CN109580733B - Electrolytic cell for electrochemical test of dregs treatment and use method thereof - Google Patents
Electrolytic cell for electrochemical test of dregs treatment and use method thereof Download PDFInfo
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- CN109580733B CN109580733B CN201811501102.6A CN201811501102A CN109580733B CN 109580733 B CN109580733 B CN 109580733B CN 201811501102 A CN201811501102 A CN 201811501102A CN 109580733 B CN109580733 B CN 109580733B
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/28—Electrolytic cell components
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/093—Cleaning containers, e.g. tanks by the force of jets or sprays
- B08B9/0933—Removing sludge or the like from tank bottoms
Abstract
The invention discloses an electrolytic cell for electrochemical test of dregs treatment and a use method thereof, and the electrolytic cell comprises a bottom plate; the bottom of the water tank is fixed on the left side of the top of the bottom plate; two sides of the bottom of the electrolytic tank are fixed on two sides of the top of the bottom plate through support columns; the invention relates to the technical field of a medicine residue electrochemical testing device, and discloses a filtering box, wherein the bottom of the filtering box is fixed on the right side of the top of a bottom plate. This electrolytic cell for electrochemical test is handled to dregs of a decoction and application method thereof can control the user state of first ration frame and second ration frame, can make the inside dregs of a decoction of first ration frame flow into the electrolysis box in, perhaps the inside dregs of a decoction of first ration frame and second ration frame all flows into the electrolysis box in, the volume of the inside dregs of a decoction of control entering electrolysis box, carry out twice electrolysis and detect, thereby under the condition of knowing twice dregs of a decoction electrolysis detection volume, contrast the testing result, improve its detection accuracy, and easy operation, be favorable to extensively using widely.
Description
Technical Field
The invention relates to the technical field of electrochemical testing devices for dregs of a decoction, in particular to an electrolytic cell for electrochemical testing of dregs of a decoction treatment and a using method thereof.
Background
The residue is residue after decocting Chinese medicine or insoluble residue left after extracting a substance (such as medicine) with solvent, the electrolytic cell is mainly used for preparing high-purity metal in industry, and can also be used for electrochemical test, and is a device (comprising an external power supply, an electrolyte solution and a cathode and anode) for converting electric energy into chemical energy, so that the current passes through the electrolyte solution or molten electrolyte to cause the process of reduction oxidation reaction at the cathode and anode, when ions reach the electrode, electrons are lost or obtained, and the process electrolysis principle of the oxidation reduction reaction is generated.
In the existing market, equipment for carrying out electrochemical testing on the dregs of a decoction is lacked, and the equipment for carrying out electrochemical testing on the dregs of a decoction is generally assembled roughly and badly by manpower, so that the dregs of a decoction are detected and processed, the detection precision is lower, the accuracy is lower, and the continuous use is not facilitated.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides an electrolytic cell for an electrochemical test of dregs treatment and a using method thereof, and solves the problems that equipment for performing the electrochemical test on the dregs is lacked in the current market and the detection precision is low.
In order to achieve the purpose, the invention is realized by the following technical scheme: an electrolytic cell for electrochemical test of dregs treatment comprises a bottom plate; the bottom of the water tank is fixed on the left side of the top of the bottom plate; the two sides of the bottom of the electrolytic tank are fixed on the two sides of the top of the bottom plate through support columns; the bottom of the filter box is fixed on the right side of the top of the bottom plate, and the left side of the filter box is communicated with the bottom of the right side of the water tank through a through pipe; the left side of the feeding box is fixed to the top of the right side of the electrolytic box through the supporting column, and the right side of the bottom of the feeding box is fixedly connected with the right side of the top of the filtering box through the supporting column; the bottom of the storage battery is fixed at the top of the electrolytic tank; the top of the anode rod is fixed on the left side of the top of the inner wall of the electrolytic tank, and the anode rod is electrically connected with the anode of the storage battery through a lead; the top end of the cathode bar is fixed on the right side of the top of the inner wall of the electrolytic tank, and the cathode bar is electrically connected with the cathode of the storage battery through the lead; the surface of the discharge pipe is communicated with the bottom of the electrolytic tank, and a discharge valve is arranged on the surface of the discharge pipe; the top of the storage box is fixed on the top of the inner wall of the feeding box; the surfaces of the first quantitative frame and the second quantitative frame respectively penetrate through two sides of the bottom of the storage box; the surface and the back of the moving plate respectively slide and contact with the surface of the inner wall and the back of the inner wall of the feeding box, and the top of the moving plate is contacted with the bottoms of the first quantitative frame and the second quantitative frame; the bottom of the stabilizing block is fixed to the top of the moving plate and is positioned on the right side of the first quantitative frame; the bottom of the first pushing block slides on the top of the moving plate, and a first spring is fixedly connected between the left side of the first pushing block and the right side of the stabilizing block; the right side of the second pushing block slides to the right side of the inner wall of the feeding box, and the left side of the second pushing block is rotatably connected with the right side of the first pushing block through a first connecting rod; the top of the third pushing block slides to the bottom of the storage box through a sliding rod, and the right side of the third pushing block is rotatably connected with the top of the second pushing block through a second connecting rod; the right side of the first baffle is fixed to the left side of the third pushing block, and the left side of the first baffle penetrates through the first quantitative frame and extends into the first quantitative frame; the bottom of the limiting block is fixed on the right side of the top of the moving plate; the right side of the first moving block is fixed on the right side of the inner wall of the feeding box through a telescopic rod; the right side of the second moving block