CN109593413A - A kind of interior wall resistant lacquer and preparation method thereof - Google Patents
A kind of interior wall resistant lacquer and preparation method thereof Download PDFInfo
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- CN109593413A CN109593413A CN201811321219.6A CN201811321219A CN109593413A CN 109593413 A CN109593413 A CN 109593413A CN 201811321219 A CN201811321219 A CN 201811321219A CN 109593413 A CN109593413 A CN 109593413A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1606—Antifouling paints; Underwater paints characterised by the anti-fouling agent
- C09D5/1637—Macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
- C09D5/1675—Polyorganosiloxane-containing compositions
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of interior wall resistant lacquer and preparation method thereof, preparing the raw material of interior wall resistant lacquer by its parts by weight includes: 16 parts~42 parts of silicone acrylic emulsion, 20 parts~35 parts of acrylic acid ester emulsion, 2.5 parts of organic silicon emulsion, 0.2 part~0.35 part of hydroxyethyl cellulose, 10 parts~20 parts of diatomite .2 parts~3.6 parts of silica 1,0.3 part~0.8 part of propylene glycol, 0.12 part~0.22 part of defoaming agent, 0.12 part~0.20 part of n-dodecane radical siloxane, ceramic 10 parts~20 parts of fine sand, 55 parts~80 parts of natural colour sand.The interior wall prepared by the present invention stable product quality of resistant lacquer, caking property is strong, is easy to construct, good waterproof performance, and surface dust not easy to pollute, stain resistance is strong, and preparation method is simple, and preparation process is easy to operate, and economy is strong, is suitble to industrialized production.
Description
Technical field
The present invention relates to decorative materials technologies, and in particular to a kind of interior wall resistant lacquer and preparation method thereof.
Background technique
Lacquer is the coating being formulated using the natural stone-powder of various colors, and decorative effect exactly likes marble, stone
Gang Yan, applied to the imitation stone effect of external wall, therefore also known as liquid stone.As people are to coating for internal and external wall cosmetic requirement
Raising, natural real stone paint increasingly liked that many high-end residentials, garden are very with its unique appearance and performance by everybody
Person's high buildings and large mansions all propose to cover with paint, lacquer, colour wash, etc. lacquer, require its hardness with higher, waterproofness, resistance to ag(e)ing etc. in aspect of performance.
But due to weather etc., existing lacquer is after the completion of painting, the phenomenon that dust and particle will cause lacquer surface contamination,
The decorative effect of lacquer is seriously affected.The lacquer and its preparation that therefore, it is necessary to a kind of water-whitening resistances is good, stain resistant is strong
Method.
Chinese patent CN106336749A discloses a kind of resistant lacquer, is made of following component: pure-acrylic emulsion, silicic acid
Ethyl ester, modified wood fibre element, castor oil, activated silica ashes, dispersing agent, neopelex, cellulose acetate, poly- ammonia
Ester thickener, coalescing agent, ethylene glycol, defoaming agent, water, natural colour sand.The patent passes through silester and cellulose acetate
Synergistic effect reduces the surface tension of lacquer liquid, the nature that makes to form a film, uniformly, has preferable waterproofness and by severe ring
The ability that border is corroded, but the waterproof performance of the standby resistant lacquer of the patent system is bad.
Chinese patent CN103819138A discloses a kind of hydrophobic antifouling lacquer, forms as follows: deionization active water is prevented
Rotten agent, 4% hydroxyethyl cellulose slurry, multifunctional assistant, dispersing agent, thick slurry thickener, organosilicon moisture repellent, lotus leaf hydrophobing agent,
Ultra-fine Bentonite, wetting agent, special emulsion, lauric acid ester, thin natural colour sand, thick natural colour sand.But the patent system is standby
The anti-pollution characteristic of hydrophobic antifouling lacquer is bad.
Summary of the invention
The present invention is in view of the above-mentioned problems, provide a kind of interior wall resistant lacquer and preparation method thereof.
