CN105862477B - A kind of textile auxiliary and preparation method thereof improving colour fixation - Google Patents
A kind of textile auxiliary and preparation method thereof improving colour fixation Download PDFInfo
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- CN105862477B CN105862477B CN201610246541.1A CN201610246541A CN105862477B CN 105862477 B CN105862477 B CN 105862477B CN 201610246541 A CN201610246541 A CN 201610246541A CN 105862477 B CN105862477 B CN 105862477B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/06—After-treatment with organic compounds containing nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of textile auxiliary improving colour fixation, the raw material proportioning with following parts by weight：45 55 parts of fatty alcohol polyoxyethylene ether, 40 50 parts of 3 chlorine, 2 hydroxypropyl-trimethyl ammonium chloride, 35 45 parts of dodecyl benzene sulfonic acid ammonium, 35 45 parts of Sodium Polyacrylate, 30 40 parts of sodium toluene sulfinate, 25 35 parts of quino dimethylacrylate, 20 30 parts of phthalic anhydride, 15 25 parts of transparent butadiene-styrene impact resin, 15 25 parts of catechin, 10 20 parts of nonylphenol polyoxyethylene ether, 10 20 parts of white carbon, 5 10 parts of crosslinking agent, 5 10 parts of softening agent reduce fabric so as to improving the colour fixation of textile and having both and scouring and bleaching the performance of temperature.Meanwhile also disclosing corresponding preparation method.
Description
Technical field
The present invention relates to technical field of textile auxiliary agent, and in particular to it is a kind of improve colour fixation textile auxiliary and its preparation
Method.
Background technology
Textile auxiliary is necessary chemicals in textile production process.Product of the textile auxiliary to raising textile
Quality and surcharge have indispensable important function, it can not only assign the various specific functions of textile and style, such as
Soft, wrinkle resistant, shrinkproof, waterproof, antibacterial, antistatic, fire-retardant etc. can also improve dyeing and finishing technology, play energy saving and reduce
The effect of processing cost.Textile auxiliary is to pass to the integral level of promotion textile industry and the effect in Textile Chain
Important.Existing textile auxiliary mainly has scouring agent, coloring agent, levelling agent, softening agent, capillary effect elevator, terylene low temperature dye
Color carrier, CT powder, preparation medium, efficiently moves back and boils powder, hydrogen peroxide stabilizer, desiliconizing agent, foaming agent, raising agent, fixation at substitute alkali
Agent etc..
But conventional textile auxiliary often helps less the colour fixation of textile dyeing, even if added with can
The chemical composition of tint retention is played, function and effect are not also notable, required dosage is larger, cannot meet textile actual production
Demand.Therefore, it is badly in need of developing a kind of composite spinning auxiliary agent that can effectively improve textile colour fixation.
Invention content
In order to solve the above technical problems, the present invention provides a kind of textile auxiliary and preparation method thereof improving colour fixation,
It is combined by using specified raw material, coordinates corresponding production technology, obtained a kind of fabric auxiliary agent, can improve
The colour fixation of textile, while having both and reduce fabric and scouring and bleaching the performance of temperature, it has a good application prospect.
The purpose of the present invention can be achieved through the following technical solutions：
A kind of textile auxiliary improving colour fixation, is made from the following raw materials in parts by weight：Fatty alcohol polyoxyethylene ether 45-
55 parts, 40-50 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, 35-45 parts of dodecyl benzene sulfonic acid ammonium, Sodium Polyacrylate 35-45
Part, 30-40 parts of sodium toluene sulfinate, 25-35 parts of quino dimethylacrylate, 20-30 parts of phthalic anhydride, butylbenzene are saturating
15-25 parts of bright anti-impact resin, 15-25 parts of catechin, 10-20 parts of nonylphenol polyoxyethylene ether, 10-20 parts of white carbon, crosslinking agent
5-10 parts, 5-10 parts of softening agent.
Preferably, the crosslinking agent is selected from polyisocyanates, polyethers amino modified polysiloxane, the aqueous isocyanide of enclosed type
One or more of acid esters.
Preferably, the softening agent is in silicone oil softener, ester based quaternary ammonium salt, dioctadecyl dimethyl ammonium chloride
One or more.
The preparation method of the textile auxiliary for improving colour fixation includes the following steps：
（1）Each raw material is weighed according to parts by weight；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, poly- third
Olefin(e) acid sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, add
The NaOH solution for entering 10% adjusts pH to 8.5, and 6-10h is stirred in the state of 7500-8500 r/m；
（3）Mixed liquor after stirring is heated to 65-75 DEG C, catechin, nonylphenol polyoxyethylene ether, hard charcoal is then added
It is black, ultrasound for the first time is carried out in ultrasonic machine, crosslinking agent, softening agent is then added, and is carried out second of ultrasound, is obtained finished product.