slides to the right side of the inner wall of the feeding box, and the left side of the second moving block is rotatably connected with the top of the first moving block through a first rotating rod; the top of the third moving block slides on the right side of the bottom of the storage box through the sliding rod, and the right side of the third moving block is rotatably connected with the top of the second moving block through a second rotating rod; the right side of the second baffle plate is fixed to the left side of the third moving block, and the left side of the second baffle plate penetrates through the second quantitative frame and extends into the second quantitative frame; the left end of the pull rod is fixed on the right side of the moving plate, and the right end of the pull rod penetrates through the feeding box and extends to the outside of the feeding box; the left side of the pull handle is fixed at the right end of the pull rod; the surface of the guide frame penetrates through the surface of the feeding box, and the left side of the guide frame penetrates through the electrolytic box and extends to the inside of the electrolytic box.
Further, the right side at the top of feeding case is run through and is had the feeder hopper, the bottom of feeder hopper runs through the material storage box just extends to the inside of material storage box.
Further, the bottom fixedly connected with water pump of the inner wall of water tank, the play water end intercommunication of water pump has first water pipe, the top of first water pipe is run through the water tank and is extended to the outside of water tank, the right side fixedly connected with second water pipe of the inner wall of electrolysis box, the left end of second water pipe is run through the electrolysis box and is extended to the outside of electrolysis box, the left side on the surface of second water pipe with the top intercommunication of first water pipe, the second water pipe is located the surface intercommunication of the inside of electrolysis box has the shower nozzle.
Further, the bottom intercommunication on the right side of electrolysis box has the leading pipe, the right-hand member of leading pipe runs through the rose box and extends to the inside of rose box, the surface of leading pipe is provided with the water valve, the equal fixedly connected with heating block in both sides of the bottom of the inner wall of electrolysis box.
Furthermore, the left side of the top of the electrolytic tank is communicated with a gas collecting pipe, and the top of the left side of the water tank is communicated with a water injection pipe.
Furthermore, the equal fixedly connected with chucking frame in both sides of the inner wall of rose box, the top of the inner wall of chucking frame and the bottom sliding connection of inner wall have the cardboard, the top and the bottom of one side of cardboard with equal fixedly connected with second spring between one side of the inner wall of chucking frame, two the joint has the filter between the relative one side of cardboard, the surface of filter runs through the rose box and extends to the outside of rose box.
Further, the both sides of the bottom of bottom plate all fixedly connected with installation piece, the surface of installation piece has seted up the mounting hole.
Further, the top fixedly connected with fixed frame of bottom plate, the top swing joint of the inner wall of fixed frame has the workbin that connects.
Further, the surface of the electrolytic box is hinged with a box door through a hinge, and the surface of the box door is provided with a perspective window.
The use method of the electrolytic cell for the electrochemical test of the dregs treatment comprises the following steps:
the first step is as follows: the medicine residues are poured into the feeding box through the feeding hopper, the medicine residues automatically flow into the first quantitative frame and the second quantitative frame, a worker pulls the pull handle, the pull handle pulls the movable plate to a certain position through the pull rod, so that the medicine residues in the first quantitative frame flow downwards, when the first quantitative frame is opened, the movable plate drives the first pushing block through the action of the first spring and the stabilizing block, the first pushing block drives the second pushing block to move through the first connecting rod, the second pushing block drives the third pushing block through the second connecting rod, the third pushing block drives the first baffle to move, so that the first baffle is inserted into the first quantitative frame, the first quantitative frame can be isolated from the storage box, the medicine residues are prevented from continuously falling, the medicine residues in the first quantitative frame are all added into the electrolytic box, and the medicine residue detection amount is the storage amount of the first quantitative frame;
the second step is that: the storage battery works to carry out electrolytic treatment on the medicine residues through the anode rod and the cathode rod, after the treatment, the discharge valve is opened to enable the medicine residues after the electrolysis to fall into the material receiving box through the discharge pipe, the material receiving box is taken down, and the next detection is carried out on the medicine residues in the material receiving box;
the third step: opening a water valve, cleaning the inside of the electrolytic tank by a water pump through a first water pipe, a second water pipe and a spray head to prevent the next use of the electrolytic tank from being influenced, feeding cleaned water into a filter tank through a water conduit, filtering the water through a filter plate, and returning the filtered water into a water tank through a through pipe;
the fourth step: after cleaning, the movable plate is pushed back to the original position, so that the first quantitative frame is filled with medicine residues, a worker can pull the pull handle, the pull handle pulls the movable plate to a certain position through the pull rod, the movable plate is far away from the first quantitative frame and the second quantitative frame, so that the medicine residues in the first quantitative frame and the second quantitative frame flow down and flow into the electrolytic tank through the material guide frame, meanwhile, the movable plate drives the limiting block to move, the limiting block contacts the first movable block and then drives the first movable block to move, the first movable block drives the second movable block to move through the first rotating rod, the second movable block drives the third movable block to move through the second rotating rod, the third movable block drives the second baffle plate to move, so that the second quantitative frame is isolated from the material storage box by the second baffle plate, meanwhile, the first quantitative frame is isolated from the material storage box by the first baffle plate, and all the medicine residues in the first quantitative frame and the second quantitative frame flow into the electrolytic tank, the amount detected is twice the amount detected in the first step described above.
