CN109577006A - A kind of production method of textile auxiliary melamine formaldehyde resin - Google Patents
A kind of production method of textile auxiliary melamine formaldehyde resin Download PDFInfo
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- CN109577006A CN109577006A CN201811275823.XA CN201811275823A CN109577006A CN 109577006 A CN109577006 A CN 109577006A CN 201811275823 A CN201811275823 A CN 201811275823A CN 109577006 A CN109577006 A CN 109577006A
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- CN
- China
- Prior art keywords
- formaldehyde resin
- melamine formaldehyde
- production method
- textile auxiliary
- added
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
- D06M15/423—Amino-aldehyde resins
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/64—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with nitrogen oxides; with oxyacids of nitrogen or their salts
- D06M11/65—Salts of oxyacids of nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/45—Shrinking resistance, anti-felting properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The invention proposes a kind of production method of textile auxiliary melamine formaldehyde resin, this method belongs to chemical field, and the raw material used includes: liquid melamine formaldehyde resin 92-93%, polyvinyl alcohol 4-5% count by weight percentage；Ammonium sulfate 2%, anti-aging agent 1% be raw material by the method that blends at a certain temperature come preparing finished articles, this method simple production process, good product quality, product is mainly used for the peace type processing of the fabrics such as polyester fiber, polyester fiber, synthetic cotton, blended product, there is following effect: increasing the elasticity of fabric, hardness, stiffening property and stability, improve feel；Wrinkle resistant polish that is shrinkproof, promoting fabric surface；Washing fastness is good.
Description
Technical field
Product of the present invention belongs to field of textiles more particularly to a kind of producer of textile auxiliary melamine formaldehyde resin
Method.
Background technique
Textile auxiliary is that have not in textile production process to the product quality and surcharge that improve textile
The important function that can or lack, it can not only assign the various specific functions of textile and style, such as soft, wrinkle resistant, shrinkproof, waterproof,
Antibacterial, antistatic, fire-retardant etc. can also improve dyeing and finishing technology, play the role of energy saving and reduce processing cost, weaving helps
Agent to promoted textile industry integral level and the effect in Textile Chain be it is vital, textile auxiliary product is about
80% is using surfactant as raw material, and about 20% is functional aid, and common textile auxiliary has refining agent, coloring agent, level dyeing
Agent, softening agent, capillary effect elevator etc..Melamine resin is widely used auxiliary agent in textile industry, existing in foreign countries
70 years history, China are just to start application the sixties, which can be improved the waterproof of fiber, anti-old and crease resistance, are made
Fabric is very scraped, good hand touch, is had bright gloss, can be used in mixed way with a variety of textile finishing aids.The auxiliary agent for polyester fiber,
The peace type of the fabrics such as polyester fiber, synthetic cotton, blended product is machined with following effect: 1. increase the elasticity of fabric, hardness, endure
Property and stability, improve feel；2. wrinkle resistant polish that is shrinkproof, promoting fabric surface；3. washing fastness is good, ultra-fine for polyester
Fiber can promote its hydrophobicity；For the calico with pigment, the fixation effect of pigment can be increased.The auxiliary agent uses Shi Kejia water
It is diluted to required concentration, then plus the catalyzer contact agent diluted and other finishing auxiliaries companion's use, setting temperature and time in forming machine
Different according to kinds of fibers, 130-160 DEG C of general temperature, the time was advisable with 130-180 seconds.
Summary of the invention
Present invention mainly solves the problem of be to provide the production method of textile auxiliary melamine formaldehyde resin a kind of, production
The raw material that the auxiliary agent uses is by weight ratio are as follows: liquid melamine formaldehyde resin 92-93%, polyvinyl alcohol 4-5%；Ammonium sulfate
2%, anti-aging agent 1%.
The present invention can be achieved through the following technical solutions:
A kind of production method of textile auxiliary melamine formaldehyde resin, feature are made of following steps:
(1) liquid melamine formaldehyde resin being added in reaction kettle, starts blender, the revolving speed of blender is 30 revs/min,
Temperature steps up 55-60 DEG C, is added the polyvinyl alcohol of formula ratio, and insulation reaction 1-1.2 hours；
(2) temperature is cut to 35-40 DEG C, continues to stir, the ammonium sulfate of formula ratio is added, is cooled to room temperature after mixing evenly,
The anti-aging agent of formula ratio is added, stops stirring to get finished product after stirring 0.2-0.3 hours.
Reaction temperature in reaction kettle described in step (1) is 57.5 DEG C, and the reaction time is 1.1 hours；
Room temperature in reaction kettle described in step (2) is 1-37 DEG C.
The beneficial effects of the present invention are: providing a kind of production method of textile auxiliary melamine formaldehyde resin, the party
Method simple process, good product quality, product be mainly used for the fabrics such as polyester fiber, polyester fiber, synthetic cotton, blended product it
The processing of peace type, have following effect: 1. increase the elasticity of fabric, hardness, stiffening property and stability, improve feel；2. wrinkle resistant shrinkproof, increasing
Into the polish of fabric surface；3. washing fastness is good.
Specific embodiment
Technical solutions according to the invention are further described in detail below by specific embodiment, but it is necessary to
It points out, following embodiment is served only for the description to summary of the invention, does not constitute a limitation on the scope of protection of the present invention.
Embodiment 1
The liquid melamine formaldehyde resin that total amount is 92% will be accounted for and be sent into reaction kettle, start blender, the revolving speed of blender is 30
Rev/min, temperature is stepped up to 55 DEG C, is added and accounts for the polyvinyl alcohol that total amount is 5%, insulation reaction 1.2 hours；Temperature tune
35 DEG C are dropped to, continues to stir, is added and accounts for the ammonium sulfate that total amount is 2%, is cooled to room temperature after mixing evenly, addition accounts for total amount and is
1% anti-aging agent stops stirring to get finished product after stirring 0.2 hour.
