CN109602646A - A kind of moisturizing beauty essential oil water and its preparation method and application - Google Patents

A kind of moisturizing beauty essential oil water and its preparation method and application Download PDF

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Publication number
CN109602646A
CN109602646A CN201910063602.4A CN201910063602A CN109602646A CN 109602646 A CN109602646 A CN 109602646A CN 201910063602 A CN201910063602 A CN 201910063602A CN 109602646 A CN109602646 A CN 109602646A
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essential oil
oil water
moisturizing beauty
moisturizing
preparation
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CN109602646B (en
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方喜燕
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Xiamen Amber Perfumery Co Ltd
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Xiamen Hupo Daily Chemical Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to flavors and fragrances field, a kind of moisturizing beauty essential oil water and its preparation method and application is disclosed.The preparation method of the moisturizing beauty essential oil water includes by the mixed liquor airtight heating of 0.01~2wt% natural plant essential oils and 90~96wt% distilled water to boiling and maintain 20~40 minutes, 2~8wt% glycerine is added at 80-90 DEG C later, stirring is cooled to room temperature, filtering.Method provided by the invention can effectively extract the essence in natural plant essential oils and activate active material therein, when using gained moisturizing beauty essential oil water as when cosmetics and skincare product, be conducive to human body fully absorbing and utilizing to essential oil nutritional ingredient, there is moisturizing, brighten, lighten the stain, moisturizing, skin care and other effects;It when gained moisturizing beauty essential oil water is used as hair lotion, can be sprayed directly on on hair, be able to maintain hair and moisten submissive, make the elegant faint scent of hair;When gained moisturizing beauty essential oil water is used as eye refreshing drop, black eye can be eliminated, asthenopia is effectively relieved, keep vision more bright.

