CN109608258A - A kind of micro-emulsion type Water soluble fertilizer anticaking agent and preparation method thereof - Google Patents
A kind of micro-emulsion type Water soluble fertilizer anticaking agent and preparation method thereof Download PDFInfo
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- CN109608258A CN109608258A CN201811598656.2A CN201811598656A CN109608258A CN 109608258 A CN109608258 A CN 109608258A CN 201811598656 A CN201811598656 A CN 201811598656A CN 109608258 A CN109608258 A CN 109608258A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of micro-emulsion type Water soluble fertilizer anticaking agents and preparation method thereof, are related to Water soluble fertilizer preventing blocking technology field;A kind of micro-emulsion type Water soluble fertilizer anticaking agent, the raw material including following parts by weight: 10-30 parts of low-carbon alcohols, 5-25 parts of surfactant, 20-40 parts of anti-caking oil, 30-50 parts of vermiculite power and 30-55 parts of sepiolite powder.The invention also provides the preparation methods of above-mentioned micro-emulsion type Water soluble fertilizer anticaking agent.Micro-emulsion type Water soluble fertilizer anticaking agent produced by the present invention is when in use by its even application on the surface of solid Water soluble fertilizer;Excellent preventing blocking effect is played to solid Water soluble fertilizer;Solid Water soluble fertilizer by the progress spray attachment anti-caking processing of micro-emulsion type Water soluble fertilizer anticaking agent can quickly dissolve in water when in use, and deposit without oil slick in field contamination-free, harmless to soil and soil property, and can improve soil quality, promote plant growth.
Description
Technical field
The present invention relates to Water soluble fertilizer preventing blocking technology field more particularly to a kind of micro-emulsion type Water soluble fertilizer anticaking agent and its systems
Preparation Method.
Background technique
Water-soluble fertilizer is to refer to be dissolved completely in the nitrogenous of water, phosphorus, potassium, calcium, magnesium, microelement, amino acid, rotten plant
The compound fertilizers such as acid, alginic acid.Being divided to from form has solid Water soluble fertilizer and two kinds of liquid Water soluble fertilizer;Water soluble fertilizer is a kind of speed
Effect property fertilizer;The good water solubility of water soluble fertilizer, without residue, can completely dissolve in water;Water soluble fertilizer can be by crop
Root system and blade face are directly absorbed and utilized.Using liquid manure with applying, with water band fertilizer, water-fertilizer integral is realized;Water soluble fertilizer has
Effect absorptivity is higher by common chemical fertilizer more than one times, reaches 80%-90%;And fertilizer efficiency is fast, can solve high-yield crop fast growing period
Nutritional need.Cooperating drip irrigation system water requirement is only the 30% of common chemical fertilizer, and fertilising operation almost can not manually, greatly
Human cost has been saved greatly.
China is poor one of the country of global freshwater resources, and agriculture seasonality and industry are unevenly distributed, are regional scarce
The problems such as water, is prominent, as the intensive of agricultural, large-scale development and drip irrigation and spray irrigation water saving facility agricultural area expand rapidly
Greatly;The development prospect of water-soluble fertilizer is bright, and demand is increasing;Meanwhile the requirement to water-soluble fertilizer also increasingly improves.
But solid water-soluble fertilizer is in ingredient production, packing and storing, handling transportational process or in specific external condition
Under, agglomeration can be generated due to temperature change, humidity variation, the variation of compressive strength, chemical change etc. itself;After agglomeration
Solid water-soluble fertilizer cause unevenness of application when in use, be easy to cause crop burning, influence crop normal growth;It mentions thus
For a kind of Water soluble fertilizer anticaking agent, Water soluble fertilizer is avoided to agglomerate.
Summary of the invention
To solve solid water-soluble fertilizer present in background technique in ingredient production, packing and storing, handling transportational process
Or under specific external condition, due to temperature change, humidity variation, the variation of compressive strength, the originals such as chemical change of itself
Because of the technical issues of generating agglomeration, the present invention proposes a kind of micro-emulsion type Water soluble fertilizer anticaking agent and preparation method thereof, the present invention
Micro-emulsion type Water soluble fertilizer anticaking agent obtained, by its even application on the surface of solid Water soluble fertilizer;Micro-emulsion type Water soluble fertilizer anti-caking
Agent is uniformly adsorbed in solid Water soluble fertilizer, and excellent preventing blocking effect is played to solid Water soluble fertilizer.