Embodiment 2
The liquid melamine formaldehyde resin that total amount is 92.5% will be accounted for and be sent into reaction kettle, start blender, the revolving speed of blender is
30 revs/min, temperature is stepped up to 57.5 DEG C, is added and accounts for the polyvinyl alcohol that total amount is 4.5%, insulation reaction 1.1 hours；?
Temperature is cut to 37.5 DEG C, continues to stir, and is added and accounts for the ammonium sulfate that total amount is 2%, be cooled to room temperature after mixing evenly, is added
The anti-aging agent that total amount is 1% is accounted for, stirring stopped stirring to get finished product after 0.25 hour.
Embodiment 3
The liquid melamine formaldehyde resin that total amount is 93% will be accounted for and be sent into reaction kettle, start blender, the revolving speed of blender is 30
Rev/min, temperature is stepped up to 60 DEG C, is added and accounts for the polyvinyl alcohol that total amount is 4%, insulation reaction 1 hour；Temperature is downgraded
To 40 DEG C, continue to stir, be added and account for the ammonium sulfate that total amount is 2%, is cooled to room temperature after mixing evenly, it is 1% that addition, which accounts for total amount,
Anti-aging agent, stirring 0.3 hour after stop stir to get finished product.
The above described is only a preferred embodiment of the present invention, be not intended to limit the present invention in any form, though
So the present invention has been disclosed as a preferred embodiment, and however, it is not intended to limit the invention, any technology people for being familiar with this profession
Member, without departing from the scope of the present invention, when the technology contents using the disclosure above make a little change or modification
It is right according to the technical essence of the invention for the equivalent embodiment of equivalent variations, but without departing from the technical solutions of the present invention
Any simple modification, equivalent change and modification made by above embodiments, all of which are still within the scope of the technical scheme of the invention.
Claims (3)
1. a kind of production method of textile auxiliary melamine formaldehyde resin, it is characterised in that: the raw material used percentage by weight
It include: liquid melamine formaldehyde resin 92-93%, polyvinyl alcohol 4-5% than calculating；Ammonium sulfate 2%, anti-aging agent 1%；(1) by liquid
State melamine resin is added in reaction kettle, starts blender, and the revolving speed of blender is 30 revs/min, and temperature is gradually mentioned
It is raised to 55-60 DEG C, is added the polyvinyl alcohol of formula ratio, insulation reaction 1-1.2 hours；
(2) temperature is cut to 35-40 DEG C, continues to stir, the ammonium sulfate of formula ratio is added, is cooled to room temperature after mixing evenly,
The anti-aging agent of formula ratio is added, stops stirring to get finished product after stirring 0.2-0.3 hours.
2. a kind of production method of textile auxiliary melamine formaldehyde resin according to claim 1, it is characterised in that: step
Suddenly the reaction temperature in reaction kettle described in (1) is 57.5 DEG C, and the reaction time is 1.1 hours.
3. a kind of production method of textile auxiliary melamine formaldehyde resin according to claim 1, it is characterised in that: step
Suddenly the room temperature in reaction kettle described in (2) is 1-37 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811275823.XA CN109577006A (en) | 2018-10-30 | 2018-10-30 | A kind of production method of textile auxiliary melamine formaldehyde resin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811275823.XA CN109577006A (en) | 2018-10-30 | 2018-10-30 | A kind of production method of textile auxiliary melamine formaldehyde resin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109577006A true CN109577006A (en) | 2019-04-05 |
Family
ID=65921185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811275823.XA Withdrawn CN109577006A (en) | 2018-10-30 | 2018-10-30 | A kind of production method of textile auxiliary melamine formaldehyde resin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109577006A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022213483A1 (en) * | 2021-04-07 | 2022-10-13 | 天台宏辉过滤科技有限公司 | Hydrophobic, anti-blocking and wear-resistant industrial filter cloth, and preparation method therefor |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1999014431A1 (en) * | 1997-09-18 | 1999-03-25 | Hollingsworth And Vose Company | Cellulose filter paper saturant |
| CN102191688A (en) * | 2010-03-11 | 2011-09-21 | 贾军 | Method for producing textile auxiliary melamine formaldehyde resin |
| WO2012085747A1 (en) * | 2010-12-21 | 2012-06-28 | Manifattura Lane Gaetano Marzotto & Figli S.P.A. | Method for treating textile materials |
| CN105506993A (en) * | 2014-10-20 | 2016-04-20 | 王光庆 | Production method of melamine formaldehyde resin textile auxiliary agent |
-
2018
- 2018-10-30 CN CN201811275823.XA patent/CN109577006A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1999014431A1 (en) * | 1997-09-18 | 1999-03-25 | Hollingsworth And Vose Company | Cellulose filter paper saturant |
| CN102191688A (en) * | 2010-03-11 | 2011-09-21 | 贾军 | Method for producing textile auxiliary melamine formaldehyde resin |
| WO2012085747A1 (en) * | 2010-12-21 | 2012-06-28 | Manifattura Lane Gaetano Marzotto & Figli S.P.A. | Method for treating textile materials |
| CN105506993A (en) * | 2014-10-20 | 2016-04-20 | 王光庆 | Production method of melamine formaldehyde resin textile auxiliary agent |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022213483A1 (en) * | 2021-04-07 | 2022-10-13 | 天台宏辉过滤科技有限公司 | Hydrophobic, anti-blocking and wear-resistant industrial filter cloth, and preparation method therefor |
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| PB01 | Publication | ||
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| WW01 | Invention patent application withdrawn after publication | ||
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Application publication date: 20190405 |