CN109554040A - A kind of self-drying aqueous dumb light glass lacquer and preparation method thereof - Google Patents
A kind of self-drying aqueous dumb light glass lacquer and preparation method thereof Download PDFInfo
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- CN109554040A CN109554040A CN201811563970.7A CN201811563970A CN109554040A CN 109554040 A CN109554040 A CN 109554040A CN 201811563970 A CN201811563970 A CN 201811563970A CN 109554040 A CN109554040 A CN 109554040A
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- dumb light
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/32—Radiation-absorbing paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/42—Gloss-reducing agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2312/00—Crosslinking
Abstract
The present invention discloses a kind of self-drying aqueous dumb light glass lacquer, it comprises the following components in parts by weight: 70~80 parts of hydroxyl acrylic emulsion, 8~12 parts of coalescing agent, 2~15 parts of deionized water, 0.6~2 part of water-based thickener, 0.4~0.8 part of substrate wetting agents, aqueous defoamer 0.2~0.6,0.3~0.6 part of aqueous dispersion, 0.1~0.3 part of aqueous levelling agent, aqueous dumb light starches 3~5 parts.The solid content of self-drying aqueous dumb light glass lacquer is higher and pre-polymerization degree is high, under air environment can rapid curing from dry, and adhesive force is excellent, simultaneously because having mushy adsorption hole in Silica hydrogel delustering agent, it can play the role of absorbing light and increase adsorption ability, make self-drying aqueous dumb light glass lacquer that there is matte effect and the Adhesion enhancement in glass surface, wetting attachment can be stablized in glass surface and certainly dry speed is fast, eventually form smooth and uniform paint layer.
Description
Technical field
The invention belongs to technical field of coatings, and in particular to a kind of self-drying aqueous dumb light glass lacquer and preparation method thereof.
Background technique
In glass industry, glass head product usually only has dull appearance color, need to use glass coating or ink
Coating carries out coating, to improve ornamental value.In the coating of glass, conventional water paint application effect is bad, this is because
The free energy of glass surface is low, and compared with oil paint, and the adhesive force and rate of drying of water paint are lower, so that aqueous painting
Material is not high to the adhesive force of glass, and paint layer is unstable easy to fall off；In addition, when smearing blocked up paint layer slow drying speed, make to be formed
Paint layer surface it is unevenly smooth.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of self-drying aqueous dumb light glass lacquer and preparation method thereof, energy
It is enough to be attached on glass well and form stable paint layer.
The technical scheme adopted by the invention to achieve the purpose is as follows:
A kind of self-drying aqueous dumb light glass lacquer, comprises the following components in parts by weight:
Further illustrate, the hydroxyl acrylic emulsion be water-soluble thermosetting acrylic acid, solid content be 60 ±
1%, hydroxyl value 85mgKOH/g, viscosity are 5000~10000s.
It further illustrating, the coalescing agent includes Lauryl Alcohol ester and propandiol butyl ether, the Lauryl Alcohol ester,
Content ratio of the propandiol butyl ether in coalescing agent is 4:1.
It further illustrates, the water-based thickener is polyurethane thickener, and selected from Guangzhou, hat will new material science and technology has
One or both of the AMS-201 thickener of limit company, AMS-301 thickener.
It further illustrates, the substrate wetting agents are polyether silicone wetting agent, create the limited public affairs of Degussa selected from winning
Take charge of one of TEGO-245 wetting agent, TEGO-260 wetting agent, TEGO-270 wetting agent.
It further illustrates, the aqueous defoamer is polyether siloxane copolymer lotion, is had selected from wound Degussa is won
Limit company, TEGO-825 defoaming agent, TEGO-845 defoaming agent one or two.
It further illustrates, the aqueous dispersion is sodium polycarboxylate salt form dispersing agent, is selected from the TaiWan, China Central Asia
Learn the SN-DISPERSANT-5040 dispersing agent of Co., Ltd.
It further illustrates, the aqueous levelling agent is polyacrylate flow agent, is selected from Bi Ke chemical company, Germany
BYK- 361N levelling agent.
It further illustrates, the aqueous dumb light slurry is a kind of Silica hydrogel delustering agent, and SiO2 content is 99%, hole
Rate is 1.8ml/g, and average particle size distribution is 4.5 microns, and the W-212 selected from good fortune mark (Guangzhou) material Science and Technology Ltd. is mute
Light starches dumb light slurry.
