CN109609266A - A kind of quick-fried pearl cream jasmin france of cigarette, preparation method and application - Google Patents
A kind of quick-fried pearl cream jasmin france of cigarette, preparation method and application Download PDFInfo
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- CN109609266A CN109609266A CN201811632310.XA CN201811632310A CN109609266A CN 109609266 A CN109609266 A CN 109609266A CN 201811632310 A CN201811632310 A CN 201811632310A CN 109609266 A CN109609266 A CN 109609266A
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- Prior art keywords
- jasmine
- cigarette
- quick
- fried pearl
- eluent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Seasonings (AREA)
Abstract
A kind of quick-fried pearl cream jasmin france of cigarette, preparation method and application, the cream jasmin france is by each at being grouped as of following mass percents: benzyl acetate 10 ~ 20%, methyl jasmonate 2 ~ 10%, jasmine lactone 10 ~ 20%, nerolidol 3 ~ 6%, linalool 15 ~ 25%, jasmone 10 ~ 20%, benzylalcohol 10 ~ 15%.The present invention prepares the cigarette with jasmin for the first time, and for raw material needed for deploying cream jasmin france by separating obtained in natural products concrete of jasmine, avoids synthetic perfume only and have natural perfume material " shape " and the defect of " mind " without natural perfume material.And by the separation of column chromatography technology, the macromolecular complex confrontation cigarette sensory quality such as pectin, protein, fiber brings the influence of miscellaneous gas in reduction concrete of jasmine, essential oil.Quick-fried pearl prepared by the present invention can lower the irritation of cigarette, cover cigarette foreign gas, the characteristic chicken flavor of cigarette jasmin can be assigned while improving the comfort level of cigarette.
Description
Technical field
The invention belongs to flavors and fragrances fields, and in particular to a kind of quick-fried pearl cream jasmin france of cigarette, preparation method and answer
With.
Background technique
Jasmine (Jasminum sambac) it is Oleaceae evergreen shrubs or liana, from ancient times to the present, Jasmine is because of it
The fragrance of simple and elegant strong fragrance is liked that the fragrance such as refined jasmine oil, medicinal extract for extracting from Jasmine are widely used in essence by people
Fragrance industry.On the one hand can be used to make daily use chemicals essence as fragrance, especially when modulating highclass perfumes jasmine perfume (or spice)
Gas is essential ingredient, or even has the saying " without jasmine just without perfume ".Jasmine fragrance may be alternatively used for production food
Edible essence in product is especially used for the essence of sweet wine cake, flavouring and bakery product.
Traditional flavoring technology is flavors and fragrances to be added in cigarette shreds, but essence added by this mode is fragrant
Often with pipe tobacco burning many chemical changes can occur for material, generate artificial uncontrollable factor, and added essence
Fragrance can lose as pipe tobacco burns.Compared to traditional flavoring technology, the quick-fried pearl flavoring of cigarette is as a kind of novel volume
Cigarette flavoring mode, this flavoring mode can effectively avoid loss of fragrance during result of combustion of tobacco, can to a certain extent gram
Take the defects of traditional flavoring mode.
With the raising of the level of consumption, people are more and more to cigarette taste requirements, in order to meet consumer's different taste
Demand, in the market occur have the quick-fried pearl of various different tastes cigarette.107034019 A of CN discloses a kind of quick-fried pearl of cigarette
With red-jujube flavor essence and its application in cigarette, prepared quick-fried pearl can cigarette mitigate cigarette irritation, promote cigarette
It is rich.107142153 A of CN discloses a kind of cigarette quick-fried pearl fructus lycii essence and its application in cigarette, can be preferable
Weaken the irritation of cigarette, improves and abundant cigarette flavor, the fragrance for being obviously improved cigarette are rich.But there is jasmin
The cigarette of taste has not been reported, and above patent essence used is deploy with medicinal extract, absolute oil and synthetic perfume.This
Invention is to be separated from concrete of jasmine using column chromatography technology, concrete of jasmine characteristic chicken flavor ingredient is prepared, because synthesis is fragrant
Material only has " shape " of natural perfume material and " mind " of natural perfume material is not available for synthetic perfume.And skill is chromatographed by column
Macromolecular substances in concrete of jasmine are removed by art, are reduced cigarette medicinal extract, the macromolecular in absolute oil, are reduced macromolecular complex
The unfavorable factor of confrontation cigarette sensory quality.