Preferably, the step（3）Middle first time ultrasonic power is 800w, ultrasonic time 6-7h, second of ultrasonic work(
Rate is 950w, ultrasonic time 4-5h.
Compared with prior art, the present invention advantage is：
（1）The textile auxiliary of the present invention is with fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, 12
Alkyl benzene sulphonate ammonium, Sodium Polyacrylate, sodium toluene sulfinate be main component, by be added quino dimethylacrylate,
Phthalic anhydride, transparent butadiene-styrene impact resin, catechin, nonylphenol polyoxyethylene ether, white carbon, crosslinking agent, softening agent, it is auxiliary
With techniques such as modification, stirring, heating, ultrasounds so that the textile auxiliary being prepared has the function of promotion fabric colour fixation,
Having both simultaneously, which reduces fabric, scourings and bleaching the performance of temperature.
（2）The textile auxiliary raw material of the present invention is cheap, simple for process, is suitable for heavy industrialization and uses, highly practical.
Specific implementation mode
The technical solution of invention is described in detail with reference to specific embodiment.
Embodiment 1
（1）According to parts by weight weigh 45 parts of fatty alcohol polyoxyethylene ether, 40 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides,
35 parts of dodecyl benzene sulfonic acid ammonium, 35 parts of Sodium Polyacrylate, 30 parts of sodium toluene sulfinate, quino dimethylacrylate 25
Part, 20 parts of phthalic anhydride, 15 parts of transparent butadiene-styrene impact resin, 15 parts of catechin, 10 parts of nonylphenol polyoxyethylene ether, hard charcoal
Black 10 parts, 5 parts of polyisocyanates, 5 parts of silicone oil softener；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, poly- third
Olefin(e) acid sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, add
The NaOH solution for entering 10% adjusts pH to 8.5, and 6h is stirred in the state of 7500 r/m；
（3）Mixed liquor after stirring is heated to 65 DEG C, catechin, nonylphenol polyoxyethylene ether, white carbon is then added,
Ultrasound for the first time is carried out in ultrasonic machine, polyisocyanates, silicone oil is then added in ultrasonic power 800w, ultrasonic time 6h
Softening agent carries out second of ultrasound, and ultrasonic power 950w, ultrasonic time 4h obtain finished product.
The performance test results of textile auxiliary obtained are as shown in table 1.
Embodiment 2
（1）According to parts by weight weigh 50 parts of fatty alcohol polyoxyethylene ether, 45 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides,
40 parts of dodecyl benzene sulfonic acid ammonium, 40 parts of Sodium Polyacrylate, 35 parts of sodium toluene sulfinate, quino dimethylacrylate 30
Part, 25 parts of phthalic anhydride, 20 parts of transparent butadiene-styrene impact resin, 20 parts of catechin, 15 parts of nonylphenol polyoxyethylene ether, hard charcoal
Black 15 parts, 7 parts of polyethers amino modified polysiloxane, 7 parts of ester based quaternary ammonium salt；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, poly- third
Olefin(e) acid sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, add
The NaOH solution for entering 10% adjusts pH to 8.5, and 8h is stirred in the state of 8000 r/m；
（3）Mixed liquor after stirring is heated to 70 DEG C, catechin, nonylphenol polyoxyethylene ether, white carbon is then added,
Ultrasound for the first time is carried out in ultrasonic machine, it is amino modified poly- that polyethers is then added in ultrasonic power 800w, ultrasonic time 6.5h
Siloxanes, ester based quaternary ammonium salt carry out second of ultrasound, and ultrasonic power 950w, ultrasonic time 4.5h obtain finished product.
The performance test results of textile auxiliary obtained are as shown in table 1.
Embodiment 3
（1）According to parts by weight weigh 55 parts of fatty alcohol polyoxyethylene ether, 50 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides,
45 parts of dodecyl benzene sulfonic acid ammonium, 45 parts of Sodium Polyacrylate, 40 parts of sodium toluene sulfinate, quino dimethylacrylate 35
Part, 30 parts of phthalic anhydride, 25 parts of transparent butadiene-styrene impact resin, 25 parts of catechin, 20 parts of nonylphenol polyoxyethylene ether, hard charcoal
Black 20 parts, 10 parts of enclosed type water-based isocyanate, 10 parts of dioctadecyl dimethyl ammonium chloride；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, poly- third
Olefin(e) acid sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, add
The NaOH solution for entering 10% adjusts pH to 8.5, and 10h is stirred in the state of 8500 r/m；
（3）Mixed liquor after stirring is heated to 75 DEG C, catechin, nonylphenol polyoxyethylene ether, white carbon is then added,
Ultrasound for the first time is carried out in ultrasonic machine, the aqueous isocyanic acid of enclosed type is then added in ultrasonic power 800w, ultrasonic time 7h
Ester, dioctadecyl dimethyl ammonium chloride carry out second of ultrasound, and ultrasonic power 950w, ultrasonic time 5h are obtained into
Product.
