CN103865649B - A kind of perfuming agent for dried flower and preparation method thereof - Google Patents
A kind of perfuming agent for dried flower and preparation method thereof Download PDFInfo
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- CN103865649B CN103865649B CN201410076159.1A CN201410076159A CN103865649B CN 103865649 B CN103865649 B CN 103865649B CN 201410076159 A CN201410076159 A CN 201410076159A CN 103865649 B CN103865649 B CN 103865649B
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- perfuming agent
- dried flower
- ester compound
- acrylic ester
- essence
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Abstract
The invention discloses a kind of perfuming agent for dried flower, comprise acrylic ester compound, essence, the mass percent of each composition in perfuming agent is, acrylic ester compound 20% ~ 50%, essence 2% ~ 10%.Also disclose preparation method simultaneously, (1) comminuted starting materials, (2) powder that (1) step prepares is mixed can obtain finished product with essence, the invention has the advantages that, have developed a kind of dried flower perfuming agent, compensate for the blank that market is specifically designed to dried flower perfuming agent, breach the bottleneck adopting perfume only, fragrance is maintained extend to half a year ~ 1 year, simultaneously can be fade-proof to dried flower, anticorrosion, moistureproof, dust-proof; The method preparing this perfuming agent is simple, saves complicated operating process, reduces energy consumption to greatest extent, has saved cost.
Description
Technical field
The present invention relates to the technical field of flower drying, in particular to a kind of sweetener for dried flower and preparation method thereof.
Background technology
Along with improving constantly of people's living standard, uphold nature and more and more higher to the grade of the pursuit of U.S..Nowadays, increasing people at home or office space all to lay out the flowers and plants oneself liked.But because the fresh flower fresh keeping time picked is very short, so fresh flower uses receive a definite limitation, even if can build the condition of flowers and plants growth at home with water or soil, but fresh and alive flowers and plants still have certain life cycle.So fresh flower is just made dried flower by ways such as dehydrations by people, then through design typification process, make the appreciation flowers can put for a long time in various place., although aesthetic appearance when dried flower can keep original fresh and alive state, really the fragrance of few flower, thus have impact on people's liking dried flower.In order to give dried flower perfuming, at present mainly by making dried flower savory to the method for perfumes on dried flower.But this method cost is expensive, and guarantor's fragrant time is short, often spray, and operates also inconvenient.
Summary of the invention
For solving in prior art to the defect that perfume cost is high, guarantor's fragrant time is short that dried flower perfuming adopts, the invention discloses a kind of perfuming agent for dried flower, cost is low, after using this perfuming agent, make the fragrant time lengthening of the guarantor of dried flower and there is fade-proof, anticorrosion, moistureproof, dustproof effect simultaneously, and then extending the duration of service of dried flower.
For achieving the above object, the technical solution used in the present invention is, a kind of perfuming agent for dried flower that the present invention develops, comprise acrylic ester compound, essence, the mass percent of each composition in perfuming agent is, acrylic ester compound 20% ~ 50%, essence 2% ~ 10%.Acrylic ester compound is adopted to replace to fall the consumption of essence, the film that the layer of transparent adopting this composition and quality proportioning can be formed on dried flower surface is very thin, when existing employing perfume is to dried flower perfuming, general fragrance retains 15-30 days, adopt this formula perfuming agent to dried flower perfuming, fragrance can retain half a year ~ 1 year.In addition also anti-moisture absorption, fade-proof, anti-dust suction effect can be played to dried flower.
This perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, the mass percent of three kinds of compositions in perfuming agent is triethyl citrate 1% ~ 5%, calcium carbonate 3% ~ 10%, glycerine 10% ~ 25%, wherein, triethyl citrate is softening agent, assist acrylic ester compound can form pliable and tough protective membrane on dried flower surface, calcium carbonate is as filler, the physical strength of protective membrane can be strengthened, prevent protective membrane from coming off in dried flower skin breakage, glycerine is softening agent, acrylic ester compound is jointly assisted to form pliable and tough protective membrane on dried flower surface with triethyl citrate.Adopt the quality proportioning of above-mentioned three kinds of compositions, can make further mutually for keep lasting while cost accomplish minimum.
