420-520 DEG C of roasting 0.8-1.8h, the attapulgite after roasting being added in deionized water, is surpassed
Sound disperses to form suspension system, and composite essential oil is taken to be dissolved in sorbierite, is then added in attapulgite suspension system, in magnetic force
It is centrifugally separating to obtain precipitating after 70-78 DEG C of stirring 1.5-2.5h on blender, by ground 300-400 mesh after precipitating drying
It is spare.
7. a kind of Antimicrobial sanitation paper according to claim 1, it is characterised in that: the softener is selected from imidazoline quaternary ammonium salt
Any one in class, ethylene ketone softening agent.
8. a kind of processing method of Antimicrobial sanitation paper, it is characterised in that: specific step is as follows:
(1) eucalyptus leaves wood pulp material, rhizome of chuanxiong leaf wood pulp material, kuh-seng leaf wood pulp material, bamboo pulp, softener, antibacterial agent are stirred
It is even, manufacture paper with pulp into l Water Paper page；
(2) by l Water Paper page cylinder dried, page moisture content is controlled in 6-10%；
(3) dry page will be completed to carry out scraper corrugation, batch coiled, preservation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910054819.9A CN109674377A (en) | 2019-01-21 | 2019-01-21 | A kind of Antimicrobial sanitation paper and its processing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910054819.9A CN109674377A (en) | 2019-01-21 | 2019-01-21 | A kind of Antimicrobial sanitation paper and its processing method |
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| Publication Number | Publication Date |
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| CN109674377A true CN109674377A (en) | 2019-04-26 |
Family
ID=66193749
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| CN201910054819.9A Pending CN109674377A (en) | 2019-01-21 | 2019-01-21 | A kind of Antimicrobial sanitation paper and its processing method |
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|---|---|---|---|---|
| JP2014054286A (en) * | 2012-09-11 | 2014-03-27 | Clinpet Japan:Kk | Toilet paper |
| CN105951494A (en) * | 2016-07-04 | 2016-09-21 | 山东太阳纸业股份有限公司 | Preparation method of toilet paper containing high-yield pulp |
| CN106235936A (en) * | 2016-07-28 | 2016-12-21 | 义乌市义南纸业有限公司 | A kind of environmental protection unstressed configuration agent body paper medicated napkin and preparation method thereof |
| KR20170000156A (en) * | 2015-06-23 | 2017-01-02 | 박승달 | the functional ionic water tissue |
| CN106592323A (en) * | 2015-10-20 | 2017-04-26 | 青岛益邦瑞达生物科技有限公司 | Preparation method of hemorrhoids-preventing toilet paper |
| CN107012741A (en) * | 2017-04-27 | 2017-08-04 | 舒尔环保科技（合肥）有限公司 | A kind of air purification filter paper and preparation method containing attapulgite clay |
| CN108103847A (en) * | 2017-12-26 | 2018-06-01 | 合肥洁诺无纺布制品有限公司 | A kind of medical tissue of disinfection |
| CN108221453A (en) * | 2017-12-29 | 2018-06-29 | 云南云景林纸股份有限公司 | A kind of preparation method of pure wood pulp true qualities paper for daily use |
| CN108867163A (en) * | 2018-08-06 | 2018-11-23 | 合肥龙发包装有限公司 | A kind of non-grease proofing food wrapper of overlay film type |
-
2019
- 2019-01-21 CN CN201910054819.9A patent/CN109674377A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014054286A (en) * | 2012-09-11 | 2014-03-27 | Clinpet Japan:Kk | Toilet paper |
| KR20170000156A (en) * | 2015-06-23 | 2017-01-02 | 박승달 | the functional ionic water tissue |
| CN106592323A (en) * | 2015-10-20 | 2017-04-26 | 青岛益邦瑞达生物科技有限公司 | Preparation method of hemorrhoids-preventing toilet paper |
| CN105951494A (en) * | 2016-07-04 | 2016-09-21 | 山东太阳纸业股份有限公司 | Preparation method of toilet paper containing high-yield pulp |
| CN106235936A (en) * | 2016-07-28 | 2016-12-21 | 义乌市义南纸业有限公司 | A kind of environmental protection unstressed configuration agent body paper medicated napkin and preparation method thereof |
| CN107012741A (en) * | 2017-04-27 | 2017-08-04 | 舒尔环保科技（合肥）有限公司 | A kind of air purification filter paper and preparation method containing attapulgite clay |
| CN108103847A (en) * | 2017-12-26 | 2018-06-01 | 合肥洁诺无纺布制品有限公司 | A kind of medical tissue of disinfection |
| CN108221453A (en) * | 2017-12-29 | 2018-06-29 | 云南云景林纸股份有限公司 | A kind of preparation method of pure wood pulp true qualities paper for daily use |
| CN108867163A (en) * | 2018-08-06 | 2018-11-23 | 合肥龙发包装有限公司 | A kind of non-grease proofing food wrapper of overlay film type |
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Application publication date: 20190426 |