CN203069549U - Electrolytic bath for large sample electrolysis - Google Patents

Electrolytic bath for large sample electrolysis Download PDF

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Publication number
CN203069549U
CN203069549U CN 201220720754 CN201220720754U CN203069549U CN 203069549 U CN203069549 U CN 203069549U CN 201220720754 CN201220720754 CN 201220720754 CN 201220720754 U CN201220720754 U CN 201220720754U CN 203069549 U CN203069549 U CN 203069549U
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CN
China
Prior art keywords
electrolytic bath
electrolysis
electrolytic tank
cell body
filter screen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201220720754
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Chinese (zh)
Inventor
薛军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Meishan Iron and Steel Co Ltd
Original Assignee
Shanghai Meishan Iron and Steel Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Meishan Iron and Steel Co Ltd filed Critical Shanghai Meishan Iron and Steel Co Ltd
Priority to CN 201220720754 priority Critical patent/CN203069549U/en
Application granted granted Critical
Publication of CN203069549U publication Critical patent/CN203069549U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model relates to an electrolytic bath, and in particular relates to an electrolytic bath for large sample electrolysis. The electrolytic bath for large sample electrolysis is mainly used for solving the problems of collection of anode mud and discharge of waste liquid after electrolysis of the test sample, temperature generated during electrolysis of electrolyte, lots of dross formed on the filter screen during electrolysis and the like. The technical scheme of the utility model is as follows: the electrolytic bath for large sample electrolysis comprises an electrolytic bath body; a test sample is placed on a test sample support above the electrolytic bath body; a cone-shaped collector is arranged at the lower part of the electrolytic bath body; and the electrolytic bath is characterized in that a cylindrical filter screen which is open at the top and closed at the bottom and used for introducing gas is arranged above the cone-shaped collector, blowing holes are fully formed in the cylindrical filter screen at intervals, and the gas opening of the cylindrical filter screen penetrates through the test sample support and is led out of the electrolytic bath. Secondly, a waste liquid discharge hole is formed at the middle lower part of the electrolytic bath body and an anode mud collecting outlet is formed at the bottom of the cone-shaped collector and penetrates through the lower part of the electrolytic bath body to be led out. The electrolytic bath is mainly used for test sample electrolysis.

Description

A kind of bulk sample electrolysis electrolytic tank
Technical field
The utility model relates to a kind of electrolytic tank, particularly a kind of bulk sample electrolysis electrolytic tank.
Background technology
There are many problems in the present electrolytic tank that uses in the process of using: 1, the waste liquid after the electrolysis cannot be discharged from electrolytic tank, needs artificial integral body of later stage that cell body is handled, and labor capacity is big, should not clean, and electrolytic solution is hurted sb.'s feelings and contaminated environment.2, electrolytic solution can produce heat in the process of electrolysis, temperature also increases, and the too high meeting of temperature causes under burning (just the Fe of the earth of positive pole the is oxidized) high temperature iron oxidized easily, if oxidation is just non-conductive, electrolytic process will finish, the process of influence test.3, the sample ferric ion that electrolysis produces in electrolytic solution can accumulate in filter screen and form dross, normally by manually electrolytic solution irregularly being stirred, its effect is not very good for we, the more recovery that influences snotter of dross, simultaneously also making filter screen can only use once, is very much waste.
Chinese patent CN2559984Y discloses a kind of bulk sample electrolysis equipment, has related to cell body, but the not discarded liquid outlet of cell body does not relate to filter screen.Mainly be at specimen mounting micromachine to be installed electrolytic solution is stirred, this will produce following problem: 1, motor damages under acid environment easily.2, motor stirs and can only carry out in the small size of liquid, stirs the net wall less than filter screen, so the dross problem of filter screen be can't resolve.Simultaneously because the stirring of small size does not arrive the bottom, so do not play effect to reducing electrolyte temperature.
Summary of the invention
The purpose of this utility model provides a kind of bulk sample electrolysis electrolytic tank, mainly solves: the eliminating of the collection of the earth of positive pole, waste liquid after the sample electrolysis; Form problems such as a large amount of drosses when the temperature that electrolytic solution produces and electrolysis at filter screen when electrolysis.
The technical solution of the utility model: a kind of bulk sample electrolysis electrolytic tank, comprise the electrolytic tank cell body, electrolytic tank cell body top specimen mounting is mounted with sample, electrolytic tank cell body bottom is provided with conical collector, it is characterized in that the conical collector top is provided with the cylinder type filter net of the top open bottom sealing of ventilation body, cylinder type filter net is covered with the interval winding-up mouth is set, and the gas port of cylinder type filter net passes specimen mounting and draws electrolytic tank.Secondly be provided with the waste liquid escape hole in electrolytic tank cell body middle and lower part, establish the earth of positive pole in the conical collector bottom and collect outlet and pass electrolytic tank cell body bottom and draw.
The beneficial effects of the utility model: the cylinder type filter net that is provided with the top open bottom sealing of ventilation body by the conical collector top, winding-up by gas, reduce the temperature of electrolytic solution, avoid occurring in the electrolytic process generation of outage problem, electrolytic process can be carried out smoothly.Ferric ion also can form a large amount of drosses at filter screen in the process of electrolysis, influence the recovery of snotter, and the winding-up by gas also can increase the recovery of snotter so that dross reduces, and makes test figure more accurate.By being provided with the waste liquid escape hole in electrolytic tank cell body middle and lower part, establishing the earth of positive pole in the conical collector bottom and collect outlet and pass electrolytic tank cell body bottom and draw.Solve the recovery of electrolyte and the eliminating of discarded liquid.
Description of drawings
Fig. 1 is the utility model structural representation.
Among the figure: 1-gas port, 2-sample, 3-specimen mounting, 4-filter screen, 5-electrolytic tank cell body, 6-are jetted mouthful, the 7-conical collector, and 8-waste liquid escape hole, the 9-earth of positive pole is collected outlet.
Embodiment
With reference to Fig. 1, a kind of bulk sample electrolysis electrolytic tank, comprise electrolytic tank cell body 5, electrolytic tank cell body top specimen mounting 3 is mounted with sample 2, electrolytic tank cell body bottom is provided with conical collector 7, be provided with the cylinder type filter net 4 of the top open bottom sealing of ventilation body above the conical collector, cylinder type filter net 4 is covered with the interval winding-up mouth 6 is set, and the gas port 1 of cylinder type filter net passes specimen mounting 3 and draws electrolytic tank.Secondly be provided with waste liquid escape hole 8 in electrolytic tank cell body middle and lower part, establish the earth of positive pole in the conical collector bottom and collect outlet 9 and pass electrolytic tank cell body bottom and draw.
Electrolysis is carried out in energising, and the earth of positive pole of electrolysis arrives in the conical collector 7 through filter screen 4, collects outlet 9 by the earth of positive pole and collects.Filter screen 4 outer electrolytes flow out by waste liquid outlet 8.In order to reduce the temperature of electrolytic tank electrolyte inside, the gas port 1 on the filter screen can be ventilated, online after filtration 6 pairs of electrolytic solution of winding-up mouth are jetted, and so just can play the effect of cooling.Also can jet to the filter screen body when gas is jetted to electrolytic solution, so just can prevent ferric ion dross on filter screen.