Technical solution used by the present invention solves the above problems is: a kind of interior wall resistant lacquer, which is characterized in that
It includes: 16 parts of silicone acrylic emulsion~42 parts, acrylic acid ester emulsion that the raw material of the interior wall resistant lacquer, which is prepared, by its parts by weight
20 parts~35 parts, 2.5 parts of organic silicon emulsion, 0.2 part~0.35 part of hydroxyethyl cellulose, 10 parts of diatomite~20 parts, titanium dioxide
1.2 parts~3.6 parts of silicon, 0.3 part~0.8 part of propylene glycol, 0.12 part~0.22 part, 0.12 part of n-dodecane radical siloxane of defoaming agent
~0.20 part, ceramic 10 parts~20 parts of fine sand, 55 parts~80 parts of natural colour sand；The solid content of silicone acrylic emulsion be 45wt~
52wt%；The solid content of organic silicon emulsion is 30wt%~45wt%；Hydroxyethyl cellulose is that non-ionic water dissolvable is fine
Tie up plain ether.Wherein, as thickener, hydroxyethyl cellulose selects non-ionic water dissolvable cellulose ether that true stone can be improved
The storage stability and workability of paint；According to inner wall decorative coating feature, it is added with suitable bergmeal particle, is not only acted as
Thickening, the effect for improving adhesive force, also have health environment-friendly, adsorb pernicious gas, improve the effect of living environment；N-dodecane
The compatibility of acrylic emulsion and organic silicon emulsion can be improved as solubilizer for radical siloxane, improve dredging for acrylic acid ester emulsion
Aqueous energy.
Further, acrylic acid ester emulsion, organic silicon emulsion weight ratio be 8~14:1.Wherein, in acrylic acid ester emulsion
The durability against pollution of lotion can be improved in the middle organic silicon emulsion for adding the specific gravity.
Further, the weight ratio of silicone acrylic emulsion and acrylic acid ester emulsion is 8~12:10.Wherein, by silicone acrylic emulsion and third
The high-dirt-resistance energy and strong adhesive force of lotion may be implemented with ratio mixing for olefin(e) acid ester lotion.
Further, the solid content of acrylic acid ester emulsion is 40wt%~50wt%.
Further, the partial size of diatomite is less than 0.33g/cm in 60 mesh~500 mesh, loose density3.Wherein, it adds small
The application property of lacquer can be improved in the diatomite of partial size, improves the dispersing uniformity of lotion.
Further, defoaming agent is silicone emulsion and polyether antifoam agent with the mixing of weight ratio 1:0.8~1.5.
Further, preparing the raw material of interior wall resistant lacquer by its parts by weight includes: 25 parts of silicone acrylic emulsion, acrylic acid
25 parts of ester lotion, 2.5 parts of organic silicon emulsion, 0.28 part of hydroxyethyl cellulose, 15 parts of diatomite, 2.4 parts of silica, propylene glycol
0.55 part, 0.17 part of defoaming agent, 0.16 part of n-dodecane radical siloxane, ceramic 15 parts of fine sand, 70 parts of natural colour sand.
Another goal of the invention of the invention is to provide a kind of preparation method of interior wall resistant lacquer, including walks as follows
It is rapid:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane low speed are dispersed, are added by step S20
Enter organic silicon emulsion high speed dispersion 10 minutes~18 minutes, obtains mixed emulsion；
Step S30 is low by the silicone acrylic emulsion of above-mentioned parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent
Speed dispersion 5 minutes~12 minutes, is added the mixed emulsion that step S20 is obtained, and high speed dispersion is filtered after 6 minutes~12 minutes, obtained
To base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Further, in step S20, the revolving speed of low speed dispersion is 260r/min~300r/min.
Further, in step S20, the revolving speed of high speed dispersion is 650r/min~750r/min.