Compared with the prior art, the invention has the beneficial effects that:
(1) this electrolytic cell for electrochemistry test is handled to dregs of a decoction and application method thereof, through the pulling pull handle, the pull handle passes through pull rod pulling movable plate to a definite position, adjust the position of use of movable plate, the user state of first quantitative frame of control and second ration frame, can make the inside dregs of a decoction of first quantitative frame flow in to the electrolysis box, perhaps the inside dregs of a decoction of first quantitative frame and second ration frame all flows in to the electrolysis box, the control gets into the amount of the inside dregs of a decoction of electrolysis box, carry out twice electrolysis and detect, thereby learn under the condition of twice dregs of a decoction electrolysis detection volume, contrast the testing result, improve its detection accuracy, and easy operation, be favorable to extensively using widely.
(2) The electrolytic cell for the electrochemical test for the dregs treatment and the using method thereof are characterized in that a water pump is fixedly connected to the bottom of the inner wall of a water tank, the water outlet end of the water pump is communicated with a first water pipe, the top end of the first water pipe penetrates through the water tank and extends to the outside of the water tank, a second water pipe is fixedly connected to the right side of the inner wall of the electrolytic tank, the left end of the second water pipe penetrates through the electrolytic tank and extends to the outside of the electrolytic tank, the left side of the surface of the second water pipe is communicated with the top end of the first water pipe, and a sprayer is communicated to the surface of the second water pipe, which is located inside the electrolytic tank.
(3) The clamping frames are fixedly connected to two sides of the inner wall of the filter box, clamping plates are connected to the top of the inner wall of the clamping frame and the bottom of the inner wall in a sliding mode, second springs are fixedly connected between the top and the bottom of one side of each clamping plate and one side of the inner wall of the clamping frame, a filter plate is clamped between the opposite sides of the two clamping plates, the surface of the filter plate penetrates through the filter box and extends to the outside of the filter box, the clamping plates are extruded through the elastic force of the second springs, the filter plate is extruded by the two clamping plates, the filter plate is clamped, the stability of the filter plate in use is improved, the filter plate is convenient to disassemble so as to be convenient to clean, the practicability of the device is improved, and the used water is filtered and recovered through the filter plate and is reused, so that the waste of water resources is reduced, and the energy conservation and emission reduction are facilitated.
Drawings
FIG. 1 is a schematic structural diagram of an electrolytic cell for electrochemical testing of dregs of decoction treatment and a method for using the same according to the present invention;
FIG. 2 is a schematic structural diagram of the surface of an electrolytic cell for electrochemical testing of dregs treatment and the electrolytic cell using the method;
FIG. 3 is a schematic view of the inside structure of a feeding box of the electrolytic cell for electrochemical testing of dregs treatment and the method of using the same according to the present invention;
FIG. 4 is an enlarged view of a portion of the electrolytic cell for electrochemical testing of dregs treatment and the method of using the same of FIG. 1;
FIG. 5 is a schematic structural diagram of a material guiding frame of the electrolytic cell for electrochemical testing of dregs treatment and the use method thereof.