A kind of micro-emulsion type Water soluble fertilizer anticaking agent proposed by the present invention, the raw material including following parts by weight: low-carbon alcohols 10-30
Part, 5-25 parts of surfactant, 20-40 parts of anti-caking oil, 30-50 parts of vermiculite power and 30-55 parts of sepiolite powder.
Preferably, the raw material including following parts by weight: 10 parts of low-carbon alcohols, 5 parts of surfactant, anti-caking oily 20 parts, vermiculite
30 parts and 30 parts of sepiolite powder of powder.
Preferably, the raw material including following parts by weight: 18 parts of low-carbon alcohols, 20 parts of surfactant, anti-caking oily 25 parts, vermiculite
38 parts and 38 parts of sepiolite powder of powder.
Preferably, the raw material including following parts by weight: 30 parts of low-carbon alcohols, 25 parts of surfactant, anti-caking oily 40 parts, vermiculite
50 parts and 55 parts of sepiolite powder of powder.
Preferably, low-carbon alcohols are the mixture of one or more of methanol, ethyl alcohol, propyl alcohol and butanol.
Preferably, surfactant is fatty alcohol polyoxyethylene ether, secondary alcohol polyoxyethylene ether, fatty acid methyl ester polyoxyethylene
Ether, AEO carboxylic acid sodium, polyoxyethylene fatty alkyl ether sulfonate, disecoctylmaleate sodium sulfonate, Asia
The mixture of one or more of the double sodium naphthalene sulfonates of methyl.
Preferably, the HLB value of surfactant is 7-14.
Preferably, anti-caking oil be peanut oil, safflower oil, leaf mustard seed oil, corn oil, Linseed oil, coconut oil, olive oil,
The mixture of one or more of macadamia nut oil, sesame oil, soybean oil and sunflower oil.
Preferably, the partial size of vermiculite power is not less than 325 mesh.
Preferably, the partial size of sepiolite powder is not less than 325 mesh.
A kind of preparation method of micro-emulsion type Water soluble fertilizer anticaking agent, including following specific steps:
S1, anti-caking oil and low-carbon alcohols are weighed by weight ratio;Anti-caking oil and low-carbon alcohols are put into blender, and by anti-caking
Oil and low-carbon alcohols are heated to 30-40 DEG C;Blender stirs 15-20min with the revolving speed of 1000-1200r/min, obtains mixture A;
S2, surfactant, mountain flour and sepiolite powder are weighed by weight ratio;And by surfactant, mountain flour and Hai Pao
Mountain flour is put into mixture A, obtains mixture B;
S3,60-80 DEG C is heated to mixture B, and to stir 15- to mixture B with the revolving speed of 1000-1200r/min
20min obtains products C;
S4, products C is cooled down, packed and is put in storage.
Further, finished product Water soluble fertilizer anticaking agent obtained is produced when in use for the present invention, needs first to be shaken
It is even;It is sprayed on the surface of solid Water soluble fertilizer again, it can uniformly be adsorbed in solid Water soluble fertilizer, rise to solid Water soluble fertilizer
To excellent preventing blocking effect.
It is when in use that its even application is water-soluble in solid for micro-emulsion type Water soluble fertilizer anticaking agent obtained in the present invention
The surface of fertilizer;Micro-emulsion type Water soluble fertilizer anticaking agent is uniformly adsorbed in solid Water soluble fertilizer, is played to solid Water soluble fertilizer excellent
Preventing blocking effect;Solid Water soluble fertilizer by the progress spray attachment anti-caking processing of micro-emulsion type Water soluble fertilizer anticaking agent when in use, can
With quickly dissolution in water, and deposited without oil slick in field contamination-free, it is harmless to soil and soil property.
In the present invention, the anti-caking oil being added in micro-emulsion type Water soluble fertilizer anticaking agent is vegetable oil, is contained in vegetable oil
Unsaturated bond is easier under the action of oxygen to degrade in air;And the product after degrading is easy to be absorbed by crops, and helps to mention
High soil fertility.