The invention has the advantages that
(1) interior wall prepared by the present invention carries out organosilicon to acrylic acid ester emulsion by physical blending process with resistant lacquer
It is modified, n-dodecane radical siloxane is added during blending as solubilizer, improves phase of the acrylate with organosilicon
Capacitive improves the water resistance and weatherability of lotion by organosilicon-modified acrylate emulsion；
(2) silicone acrylic emulsion and acrylic acid ester emulsion are carried out proper proportion with resistant lacquer by interior wall prepared by the present invention
Blending can increase adhesive force, improve the compactness of lacquer paint film, prevent solia particle, moisture from going deep into making table in paint film
There is dirt and water stain in face, enhances anti-pollution, the waterproof effect of lacquer；
(3) the interior wall prepared by the present invention stable product quality of resistant lacquer, caking property is strong, is easy to construct, waterproof
Property good, surface dust not easy to pollute, stain resistance is strong, and preparation method is simple, and preparation process is easy to operate, and economy is strong, fit
Close industrialized production.
Specific embodiment
The embodiment of the present invention is described in detail below, but what the present invention can be defined by the claims and cover
Multitude of different ways is implemented.
Embodiment 1
A kind of interior wall resistant lacquer and preparation method thereof
The raw material for preparing the interior wall resistant lacquer includes: silicone acrylic emulsion 16kg, acrylic acid ester emulsion 20kg, organic
Silicon emulsion 2.5kg, hydroxyethyl cellulose 0.25kg, diatomite 10kg, silica 1 .5kg, propylene glycol 0.7kg, defoaming agent
0.22kg, n-dodecane radical siloxane 0.12kg, ceramic fine sand 12kg, natural colour sand 70kg；The solid content of silicone acrylic emulsion is
52wt%；The solid content of organic silicon emulsion is 40wt%；Hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether；Third
Olefin(e) acid ester lotion, the weight ratio of organic silicon emulsion are 8:1；The weight ratio of silicone acrylic emulsion and acrylic acid ester emulsion is 8:10；Third
The solid content of olefin(e) acid ester lotion is 40wt%；The partial size of diatomite is less than 0.33g/cm in 60 mesh~100 mesh, loose density3；Disappear
Infusion is silicone emulsion and polyether antifoam agent with weight ratio 1:1.0 mixing.
Interior wall resistant lacquer, is prepared via a method which:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane be by step S20 in revolving speed
Low speed disperses under 260r/min, and organic silicon emulsion is added, and in the case where revolving speed is 680r/min high speed dispersion 18 minutes, obtains mixing cream
Liquid；
Step S30 exists the silicone acrylic emulsion of above-mentioned parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent
Revolving speed is that low speed disperses 10 minutes under 280r/min, and the mixed emulsion that step S20 is obtained is added, high in the case where revolving speed is 600r/min
Speed dispersion is filtered after 6 minutes, obtains base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Embodiment 2
A kind of interior wall resistant lacquer and preparation method thereof
The raw material for preparing the interior wall resistant lacquer includes: silicone acrylic emulsion 25kg, acrylic acid ester emulsion 25kg, organic
Silicon emulsion 2.5kg, hydroxyethyl cellulose 0.20kg, diatomite 20kg, silica 3.0kg, propylene glycol 0.4kg, defoaming agent
0.12kg, n-dodecane radical siloxane 0.14kg, ceramic fine sand 18kg, natural colour sand 80kg；The solid content of silicone acrylic emulsion is
45wt%；The solid content of organic silicon emulsion is 35wt%；Hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether；Third
Olefin(e) acid ester lotion, the weight ratio of organic silicon emulsion are 10:1；The weight ratio of silicone acrylic emulsion and acrylic acid ester emulsion is 10:10；
The solid content of acrylic acid ester emulsion is 42wt%；The partial size of diatomite is less than 0.33g/ in 100 mesh~500 mesh, loose density
cm3；Defoaming agent is silicone emulsion and polyether antifoam agent with weight ratio 1:1.5 mixing.
