CN109528509A - A kind of moisture-proof effervesce bath balls and preparation method thereof - Google Patents
A kind of moisture-proof effervesce bath balls and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8176—Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a kind of moisture-proof effervesce bath balls and preparation method thereof, this kind of bath balls include following component by mass parts: 30-60 parts of alkali source, 20-50 parts of acid source, 1-10 parts of covering material, 5-20 parts of filler and 0.5-3 parts of adhesive, the covering material is coated on the outer surface of the alkali source or acid source；This kind bath bath balls coat alkali source or acid source by covering material, completely cut off alkali source or acid source and outside air, avoid the generation for deliquescing phenomenon, it ensure that the autoreactivity quality of acid-base reaction object, bath balls are made to reach target effervesce effect, meanwhile also greatly extending the shelf life of bath balls；Furthermore the present invention, which also passes through lubricant and essence, makes consumer increase more pleasant experience sense when in use.
Description
Technical field
The present invention relates to daily chemical product fields, and in particular to a kind of moisture-proof effervesce bath balls and preparation method thereof.
Background technique
Effervesce formula bath balls are a daily chemical products of development and application in recent years, similar to the effervescent tablet in medicine.When
After bath balls are lost in water, main ingredient carbonate and acid react and generate a large amount of bubbles (CO2), are disintegrated bath ball, release
It is soluble in water to release other effective ingredients.But existing bath ball is easy to happen reaction in wet air, and bath ball is caused to be made moist
Failure, disintegration are slow, to influence the effect of bath balls and shorten its storage shelf-life.
Summary of the invention
It is an object of the present invention in view of the above shortcomings of the prior art, a kind of moisture-proof effervesce bath balls and its system are proposed
Preparation Method, this kind of bath balls are by the cladding to alkali source or acid source, so that reaching prevents bath balls from deliquescing, ensure that bath balls
Using effect storage time limit.
A kind of moisture-proof effervesce bath balls proposed by the present invention, include following component by mass parts: 30-60 parts of alkali source, acid source
20-50 parts, 1-10 parts of covering material, 5-20 parts of filler and 0.5-3 parts of adhesive, the covering material be coated on the alkali source or
The outer surface of person's acid source.
After the cladding that alkali source or acid source of the invention passes through covering material, the alkali source and acid acid source of alkalinity are avoided
Occur to deliquesce perhaps that hydrolysis or even redox reaction can not lead to the ingredient of alkali source or acid source with the moisture in air
Effect is reduced and is lost, and then when in use, realization neutralization reaction that can be quick and complete reaches target effect.
Cladding object can be selected in the present invention according to the practical stability of alkali source or acid source, to unstable reaction bottom
Object is coated, and after coating to alkali source or acid source one of which reaction substrate, another reaction substrate is upon mixing, all
Multiple reaction substrates being wrapped by can be arranged by adhesive and filler adhesion by enclosing, in this way, the reaction substrate of cladding again can be to not
The reaction substrate of cladding carries out protection isolation, keeps the dampproof effect in whole system more stable.Meanwhile the present invention can also adopt
After being coated respectively with alkali source and acid source, then mixed.
Further, the alkali source be one of sodium carbonate, sodium bicarbonate, potassium carbonate, saleratus and calcium carbonate or
Person is a variety of.
Further, the acid source is one of citric acid, tartaric acid, fumaric acid, hexanedioic acid and malic acid or more
Kind.
Further, the covering material is Macrogol 6000, Macrogol 4000, PVP K30, hydroxyl
Methylcellulose, methylcellulose, ethyl cellulose, hydroxypropyl methylcellulose, cellulose acetate, cellacefate, poly- methyl-prop
One or more of olefin(e) acid ester, zein, Compritol 888 ATO and carbomer.
Further, the filler is sucrose, anhydrous sodium sulphate, starch, maltodextrin, mannitol, lactose, sodium alginate and nothing
One or more of water magnesium sulfate.
Further, described adhesive is one of polyethylene glycol 400, water, dehydrated alcohol, 95% ethyl alcohol and isopropanol
Or it is a variety of.
It further, further include following component by mass parts: 0.01-0.2 parts of lubricant, 0.05-0.1 parts of pigment and essence
0.01-0.05 parts.
Further, the lubricant is in Macrogol 6000, magnesium stearate, isopropyl palmitate and hydrogenated vegetable oil
One or more.