In the present invention, vermiculite power is added in micro-emulsion type Water soluble fertilizer anticaking agent;Vermiculite power adsorbent solid Water soluble fertilizer surface;
Since the water absorption character of vermiculite fully absorbs the moisture on solid Water soluble fertilizer surface, solid Water soluble fertilizer is avoided to agglomerate;Vermiculite simultaneously
With good cationic exchangeability and adsorptivity, the structure of soil can be improved, water storage soil moisture conservation, the gas permeability of soil is improved and contain
It is aqueous;Acid soil is set to become neutral soil;Vermiculite may also function as buffer function, hinder the rapid variation of pH value;Fertilizer is set to exist
Slow release in plant growth medium, and allow slightly excessively to be safe from harm to plant using fertilizer;Vermiculite can also be to crop
The elements such as K, Mg, Ca, the Fe itself contained and micro Mn, Cu, Zn are provided.The water imbibition of vermiculite, cationic exchangeability and
Properties of chemical composition makes it play the multiple actions such as fertilizer conservation, water conservation, water storage, ventilative and mineral fertilizer;Soil quality can be improved
And it increases soil fertility.
In the present invention, sepiolite powder is added in micro-emulsion type Water soluble fertilizer anticaking agent;Sepiolite powder adsorbent solid Water soluble fertilizer
Surface;Since the water absorption character of vermiculite fully absorbs the moisture on solid Water soluble fertilizer surface, solid Water soluble fertilizer is avoided to agglomerate;Hai Pao
Stone has the characteristics that large specific surface area, absorption property are good and ion-exchange capacity is strong due to unique crystal structure;Sepiolite
There is stronger adsorption capacity to heavy metal ion, can be used for the improvement of heavy metals exceeding standard soil;So as to improve soil quality.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of micro-emulsion type Water soluble fertilizer anticaking agent proposed by the present invention, the raw material including following parts by weight: 10 parts of low-carbon alcohols,
5 parts of surfactant, 20 parts of anti-caking oil, 30 parts of vermiculite power and 30 parts of sepiolite powder.
In a specific embodiment, low-carbon alcohols are the mixture of one or more of methanol, ethyl alcohol, propyl alcohol and butanol.
In a specific embodiment, surfactant is fatty alcohol polyoxyethylene ether, secondary alcohol polyoxyethylene ether, fatty acid methyl
Ester APEO, AEO carboxylic acid sodium, polyoxyethylene fatty alkyl ether sulfonate, maleic acid di-sec-octyl
The mixture of one or more of sodium sulfonate, sodium methylene bis-naphthalene sulfonate.
Further, the HLB value of surfactant is 7-14.
In a specific embodiment, anti-caking oil is peanut oil, safflower oil, leaf mustard seed oil, corn oil, Linseed oil, coconut
The mixture of one or more of oil, olive oil, macadamia nut oil, sesame oil, soybean oil and sunflower oil.
In a specific embodiment, the partial size of vermiculite power is not less than 325 mesh.
In a specific embodiment, the partial size of sepiolite powder is not less than 325 mesh.
The preparation method of above-mentioned micro-emulsion type Water soluble fertilizer anticaking agent, including following specific steps:
S1, anti-caking oil and low-carbon alcohols are weighed by weight ratio;Anti-caking oil and low-carbon alcohols are put into blender, and by anti-caking
Oil and low-carbon alcohols are heated to 30-40 DEG C;Blender stirs 15-20min with the revolving speed of 1000-1200r/min, obtains mixture A;
S2, surfactant, mountain flour and sepiolite powder are weighed by weight ratio;And by surfactant, mountain flour and Hai Pao
Mountain flour is put into mixture A, obtains mixture B;
S3,60-80 DEG C is heated to mixture B, and to stir 15- to mixture B with the revolving speed of 1000-1200r/min
20min obtains products C;
S4, products C is cooled down, packed and is put in storage.
Further, finished product Water soluble fertilizer anticaking agent obtained is produced when in use for the present invention, needs first to be shaken
It is even;It is sprayed on the surface of solid Water soluble fertilizer again, it can uniformly be adsorbed in solid Water soluble fertilizer, rise to solid Water soluble fertilizer
To excellent preventing blocking effect.
Embodiment 2
A kind of micro-emulsion type Water soluble fertilizer anticaking agent proposed by the present invention, the raw material including following parts by weight: 18 parts of low-carbon alcohols,
20 parts of surfactant, 25 parts of anti-caking oil, 38 parts of vermiculite power and 38 parts of sepiolite powder.
In a specific embodiment, low-carbon alcohols are the mixture of one or more of methanol, ethyl alcohol, propyl alcohol and butanol.