In the figure: 1-bottom plate, 2-water tank, 3-electrolytic tank, 4-feeding tank, 5-filtering tank, 6-storage battery, 7-anode rod, 8-cathode rod, 9-water conduit, 10-water valve, 11-heating block, 12-discharging pipe, 13-discharging valve, 14-storage tank, 15-first quantitative frame, 16-second quantitative frame, 17-moving plate, 18-guide frame, 19-stabilizing block, 20-first spring, 21-first pushing block, 22-first connecting rod, 23-second pushing block, 24-second connecting rod, 25-third pushing block, 26-first baffle, 27-limiting block, 28-first moving block, 29-telescopic rod, 30-first rotating rod, 31-second moving block, 32-second rotating rod, 33-third moving block, 34-second baffle, 35-pull rod, 36-pull handle, 37-feed hopper, 38-water pump, 39-first water pipe, 40-second water pipe, 41-spray head, 42-gas collecting pipe, 43-water injection pipe, 44-mounting block, 45-mounting hole, 46-fixing frame, 47-material receiving box, 48-clamping frame, 49-clamping plate, 50-second spring, 51-filter plate, 52-box door and 53-perspective window.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-5, the present invention provides a technical solution: an electrolytic cell for electrochemical test of dregs treatment comprises a bottom plate 1; the bottom of the water tank 2 is fixed on the left side of the top of the bottom plate 1; the two sides of the bottom of the electrolytic tank 3 are fixed on the two sides of the top of the bottom plate 1 through support columns; the bottom of the filter box 5 is fixed on the right side of the top of the bottom plate 1, the left side of the filter box 5 is communicated with the bottom of the right side of the water tank 2 through a through pipe, and a water outlet is formed in the filter box 5; the left side of the feeding box 4 is fixed on the top of the right side of the electrolytic box 3 through the supporting column, and the right side of the bottom of the feeding box 4 is fixedly connected with the right side of the top of the filtering box 5 through the supporting column; the bottom of the storage battery 6 is fixed at the top of the electrolytic tank 3, and the storage battery 6 can be connected with an external power supply through an external power line for charging; the top of the anode rod 7 is fixed on the left side of the top of the inner wall of the electrolytic tank 3, and the anode rod 7 is electrically connected with the anode of the storage battery 6 through a lead; the top end of the cathode bar 8 is fixed on the right side of the top of the inner wall of the electrolytic tank 3, and the cathode bar 8 is electrically connected with the cathode of the storage battery 6 through the lead; the surface of the discharge pipe 12 is communicated with the bottom of the electrolytic tank 3, and a discharge valve 13 is arranged on the surface of the discharge pipe 12; the top of the storage box 14 is fixed on the top of the inner wall of the feeding box 4; the surfaces of the first quantitative frame 15 and the second quantitative frame 16 respectively penetrate through two sides of the bottom of the storage box 14, the first quantitative frame 15 and the second quantitative frame 16 can have the same storage capacity, and the first quantitative frame 15 and the second quantitative frame 16 are square frames and are both hollow structures; the surface and the back of the moving plate 17 slide on the surface of the inner wall of the feeding box 4 and the back of the inner wall respectively, and the top of the moving plate 17 is contacted with the bottoms of the first quantitative frame 15 and the second quantitative frame 16; a stabilizing block 19, the bottom of which is fixed on the top of the moving plate 17 and is positioned at the right side of the first quantitative frame 15; the bottom of the first pushing block 21 slides on the top of the moving plate 17, a first spring 20 is fixedly connected between the left side of the first pushing block 21 and the right side of the stabilizing block 19, and the first spring 20 is used for sliding the first pushing block 21 on the moving plate 17 along with the movement of the moving plate 17 after the first baffle 26 contacts the inner wall of the first quantitative frame 15, so that the second spring 20 is compressed without affecting the normal movement of the moving plate 17; the right side of the second pushing block 23 slides on the right side of the inner wall of the feeding box 4, and the left side of the second pushing block 23 is rotatably connected with the right side of the first pushing block 21 through a first connecting rod 22; the top of the third pushing block 25 slides to the bottom of the storage box 14 through a sliding rod, and the right side of the third pushing block 25 is rotatably connected with the top of the second pushing block 21 through a second connecting rod 24; a first baffle 26, the right side of the first baffle 26 is fixed on the left side of the third pushing block 25, and the left side of the first baffle 26 penetrates through the first quantitative frame 15 and extends to the inside of the first quantitative frame 15; a limiting block 27, wherein the bottom of the limiting block 27 is fixed on the right side of the top of the moving plate 17; the right side of the first moving block 28 is fixed on the right side of the inner wall of the feeding box 4 through a telescopic rod 29; the right side of the second moving block 31 slides on the right side of the inner wall of the feeding box 4, and the left side of the second moving block 31 is rotatably connected with the top of the first moving block 28 through a first rotating rod 30; a third moving block 33, the top of the third moving block 33 slides on the right side of the bottom of the storage box 14 through the sliding rod, and the right side of the third moving block 33 is rotatably connected with the top of the second moving block 31 through a second rotating rod 32; a second stopper 34, a right side of the second stopper 34 being fixed to a left side of the third moving block 33, and a left side of the second stopper 34 penetrating through the second fixed frame 16 and extending into the second fixed frame 16; the left end of the pull rod 35 is fixed on the right side of the moving plate 17, and the right end of the pull rod 35 penetrates through the feeding box 4 and extends to the outside of the feeding box 4; the left side of the pull handle 36 is fixed at the right end of the pull rod 35; the surface of the material guiding frame 18 penetrates through the surface of the material feeding box 4, the left side of the material guiding frame 18 penetrates through the electrolytic box 3 and extends to the inside of the electrolytic box 3, and the material guiding frame 18 is of a semi-circular ring type.