The performance test results of textile auxiliary obtained are as shown in table 1.
Embodiment 4
（1）According to parts by weight weigh 45 parts of fatty alcohol polyoxyethylene ether, 50 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides,
35 parts of dodecyl benzene sulfonic acid ammonium, 45 parts of Sodium Polyacrylate, 30 parts of sodium toluene sulfinate, quino dimethylacrylate 35
Part, 20 parts of phthalic anhydride, 25 parts of transparent butadiene-styrene impact resin, 15 parts of catechin, 20 parts of nonylphenol polyoxyethylene ether, hard charcoal
Black 10 parts, 5 parts of polyethers amino modified polysiloxane, 10 parts of dioctadecyl dimethyl ammonium chloride；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, poly- third
Olefin(e) acid sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, add
The NaOH solution for entering 10% adjusts pH to 8.5, and 10h is stirred in the state of 7500 r/m；
（3）Mixed liquor after stirring is heated to 65 DEG C, catechin, nonylphenol polyoxyethylene ether, white carbon is then added,
Ultrasound for the first time is carried out in ultrasonic machine, the amino modified poly- silicon of polyethers is then added in ultrasonic power 800w, ultrasonic time 7h
Oxygen alkane, dioctadecyl dimethyl ammonium chloride carry out second of ultrasound, and ultrasonic power 950w, ultrasonic time 4h are obtained into
Product.
The performance test results of textile auxiliary obtained are as shown in table 1.
Comparative example 1
（1）45 parts of fatty alcohol polyoxyethylene ether, 35 parts of dodecyl benzene sulfonic acid ammonium, Sodium Polyacrylate are weighed according to parts by weight
35 parts, 30 parts of sodium toluene sulfinate, 25 parts of quino dimethylacrylate, 20 parts of phthalic anhydride, styrene-butadiene transparent anti-impact
15 parts of resin, 15 parts of catechin, 10 parts of nonylphenol polyoxyethylene ether, 5 parts of polyisocyanates, 5 parts of silicone oil softener；
（2）By fatty alcohol polyoxyethylene ether, dodecyl benzene sulfonic acid ammonium, Sodium Polyacrylate, sodium toluene sulfinate, quino
Dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, be added 10% NaOH solution adjust pH to
8.5, stir 6h in the state of 7500 r/m；
（3）Mixed liquor after stirring is heated to 65 DEG C, catechin, nonylphenol polyoxyethylene ether is then added, in ultrasound
Ultrasound for the first time is carried out in machine, polyisocyanates, silicone oil softener is then added in ultrasonic power 800w, ultrasonic time 6h,
Second of ultrasound is carried out, ultrasonic power 950w, ultrasonic time 4h obtain finished product.
The performance test results of textile auxiliary obtained are as shown in table 1.
Comparative example 2
（1）According to parts by weight weigh 55 parts of fatty alcohol polyoxyethylene ether, 50 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides,
45 parts of dodecyl benzene sulfonic acid ammonium, 45 parts of Sodium Polyacrylate, 40 parts of sodium toluene sulfinate, quino dimethylacrylate 35
It is part, 30 parts of phthalic anhydride, 20 parts of nonylphenol polyoxyethylene ether, 20 parts of white carbon, 10 parts of enclosed type water-based isocyanate, double
10 parts of octadecyldimethyl ammonium chloride；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, poly- third
Olefin(e) acid sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride mixing, are added 10% NaOH solution tune
PH to 8.5 is saved, 10h is stirred in the state of 8500 r/m；
（3）Mixed liquor after stirring is heated to 75 DEG C, nonylphenol polyoxyethylene ether, white carbon is then added, in ultrasound
Carry out ultrasound for the first time in machine, enclosed type water-based isocyanate, double is then added in ultrasonic power 800w, ultrasonic time 7h
Octadecyldimethyl ammonium chloride carries out second of ultrasound, and ultrasonic power 950w, ultrasonic time 5h obtain finished product.
The performance test results of textile auxiliary obtained are as shown in table 1.
After the textile auxiliary of embodiment 1-4 and comparative example 1-2 are applied to fabric, its colour fixation and reduction are tested respectively
Fabric is scouringed and bleaching temperature effect.