Interior wall resistant lacquer, is prepared via a method which:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane be by step S20 in revolving speed
Low speed disperses under 270r/min, and organic silicon emulsion is added, and in the case where revolving speed is 720r/min high speed dispersion 10 minutes, obtains mixing cream
Liquid；
Step S30 exists the silicone acrylic emulsion of above-mentioned parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent
Revolving speed is that low speed disperses 6 minutes under 260r/min, and the mixed emulsion that step S20 is obtained is added, high in the case where revolving speed is 700r/min
Speed dispersion is filtered after 12 minutes, obtains base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Embodiment 3
A kind of interior wall resistant lacquer and preparation method thereof
The raw material for preparing the interior wall resistant lacquer includes: silicone acrylic emulsion 36kg, acrylic acid ester emulsion 30kg, organic
Silicon emulsion 2.5kg, hydroxyethyl cellulose 0.3kg, diatomite 12kg, silica 3.6kg, propylene glycol 0.3kg, defoaming agent
0.20kg, n-dodecane radical siloxane 0.2kg, ceramic fine sand 10g, natural colour sand 60kg；The solid content of silicone acrylic emulsion is
50wt%；The solid content of organic silicon emulsion is 30wt%；Hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether；Third
Olefin(e) acid ester lotion, the weight ratio of organic silicon emulsion are 12:1；The weight ratio of silicone acrylic emulsion and acrylic acid ester emulsion is 12:10；
The solid content of acrylic acid ester emulsion is 48wt%；The partial size of diatomite is less than 0.33g/ in 200 mesh~500 mesh, loose density
cm3；Defoaming agent is silicone emulsion and polyether antifoam agent with weight ratio 1:0.8 mixing.
Interior wall resistant lacquer, is prepared via a method which:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane be by step S20 in revolving speed
Low speed disperses under 290r/min, and organic silicon emulsion is added, and in the case where revolving speed is 650r/min high speed dispersion 16 minutes, obtains mixing cream
Liquid；
Step S30 exists the silicone acrylic emulsion of above-mentioned parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent
Revolving speed is that low speed disperses 12 minutes under 300r/min, and the mixed emulsion that step S20 is obtained is added, high in the case where revolving speed is 720r/min
Speed dispersion is filtered after 8 minutes, obtains base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Embodiment 4
A kind of interior wall resistant lacquer and preparation method thereof
The raw material for preparing the interior wall resistant lacquer includes: silicone acrylic emulsion 42kg, acrylic acid ester emulsion 35kg, organic
Silicon emulsion 2.5kg, hydroxyethyl cellulose 0.35kg, diatomite 18kg, silica 1 .2kg, propylene glycol 0.8kg, defoaming agent
0.15kg, n-dodecane radical siloxane 0.18kg, ceramic fine sand 20kg, natural colour sand 55kg；The solid content of silicone acrylic emulsion is
47wt%；The solid content of organic silicon emulsion is 45wt%；Hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether；Third
Olefin(e) acid ester lotion, the weight ratio of organic silicon emulsion are 14:1；The weight ratio of silicone acrylic emulsion and acrylic acid ester emulsion is 12:10；
The solid content of acrylic acid ester emulsion is 50wt%；The partial size of diatomite is less than 0.33g/ in 200 mesh~400 mesh, loose density
cm3；Defoaming agent is silicone emulsion and polyether antifoam agent with weight ratio 1:1.3 mixing.