Described acrylic ester compound is mixed formed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
Apart from the above, the invention also discloses the method for this perfuming agent of preparation, comprise the steps, (1) comminuted starting materials: acrylic ester compound being crushed to granularity is 100 object powder;
(2) acrylic ester compound (1) step prepared and essence Homogeneous phase mixing, the mass percent of each composition in perfuming agent is, acrylic ester compound 20% ~ 50%, essence 2% ~ 10%, both obtains perfuming agent after mixing.Starting material are ground into the powder of 100 granularities, be in order to essence combine prepare finished product after, in use, dissolve to greatest extent after adding ethanol, and a kind of film can be formed at dried flower surface spreading after ejection, make dried flower fragrance be maintained lastingly, fade-proof effect can be accomplished again, through test, finally obtaining this preparation method is method that is the easiest, that economize operating process, most cost-saving most, can also play simultaneously and maintain fragrance, bleed off look, rot-resistant best effect.
When perfuming agent comprises triethyl citrate, calcium carbonate, glycerine, preparation method is, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound, Paris white are broken to granularity;
(2) after the powder that (1) step prepares being mixed with triethyl citrate, glycerine, mix with essence again, both perfuming agent is obtained after Homogeneous phase mixing, each composition is acrylic ester compound 20% ~ 50% in the mass percent of perfuming agent, essence 2% ~ 10%, triethyl citrate 1% ~ 5%, calcium carbonate 3% ~ 10%, glycerine 10% ~ 25%.When perfuming agent adds triethyl citrate, calcium carbonate, glycerine, just perfuming agent can be obtained according to its preparation method.
The using method of this perfuming agent, during use, the perfuming agent getting about 8 grams is poured in 100ml95% ethanol, stirs and makes to be uniformly dispersed, be mixed with suspension, suspension is loaded in spraying equipment, evenly be sprayed on dried flower surface energy when forming certain film, dried flower is dry under 25 DEG C of-32 DEG C of conditions, can obtain keeping dried flower fragrant for a long time, this dried flower can be placed on indoor naturally, play beautify the environment, the effect of fragrant room air.
To sum up, the invention has the beneficial effects as follows, have developed a kind of dried flower perfuming agent, compensate for blank market being specifically designed to dried flower perfuming agent, breach the bottleneck adopting perfume only, fragrance is held time extend to half a year ~ 1 year, can play dried flower simultaneously anticorrosion, anti-ly to fade, moistureproof, dust-proof effect, dried flower still fresh and alive, lasting fragrance of color in triennium can be made, extend the duration of service of dried flower; The method preparing this perfuming agent is simple, saves complicated operating process, reduces energy consumption to greatest extent, has saved cost.
Embodiment
Content of the present invention is further illustrated below in conjunction with specific embodiment.
Embodiment one: a kind of perfuming agent for dried flower that the present invention develops, this perfuming agent comprises acrylic ester compound, essence, and the mass percent of each composition in perfuming agent is, acrylic ester compound 20%, essence 10%.
Acrylic ester compound is mixed formed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
The acrylic compounds of above-mentioned three kinds of compositions composition also can buy finished product use on the market, and this name of product is EudragitRS100, and manufacturer is German Romo Co., Ltd.
Prepare the method for this perfuming agent, comprise the steps, (1) comminuted starting materials: acrylic ester compound being crushed to granularity is 100 object powder;
(2) acrylic ester compound (1) step prepared and essence Homogeneous phase mixing, the mass percent of each composition in perfuming agent is, acrylic ester compound 20%, essence 10%, both obtains perfuming agent after mixing.Not in addition specified otherwise in preparation method below, condition is all produce under room temperature condition, condition of normal pressure.