A kind of preparation method of moisture-proof effervesce bath balls, comprising the following steps:
S1: covering material is dissolved in dehydrated alcohol or water, and it is 5-20% cladding solution that mass concentration, which is made,；
S2: the cladding solution being mixed with alkali source or acid source, is coated, after cladding, the dry 15- at 45-55 DEG C
25min, and 80 meshes are crossed, obtain intermediate product A；
S3: intermediate product A and filler, acid source or alkali source, adhesive and essence are carried out to be mixed to get intermediate product B；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Further, the alkali source needs follow the steps below processing: first by pigmentolysis, obtaining color water；Again by color water
Alkali source is mixed, until colouring；The alkali source after colouring is finally crossed into 80 meshes.
A kind of moisture-proof effervesce bath balls of the invention and preparation method thereof, this kind of bath salt ball by covering material to alkali source or
Person's acid source coats, and completely cuts off alkali source or acid source and outside air, avoids the generation for deliquescing phenomenon, ensure that soda acid is anti-
The autoreactivity quality for answering object makes bath balls reach target effervesce effect, meanwhile, also greatly extend the Storage period of bath balls
Limit；Furthermore the present invention, which also passes through lubricant and essence, makes consumer increase more pleasant experience sense when in use.
Specific embodiment
For present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate this hair
It is bright rather than limit the scope of the invention.In addition, various changes or modification that those skilled in the art make the present invention, this
A little equivalent forms are equally fallen in the application range claimed.Proportion in the embodiment of the present invention is by weight.
Embodiment 1
Alkali source pre-treatment: first 0.05 part of water colo(u)r is dissolved, obtains color water；Color water is mixed with 30 parts of sodium carbonate again and is stirred
It mixes, until colouring；Sodium carbonate after colouring is finally dried to 15min at 45 DEG C, and crosses 80 meshes, for use.
S1: 1 part of ethyl cellulose is dissolved in dehydrated alcohol or water, and it is 5% cladding solution that mass concentration, which is made,；
S2: by the cladding solution, sodium carbonate is mixed with treated, is coated, after cladding, the dry 15min at 45 DEG C,
And 80 meshes are crossed, obtain intermediate product A；
S3: by intermediate product A and 5 parts of maltodextrin, 20 parts of hexanedioic acid, 0.5 part of isopropanol, 0.01 part of isopropyl palmitate and essence
0.01 part carries out being mixed to get intermediate product B；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Embodiment 2
Alkali source pre-treatment: first 0.3 part of water colo(u)r is dissolved, obtains color water；Again by color water and 15 parts of potassium carbonate, saleratus
15 parts of mixings, until colouring；Finally by potassium carbonate, the saleratus dry 20min at 50 DEG C after colouring, and cross 80 mesh
Sieve, for use.
S1: 6 parts of Compritol 888 ATO are dissolved in dehydrated alcohol or water, and it is 13% cladding solution that mass concentration, which is made,；
S2: the cladding solution is mixed with treated potassium carbonate, saleratus, is coated, after cladding, is done at 50 DEG C
Dry 20min, and 80 meshes are crossed, obtain intermediate product A；
S3: by intermediate product A and 13 parts of anhydrous sodium sulphate, 35 parts of citric acid, 1.8 parts of 95% ethyl alcohol, 0.1 part of isopropyl palmitate and essence
0.3 part carries out being mixed to get intermediate product B；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Embodiment 3
Alkali source pre-treatment: first 0.1 part of water colo(u)r is dissolved, obtains color water；Color water is mixed with 60 parts of sodium bicarbonate again and is stirred
It mixes, until colouring；Sodium bicarbonate after colouring is finally dried to 25min at 55 DEG C, and crosses 80 meshes, for use.
S1: 10 parts of methylcellulose are dissolved in dehydrated alcohol or water, and it is 20% cladding solution that mass concentration, which is made,；
S2: the cladding solution being mixed with 50 parts of fumaric acid, is coated, after cladding, the dry 25min at 55 DEG C, and mistake
80 meshes obtain intermediate product A；
S3: by 20 parts of intermediate product A and filler, treated 50 parts of sodium bicarbonate, 0.3 part of Macrogol 4000, hydrogenated vegetable oil
0.2 part and 0.05 part of essence carries out being mixed to get intermediate product B；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Embodiment 4
Alkali source pre-treatment: first 0.1 part of water colo(u)r is dissolved, obtains color water；Color water is mixed with 50 parts of sodium bicarbonate again and is stirred
It mixes, until colouring；Sodium bicarbonate after colouring is finally dried to 20min at 50 DEG C, and crosses 80 meshes, for use.