Claims (2)

1. bulk sample electrolysis electrolytic tank, comprise the electrolytic tank cell body, electrolytic tank cell body top specimen mounting is mounted with sample, electrolytic tank cell body bottom is provided with conical collector, it is characterized in that the conical collector top is provided with the cylinder type filter net of the top open bottom sealing of ventilation body, cylinder type filter net is covered with the interval winding-up mouth is set, and the gas port of cylinder type filter net passes specimen mounting and draws electrolytic tank.
2. a kind of bulk sample electrolysis electrolytic tank according to claim 1 is characterized in that being provided with the waste liquid escape hole in electrolytic tank cell body middle and lower part, establishes the earth of positive pole in conical collector bottom and collects outlet and pass electrolytic tank cell body bottom and draw.
CN 201220720754 2012-12-25 2012-12-25 Electrolytic bath for large sample electrolysis Expired - Fee Related CN203069549U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220720754 CN203069549U (en) 2012-12-25 2012-12-25 Electrolytic bath for large sample electrolysis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220720754 CN203069549U (en) 2012-12-25 2012-12-25 Electrolytic bath for large sample electrolysis

Publications (1)

Publication Number Publication Date
CN203069549U true CN203069549U (en) 2013-07-17

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220720754 Expired - Fee Related CN203069549U (en) 2012-12-25 2012-12-25 Electrolytic bath for large sample electrolysis

Country Status (1)

Country Link
CN (1) CN203069549U (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107012487A (en) * 2017-04-14 2017-08-04 河北安泰可耐特冶金科技股份有限公司 A kind of earth of positive pole clears up system and earth of positive pole automatic cleaning method automatically
CN107201536A (en) * 2017-05-11 2017-09-26 河南中原黄金冶炼厂有限责任公司 A kind of novel electrolytic bath sludge drainage system and its method
CN109580733A (en) * 2018-12-10 2019-04-05 亳州学院 A kind of dregs of a decoction processing electrolytic cell in use for electrochemical tests and its application method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107012487A (en) * 2017-04-14 2017-08-04 河北安泰可耐特冶金科技股份有限公司 A kind of earth of positive pole clears up system and earth of positive pole automatic cleaning method automatically
CN107201536A (en) * 2017-05-11 2017-09-26 河南中原黄金冶炼厂有限责任公司 A kind of novel electrolytic bath sludge drainage system and its method
CN107201536B (en) * 2017-05-11 2020-05-19 河南中原黄金冶炼厂有限责任公司 Novel electrolytic bath sludge discharge system and method thereof
CN109580733A (en) * 2018-12-10 2019-04-05 亳州学院 A kind of dregs of a decoction processing electrolytic cell in use for electrochemical tests and its application method

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130717

Termination date: 20211225

CF01 Termination of patent right due to non-payment of annual fee