The preparation method of above-mentioned self-drying aqueous dumb light glass lacquer, is implemented by following steps:
Each component is weighed by component ratio, Scattered Kettle is arranged 60~80 DEG C of constant temperature, hydroxy acrylic acid is added in Scattered Kettle
Lotion, coalescing agent, aqueous dispersion, deionized water low speed dispersion mixing 10min, then sequentially add water-based thickener, base
Material wetting agent, aqueous defoamer, aqueous levelling agent high speed dispersion mix 30min, are eventually adding aqueous dumb light slurry high speed dispersion, until
Mixture viscosity is down to room temperature after 1000~2000Pas in kettle, uses pH adjusting agent adjusting pH value to 7.0~7.6, mistake
100 mesh screens, the encapsulation of gained screening save, and obtain self-drying aqueous dumb light glass lacquer.
Compared with prior art, the beneficial effects of the present invention are:
Using the higher hydroxyl acrylic emulsion of solid content as basic paint vehicle, pre-polymerization degree is higher, and the activity of polymerization is strong,
Autohemagglutination can occur, add coalescing agent and promote cross-linked polymeric, cooperation keeps whole polymer material viscous with all kinds of aqueous promoters
It is thick submissive, it is homogeneous, it is eventually adding Silica hydrogel delustering agent and is uniformly dispersed and obtain self-drying aqueous dumb light glass lacquer, self-drying type
The solid content of aqueous dumb light glass lacquer is higher and pre-polymerization degree is high, under air environment can rapid curing from dry, and adhesive force
It is excellent, simultaneously because having mushy adsorption hole in Silica hydrogel delustering agent, it can play and absorb light and increase adsorption
The effect of ability makes self-drying aqueous dumb light glass lacquer have matte effect and the Adhesion enhancement in glass surface, Neng Gou
Glass surface stablizes wetting attachment and certainly dry speed is fast, eventually forms smooth and uniform paint layer.
Specific embodiment
In order to further understand the content, features and effects of the present invention, hereby enumerating following embodiment explanation.
Embodiment 1
A kind of self-drying aqueous dumb light glass lacquer, comprises the following components in parts by weight: hydroxyl acrylic emulsion 74g, and 12
Carbon alcohol ester 8g, propandiol butyl ether 2g, deionized water 9.1g, AMS-201 thickener 0.8g, AMS-301 thickener 0.6g, TEGO-
245 wetting agent 0.5g, TEGO-825 defoaming agent 0.2g, TEGO-845 defoaming agent 0.2g, aqueous dispersion 0.4g, aqueous levelling agent
0.2g, aqueous dumb light starch 4g.
Preparation process: weighing each component by component ratio, and 65 DEG C of constant temperature are arranged in Scattered Kettle, and hydroxyl third is added in Scattered Kettle
Olefin(e) acid lotion, Lauryl Alcohol ester, propandiol butyl ether, aqueous dispersion, deionized water low speed dispersion mixing 10min, then successively
Be added AMS-201 thickener, AMS-301 thickener, TEGO-245 wetting agent, TEGO-825 defoaming agent, TEGO-845 defoaming agent,
Aqueous levelling agent high speed dispersion mixes 30min, aqueous dumb light slurry high speed dispersion is eventually adding, until mixture viscosity exists in kettle
After 1563Pas, it to be down to room temperature, using pH adjusting agent adjusting pH value to 7.4, sieves with 100 mesh sieve net, the encapsulation of gained screening saves,
Obtain the self-drying aqueous dumb light glass lacquer in the present embodiment.
Embodiment 2
A kind of self-drying aqueous dumb light glass lacquer, comprises the following components in parts by weight: hydroxyl acrylic emulsion 76g, and 12
Carbon alcohol ester 8g, propandiol butyl ether 2g, deionized water 7g, AMS-201 thickener 0.8g, AMS-301 thickener 0.6g, TEGO-
260 0.6 part of wetting agents, TEGO-825 defoaming agent 0.2g, TEGO-845 defoaming agent 0.2g, aqueous dispersion 0.5g, aqueous levelling
Agent 0.2g, aqueous dumb light starch 3.9g.
Preparation process: weighing each component by component ratio, and 65 DEG C of constant temperature are arranged in Scattered Kettle, and hydroxyl third is added in Scattered Kettle
Olefin(e) acid lotion, Lauryl Alcohol ester, propandiol butyl ether, aqueous dispersion, deionized water low speed dispersion mixing 10min, then successively
Be added AMS-201 thickener, AMS-301 thickener, TEGO-260 wetting agent, TEGO-825 defoaming agent, TEGO-845 defoaming agent,
Aqueous levelling agent high speed dispersion mixes 30min, aqueous dumb light slurry high speed dispersion is eventually adding, until mixture viscosity exists in kettle
After 1432Pas, it to be down to room temperature, using pH adjusting agent adjusting pH value to 7.3, sieves with 100 mesh sieve net, the encapsulation of gained screening saves,
Obtain self-drying aqueous dumb light glass lacquer in the present embodiment.