In a specific embodiment, surfactant is fatty alcohol polyoxyethylene ether, secondary alcohol polyoxyethylene ether, fatty acid methyl
Ester APEO, AEO carboxylic acid sodium, polyoxyethylene fatty alkyl ether sulfonate, maleic acid di-sec-octyl
The mixture of one or more of sodium sulfonate, sodium methylene bis-naphthalene sulfonate.
Further, the HLB value of surfactant is 7-14.
In a specific embodiment, anti-caking oil is peanut oil, safflower oil, leaf mustard seed oil, corn oil, Linseed oil, coconut
The mixture of one or more of oil, olive oil, macadamia nut oil, sesame oil, soybean oil and sunflower oil.
In a specific embodiment, the partial size of vermiculite power is not less than 325 mesh.
In a specific embodiment, the partial size of sepiolite powder is not less than 325 mesh.
The preparation method of above-mentioned micro-emulsion type Water soluble fertilizer anticaking agent, including following specific steps:
S1, anti-caking oil and low-carbon alcohols are weighed by weight ratio;Anti-caking oil and low-carbon alcohols are put into blender, and by anti-caking
Oil and low-carbon alcohols are heated to 30-40 DEG C;Blender stirs 15-20min with the revolving speed of 1000-1200r/min, obtains mixture A;
S2, surfactant, mountain flour and sepiolite powder are weighed by weight ratio;And by surfactant, mountain flour and Hai Pao
Mountain flour is put into mixture A, obtains mixture B;
S3,60-80 DEG C is heated to mixture B, and to stir 15- to mixture B with the revolving speed of 1000-1200r/min
20min obtains products C;
S4, products C is cooled down, packed and is put in storage.
Further, finished product Water soluble fertilizer anticaking agent obtained is produced when in use for the present invention, needs first to be shaken
It is even;It is sprayed on the surface of solid Water soluble fertilizer again, it can uniformly be adsorbed in solid Water soluble fertilizer, rise to solid Water soluble fertilizer
To excellent preventing blocking effect.
Embodiment 3
A kind of micro-emulsion type Water soluble fertilizer anticaking agent proposed by the present invention, the raw material including following parts by weight: including weighing as follows
Measure the raw material of part: 30 parts of low-carbon alcohols, 25 parts of surfactant, 40 parts of anti-caking oil, 50 parts of vermiculite power and 55 parts of sepiolite powder.
In a specific embodiment, low-carbon alcohols are the mixture of one or more of methanol, ethyl alcohol, propyl alcohol and butanol.
In a specific embodiment, surfactant is fatty alcohol polyoxyethylene ether, secondary alcohol polyoxyethylene ether, fatty acid methyl
Ester APEO, AEO carboxylic acid sodium, polyoxyethylene fatty alkyl ether sulfonate, maleic acid di-sec-octyl
The mixture of one or more of sodium sulfonate, sodium methylene bis-naphthalene sulfonate.
Further, the HLB value of surfactant is 7-14.
In a specific embodiment, anti-caking oil is peanut oil, safflower oil, leaf mustard seed oil, corn oil, Linseed oil, coconut
The mixture of one or more of oil, olive oil, macadamia nut oil, sesame oil, soybean oil and sunflower oil.
In a specific embodiment, the partial size of vermiculite power is not less than 325 mesh.
In a specific embodiment, the partial size of sepiolite powder is not less than 325 mesh.
The preparation method of above-mentioned micro-emulsion type Water soluble fertilizer anticaking agent, including following specific steps:
S1, anti-caking oil and low-carbon alcohols are weighed by weight ratio;Anti-caking oil and low-carbon alcohols are put into blender, and by anti-caking
Oil and low-carbon alcohols are heated to 30-40 DEG C;Blender stirs 15-20min with the revolving speed of 1000-1200r/min, obtains mixture A;
S2, surfactant, mountain flour and sepiolite powder are weighed by weight ratio;And by surfactant, mountain flour and Hai Pao
Mountain flour is put into mixture A, obtains mixture B;
S3,60-80 DEG C is heated to mixture B, and to stir 15- to mixture B with the revolving speed of 1000-1200r/min
20min obtains products C;
S4, products C is cooled down, packed and is put in storage.