Interior wall resistant lacquer, is prepared via a method which:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane be by step S20 in revolving speed
Low speed disperses under 300r/min, and organic silicon emulsion is added, and in the case where revolving speed is 750r/min high speed dispersion 12 minutes, obtains mixing cream
Liquid；
Step S30 exists the silicone acrylic emulsion of above-mentioned parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent
Revolving speed is that low speed disperses 5 minutes under 250r/min, and the mixed emulsion that step S20 is obtained is added, high in the case where revolving speed is 750r/min
Speed dispersion is filtered after ten minutes, obtains base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Embodiment 5
A kind of interior wall resistant lacquer and preparation method thereof
The raw material for preparing interior wall resistant lacquer includes: silicone acrylic emulsion 25kg, acrylic acid ester emulsion 25kg, organosilicon cream
Liquid 2.5kg, hydroxyethyl cellulose 0.28kg, diatomite 15kg, silica 2.4kg, propylene glycol 0.55kg, defoaming agent
0.17kg, n-dodecane radical siloxane 0.16kg, ceramic fine sand 15kg, natural colour sand 70kg；The solid content of silicone acrylic emulsion is
48wt%；The solid content of organic silicon emulsion is 40wt%；Hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether；Third
Olefin(e) acid ester lotion, the weight ratio of organic silicon emulsion are 10:1；The weight ratio of silicone acrylic emulsion and acrylic acid ester emulsion is 10:10；
The solid content of acrylic acid ester emulsion is 45wt%；The partial size of diatomite is less than 0.33g/cm in 10 mesh~300 mesh, loose density3；
Defoaming agent is silicone emulsion and polyether antifoam agent with weight ratio 1:1.2 mixing.
Interior wall resistant lacquer, is prepared via a method which:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane be by step S20 in revolving speed
Low speed disperses under 260r/min, and organic silicon emulsion is added, and in the case where revolving speed is 680r/min high speed dispersion 18 minutes, obtains mixing cream
Liquid；
Step S30 exists the silicone acrylic emulsion of above-mentioned parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent
Revolving speed is that low speed disperses 10 minutes under 280r/min, and the mixed emulsion that step S20 is obtained is added, high in the case where revolving speed is 700r/min
Speed dispersion is filtered after 6 minutes, obtains base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Comparative example
A kind of interior wall resistant lacquer and preparation method thereof
The raw material for preparing interior wall resistant lacquer includes: acrylic acid ester emulsion 25kg, organic silicon emulsion 2.5kg, hydroxyl second
Base cellulose 0.28kg, diatomite 15kg, silica 2.4kg, propylene glycol 0.55kg, defoaming agent 0.17kg, dodecyl
Siloxanes 0.16kg, ceramic fine sand 15kg, natural colour sand 70kg；The solid content of silicone acrylic emulsion is 48wt%；Organic silicon emulsion
Solid content is 40wt%；Hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether；Acrylic acid ester emulsion, organosilicon cream
The weight ratio of liquid is 10:1；The solid content of acrylic acid ester emulsion is 45wt%；The partial size of diatomite is in 10 mesh~300 mesh, loose
Density is less than 0.33g/cm3；Defoaming agent is silicone emulsion and polyether antifoam agent with weight ratio 1:1.2 mixing.
Interior wall resistant lacquer, is prepared via a method which:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by above-mentioned parts by weight；
The acrylic acid ester emulsion of above-mentioned parts by weight, propylene glycol, n-dodecane radical siloxane be by step S20 in revolving speed
Low speed disperses under 260r/min, and organic silicon emulsion is added, and in the case where revolving speed is 680r/min high speed dispersion 18 minutes, obtains mixing cream
Liquid；
The hydroxyethyl cellulose of above-mentioned parts by weight, diatomite, silica, defoaming agent be by step S30 in revolving speed
Low speed disperses 10 minutes under 280r/min, and the mixed emulsion that step S20 is obtained is added, the high speed dispersion in the case where revolving speed is 700r/min
It is filtered after 6 minutes, obtains base paste；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of above-mentioned parts by weight,
It is uniformly mixed, obtains interior wall resistant lacquer.
Experimental example
Technical progress in order to further illustrate the present invention is now further illustrated using experiment.
Experimental material: 1~5 interior wall produced resistant lacquer of the embodiment of the present invention.
Experimental method: compare the properties of a variety of materials under square one.
1. Examples 1 to 5 of table prepares the test result of interior wall resistant lacquer
The experimental results showed that uniform in quality of the interior wall prepared by the present invention with resistant lacquer, no caking phenomenon are applied
Work is good；Film adhesion strength is big, not easily to fall off, and water-fast, stain resistant, water-whitening resistance are strong, long service life.