Embodiment 3
A kind of self-drying aqueous dumb light glass lacquer, comprises the following components in parts by weight: hydroxyl acrylic emulsion 79g, and 12
Carbon alcohol ester 9g, propandiol butyl ether 2.25g, deionized water 3.15g, AMS-201 thickener 0.6g, AMS-301 thickener 0.4g,
0.5 part of TEGO-245 wetting agent, TEGO-825 defoaming agent 0.2g, TEGO-845 defoaming agent 0.2g, aqueous dispersion 0.4g, water
Property levelling agent 0.2g, aqueous dumb light starches 4.1g.
Preparation process: weighing each component by component ratio, and 65 DEG C of constant temperature are arranged in Scattered Kettle, and hydroxyl third is added in Scattered Kettle
Olefin(e) acid lotion, Lauryl Alcohol ester, propandiol butyl ether, aqueous dispersion, deionized water low speed dispersion mixing 10min, then successively
Be added AMS-201 thickener, AMS-301 thickener, TEGO-245 wetting agent, TEGO-825 defoaming agent, TEGO-845 defoaming agent,
Aqueous levelling agent high speed dispersion mixes 30min, aqueous dumb light slurry high speed dispersion is eventually adding, until mixture viscosity exists in kettle
After 1384Pas, it to be down to room temperature, using pH adjusting agent adjusting pH value to 7.5, sieves with 100 mesh sieve net, the encapsulation of gained screening saves,
Obtain self-drying aqueous dumb light glass lacquer in the present embodiment.
Coating is carried out using embodiment 1 to 3 gained bi-component waterborne matte varnish of embodiment, performance survey is carried out to coating
Examination, the performance test results are shown in Table 1.
Table 1
The above is only the preferred embodiments of the present invention, and is not intended to limit the present invention in any form,
Any simple modification made to the above embodiment according to the technical essence of the invention, equivalent variations and modification, belong to
The range of technical solution of the present invention.
Claims (10)
1. a kind of self-drying aqueous dumb light glass lacquer, it is characterised in that: comprise the following components in parts by weight:
2. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the hydroxy yogurt
Liquid is water-soluble thermosetting acrylic acid, and solid content is 60 ± 1%, and hydroxyl value 85mgKOH/g, viscosity is 5000~10000s.
3. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the coalescing agent includes
Lauryl Alcohol ester and propandiol butyl ether, the content ratio of the Lauryl Alcohol ester, propandiol butyl ether in coalescing agent are 4:1.
4. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the water-based thickener is
Polyurethane thickener.
5. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the substrate wetting agents are
Polyether silicone wetting agent.
6. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the aqueous defoamer is
Polyether siloxane copolymer lotion.
7. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the aqueous dispersion is
Sodium polycarboxylate salt form dispersing agent.
8. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the aqueous levelling agent is
Polyacrylate flow agent.
9. a kind of self-drying aqueous dumb light glass lacquer according to claim 1, it is characterised in that: the aqueous dumb light, which is starched, is
A kind of Silica hydrogel delustering agent, SiO2 content are 99%, and porosity 1.8ml/g, average particle size distribution is 4.5 microns.
10. a kind of preparation method of the described in any item self-drying aqueous dumb light glass lacquers of claim 1 to 9, it is characterised in that:
Implemented by following steps: weighing each component by component ratio, Scattered Kettle is arranged 60~80 DEG C of constant temperature, hydroxyl is added in Scattered Kettle
Base acrylic emulsion, coalescing agent, aqueous dispersion, deionized water low speed dispersion mixing 10min, then sequentially add aqueous increasing
Thick dose, substrate wetting agents, aqueous defoamer, aqueous levelling agent high speed dispersion mixing 30min, are eventually adding aqueous dumb light slurry high speed
Dispersion, until mixture viscosity is down to room temperature after 1000~2000Pas in kettle, using pH adjusting agent adjust pH value to 7.0~
7.6, net is sieved with 100 mesh sieve, the encapsulation of gained screening saves, and obtains self-drying aqueous dumb light glass lacquer.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112409844A (en) * | 2020-07-14 | 2021-02-26 | 湖南松井新材料股份有限公司 | Water-based ink for realizing 3D glass matte effect and preparation method and application thereof |
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Application publication date: 20190402 |