Summary of the invention
It is an object of that present invention to provide it is a kind of targetedly in cigarette filter rod cream jasmin france, preparation method and
Using, thus abundant cigarette product type, to provide the cigarette product of different-style feature.
A kind of method for separating and preparing of jasmine characteristic component, using concrete of jasmine as raw material, silica gel is adsorbent, petroleum ether-
Ethyl acetate is eluant, eluent, is separated, is prepared to concrete of jasmine characteristic component, specifically includes the following steps:
(1) silica gel is weighed in beaker, and eluant, eluent is added, disposably pours into the cm splitter of Φ 2.1cm × 70 after mixing evenly
In；
(2) concrete of jasmine is weighed in eggplant-shape bottle, is added in splitter with after ethyl acetate dissolved dilution after processing；
(3) eluant, eluent flow velocity is controlled with constant flow pump, is in charge of collection eluent with collector；
(4) eluent collected by every pipe is concentrated with Rotary Evaporators, and collected eluent is detected with GC-MS
Analysis；
(5) merge the concentrate with same composition, remove solvent therein with rotary evaporator to get jasmine characteristic component,
The jasmine characteristic component includes benzyl acetate, methyl jasmonate, jasmine lactone, nerolidol, linalool, jasmone and benzyl
Alcohol.
Further, the granularity of selected silica gel is 200-300 mesh in the step (1), and the weighed silica gel quality of institute is
120 g；The volume ratio of petroleum ether and ethyl acetate is 12-4:1.
Further, weighed concrete of jasmine is 0.6 g in the step (2).
Further, the flow velocity of eluant, eluent is 3 mL/min in the step (3).
Further, every gradient elution agent volume is 400 mL, and eluant, eluent is temporally collected, and every pipe acquisition time is 12
min。
A kind of quick-fried pearl cream jasmin france of cigarette, by each at being grouped as of following mass percents: benzyl acetate 10 ~ 20%, jasmine
Jasmine ketone acid methyl esters 2 ~ 10%, jasmine lactone 10 ~ 20%, nerolidol 3 ~ 6%, linalool 15 ~ 25%, jasmone 10 ~ 20%, benzylalcohol 10 ~
15%。
The method that above-mentioned cream jasmin france preparation has the quick-fried pearl of cigarette of Jasmine note feature, cream jasmin france and Xin Kui acid are sweet
Grease (10-16) in mass ratio: it is added in quick-fried pearl after (84-90) dilution.
The quick-fried pearl of cigarette refers to natural macromolecular material or synthesizes high molecular material, and flavors and fragrances is wrapped in one
Among closed quick-fried pearl, a kind of quick-fried pearl of sealing with round different colours in the majority is formed, the diameter of quick-fried pearl is 2.0 ~ 4.0mm,
Essence content is 20 ~ 30 μ L/ in quick-fried pearl；Specifically for example: quick-fried pearl diameter is 4mm, weight is 30mg/；Essence contains in quick-fried pearl
Amount is 29 μ L/, in short, its concrete specification can be adjusted according to machinery equipment difference and institute using filter stick specification difference.
Application of the quick-fried pearl of cigarette with Jasmine note feature in cigarette, the quick-fried pearl of cigarette is made an addition to commonly
In (circumference 24.3mm) cigarette filter rod, quick-fried pearl position is apart from lip end 12.5mm, and every cigarette adds a quick-fried pearl.
The beneficial effects of the invention are that preparing the cigarette with jasmin for the first time, and for deploying cream jasmin france institute
The raw material needed by separating obtained in natural products concrete of jasmine, avoid synthetic perfume only there is natural perfume material " shape " and without natural
The defect of " mind " of fragrance.And pass through the separation of column chromatography technology, pectin, protein, fiber in reduction concrete of jasmine, essential oil
Equal macromolecular complex confrontation cigarette sensory quality brings the influence of miscellaneous gas.Quick-fried pearl prepared by the present invention can lower the thorn of cigarette
Swash property, cover cigarette foreign gas, the characteristic chicken flavor of cigarette jasmin can be assigned while improving the comfort level of cigarette, to provide
The cigarette product of different-style feature.
Detailed description of the invention
Fig. 1 be with the total ion current figure of concrete of jasmine of the present invention under the conditions of GC-MS combination analysis, in figure, 1. benzylalcohols, 2. second
Sour Bian ester, 3. jasmones, 4. jasmine lactones, 5. methyl jasmonates；Nerolidol and fragrant alcohol content are less not in figure acceptance of the bid
Out.