Description

A kind of moisturizing beauty essential oil water and its preparation method and application
Technical field
The invention belongs to flavors and fragrances field, it is related to a kind of moisturizing beauty essential oil water and its preparation method and application.
Background technique
Plants essential oil is to pass through steam distillation, extrusion, cold-maceration in the flower from plant, leaf, stem, root or fruit Or solvent extraction method refines the volatile flavor of extraction.Plants essential oil is made of the molecule of some very littles, they are very It is readily soluble in alcohol/emulsifier, especially fatty, this permeates it easily in skin, and through the mixing with fatty fiber And enter internal.When the volatilization of these high flow substances, they are also absorbed by ten hundreds of cells simultaneously, are exhaled by nasal cavity It inhales and enters body in road, message is directly sent to brain, against the running of cerebellum system, control the emotion other for also controlling body Major function, so in aromatherapy, essential oil can strengthen the function of physiology and psychology.Each plants essential oil has a change Learn structure come determine it fragrance, color, mobility and it and system operation mode, but also each plants essential oil respectively has A set of special function speciality.
Vitamin A rich in, B, C, E, K etc. in plants essential oil, having improves endocrine disorder, conditioning female pathology Problem, promote blood circulation, menstruation regulating, anti-wrinkle, anti-frostbite, skin maintenance and cosmetic benefits the effect of.Currently, essential oil after shave lotion system on the market It is cumbersome to make technique, is generally prepared with plant fresh flower, or needs through many cumbersome process such as over cleaning decontamination, or needs to add Add excessive chemical component, such as alcohol pigment etc., this is harmful to the human body unhelpful.
Summary of the invention
The present invention is intended to provide a kind of new moisturizing beauty essential oil water and its preparation method and application.
The present invention provides a kind of preparation methods of moisturizing beauty essential oil water, wherein this method includes by natural plants essence Glycerine is added at 80~90 DEG C later to boiling and maintaining 20~40 minutes in the mixed liquor airtight heating of oil and distilled water, Stirring is cooled to room temperature, and filtering obtains moisturizing beauty essential oil water;With the total weight of natural plant essential oils, distilled water and glycerine On the basis of, the dosage of natural plant essential oils is 0.01~2wt%, and the dosage of distilled water is 90~96wt%, the dosage of glycerine For 2~8wt%.At this point, three of the above substance can play the role of very perfect coordinated.
Preferably, the natural plant essential oils be selected from rose ethereal oil, jasmine essential oil, tea tree ethereal oil, Lavender, At least one of osmanthus essential oil and cloves flower essential oil.
Preferably, the heating rate of the heating is 8-10 DEG C/min, can more effectively extract and activate natural at this time Essence and active material in plants essential oil.
Preferably, the rate of temperature fall of the cooling is 3-5 DEG C/min, oil water mixture can be allowed to stablize miscible reach at this time To optimum state, keep essential oil and water, glycerine fused uniform, do not generate lamination, cools too fast or too slow, be easy Lead to water-oil separating.
Preferably, the rate of the stirring is 300-500rpm.
Preferably, aperture of filter screen used by the filtering is 200-300 mesh.
The present invention also provides moisturizing beauty essential oil water prepared by the above method.
In addition, the present invention also provides the moisturizing beauty essential oil water as cosmetics and skincare product, hair lotion or eye refreshing drop Using.
The preparation method of moisturizing beauty essential oil water provided by the invention can effectively extract the essence in natural plant essential oils And active material therein is activated, when being conducive to human body to essential oil using gained moisturizing beauty essential oil water as when cosmetics and skincare product Nutritional ingredient fully absorbing and utilizing, and has moisturizing, brightens, lightens the stain, moisturizing, skin care and other effects, especially suitable for right The moisturizing of dry skin, moisture necessary to capable of supplementing skin daily, effective active cell vigor promote skin new old generation It thanks, comprehensively regulating skin quality, keeps skin exquisiteness water tender flexible;It, can be straight when gained moisturizing beauty essential oil water is used as hair lotion It connects and is sprayed on hair, be able to maintain hair and moisten submissive, make the elegant faint scent of hair;It is protected when gained moisturizing beauty essential oil water to be used as When ocular fluid, a small amount of essential oil water is dipped with cotton piece, spreads on eyes, black eye can be effectively eliminated, alleviate asthenopia, improves vision effect Fruit.In addition, the preparation process of moisturizing beauty essential oil water provided by the invention is simple, can effectively avoid using being harmful to the human body Chemical substance, products obtained therefrom non-pigment, preservative free.