Table 1
| Water logging fastness | Light fastness | It scourings and bleaching temperature lapse rate | |
| Embodiment 1 | 5 grades | 8 grades | 76% |
| Embodiment 2 | 5 grades | 8 grades | 73% |
| Embodiment 3 | 5 grades | 8 grades | 77% |
| Embodiment 4 | 5 grades | 8 grades | 68% |
| Comparative example 1 | 3 grades | 6 grades | 14% |
| Comparative example 2 | 3 grades | 5 grades | 12% |
The present invention with fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium,
Sodium Polyacrylate, sodium toluene sulfinate be main component, by be added quino dimethylacrylate, phthalic anhydride,
Transparent butadiene-styrene impact resin, catechin, nonylphenol polyoxyethylene ether, white carbon, crosslinking agent, softening agent, be aided with modified, stirring,
The techniques such as heating, ultrasound so that the textile auxiliary being prepared has the function of promoting fabric colour fixation, while having both reduction
Fabric is scouringed and bleaching the performance of temperature, and application prospect is good, has good social benefit.
Example the above is only the implementation of the present invention is not intended to limit the scope of the invention, every to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (1)
1. a kind of textile auxiliary improving colour fixation, it is characterised in that：It is made from the following raw materials in parts by weight：Fatty alcohol polyoxy
45-55 parts of vinethene, 40-50 parts of 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, 35-45 parts of dodecyl benzene sulfonic acid ammonium, polypropylene
Sour sodium 35-45 parts, 30-40 parts of sodium toluene sulfinate, 25-35 parts of quino dimethylacrylate, phthalic anhydride 20-30
Part, 15-25 parts of transparent butadiene-styrene impact resin, 15-25 parts of catechin, 10-20 parts of nonylphenol polyoxyethylene ether, white carbon 10-20
Part, 5-10 parts of crosslinking agent, 5-10 parts of softening agent；
The crosslinking agent in polyisocyanates, polyethers amino modified polysiloxane, enclosed type water-based isocyanate one
Kind is several；
The one kind or several of the softening agent in silicone oil softener, ester based quaternary ammonium salt, dioctadecyl dimethyl ammonium chloride
Kind；
The textile auxiliary of the raising colour fixation is prepared by following preparation methods：
（1）Each raw material is weighed according to parts by weight；
（2）By fatty alcohol polyoxyethylene ether, 3- chloro-2-hydroxypropyl-trimethyl ammonium chlorides, dodecyl benzene sulfonic acid ammonium, polyacrylic acid
Sodium, sodium toluene sulfinate, quino dimethylacrylate, phthalic anhydride, transparent butadiene-styrene impact resin mixing, are added
10% NaOH solution adjusts pH to 8 .5, and 6-10h is stirred in the state of 7500-8500 r/m；
（3）Mixed liquor after stirring is heated to 65-75 DEG C, catechin, nonylphenol polyoxyethylene ether, white carbon is then added,
Ultrasound for the first time is carried out in ultrasonic machine, crosslinking agent, softening agent is then added, and is carried out second of ultrasound, is obtained finished product；
The step（3）Middle first time ultrasonic power is 800w, and ultrasonic time 6-7h, second of ultrasonic power is 950w, is surpassed
The sound time is 4-5h.
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| CN107034700A (en) * | 2016-11-03 | 2017-08-11 | 江苏海云花新材料有限公司 | A kind of dyeing nylon acid-releasing agent and preparation method thereof |
| CN106637954A (en) * | 2016-12-16 | 2017-05-10 | 吴江市北厍盛源纺织品助剂厂 | Environment-friendly textile auxiliary and preparation method thereof |
| CN106939516A (en) * | 2017-05-22 | 2017-07-11 | 苏州凯邦生物技术有限公司 | A kind of textile auxiliary for improving color fastness and preparation method thereof |
| CN110344251A (en) * | 2019-07-15 | 2019-10-18 | 江苏方成生物科技有限公司 | A kind of environment-friendly type textile auxiliary |
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| CN101768883A (en) * | 2009-12-25 | 2010-07-07 | 青岛大学 | Preparation method of formaldehyde-free active dye fixing agent |
| CN104562804A (en) * | 2015-01-22 | 2015-04-29 | 南通优尼科化工有限公司 | Dye color fixing agent |
| CN104562805A (en) * | 2015-01-28 | 2015-04-29 | 桑达化工（南通）有限公司 | Fabric fixative |
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| CN105133391A (en) * | 2015-09-01 | 2015-12-09 | 桐乡市濮院毛针织技术服务中心 | Dyeing assistant for pure-cashmere products |
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| CN101768883A (en) * | 2009-12-25 | 2010-07-07 | 青岛大学 | Preparation method of formaldehyde-free active dye fixing agent |
| CN104562804A (en) * | 2015-01-22 | 2015-04-29 | 南通优尼科化工有限公司 | Dye color fixing agent |
| CN104562805A (en) * | 2015-01-28 | 2015-04-29 | 桑达化工（南通）有限公司 | Fabric fixative |
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