S1: the third cellulose of hydroxyl first is dissolved in dehydrated alcohol or water for 5 parts, and it is 20% cladding solution that mass concentration, which is made,；
S2: by the cladding solution, sodium bicarbonate is mixed with treated, is coated, dry at 50 DEG C after cladding
20min, and 80 meshes are crossed, obtain intermediate product A；
S3: by intermediate product A and 2 parts of starch, 3 parts of lactose, 22.4 parts of tartaric acid, 1 part of polyethylene glycol 400,0.1 part of magnesium stearate
It carries out being mixed to get intermediate product B with 0.1 part of essence；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Embodiment 5
Alkali source pre-treatment: first 0.1 part of water colo(u)r is dissolved, obtains color water；Again by color water and 30 parts of sodium carbonate, sodium bicarbonate
20 parts of mixings, until colouring；Finally by sodium carbonate, the sodium bicarbonate dry 20min at 50 DEG C after colouring, and cross 80 mesh
Sieve, for use.
S1: 2.4 parts of PVP K30 are dissolved in dehydrated alcohol or water, and it is 20% packet that mass concentration, which is made,
Cover solution；
S2: the cladding solution being mixed with 35 parts of tartaric acid, is coated, after cladding, the dry 20min at 50 DEG C, and mistake
80 meshes obtain intermediate product A；
S3: by intermediate product A and 5 parts of starch, 5 parts of anhydrous magnesium sulfate, treated sodium carbonate, sodium bicarbonate, polyethylene glycol 400 1
Part, 0.5 part of magnesium stearate and 0.1 part of essence carry out being mixed to get intermediate product B；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Commercially available comparative example 1
Alkali source pre-treatment: first 0.05 part of water colo(u)r is dissolved, obtains color water；Color water is mixed with 50 parts of sodium carbonate again and is stirred
It mixes, until colouring；And 80 meshes are crossed, for use.
S1: after alkali source is handled with 3 parts of DEXTROSE ANHYDROUS, 7 parts of maltodextrin, 1 part of polyethylene glycol 400 and 0.1 part of essence
What is mixed arrives intermediate product A；
S2: it is uniformly mixed intermediate product A and 50 parts of citric acid to obtain intermediate product B；
S3: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Commercially available comparative example 2
Alkali source pre-treatment: first 0.05 part of water colo(u)r is dissolved, obtains color water；Color water is mixed with 40 parts of sodium carbonate again and is stirred
It mixes, until colouring；And 80 meshes are crossed, for use.
S1: after alkali source is handled with 3 parts of DEXTROSE ANHYDROUS, 3 parts of anhydrous sodium sulphate, 4 parts of maltodextrin, 1 part of polyethylene glycol 400
With 0.1 part of essence mixed to intermediate product A；
S2: it is uniformly mixed intermediate product A and 40 parts of citric acid to obtain intermediate product B；
S3: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
Evaluation:
Effervesce disintegration will be carried out by embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5 and its commercial goods, deposited
The storage time compares experiment, and correlation data is shown in Table 1.
It can be seen from Table 1 that the data that a kind of moisture-proof effervesce bath balls of the invention obtain will sufficiently be better than commercially available production
Product, bath balls covered effect of the invention is good, not moisture-sensitive, and disintegration rate is fast, absolutely proves that the present invention has in the technical field
It has large improvement.
Exemplary illustration is carried out to the embodiment of the present invention above, but the content is only preferable implementation of the invention
Example, should not be considered as limiting the scope of the invention.All the changes and improvements etc. of all application ranges according to the present invention,
It should all fall within the scope of the patent of the present invention.
Claims (10)
1. a kind of moisture-proof effervesce bath balls, it is characterised in that: by mass parts include following component: 30-60 parts of alkali source, acid source 20-
50 parts, 1-10 parts of covering material, 5-20 parts of filler and 0.5-3 parts of adhesive, the covering material be coated on the alkali source or
The outer surface of acid source.
2. a kind of moisture-proof effervesce bath balls as described in claim 1, it is characterised in that: the alkali source is sodium carbonate, bicarbonate
One or more of sodium, potassium carbonate, saleratus and calcium carbonate.
3. a kind of moisture-proof effervesce bath balls as described in claim 1, it is characterised in that: the acid source be citric acid, tartaric acid,
One or more of fumaric acid, hexanedioic acid and malic acid.
4. a kind of moisture-proof effervesce bath balls as described in claim 1, it is characterised in that: the covering material is polyethylene glycol
6000, Macrogol 4000, PVP K30, hydroxymethyl cellulose, methylcellulose, ethyl cellulose, hydroxypropyl first
One in cellulose, cellulose acetate, cellacefate, polymethacrylates, zein, Compritol 888 ATO and carbomer
Kind is a variety of.