Specific embodiment
The embodiment of the present invention is described below in detail, the examples of the embodiments are intended to be used to explain the present invention, and cannot It is interpreted as limitation of the present invention.In the examples where no specific technique or condition is specified, described according to the literature in the art Technology or conditions or carried out according to product description.Reagents or instruments used without specified manufacturer is that can lead to Cross the conventional products of commercially available acquisition.
Embodiment 1
The embodiment is for illustrating moisturizing beauty essential oil water provided by the invention and preparation method thereof.
0.05wt% rose ethereal oil and 94.95wt% distilled water are placed in closed container, with 8 DEG C/min of rate It is heated to boiling (100 DEG C) and maintains 30 minutes, 5wt% glycerine is added at 80 DEG C later, is stirred with the rate of 300rpm And (15~25 DEG C) are cooled to room temperature with 3 DEG C/min of rate, use aperture to obtain moisturizing for the screen to filtrate of 200 mesh later Beauty essential oil water, is denoted as JY-1.
Embodiment 2
The embodiment is for illustrating moisturizing beauty essential oil water provided by the invention and preparation method thereof.
The distilled water of the jasmine essential oil of 2wt% and 96wt% is placed in closed container, the rate with 10 DEG C/min adds Heat is to boiling (100 DEG C) and maintains 20 minutes, and 2wt% glycerine is added at 90 DEG C later, simultaneously with the rate stirring of 500rpm (15~25 DEG C) are cooled to room temperature with 5 DEG C/min of rate, use aperture later as the screen to filtrate of 300 mesh, obtain moisturizing beauty Hold essential oil water, is denoted as JY-2.
Embodiment 3
The embodiment is for illustrating moisturizing beauty essential oil water provided by the invention and preparation method thereof.
The distilled water of the tea tree ethereal oil of 0.01wt% and 91.99wt% is placed in closed container, with 9 DEG C/min of speed Rate is heated to boiling (100 DEG C) and maintains 40 minutes, and 8wt% glycerine is added at 85 DEG C later, is stirred with the rate of 400rpm It mixes and (15~25 DEG C) is cooled to room temperature with 4 DEG C/min of rate, aperture is used to be protected for the screen to filtrate of 250 mesh later Wet beauty essential oil water, is denoted as JY-3.
Embodiment 4
The embodiment is for illustrating moisturizing beauty essential oil water provided by the invention and preparation method thereof.
Moisturizing beauty essential oil water is prepared according to the method for embodiment 1, unlike, the rate of heat addition is for 12 DEG C/min and cold But rate is 8 DEG C/min, the specific steps are as follows:
0.05wt% rose ethereal oil and 94.95wt% distilled water are placed in closed container, with 12 DEG C/min of rate It is heated to boiling (100 DEG C) and maintains 30 minutes, 5wt% glycerine is added at 80 DEG C later, is stirred with the rate of 300rpm And (15~25 DEG C) are cooled to room temperature with 8 DEG C/min of rate, use aperture to obtain moisturizing for the screen to filtrate of 200 mesh later Beauty essential oil water, is denoted as JY-4.
Comparative example 1
The comparative example is for illustrating moisturizing beauty essential oil water of reference and preparation method thereof.
Moisturizing beauty essential oil water is prepared according to the method for embodiment 3, unlike, by tea tree ethereal oil and distilled water closed Vessel in heating is to 50 DEG C and maintains 40 minutes, the specific steps are as follows:
The distilled water of the tea tree ethereal oil of 0.01wt% and 91.99wt% is placed in closed container, with 9 DEG C/min of speed Rate is heated to 50 DEG C and maintains 40 minutes, and 8wt% glycerine is added at 50 DEG C later, with the rate stirring of 400rpm and with 4 DEG C/min rate be cooled to room temperature (15~25 DEG C), use aperture to obtain reference moisturizing for the screen to filtrate of 250 mesh later Beauty essential oil water, is denoted as DJY-1.
Comparative example 2
The comparative example is for illustrating moisturizing beauty essential oil water of reference and preparation method thereof.
Moisturizing beauty essential oil water is prepared according to the method for embodiment 3, unlike, tea tree ethereal oil and distilled water are in closed appearance The time that boiling is maintained in device is 5 minutes, the specific steps are as follows:
The distilled water of the tea tree ethereal oil of 0.01wt% and 91.99wt% is placed in closed container, with 9 DEG C/min of speed Rate is heated to boiling (100 DEG C) and maintains 5 minutes, and 8wt% glycerine is added at 85 DEG C later, is stirred with the rate of 400rpm And (15~25 DEG C) are cooled to room temperature with 4 DEG C/min of rate, use aperture to obtain reference for the screen to filtrate of 250 mesh later Moisturizing beauty essential oil water, is denoted as DJY-2.
Comparative example 3
The comparative example is for illustrating moisturizing beauty essential oil water of reference and preparation method thereof.
Moisturizing beauty essential oil water is prepared according to the method for embodiment 3, unlike, by the glycerine second of identical weight part Glycol substitution, the specific steps are as follows:
