CN109652177A - A kind of Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus - Google Patents
A kind of Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus Download PDFInfo
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- CN109652177A CN109652177A CN201811612461.9A CN201811612461A CN109652177A CN 109652177 A CN109652177 A CN 109652177A CN 201811612461 A CN201811612461 A CN 201811612461A CN 109652177 A CN109652177 A CN 109652177A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/16—Naphthenic acids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/08—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having metal-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/40—Low content or no content compositions
- C10N2030/42—Phosphor free or low phosphor content compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/40—Low content or no content compositions
- C10N2030/43—Sulfur free or low sulfur content compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The present invention relates to industrial oil additive technology fields, provide a kind of Novel oil product additive of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus.The additive is made of the raw material of following mass parts: 32-38 parts of non-sulphur phosphorus organic-molybdenum, 32-38 parts of cetyl line borate (T362), 6-10 parts of high base number calcium mahogany sulfonate, 6-10 parts of turbine oil, 5-9 parts of aviation kerosine, 3-5 parts of aphthenic acids, 2-4 parts of steady spar ink.Novel oil product additive provided by the invention, without sulphur, without phosphorus, nontoxic, as additive application in base oil, it is good in compatibility, the abrasion resistance of product oil can be effectively improved, can be used in vapour, bavin engine oil, I. C. engine oil, gear oil, antiwear hydraulic oil, metal-cutting oil, metal forming oil and lubricating grease as single dose.
Description
Technical field
The present invention relates to industrial oil additive technology fields, and in particular to a kind of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus it is new
Type oil dope.
Background technique
According to according to data, the metal material of the annual about one third in the whole world is consumed in oxidation corrosion and mechanical wear, I
Annual up to more than 1,800 hundred million yuan of the loss of state's this respect, it is seen that prevent metal erosion and improvement lubrication abrasion resistance how important.Half
Since a more centuries, people have done unremitting effort in terms of improving greasy property, have developed more in research and development extreme-pressure anti-wear antifriction finish
Kind single dose and multiple agent.Such as sulphur phosphorous (SP) gear oil extreme pressure antiwear additive, I. C. engine oil, antiwear hydraulic oil dialkyl dithio phosphorus
Sour zinc (ZDDP) antioxygen, anti-rotten, wear-resistant multipurpose, organic copper and nano-copper sulfide anti-friction agent, aquadag, molybdenum dioxide gather
Tetrafluoroethene antifriction and antiwear agents etc., these additives have preferable effect to mechanical extreme-pressure anti-wear antifriction performance is improved.
In recent years, country increasingly payes attention to environmental protection, and the cry of energy-saving and emission-reduction, low-carbon environment-friendly is increasingly strong.In order to save
The energy and the economy for improving fuel oil, it is higher and higher to the performance requirement of lube oil additive, while environmental requirement is again to lubrication
Oil proposes the low-phosphorous requirement of low-sulfur.In face of the pressure and limitation of environmental protection, it is highly important that multiple additives, which select compatibility,.It crosses
Go during the decade, I. C. engine oil under conditions of quality constantly upgrades, additive total amount (without it is viscous refer to, pour-point depressant) from 10% -12%
Be down to 5% -10%, mainly by selecting single dose pleiotropism and optimization to multiple agent compatibility, should according to energy-saving and environmental protection regulation,
Application and cost performance are optimized with the optimization of realisation effect cost；It is no more than in advanced steam turbine oil by phosphorus content
Under 0.08% requirement, the use of ZDDP is restricted, and under the pressure of numerous control, people have to find new additive agent
Substitution.
Summary of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of the novel of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus
Oil dope.
To achieve the goals above, the present invention adopts the following technical scheme:
A kind of Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus, is made of the raw material of following mass parts: non-sulphur phosphorus has
32-38 parts of machine molybdenum, 32-38 parts of cetyl line borate (T362), 6-10 parts of high base number calcium mahogany sulfonate, 6-10 parts of turbine oil,
5-9 parts of aviation kerosine, 3-5 parts of aphthenic acids, 2-4 parts of steady spar ink.
As a representative formula, the Novel oil product additive of the nontoxic extreme-pressure anti-wear of a kind of not sulfur-bearing phosphorus, by following quality
Part raw material composition: non-35 parts of sulphur phosphorus organic-molybdenum, 35 parts of cetyl line borate (T362), 8 parts of high base number calcium mahogany sulfonate, thoroughly
Flat 8 parts of oil, 7 parts of aviation kerosine, 4 parts of aphthenic acids, 3 parts of steady spar ink.