These are only the preferred embodiment of the present invention, is not intended to restrict the invention, for those skilled in the art
For member, the invention may be variously modified and varied.All within the spirits and principles of the present invention, it is made it is any modification,
Equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of interior wall resistant lacquer, which is characterized in that prepare the raw material of the interior wall resistant lacquer by its weight
Part includes: 16 parts~42 parts of silicone acrylic emulsion, 20 parts~35 parts of acrylic acid ester emulsion, 2.5 parts of organic silicon emulsion, hydroxyethyl cellulose
0.2 part~0.35 part, 10 parts~20 parts of diatomite .2 parts~3.6 parts of silica 1,0.3 part of propylene glycol~0.8 part, defoaming agent
0.12 part~0.22 part, 0.12 part~0.20 part of n-dodecane radical siloxane, ceramic 10 parts~20 parts, 55 parts of natural colour sand of fine sand
~80 parts；The solid content of the silicone acrylic emulsion is 45wt~52wt%；The solid content of the organic silicon emulsion be 30wt%~
45wt%；The hydroxyethyl cellulose is non-ionic water dissolvable cellulose ether.
2. interior wall according to claim 1 resistant lacquer, which is characterized in that the acrylic acid ester emulsion, organosilicon
The weight ratio of lotion is 8~14:1.
3. interior wall according to claim 1 resistant lacquer, which is characterized in that the silicone acrylic emulsion and acrylate cream
The weight ratio of liquid is 8~12:10.
4. interior wall according to claim 1 resistant lacquer, which is characterized in that the solid content of the acrylic acid ester emulsion
For 40wt%~50wt%.
5. interior wall according to claim 1 resistant lacquer, which is characterized in that the partial size of the diatomite 60 mesh~
500 mesh, loose density are less than 0.33g/cm3。
6. interior wall according to claim 1 resistant lacquer, which is characterized in that the defoaming agent is silicone emulsion and gathers
Ether defoaming agent is with the mixing of weight ratio 1:0.8~1.5.
7. interior wall according to claim 1 resistant lacquer, which is characterized in that prepare the interior wall resistant lacquer
Raw material by its parts by weight include: 25 parts of silicone acrylic emulsion, 25 parts of acrylic acid ester emulsion, 2.5 parts of organic silicon emulsion, hydroxy ethyl fiber
Plain 0.28 part, 15 parts of diatomite, 2.4 parts of silica, 0.55 part of propylene glycol, 0.17 part of defoaming agent, n-dodecane radical siloxane
0.16 part, ceramic 15 parts of fine sand, 70 parts of natural colour sand.
8. a kind of preparation method of interior wall according to any one of claims 1 to 7 resistant lacquer, feature exist
In, comprising the following steps:
Step S10 is weighed the raw material for preparing interior wall resistant lacquer by the parts by weight；
Step S20 disperses the acrylic acid ester emulsion of the parts by weight, propylene glycol, n-dodecane radical siloxane low speed, and addition has
Machine silicon emulsion high speed dispersion 10 minutes~18 minutes, obtain mixed emulsion；
Step S30, by the silicone acrylic emulsion of the parts by weight, hydroxyethyl cellulose, diatomite, silica, defoaming agent low speed point
It dissipates 5 minutes~12 minutes, the mixed emulsion that step S20 is obtained is added, high speed dispersion filters after 6 minutes~12 minutes, obtains base
Plinth slurry；
Step S40 mixes the base paste that step S30 is obtained with the ceramic fine sand and natural colour sand of the parts by weight, mixing
Uniformly, interior wall resistant lacquer is obtained.
9. preparation method according to claim 8, which is characterized in that in step S20, the revolving speed of the low speed dispersion is
260r/min~300r/min.