The distilled water of the tea tree ethereal oil of 0.01wt% and 91.99wt% is placed in closed container, with 9 DEG C/min of speed Rate is heated to boiling (100 DEG C) and maintains 40 minutes, and 8wt% ethylene glycol is added at 85 DEG C later, is stirred with the rate of 400rpm It mixes and (15~25 DEG C) is cooled to room temperature with 4 DEG C/min of rate, aperture is used to be joined for the screen to filtrate of 250 mesh later Than moisturizing beauty essential oil water, it is denoted as DJY-3.
Comparative example 4
The comparative example is for illustrating moisturizing beauty essential oil water of reference and preparation method thereof.
Moisturizing beauty essential oil water is prepared according to the method for embodiment 3, unlike, tea tree ethereal oil, distilled water and glycerine Dosage it is different, the specific steps are as follows:
10wt% tea tree ethereal oil and 85wt% distilled water are placed in closed container, are heated to boiling with 9 DEG C/min of rate Rise (100 DEG C) and maintain 40 minutes, 5wt% glycerine is added at 85 DEG C later, with the stirring of the rate of 400rpm and with 4 DEG C/ The rate of minute is cooled to room temperature (15~25 DEG C), uses aperture later as the screen to filtrate of 250 mesh, obtains reference moisturizing beauty Essential oil water, is denoted as DJY-4.
Test case
Choose 10 30-40 years old healthy women experimenters, the history of disease such as no skin, hair, eyes, subject's test preceding 3 In same urban work and life, the climate temperature and humidity contacted with skin before guarantee test is almost the same within a month.
(1) moisturizing beauty:
Tested test position be face, tested test position experiment first three days cannot use any sample (including makeup Product and topical drug), before test, subject face is cleaned with perfumed soap and with dry face tissue wiped clean, later by moisturizing beauty Essential oil water is applied to subject face and chooses face's the same area as test area, when initially using essential oil water, makes subject It controls between 42.50-42.55 in the skin keratin water content of test area, is tested later using keratoderma water content Instrument (corneometer Courage&Khazaka, Germany) measurement uses moisturizing beauty essential oil water 1 hour, 3 hours, 5 hours, 7 The water content of the test area, acquired results are as shown in table 1 after hour, 9 hours and 12 hours.
Table 1
Sample/time 0 hour 1 hour 3 hours 5 hours 7 hours 9 hours 12 hours 12 hours fluid losses
Embodiment 1 42.52 40.38 38.21 36.90 36.25 35.94 35.73 6.79
Embodiment 2 42.50 40.36 38.18 36.89 36.24 35.92 35.71 6.79
Embodiment 3 42.55 40.40 38.22 36.94 36.28 36.13 35.93 6.62
Embodiment 4 42.52 40.32 38.05 36.40 35.38 34.25 33.35 9.17
Comparative example 1 42.53 40.25 38.01 36.38 34.86 32.44 30.27 12.26
Comparative example 2 42.50 40.28 38.05 36.33 33.59 31.06 28.83 13.67
Comparative example 3 42.55 40.22 38.06 36.35 33.65 31.62 29.35 13.20
Comparative example 4 42.52 40.26 38.04 36.33 33.92 32.44 31.02 11.50
As can be seen from result of Table 1,12 hours 11.50 > of skin fluid loss 13.67 >, 13.20 >, 12.26 >, 9.17 > 6.79 > 6.62, the essential oil water moistening effect embodiment 1-3 that above scheme is produced are better than comparative example 1-4 better than embodiment 4.
(2) it takes care of hair:
Above 10 healthy women subjects are selected, are separately encoded according to the product that embodiment 1-4 and comparative example 1-4 are produced Subject is transferred to spread on eyes with cotton piece for A/B/C/D/E/F/G/H, allowing subject, voluntarily sensory evaluation (eliminates black eye, anti- Asthenopia), it obtains a result as shown in table 2 below (ranking number more big more rearward).
Table 2
Subject Subjective assessment ranking A B C D E F G H
1 CABEDHGF 2 3 1 5 4 8 7 6
2 ABCHEDFG 1 2 3 6 5 7 8 4
3 BACFEDGH 2 1 3 6 5 4 7 8
4 CBAEDHFG 3 2 1 5 4 7 8 6
5 BCAEDGHF 3 1 2 5 4 8 6 7
6 CABDHEFG 2 3 1 4 6 7 8 5
7 ACBEHDGF 1 3 2 6 4 8 7 5
8 BCAFHEDG 3 1 2 7 6 4 8 5
9 BCAEDHGF 3 1 2 5 4 8 7 6
10 CBAEDHFG 3 2 1 5 4 7 8 6
Average ranking BCAEDHFG 2.3 1.9 1.8 5.4 4.6 6.8 7.4 5.8
(3) eyeshield:
Above 10 healthy women subjects are selected, are separately encoded according to the product that embodiment 1-4 and comparative example 1-4 are produced Hair is applied to as essential oil water after transferring to subject to have one's hair wash for A/B/C/D/E/F/G/H, allows subject's voluntarily sensory evaluation (essence Oily lasting and hair are along refreshing effect), it obtains a result (ranking number more big more rearward) as shown in table 3 below.
Table 3
Subject Subjective assessment ranking A B C D E F G H
1 BCAEDHFG 3 1 2 5 4 7 8 6
2 CABDHEFG 2 3 1 4 6 7 8 5
3 BACEHDFG 2 1 3 6 4 7 8 5
4 CBEADHFG 4 2 1 5 3 7 8 6
5 BCAEDHFG 3 1 2 5 4 7 8 6
6 BACFEDHG 2 1 3 6 5 4 8 7
7 CBAEDHFG 3 2 1 5 4 7 8 6
8 BCAFHEDG 3 1 2 7 6 4 8 5
9 CBAEDHFG 3 2 1 5 4 7 8 6
10 ACBEHDGF 1 3 2 6 4 8 7 5
Average ranking BCAEDHFG 2.6 1.7 1.8 5.4 4.4 6.5 7.9 5.7
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example Property, it is not considered as limiting the invention, those skilled in the art are not departing from the principle of the present invention and objective In the case where can make changes, modifications, alterations, and variations to the above described embodiments within the scope of the invention.