Specific embodiment
The present invention is further explained combined with specific embodiments below, and is only used for further specific descriptions of the invention.
Concrete of jasmine in following embodiments is purchased from Yunnan Reascend Tobacco Tech.(Group) Co., Ltd., gained jasmine
Medicinal extract is detailed in Fig. 1 with the total ion current figure of GC-MS combination analysis concrete of jasmine of the present invention, is carried out by standard spectrum library NIST14.L
Compare the characteristic component extracted needed for determining in the application.
Embodiment 1
A kind of method for separating and preparing of jasmine characteristic component, steps are as follows:
(1) 120 g of silica gel is weighed in 500 mL beakers, and the mixing that petroleum ether and ethyl acetate that volume ratio is 12:1 is added is molten
Agent, disposably pours into the cm splitter of Φ 2.1cm × 70 after stirring, repeated flushing makes the uniform consolidation of silica gel；
(2) 0.6 g of concrete of jasmine is weighed in 50 mL eggplant-shape bottles, 2 mL ethyl acetate dissolved dilutions are added, then with disposable
Dropper is slowly evenly laid out on silica gel face by the concrete of jasmine after dilution；
It (3) is 3mL/min with DHL-N computer digital display timing constant flow pump control eluant, eluent flow velocity, according to petroleum ether and ethyl acetate
Volume proportion is that 12-4:1 gradient is eluted, and each gradient elution agent volume is 400 mL, with DBS-40 computer full-automatic portion
Part collector is in charge of collection eluent, and every pipe collects 12 min；
(4) eluent that each test tube is collected is concentrated into 5 mL with Rotary Evaporators, takes appropriate concentrate in chromatogram bottle, carries out
It tests and analyzes, the eluent with identical component is merged, be concentrated under reduced pressure and remove solvent, obtain jasmine characteristic component；
(5) detection and standard spectrum library NIST14.L are compared after GC-MS analysis, save the required benzyl acetate of the present invention, jasmine
The substances such as jasmine ketone acid methyl esters, jasmine lactone, nerolidol, linalool, jasmone, benzylalcohol.
The cream jasmin france of the present embodiment is calculated in mass percent by following material composition: 15% benzyl acetate, 5% jasmonic acid
Methyl esters, 20% jasmine lactone, 5% nerolidol, 25% linalool, 20% jasmone, 10% benzylalcohol.
It is prepared after cream jasmin france and Xin Kui acid glyceride 14:86 in mass ratio dilution with Jasmine feature note
The quick-fried pearl of cigarette, the diameter of quick-fried pearl are 4mm.Essence content is 29 μ L/ in quick-fried pearl.
The theoretical content value of each characteristic component in concrete of jasmine: 285362.37 μ g/g of acetic acid Bian ester, methyl jasmonate
17145.68 μ g/g, 16323.61 μ g/g of jasmine lactone, 58120.61 μ g/g of nerolidol, 23564.61 μ g/g of linalool, jasmine
37699.19 μ g/g of jasmine ketone, 35465.50 μ g/g of benzylalcohol；
The extraction content and recovery rate of each characteristic component in concrete of jasmine: benzyl acetate extracts 104785.06 μ g/g, recovery rate
36.72%；Methyl jasmonate extracts 360.06 μ g/g, recovery rate 2.10%；Jasmine lactone extracts 171.40 μ g/g, mentions
Taking rate is 1.05%；Nerolidol extracts 871.81 μ g/g, recovery rate 1.50%；Linalool extracts 294.56 μ g/g, mentions
Taking rate is 1.25%；Jasmone extracts 376.99 μ g/g, recovery rate 1.00%；Benzylalcohol extracts 602.91 μ g/g, recovery rate
It is 1.70%.
Embodiment 2
Jasmine characteristic chicken flavor ingredient benzyl acetate, methyl jasmonate, jasmine lactone, flores aurantii are obtained by prepared in embodiment 1
The tertiary alcohol, linalool, jasmone, benzylalcohol substance are configured to cream jasmin france according to mass percent, and ratio is as follows:
20% benzyl acetate, 10% methyl jasmonate, 16% jasmine lactone, 6% nerolidol, 20% linalool, 20% jasmone, 8%
Benzylalcohol.
The volume with Jasmine note feature is prepared according to mass ratio 10:90 in refined jasmine oil and Xin Kui acid glyceride
The quick-fried pearl of cigarette, the diameter of quick-fried pearl are 2mm.Essence content is 22 μ L/ in quick-fried pearl.