Further, a feed hopper 37 penetrates through the right side of the top of the feed box 4, and the bottom of the feed hopper 37 penetrates through the storage box 14 and extends to the inside of the storage box 14.
Further, the bottom fixedly connected with water pump 38 of the inner wall of water tank 2, the play water end intercommunication of water pump 38 has first water pipe 39, the top of first water pipe 39 runs through the water tank 2 and extends to the outside of water tank 2, the right side fixedly connected with second water pipe 40 of the inner wall of electrolysis box 3, the left end of second water pipe 40 runs through electrolysis box 3 and extends to the outside of electrolysis box 3, the left side on the surface of second water pipe 40 with the top intercommunication of first water pipe 39, second water pipe 40 is located the surface intercommunication of the inside of electrolysis box 3 has shower nozzle 41, and the quantity of shower nozzle 41 is a plurality of.
Further, the bottom intercommunication on electrolytic tank 3's right side has leading pipe 9, the right-hand member of leading pipe 9 runs through filter tank 5 just extends to the inside of filter tank 5, the surface of leading pipe 9 is provided with water valve 10, the equal fixedly connected with heating block 11 in both sides of the bottom of electrolytic tank 3's inner wall, heating block 11 can heat the dregs of a decoction, improves its reaction rate.
Further, a gas collecting pipe 42 is communicated with the left side of the top of the electrolytic tank 3, the gas collecting pipe 42 is communicated with an external gas collecting device and can collect gas generated after the electrolysis of the decoction dregs, and a water injection pipe 43 is communicated with the top of the left side of the water tank 2.
Further, the equal fixedly connected with chucking frame 48 in both sides of the inner wall of rose box 5, the top of the inner wall of chucking frame 48 and the bottom sliding connection of inner wall have cardboard 49, the top and the bottom of one side of cardboard 49 with equal fixedly connected with second spring 50, two between one side of the inner wall of chucking frame 48 the joint has filter 51 between the relative one side of cardboard 49, the surface of filter 51 runs through rose box 5 just extends to the outside of rose box 5, extrudes cardboard 49 through the elasticity of second spring 50, and two cardboard 46 extrude filter 51, carry out the chucking to filter 51, improve its stability when using, and be convenient for to dismantle filter 51 so that clear up it, improved the practicality of device.
Further, the both sides of the bottom of bottom plate 1 all fixedly connected with installation piece 44, mounting hole 45 has been seted up on the surface of installation piece 44, can improve the stability of its when using with equipment fixing in assigned position.
Further, the fixed frame 46 of top fixedly connected with of bottom plate 1, the top swing joint of the inner wall of fixed frame 46 has the material receiving box 47, and fixed frame 46 is the U type frame.
Further, the surface of electrolytic box 3 is articulated with chamber door 52 through the hinge, perspective window 53 has been seted up on the surface of chamber door 52, and the contact department of chamber door 52 and electrolytic box 3 is provided with the sealed pad, and the available staff of perspective window 53 observes the electrolysis condition.