Claims (8)

1. a kind of preparation method of moisturizing beauty essential oil water, which is characterized in that this method includes by natural plant essential oils and distillation The mixed liquor airtight heating of water is added glycerine at 80~90 DEG C later, stirs evenly to boiling and maintaining 20~40 minutes After be cooled to room temperature, filter, obtain moisturizing beauty essential oil water;Total weight with natural plant essential oils, distilled water and glycerine is Benchmark, the dosage of natural plant essential oils are 0.01~2wt%, and the dosage of distilled water is 90~96wt%, and the dosage of glycerine is 2 ~8wt%.
2. the preparation method of moisturizing beauty essential oil water according to claim 1, which is characterized in that the natural plant essential oils At least one in rose ethereal oil, jasmine essential oil, tea tree ethereal oil, Lavender, osmanthus essential oil and cloves flower essential oil Kind.
3. the preparation method of moisturizing beauty essential oil water according to claim 1 or 2, which is characterized in that the liter of the heating Warm rate is 8-10 DEG C/min.
4. the preparation method of moisturizing beauty essential oil water according to claim 1 or 2, which is characterized in that the drop of the cooling Warm rate is 3-5 DEG C/min.
5. the preparation method of moisturizing beauty essential oil water according to claim 1 or 2, which is characterized in that the speed of the stirring Rate is 300-500rpm.
6. the preparation method of moisturizing beauty essential oil water according to claim 1 or 2, which is characterized in that the filtering is adopted Aperture of filter screen is 200-300 mesh.
7. the moisturizing beauty essential oil water that the method as described in any one of claim 1-6 is prepared.
8. application of the moisturizing beauty essential oil water as claimed in claim 7 as cosmetics and skincare product, hair lotion or eye refreshing drop.
CN201910063602.4A 2019-01-23 2019-01-23 Moisturizing and beautifying essential oil water and preparation method and application thereof Active CN109602646B (en)

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CN106880519A (en) * 2015-12-16 2017-06-23 闫战军 A kind of Rosa Damascana Jojoba Oil beautifying face, preserving moisture nourishes oil and preparation method thereof
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Address after: No. 308, Tong'an Park, Tong'an industrial concentration zone, Xiamen City, Fujian Province, 361000

Patentee after: Xiamen Amber Flavor Co.,Ltd.

Address before: No. 308, Tong'an Park, Tong'an industrial concentration zone, Xiamen City, Fujian Province, 361000

Patentee before: XIAMEN AMBER DAILY CHEMICAL TECHNOLOGY CO.,LTD.