Embodiment 3
Jasmine flower concrete characteristic chicken flavor ingredient benzyl acetate, methyl jasmonate are obtained, in jasmine for prepared in embodiment 1
Ester, nerolidol, linalool, jasmone, benzylalcohol substance are configured to cream jasmin france, the following institute of ratio according to mass percent
Show:
12% benzyl acetate, 8% methyl jasmonate, 20% jasmine lactone, 4% nerolidol, 24% linalool, 20% jasmone, 12%
Benzylalcohol.
The volume with Jasmine feature note is prepared according to mass ratio 12:88 in refined jasmine oil and Xin Kui acid glyceride
The quick-fried pearl of cigarette, the diameter of quick-fried pearl are 2.8 mm.Essence content is 25 μ L/ in quick-fried pearl.
By existing filter stick production technology, quick-fried pearl is placed in by filter stick center by filter-stick forming device, makes an addition to common circumference
In (24.3mm) cigarette filter rod, quick-fried pearl position is apart from lip end 12.5mm, and every cigarette adds a quick-fried pearl, as quick-fried pearl filter
Stick, and be the quick-fried pearl cigarette with Jasmine note feature after cigarette cigarette sample.
To the prepared quick-fried pearl cigarette with Jasmine note feature, by 7 professional sensory evaluation personnel to the sample
Suction evaluation is detected and compared with reference examples blank cigarette sample (same position adds the quick-fried pearl of blank).
Flue gas inspection and specific suction evaluation score value are referring to successive table.
Quick-fried pearl product prepared by different embodiments is detected, while cigarette prepared in above-described embodiment is carried out
Conventional detection, to the physical and chemical index of diacetate fiber sample, the physical index of filter stick sample, the reason of cigarette sample in cigarette sample
Change index be measured, further according to " 19609-2004 cigarette conventional analysis of GB/T with smoking machine measure total granules and
Tar " method measurement cigarette mainstream flue gas in the indexs such as total granules, tar, nicotine and moisture detected, it is specific to tie
Fruit is as shown in the table.
The testing result of prepared quick-fried pearl in the different embodiments of table 1
(note: control sample 1,2 is with the cigarette for not adding the quick-fried pearl of cream jasmin france)
Table 2, the physical index and main flume testing result of kinds of cigarettes sample:
(note: control sample 1,2 is with the cigarette for not adding the quick-fried pearl of cream jasmin france)
It can be seen that compared with the quick-fried pearl for not placing essence from above-mentioned 1 data of table, place the cigarette with Jasmine note feature
The physical index of quick-fried pearl is without significant difference.As can be seen from Table 2, compared with the normal cigarette of reference examples, there is jasmin
The main flume of the cigarette of rhythm feature, the key index tar and nicotine for influencing cigarette sense organ are without significant changes.
Table 3, kinds of cigarettes sample sensory quality assessment result:
As can be seen from Table 3, compared with the control, it is added to the quick-fried pearl of cigarette with Jasmine note feature and can be improved and suck
The sense organ comfort level of person, personalized note is prominent, and quick-fried pearl fragrance and cigarette perfume harmony itself increase, and pleasant impression improves, irritation with
Miscellaneous gas also has larger reduction, and whole aromatic style is comfortable, coordinates, is natural.
It is emphasized that above-mentioned quick-fried pearl formula is directed to conventional formulation cigarette improvement design, when being applied to ramuscule cigarette,
Equally there is preferable application effect, but need to be added according to specific tobacco blend and design requirement to quick-fried pearl specification and in filter stick
Amount carries out appropriate adjustment, and this will not be detailed here.
Claims (8)
1. a kind of method for separating and preparing of jasmine characteristic component, which is characterized in that using concrete of jasmine as raw material, silica gel is absorption
Agent, petroleum ether-ethyl acetate are eluant, eluent, are separated, are prepared to concrete of jasmine characteristic component, specifically includes the following steps:
(1) silica gel is weighed in beaker, and eluant, eluent is added, disposably pours into splitter after mixing evenly；
(2) concrete of jasmine is weighed in eggplant-shape bottle, is added in splitter with after ethyl acetate dissolved dilution after processing；
(3) eluant, eluent flow velocity is controlled with constant flow pump, is in charge of collection eluent with collector；
(4) eluent collected by every pipe is concentrated with Rotary Evaporators, and collected eluent is detected with GC-MS
Analysis；
(5) merge the concentrate with same composition, remove solvent therein with rotary evaporator to get jasmine characteristic component,
The jasmine characteristic component includes benzyl acetate, methyl jasmonate, jasmine lactone, nerolidol, linalool, jasmone and benzyl
Alcohol.