10. preparation method according to claim 8, which is characterized in that in step S20, the revolving speed of the high speed dispersion is
650r/min~750r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811321219.6A CN109593413A (en) | 2018-11-07 | 2018-11-07 | A kind of interior wall resistant lacquer and preparation method thereof |
Applications Claiming Priority (1)
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113683948A (en) * | 2021-07-30 | 2021-11-23 | 安徽众雁涂料有限公司 | Production method of wind-crack-resistant and impact-resistant stone-like paint |
| CN114058231A (en) * | 2021-11-10 | 2022-02-18 | 福建泉州市莱欧环保新材料有限责任公司 | Granite paint and preparation method thereof |
| CN114350258A (en) * | 2022-01-21 | 2022-04-15 | 宁国市茂发装饰材料有限公司 | Transparent waterproof antibacterial water-based paint and preparation method thereof |
| CN116496674A (en) * | 2023-06-21 | 2023-07-28 | 山东新广恒节能科技有限公司 | Real stone paint for outer wall |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557850A (en) * | 2004-02-13 | 2004-12-29 | 杨慕杰 | Process for preparing organosilicon modified acrylic ester elastic emulsion |
| CN104692707A (en) * | 2015-01-29 | 2015-06-10 | 三棵树涂料股份有限公司 | Functional real stone paint building exterior wall coating material and preparation method thereof |
| CN105601166A (en) * | 2016-01-27 | 2016-05-25 | 广东施彩涂料有限公司 | Stone-like coating resisting temperature variation construction and preparation method thereof |
| CN105621959A (en) * | 2015-12-18 | 2016-06-01 | 三棵树涂料股份有限公司 | Flexible true stone paint and preparation method thereof |
| CN106752482A (en) * | 2015-11-25 | 2017-05-31 | 铂恩塞尔新材料（上海）股份有限公司 | A kind of water burnt-in sand multicolor finish and preparation method thereof |
| CN107512871A (en) * | 2017-06-30 | 2017-12-26 | 阜阳富瑞雪化工科技有限公司 | A kind of native annulus fidelity mineral varnish |
-
2018
- 2018-11-07 CN CN201811321219.6A patent/CN109593413A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557850A (en) * | 2004-02-13 | 2004-12-29 | 杨慕杰 | Process for preparing organosilicon modified acrylic ester elastic emulsion |
| CN104692707A (en) * | 2015-01-29 | 2015-06-10 | 三棵树涂料股份有限公司 | Functional real stone paint building exterior wall coating material and preparation method thereof |
| CN106752482A (en) * | 2015-11-25 | 2017-05-31 | 铂恩塞尔新材料（上海）股份有限公司 | A kind of water burnt-in sand multicolor finish and preparation method thereof |
| CN105621959A (en) * | 2015-12-18 | 2016-06-01 | 三棵树涂料股份有限公司 | Flexible true stone paint and preparation method thereof |
| CN105601166A (en) * | 2016-01-27 | 2016-05-25 | 广东施彩涂料有限公司 | Stone-like coating resisting temperature variation construction and preparation method thereof |
| CN107512871A (en) * | 2017-06-30 | 2017-12-26 | 阜阳富瑞雪化工科技有限公司 | A kind of native annulus fidelity mineral varnish |
Non-Patent Citations (1)
| Title |
|---|
| 张学敏等: "《涂料与涂装技术》", 31 January 2006, 化学工业出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113683948A (en) * | 2021-07-30 | 2021-11-23 | 安徽众雁涂料有限公司 | Production method of wind-crack-resistant and impact-resistant stone-like paint |
| CN114058231A (en) * | 2021-11-10 | 2022-02-18 | 福建泉州市莱欧环保新材料有限责任公司 | Granite paint and preparation method thereof |
| CN114350258A (en) * | 2022-01-21 | 2022-04-15 | 宁国市茂发装饰材料有限公司 | Transparent waterproof antibacterial water-based paint and preparation method thereof |
| CN116496674A (en) * | 2023-06-21 | 2023-07-28 | 山东新广恒节能科技有限公司 | Real stone paint for outer wall |
| CN116496674B (en) * | 2023-06-21 | 2023-08-25 | 山东新广恒节能科技有限公司 | Real stone paint for outer wall |
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