The use method of the electrolytic cell for the electrochemical test of the dregs treatment comprises the following steps:
the first step is as follows: the medicine residues are poured into the feeding box 4 through the feeding hopper 37, the medicine residues automatically flow into the first quantitative frame 15 and the second quantitative frame 16, a worker pulls the pull handle 36, the pull handle 36 pulls the movable plate 17 to a certain position through the pull rod 35, so that the medicine residues in the first quantitative frame 15 flow downwards, when the first quantitative frame 15 is opened, the movable plate 17 drives a first pushing block 21 through the action of a first spring 20 and a stabilizing block 19, the first pushing block 21 drives a second pushing block 23 to move through a first connecting rod 22, the second pushing block 23 drives a third pushing block 25 through a second connecting rod 24, the third pushing block 25 drives a first baffle 26 to move, so that the first baffle 26 is inserted into the first quantitative frame 15, the first quantitative frame 15 can be isolated from the storage box 14, medicine residues are prevented from continuously falling down, the medicine residues in the first quantitative frame 15 are completely added into the electrolytic box 3, and the detection amount of the medicine residues is the storage amount of the first quantitative frame 15;
the second step is that: the storage battery 6 works to carry out electrolytic treatment on the medicine residues through the anode rod 7 and the cathode rod 8, after the treatment, the discharge valve 13 is opened, the medicine residues after the electrolysis fall into the material receiving box 47 through the discharge pipe 12, the material receiving box 47 is taken down, and the medicine residues in the material receiving box 47 are subjected to next detection;
the third step: the water valve 10 is opened, the water pump 38 works to clean the inside of the electrolytic tank 3 through the first water pipe 39, the second water pipe 40 and the spray head 41 to prevent the influence on the next use, the cleaned water enters the filter tank 5 through the water conduit 9, the water is filtered through the filter plate 51, and the filtered water flows back to the water tank 2 through the through pipe;
the fourth step: after cleaning, the moving plate 17 is pushed back to the original position, so that the first quantitative frame 15 is filled with herb residues, a worker can pull the pull handle 36, the pull handle 36 pulls the moving plate 17 to a certain position through the pull rod 35, so that the moving plate 17 is far away from the first quantitative frame 15 and the second quantitative frame 16, so that herb residues in the first quantitative frame 15 and the second quantitative frame 16 flow down and flow into the electrolytic tank 3 through the material guide frame 18, meanwhile, the moving plate 17 drives the limit block 27 to move, after the limit block 27 contacts the first moving block 28, the first moving block 28 is driven to move, the first moving block 28 drives the second moving block 31 to move through the first rotating rod 30, the second moving block 31 drives the third moving block 33 to move through the second rotating rod 32, the third moving block 33 drives the second baffle plate 34 to move, so that the second quantitative frame 16 is isolated from the material storage tank 14 by the second baffle plate 34, and meanwhile, the first quantitative frame 15 is isolated from the material storage tank 14, the medicine residue in the first and second quantitative frames 15 and 16 is prevented from flowing down continuously, and the medicine residue is detected by flowing into the electrolytic tank 3 in an amount twice the amount detected in the first step
When the quantitative box is used, medicine residues are poured into the feeding box 4 through the feeding hopper 37, the medicine residues automatically flow into the first quantitative frame 15 and the second quantitative frame 16 to fill the first quantitative frame 15 and the second quantitative frame 16, a worker can pull the pull handle 36 through the pull rod 35 to pull the movable plate 17 to a certain position, adjust the position of the movable plate 17, control the using state of the first quantitative frame 15 and the second quantitative frame 16, when the first quantitative frame 15 is opened, the movable plate 17 drives the first pushing block 21 through the action of the first spring 20 and the stabilizing block 19, the first pushing block 21 drives the second pushing block 23 to move through the first connecting rod 22, the second pushing block 23 drives the third pushing block 25 through the second connecting rod 24, the third pushing block 25 drives the first baffle 26 to move, so that the first baffle 26 is inserted into the first quantitative frame 15, and the storage box 14 can be isolated, the medicine dregs are prevented from continuously falling down, the medicine dregs in the first quantitative frame 15 are all added into the electrolytic tank 3, the detection quantity of the medicine dregs is the storage quantity of the first quantitative frame 15, the storage battery 6 works to carry out electrolytic treatment on the medicine dregs through the anode rod 7 and the cathode rod 8, the discharge valve 13 is opened after the treatment, the electrolyzed medicine dregs fall into the material receiving tank 47 through the discharge pipe 12, the material receiving tank 47 is taken down, the medicine dregs in the material receiving tank 47 are detected in the next step, the water valve 10 is opened, the water pump 38 works to clean the inside of the electrolytic tank 3 through the first water pipe 39, the second water pipe 40 and the spray head 41, the next use is prevented from being influenced, the cleaned water enters the filter tank 5 through the water guide pipe 9, the water is filtered through the filter plate 51, the filtered water flows back into the water tank 2 through the through pipe, the water is recycled, the waste of the water resource is reduced, the first quantitative frame 15 is filled with medicine residues, a worker can pull the pull handle 36 through the pull rod 35 to pull the movable plate 17 to a certain position, so that the movable plate 17 is far away from the first quantitative frame 15 and the second quantitative frame 16, so that the medicine residues in the first quantitative frame 15 and the second quantitative frame 16 flow down through the pull rod 35 and flow into the electrolytic tank 3 through the material guide frame 18, meanwhile, the movable plate 17 drives the limit block 27 to move, after the limit block 27 contacts the first movable block 28, the first movable block 28 drives the first movable block 28 to move, the first movable block 28 drives the second movable block 31 to move through the first rotating rod 30, the second movable block 31 drives the third movable block 33 through the second rotating rod 32 to move, the third movable block 33 drives the second baffle 34 to move, so that the second quantitative frame 16 is isolated from the storage tank 14 by the second baffle 34, meanwhile, the first quantitative frame 15 is isolated from the storage tank 14 by the first baffle 26 to prevent the medicine residues from continuously flowing, the medicine dregs in the first quantitative frame 15 and the second quantitative frame 16 all flow into the electrolytic tank 3 for detection, and the detection amount is twice of the detection amount in the first step, so that comparison is facilitated, the detection precision is improved, and wide popularization is facilitated.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. An electrolytic cell for electrochemical test of dregs treatment is characterized in that: comprises that