5. a kind of moisture-proof effervesce bath balls as described in claim 1, it is characterised in that: the filler is sucrose, anhydrous sodium sulphate, shallow lake
One or more of powder, maltodextrin, mannitol, lactose, sodium alginate and anhydrous magnesium sulfate.
6. a kind of moisture-proof effervesce bath balls as described in claim 1, it is characterised in that: described adhesive be polyethylene glycol 400,
One or more of water, dehydrated alcohol, 95% ethyl alcohol and isopropanol.
7. a kind of moisture-proof effervesce bath balls as described in claim 1, it is characterised in that: by mass parts further include following component:
0.01-0.2 parts of lubricant, 0.05-0.1 parts of pigment and 0.01-0.05 parts of essence.
8. a kind of moisture-proof effervesce bath balls as claimed in claim 7, it is characterised in that: the lubricant is polyethylene glycol
6000, one or more of magnesium stearate, isopropyl palmitate and hydrogenated vegetable oil.
9. a kind of preparation method of moisture-proof effervesce bath balls as described in claim 1-8 any one, it is characterised in that: including
Following steps:
S1: covering material is dissolved in dehydrated alcohol or water, and it is 5-20% cladding solution that mass concentration, which is made,；
S2: the cladding solution being mixed with alkali source or acid source, is coated, after cladding, the dry 15- at 45-55 DEG C
25min, and 80 meshes are crossed, obtain intermediate product A；
S3: intermediate product A and filler, acid source or alkali source, adhesive, lubricant and essence are carried out to be mixed to get intermediate product B；
S4: by intermediate product B compression moulding, and dehumidifier drying is carried out, obtains a kind of moisture-proof effervesce bath balls.
10. a kind of preparation method of moisture-proof effervesce bath balls as claimed in claim 9, it is characterised in that: the alkali source needs
It follows the steps below processing: first by pigmentolysis, obtaining color water；Color scale source is mixed again, until colouring；It finally will be upper
Alkali source after color crosses 80 meshes.
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| CN201811311504.XA CN109528509A (en) | 2018-11-06 | 2018-11-06 | A kind of moisture-proof effervesce bath balls and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110292566A (en) * | 2019-07-08 | 2019-10-01 | 上海中医药大学 | A method of reducing effervescent tablet sticking amount in actual production |
| CN110559208A (en) * | 2019-10-15 | 2019-12-13 | 华熙生物科技股份有限公司 | Bathing effervescent tablet containing hyaluronic acid |
| CN111150664A (en) * | 2020-01-09 | 2020-05-15 | 东莞市星泽日用品有限公司 | Moisture-proof particle bath salt ball and preparation method thereof |
| CN111234943A (en) * | 2020-03-02 | 2020-06-05 | 惠州市多美日用品有限公司 | Aerobic laundry explosive ball and preparation method thereof |
| CN111265417A (en) * | 2020-02-12 | 2020-06-12 | 东莞市星泽日用品有限公司 | Efficient moisture-proof coated bath salt ball and preparation method thereof |
| CN114767601A (en) * | 2022-03-02 | 2022-07-22 | 南京思麦高医药科技有限公司 | Traditional Chinese medicine effervescent bath ball and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110292566A (en) * | 2019-07-08 | 2019-10-01 | 上海中医药大学 | A method of reducing effervescent tablet sticking amount in actual production |
| CN110292566B (en) * | 2019-07-08 | 2022-03-29 | 上海中医药大学 | Method for reducing sticking quantity of effervescent tablets in actual production |
| CN110559208A (en) * | 2019-10-15 | 2019-12-13 | 华熙生物科技股份有限公司 | Bathing effervescent tablet containing hyaluronic acid |
| CN111150664A (en) * | 2020-01-09 | 2020-05-15 | 东莞市星泽日用品有限公司 | Moisture-proof particle bath salt ball and preparation method thereof |
| CN111265417A (en) * | 2020-02-12 | 2020-06-12 | 东莞市星泽日用品有限公司 | Efficient moisture-proof coated bath salt ball and preparation method thereof |
| CN111234943A (en) * | 2020-03-02 | 2020-06-05 | 惠州市多美日用品有限公司 | Aerobic laundry explosive ball and preparation method thereof |
| CN114767601A (en) * | 2022-03-02 | 2022-07-22 | 南京思麦高医药科技有限公司 | Traditional Chinese medicine effervescent bath ball and preparation method thereof |
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Application publication date: 20190329 |