Beneficial effects of the present invention:
Non- sulphur phosphorus organic molybdenum additive is a kind of oil-soluble molybdenum ammonium complex compound, it and molybdenum dialkyl-dithiophosphate, sulphur phosphorus nitrogen molybdenum
Difference with molybdenum dialkyldithiocarbamacompositions is, not sulfur-bearing and phosphorus in the molecular structure of non-sulphur phosphorus organic molybdenum additive,
Most important is that non-sulphur phosphorus organic-molybdenum has splendid compatibility, can be used as lubricating oil especially I. C. engine and moistens
The friction improver of lubricating oil, antiwear additive and antioxidant.
Borate family additive is low with coefficient of friction, bearing capacity is strong, wear resistence is better, oxidation resistance temperature is high, changes oil
The advantages that period length, good dispersion, capacity of resisting impact load are strong, intermiscibility is good, can be one times of prolonged mechanical service life or more.
The present invention with non-sulphur phosphorus organic-molybdenum, cetyl line borate (T362) be major ingredient, be aided with high base number calcium mahogany sulfonate,
Turbine oil, aviation kerosine, aphthenic acids, steady spar ink, form a kind of novel oil dope, no sulphur, without phosphorus, nontoxic, as
Additive application is good in compatibility in base oil, can effectively improve the abrasion resistance of product oil, can be in vapour, bavin engine
It is used in oil, I. C. engine oil, gear oil, antiwear hydraulic oil, metal-cutting oil, metal forming oil and lubricating grease as single dose.
Specific embodiment
The present invention is described further combined with specific embodiments below.
Embodiment one
A kind of Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus, is made of the raw material of following mass parts: non-sulphur phosphorus has
35 parts of machine molybdenum, 35 parts of cetyl line borate (T362), 8 parts of high base number calcium mahogany sulfonate, 8 parts of turbine oil, 7 parts of aviation kerosine,
4 parts of aphthenic acids, 3 parts of steady spar ink.
Embodiment two
The Novel oil product additive of the nontoxic extreme-pressure anti-wear of a kind of not sulfur-bearing phosphorus, which is characterized in that by the raw material group of following mass parts
At: non-32 parts of sulphur phosphorus organic-molybdenum, 36 parts of cetyl line borate (T362), 7 parts of high base number calcium mahogany sulfonate, 7 parts of turbine oil, boat
8 parts of empty kerosene, 3 parts of aphthenic acids, 4 parts of steady spar ink.
Embodiment three
The Novel oil product additive of the nontoxic extreme-pressure anti-wear of a kind of not sulfur-bearing phosphorus, which is characterized in that by the raw material group of following mass parts
At: non-38 parts of sulphur phosphorus organic-molybdenum, 32 parts of cetyl line borate (T362), 10 parts of high base number calcium mahogany sulfonate, 10 parts of turbine oil,
5 parts of aviation kerosine, 5 parts of aphthenic acids, 2 parts of steady spar ink.
Example IV
The Novel oil product additive of the nontoxic extreme-pressure anti-wear of a kind of not sulfur-bearing phosphorus, which is characterized in that by the raw material group of following mass parts
At: non-34 parts of sulphur phosphorus organic-molybdenum, 38 parts of cetyl line borate (T362), 6 parts of high base number calcium mahogany sulfonate, 6 parts of turbine oil, boat
9 parts of empty kerosene, 4 parts of aphthenic acids, 3 parts of steady spar ink.
The Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus provided by the invention, physical and chemical index are as shown in table 1.
The physical and chemical index of 1 product of the present invention of table
Oil-soluble comparative test:
New product and certain external brand (containing organic-molybdenum) are added to three kinds of 150SN, 500BS and III class hydrogenated oil with identical dosage
In base oil, compare its oil-soluble, test result is shown in Table 2.
The oil-soluble comparative test of 2 product of table
Abrasion resistance comparative test:
New product and certain external brand (containing organic-molybdenum) are added in 150SN base oil with identical dosage respectively, utilize four balls
Method has rated the wear scar diameter under 392N and 294N, four ball of four ball of extreme pressure (3142) maximum nonseizure load PB and extreme pressure respectively
(3142) sintering load PD, test result are shown in Table 3.
The wear resistance comparative test of 3 product of table
The compatibility coordinative role comparative test of product of the present invention and ZDDP:
By product of the present invention and certain external brand (containing organic-molybdenum) respectively with identical dosage and ZDDP(T202- dialkyl
Trbasic zinc phosphate) various dose proportion, it is then added in 150SN base oil, has rated the mill of 392N and 294N respectively using four ball method
Spot Taoist scripture, four ball of extreme pressure (3142) maximum nonseizure load PB and four ball of extreme pressure (3142) sintering load PD, test result are shown in Table
4。
The wear-resistant coordination performance comparison test of 4 product of table and T202
It can be seen from the above result that product of the present invention as additive application in base oil, it is good in compatibility, can effectively improve
The abrasion resistance of product oil, can be with ZDDP(T202- zine dialkyldithiophosphates) it is used in compounding, reach more excellent performance.