Further, finished product Water soluble fertilizer anticaking agent obtained is produced when in use for the present invention, needs first to be shaken
It is even;It is sprayed on the surface of solid Water soluble fertilizer again, it can uniformly be adsorbed in solid Water soluble fertilizer, rise to solid Water soluble fertilizer
To excellent preventing blocking effect.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of micro-emulsion type Water soluble fertilizer anticaking agent, which is characterized in that the raw material including following parts by weight: 10-30 parts of low-carbon alcohols,
5-25 parts of surfactant, 20-40 parts of anti-caking oil, 30-50 parts of vermiculite power and 30-55 parts of sepiolite powder.
2. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that including following parts by weight
Raw material: 10 parts of low-carbon alcohols, 5 parts of surfactant, 20 parts of anti-caking oil, 30 parts of vermiculite power and 30 parts of sepiolite powder.
3. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that including following parts by weight
Raw material: 18 parts of low-carbon alcohols, 20 parts of surfactant, 25 parts of anti-caking oil, 38 parts of vermiculite power and 38 parts of sepiolite powder.
4. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that including following parts by weight
Raw material: 30 parts of low-carbon alcohols, 25 parts of surfactant, 40 parts of anti-caking oil, 50 parts of vermiculite power and 55 parts of sepiolite powder.
5. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that low-carbon alcohols are methanol, second
The mixture of one or more of alcohol, propyl alcohol and butanol.
6. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that surfactant is fat
Alcohol polyoxyethylene ether, secondary alcohol polyoxyethylene ether, fatty acid methyl ester APEO, AEO carboxylic acid sodium, fat
One or more of alcohol sodium sulfonate of ethoxylated, disecoctylmaleate sodium sulfonate, sodium methylene bis-naphthalene sulfonate
Mixture.
7. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that anti-caking oil be peanut oil,
In safflower oil, leaf mustard seed oil, corn oil, Linseed oil, coconut oil, olive oil, macadamia nut oil, sesame oil, soybean oil and sunflower oil
One or more of mixtures.
8. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that the partial size of vermiculite power is not small
In 325 mesh.
9. a kind of micro-emulsion type Water soluble fertilizer anticaking agent according to claim 1, which is characterized in that the partial size of sepiolite powder is not
Less than 325 mesh.
10. a kind of a kind of preparation method of micro-emulsion type Water soluble fertilizer anticaking agent a method as claimed in any one of claims 1-8, feature exist
In, including following specific steps:
S1, anti-caking oil and low-carbon alcohols are weighed by weight ratio;Anti-caking oil and low-carbon alcohols are put into blender, and by anti-caking oil and
Low-carbon alcohols are heated to 30-40 DEG C;Blender stirs 15-20min with the revolving speed of 1000-1200r/min, obtains mixture A;
S2, surfactant, mountain flour and sepiolite powder are weighed by weight ratio;And by surfactant, mountain flour and sepiolite powder
It puts into mixture A, obtains mixture B;
S3,60-80 DEG C is heated to mixture B, and to stir 15- to mixture B with the revolving speed of 1000-1200r/min
20min obtains products C;
S4, products C is cooled down, packed and is put in storage.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110835097A (en) * | 2019-11-21 | 2020-02-25 | 太原科技大学 | High-yield nano-sulfur particle microemulsion preparation method |
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CN103664334A (en) * | 2013-11-14 | 2014-03-26 | 北京富瑞雪科技发展有限公司 | Anti-blocking agent of fertilizer and application thereof |
CN106748287A (en) * | 2017-02-08 | 2017-05-31 | 武汉铂莱材料科技有限公司 | A kind of aqueous fertiliser anticaking agent and preparation method thereof |
CN108794206A (en) * | 2018-08-22 | 2018-11-13 | 苏州丰倍生物科技有限公司 | A kind of micro-emulsion type Water soluble fertilizer anticaking agent and preparation method thereof |
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- 2018-12-26 CN CN201811598656.2A patent/CN109608258A/en active Pending
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Publication number | Priority date | Publication date | Assignee | Title |
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US5451243A (en) * | 1991-07-04 | 1995-09-19 | Kemira Oy | Controlled-release fertilizer composition in the form of a paste |
CN102050679A (en) * | 2011-01-14 | 2011-05-11 | 福建工程学院 | Straw powder-based anti-blocking agent of compound fertilizer |
CN103664334A (en) * | 2013-11-14 | 2014-03-26 | 北京富瑞雪科技发展有限公司 | Anti-blocking agent of fertilizer and application thereof |
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Application publication date: 20190412 |