2. the method for separating and preparing of jasmine characteristic component according to claim 1, which is characterized in that institute in the step (1)
The granularity for selecting silica gel is 200-300 mesh, and the weighed silica gel quality of institute is 120 g；Petroleum ether and ethyl acetate in eluant, eluent
Volume ratio is 12-4:1.
3. the method for separating and preparing of jasmine characteristic component according to claim 1, which is characterized in that claim in the step (2)
The concrete of jasmine taken is 0.6 g.
4. the method for separating and preparing of jasmine characteristic component according to claim 1, which is characterized in that washed in the step (3)
The flow velocity of de- agent is 3 mL/min.
5. the method for separating and preparing of jasmine characteristic component according to claim 1, which is characterized in that every gradient elution agent volume
For 400 mL, eluant, eluent is temporally collected, and every pipe acquisition time is 12 min.
6. a kind of quick-fried pearl cream jasmin france of cigarette, the jasmine feature isolated by any separation method of claim 1 to 5
At being grouped as, which is characterized in that the cream jasmin france is by each at being grouped as of following mass percents: benzyl acetate 10 ~ 20%,
Methyl jasmonate 2 ~ 10%, jasmine lactone 10 ~ 20%, nerolidol 3 ~ 6%, linalool 15 ~ 25%, jasmone 10 ~ 20%, benzylalcohol
10~15%。
7. there is the method for the quick-fried pearl of cigarette of Jasmine note feature using cream jasmin france preparation as claimed in claim 6, it is special
Sign is, cream jasmin france and Xin Kui acid glyceride (10-16) in mass ratio: is added in quick-fried pearl after (84-90) dilution.
8. utilizing the cigarette quick-fried pearl obtained with Jasmine note feature of preparation method described in claim 7, which is characterized in that
The diameter of quick-fried pearl is 2.0 ~ 4.0mm, and essence content is 20 ~ 30 μ L/ in quick-fried pearl.
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| CN201811632310.XA CN109609266A (en) | 2018-12-29 | 2018-12-29 | A kind of quick-fried pearl cream jasmin france of cigarette, preparation method and application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112048389A (en) * | 2020-09-07 | 2020-12-08 | 泛亚（武汉）食品科技有限公司 | Tea-flavored mint compound essence suitable for bead blasting for cigarettes and preparation method thereof |
| CN115637196A (en) * | 2022-09-16 | 2023-01-24 | 中国烟草总公司郑州烟草研究院 | Spice for blasting beads capable of highlighting tea fragrance characteristics of cigarettes and preparation method thereof, blasting beads and cigarettes |
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| CN102041173A (en) * | 2010-12-22 | 2011-05-04 | 华芳烟用香料有限公司 | Extraction and separation method of aromatic part in aromatic tobacco extract and application thereof to cigarettes |
| CN104560399A (en) * | 2014-12-16 | 2015-04-29 | 湖北中烟工业有限责任公司 | Method for purifying jasmine flower extract for cigarettes |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102041173A (en) * | 2010-12-22 | 2011-05-04 | 华芳烟用香料有限公司 | Extraction and separation method of aromatic part in aromatic tobacco extract and application thereof to cigarettes |
| CN104560399A (en) * | 2014-12-16 | 2015-04-29 | 湖北中烟工业有限责任公司 | Method for purifying jasmine flower extract for cigarettes |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112048389A (en) * | 2020-09-07 | 2020-12-08 | 泛亚（武汉）食品科技有限公司 | Tea-flavored mint compound essence suitable for bead blasting for cigarettes and preparation method thereof |
| CN115637196A (en) * | 2022-09-16 | 2023-01-24 | 中国烟草总公司郑州烟草研究院 | Spice for blasting beads capable of highlighting tea fragrance characteristics of cigarettes and preparation method thereof, blasting beads and cigarettes |
| CN115637196B (en) * | 2022-09-16 | 2024-03-22 | 中国烟草总公司郑州烟草研究院 | Bead-bursting perfume capable of highlighting clear fragrance characteristics of cigarette tea, preparation method of bead-bursting perfume, bead-bursting perfume and cigarette |
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