It is to be understood that being merely to illustrate the present invention above with respect to specific descriptions of the invention and being not limited to this
Technical solution described in inventive embodiments, those skilled in the art should understand that, still the present invention can be carried out
Modification or equivalent replacement, to reach identical technical effect；As long as meet use needs, all protection scope of the present invention it
It is interior.
Claims (5)
1. a kind of Novel oil product additive of the not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus, which is characterized in that by the raw material of following mass parts
Composition: 32-38 parts of non-sulphur phosphorus organic-molybdenum, 32-38 parts of cetyl line borate (T362), 6-10 parts of high base number calcium mahogany sulfonate,
6-10 parts of turbine oil, 5-9 parts of aviation kerosine, 3-5 parts of aphthenic acids, 2-4 parts of steady spar ink.
2. a kind of Novel oil product additive of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus according to claim 1, which is characterized in that
It is made of the raw material of following mass parts: non-35 parts of sulphur phosphorus organic-molybdenum, 35 parts of cetyl line borate (T362), high base number petroleum sulphur
8 parts of sour calcium, 8 parts of turbine oil, 7 parts of aviation kerosine, 4 parts of aphthenic acids, 3 parts of steady spar ink.
3. a kind of Novel oil product additive of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus according to claim 1, which is characterized in that
It is made of the raw material of following mass parts: non-32 parts of sulphur phosphorus organic-molybdenum, 36 parts of cetyl line borate (T362), high base number petroleum sulphur
7 parts of sour calcium, 7 parts of turbine oil, 8 parts of aviation kerosine, 3 parts of aphthenic acids, 4 parts of steady spar ink.
4. a kind of Novel oil product additive of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus according to claim 1, which is characterized in that
It is made of the raw material of following mass parts: non-38 parts of sulphur phosphorus organic-molybdenum, 32 parts of cetyl line borate (T362), high base number petroleum sulphur
10 parts of sour calcium, 10 parts of turbine oil, 5 parts of aviation kerosine, 5 parts of aphthenic acids, 2 parts of steady spar ink.
5. a kind of Novel oil product additive of not nontoxic extreme-pressure anti-wear of sulfur-bearing phosphorus according to claim 1, which is characterized in that
It is made of the raw material of following mass parts: non-34 parts of sulphur phosphorus organic-molybdenum, 38 parts of cetyl line borate (T362), high base number petroleum sulphur
6 parts of sour calcium, 6 parts of turbine oil, 9 parts of aviation kerosine, 4 parts of aphthenic acids, 3 parts of steady spar ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811612461.9A CN109652177A (en) | 2018-12-24 | 2018-12-24 | A kind of Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811612461.9A CN109652177A (en) | 2018-12-24 | 2018-12-24 | A kind of Novel oil product additive of the nontoxic extreme-pressure anti-wear of not sulfur-bearing phosphorus |
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| CN109652177A true CN109652177A (en) | 2019-04-19 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1160753A (en) * | 1996-06-06 | 1997-10-01 | 李平 | Multifunctional efficient, energy-saving and antiwear composite additive for modifying lubricating oil |
| US9228151B1 (en) * | 2012-11-07 | 2016-01-05 | Rand Innovations, Llc | Lubricant additive composition, lubricant, and method of preparing the same |
| CN105400577A (en) * | 2015-12-02 | 2016-03-16 | 烟台狮王石化工业有限公司 | Nano borate engine oil |
| CN105542922A (en) * | 2016-01-07 | 2016-05-04 | 北京雅士科莱恩石油化工有限公司 | Energy-saving diesel engine oil with ultra-long oil change mileage and preparation method thereof |
| CN107312598A (en) * | 2017-06-30 | 2017-11-03 | 北京雅士科莱恩石油化工有限公司 | A kind of overweight load synthetic gear oil of low temperature |
-
2018
- 2018-12-24 CN CN201811612461.9A patent/CN109652177A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1160753A (en) * | 1996-06-06 | 1997-10-01 | 李平 | Multifunctional efficient, energy-saving and antiwear composite additive for modifying lubricating oil |
| US9228151B1 (en) * | 2012-11-07 | 2016-01-05 | Rand Innovations, Llc | Lubricant additive composition, lubricant, and method of preparing the same |
| CN105400577A (en) * | 2015-12-02 | 2016-03-16 | 烟台狮王石化工业有限公司 | Nano borate engine oil |
| CN105542922A (en) * | 2016-01-07 | 2016-05-04 | 北京雅士科莱恩石油化工有限公司 | Energy-saving diesel engine oil with ultra-long oil change mileage and preparation method thereof |
| CN107312598A (en) * | 2017-06-30 | 2017-11-03 | 北京雅士科莱恩石油化工有限公司 | A kind of overweight load synthetic gear oil of low temperature |
Non-Patent Citations (1)
| Title |
|---|
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