A base plate;
the bottom of the water tank is fixed on the left side of the top of the bottom plate;
the two sides of the bottom of the electrolytic tank are fixed on the two sides of the top of the bottom plate through support columns;
the bottom of the filter box is fixed on the right side of the top of the bottom plate, and the left side of the filter box is communicated with the bottom of the right side of the water tank through a through pipe;
the left side of the feeding box is fixed to the top of the right side of the electrolytic box through the supporting column, and the right side of the bottom of the feeding box is fixedly connected with the right side of the top of the filtering box through the supporting column;
the bottom of the storage battery is fixed at the top of the electrolytic tank;
the top of the anode rod is fixed on the left side of the top of the inner wall of the electrolytic tank, and the anode rod is electrically connected with the anode of the storage battery through a lead;
the top end of the cathode bar is fixed on the right side of the top of the inner wall of the electrolytic tank, and the cathode bar is electrically connected with the cathode of the storage battery through the lead;
the surface of the discharge pipe is communicated with the bottom of the electrolytic tank, and a discharge valve is arranged on the surface of the discharge pipe;
the top of the storage box is fixed on the top of the inner wall of the feeding box;
the surfaces of the first quantitative frame and the second quantitative frame respectively penetrate through two sides of the bottom of the storage box;
the surface and the back of the moving plate respectively slide and contact with the surface of the inner wall and the back of the inner wall of the feeding box, and the top of the moving plate is contacted with the bottoms of the first quantitative frame and the second quantitative frame;
the bottom of the stabilizing block is fixed to the top of the moving plate and is positioned on the right side of the first quantitative frame;
the bottom of the first pushing block slides on the top of the moving plate, and a first spring is fixedly connected between the left side of the first pushing block and the right side of the stabilizing block;
the right side of the second pushing block slides to the right side of the inner wall of the feeding box, and the left side of the second pushing block is rotatably connected with the right side of the first pushing block through a first connecting rod;
the top of the third pushing block slides to the bottom of the storage box through a sliding rod, and the right side of the third pushing block is rotatably connected with the top of the second pushing block through a second connecting rod;
the right side of the first baffle is fixed to the left side of the third pushing block, and the left side of the first baffle penetrates through the first quantitative frame and extends into the first quantitative frame;
the bottom of the limiting block is fixed on the right side of the top of the moving plate;
the right side of the first moving block is fixed on the right side of the inner wall of the feeding box through a telescopic rod;
the right side of the second moving block slides to the right side of the inner wall of the feeding box, and the left side of the second moving block is rotatably connected with the top of the first moving block through a first rotating rod;
the top of the third moving block slides on the right side of the bottom of the storage box through the sliding rod, and the right side of the third moving block is rotatably connected with the top of the second moving block through a second rotating rod;
the right side of the second baffle plate is fixed to the left side of the third moving block, and the left side of the second baffle plate penetrates through the second quantitative frame and extends into the second quantitative frame;
the left end of the pull rod is fixed on the right side of the moving plate, and the right end of the pull rod penetrates through the feeding box and extends to the outside of the feeding box;
the left side of the pull handle is fixed at the right end of the pull rod;
the surface of the guide frame penetrates through the surface of the feeding box, and the left side of the guide frame penetrates through the electrolytic box and extends to the inside of the electrolytic box.
2. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the right side at the top of feeding case is run through there is the feeder hopper, the bottom of feeder hopper is run through the material storage box and is extended to the inside of material storage box.
3. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the bottom fixedly connected with water pump of the inner wall of water tank, the play water end intercommunication of water pump has first water pipe, the top of first water pipe is run through the water tank and is extended to the outside of water tank, the right side fixedly connected with second water pipe of the inner wall of electrolysis box, the left end of second water pipe is run through the electrolysis box and is extended to the outside of electrolysis box, the left side on surface of second water pipe with the top intercommunication of first water pipe, the second water pipe is located the surface intercommunication of the inside of electrolysis box has the shower nozzle.
4. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the bottom on the right side of the electrolytic tank is communicated with a water conduit, the right end of the water conduit penetrates through the filter tank and extends to the inside of the filter tank, a water valve is arranged on the surface of the water conduit, and heating blocks are fixedly connected to the two sides of the bottom of the inner wall of the electrolytic tank.
5. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the left side of the top of the electrolytic tank is communicated with a gas collecting pipe, and the top of the left side of the water tank is communicated with a water injection pipe.
6. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the filter box is characterized in that clamping frames are fixedly connected to two sides of the inner wall of the filter box, clamping plates are slidably connected to the top of the inner wall of each clamping frame and the bottom of the inner wall of each clamping frame, second springs are fixedly connected to the top and the bottom of one side of each clamping plate and one side of the inner wall of each clamping frame, a filter plate is clamped between one opposite sides of the clamping plates, and the surface of the filter plate penetrates through the filter box and extends to the outside of the filter box.
7. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the mounting block is fixedly connected to the two sides of the bottom plate, and mounting holes are formed in the surface of the mounting block.
8. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the top fixedly connected with fixed frame of bottom plate, the top swing joint of the inner wall of fixed frame has the workbin that connects.
9. The electrolytic cell for the electrochemical test of the dregs of a decoction according to claim 1, which is characterized in that: the surface of the electrolytic tank is hinged with a tank door through a hinge, and the surface of the tank door is provided with a perspective window.
10. The use method of the electrolytic cell for the electrochemical test of the dregs of a decoction is characterized in that: the method comprises the following steps:
the first step is as follows: the medicine residues are poured into the feeding box through the feeding hopper, the medicine residues automatically flow into the first quantitative frame and the second quantitative frame, a worker pulls the pull handle, the pull handle pulls the movable plate to a certain position through the pull rod, so that the medicine residues in the first quantitative frame flow downwards, when the first quantitative frame is opened, the movable plate drives the first pushing block through the action of the first spring and the stabilizing block, the first pushing block drives the second pushing block to move through the first connecting rod, the second pushing block drives the third pushing block through the second connecting rod, the third pushing block drives the first baffle to move, so that the first baffle is inserted into the first quantitative frame, the first quantitative frame can be isolated from the storage box, the medicine residues are prevented from continuously falling, the medicine residues in the first quantitative frame are all added into the electrolytic box, and the medicine residue detection amount is the storage amount of the first quantitative frame;
the second step is that: the storage battery works to carry out electrolytic treatment on the medicine residues through the anode rod and the cathode rod, after the treatment, the discharge valve is opened to enable the medicine residues after the electrolysis to fall into the material receiving box through the discharge pipe, the material receiving box is taken down, and the next detection is carried out on the medicine residues in the material receiving box;
the third step: opening a water valve, cleaning the inside of the electrolytic tank by a water pump through a first water pipe, a second water pipe and a spray head to prevent the next use of the electrolytic tank from being influenced, feeding cleaned water into a filter tank through a water conduit, filtering the water through a filter plate, and returning the filtered water into a water tank through a through pipe;
the fourth step: after cleaning, the movable plate is pushed back to the original position, so that the first quantitative frame is filled with medicine residues, a worker can pull the pull handle to pull the movable plate to a certain position through the pull rod, the movable plate is far away from the first quantitative frame and the second quantitative frame, so that the medicine residues in the first quantitative frame and the second quantitative frame flow down and flow into the electrolytic tank through the material guide frame, the movable plate drives the limiting block to move simultaneously, the limiting block contacts the first movable block to drive the first movable block to move, the first movable block drives the second movable block to move through the first rotating rod, the second movable block drives the third movable block to move through the second rotating rod, the third movable block drives the second baffle plate to move, so that the second quantitative frame is isolated from the material storage box by the second baffle plate, meanwhile, the first quantitative frame is isolated from the material storage box by the first baffle plate, the medicine residues are prevented from continuously flowing down, and all the medicine residues in the first quantitative frame and the second quantitative frame flow into the electrolytic tank to be, the amount detected is twice the amount detected in the first step described above.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811501102.6A CN109580733B (en) | 2018-12-10 | 2018-12-10 | Electrolytic cell for electrochemical test of dregs treatment and use method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811501102.6A CN109580733B (en) | 2018-12-10 | 2018-12-10 | Electrolytic cell for electrochemical test of dregs treatment and use method thereof |
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| CN109580733A CN109580733A (en) | 2019-04-05 |
| CN109580733B true CN109580733B (en) | 2020-10-30 |
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| CN201173907Y (en) * | 2008-03-13 | 2008-12-31 | 王文斌 | Coulomb sulphur-measuring instrument electrolytic cell free of detaching and cleaning |
| CN103512935B (en) * | 2012-06-20 | 2015-12-02 | 鞍钢股份有限公司 | A kind of electrolytic cell of testing coating chemical property |
| JP2014015646A (en) * | 2012-07-06 | 2014-01-30 | Benten:Kk | Electrolytic treatment water generator and method for generating electrolytic treatment water |
| CN203069549U (en) * | 2012-12-25 | 2013-07-17 | 上海梅山钢铁股份有限公司 | Electrolytic bath for large sample electrolysis |
| CN108217856B (en) * | 2018-01-30 | 2024-02-20 | 武汉工程大学 | Electrochemical water treatment system and water treatment method thereof |
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