The using method of this perfuming agent, during use, getting 8 grams of perfuming agents pours in 95% ethanol of 100ml, stirs and makes to be uniformly dispersed, be mixed with suspension, suspension is loaded in spraying equipment, evenly be sprayed on dried flower surface energy when forming certain film, dried flower is dry under 25 DEG C of-32 DEG C of conditions, can obtain keeping dried flower fragrant for a long time, this dried flower can be placed on indoor naturally, play beautify the environment, the effect of fragrant room air.
Below adopt perfuming agent of the present invention to dried flower process and existing perfume to the contrast effect of dried flower process:
Embodiment two: a kind of perfuming agent for dried flower that the present invention develops, comprises acrylic ester compound, essence, and the mass percent of each composition in perfuming agent is, acrylic ester compound 50%, essence 5%.
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and the mass percent of three kinds of compositions in perfuming agent is triethyl citrate 1%, calcium carbonate 3%, glycerine 10%.
Acrylic ester compound is mixed formed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
The method preparing perfuming agent of the present invention is, preparation method is, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound, Paris white are broken to granularity;
(2) after the powder that (1) step prepares being mixed with triethyl citrate, glycerine, mix with essence again, both perfuming agent is obtained after Homogeneous phase mixing, each composition is acrylic ester compound 50% in the mass percent of perfuming agent, essence 5%, triethyl citrate 1%, calcium carbonate 3%, glycerine 10%.
Below adopt perfuming agent of the present invention to dried flower process and existing perfume to the contrast effect of dried flower process:
Embodiment three: a kind of perfuming agent for dried flower that the present invention develops, comprises acrylic ester compound, essence, and the mass percent of each composition in perfuming agent is, acrylic ester compound 25%, essence 2%.
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and the mass percent of three kinds of compositions in perfuming agent is triethyl citrate 5%, calcium carbonate 10%, glycerine 25%.
Acrylic ester compound is mixed formed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
Preparation method is with embodiment two.
Below adopt perfuming agent of the present invention to dried flower process and existing perfume to the contrast effect of dried flower process:
Embodiment four: a kind of perfuming agent for dried flower that the present invention develops, comprises acrylic ester compound, essence, and the mass percent of each composition in perfuming agent is, acrylic ester compound 40%, essence 8%.
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and the mass percent of three kinds of compositions in perfuming agent is triethyl citrate 3%, calcium carbonate 5%, glycerine 12%.
Acrylic ester compound is mixed formed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
Preparation method is with embodiment two.
Below adopt perfuming agent of the present invention to dried flower process and existing perfume to the contrast effect of dried flower process:
Technique scheme only embodies the optimal technical scheme of technical solution of the present invention, and those skilled in the art all embody principle of the present invention to some variations that wherein some part may be made, and belong within protection scope of the present invention.
Claims (2)
1. for a perfuming agent for dried flower, it is characterized in that, this perfuming agent comprises acrylic ester compound, essence, and the mass percent of each composition in perfuming agent is, acrylic ester compound 20% ~ 50%, essence 2% ~ 10%;
Perfuming agent also comprises triethyl citrate, calcium carbonate, glycerine, and the mass percent of three kinds of compositions in perfuming agent is triethyl citrate 1% ~ 5%, calcium carbonate 3% ~ 10%, glycerine 10% ~ 25%;
Acrylic ester compound is mixed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1.
2. prepare a method for perfuming agent described in claim 1, it is characterized in that, the method comprises the steps, (1) comminuted starting materials: it is 100 object powder that acrylic ester compound, Paris white are broken to granularity; Wherein, acrylic ester compound is mixed by ethyl propenoate, methyl methacrylate, methacrylic acid trimethyl ammonium chloride base ethyl ester, and the mass ratio of three kinds of compositions is 1:2:0.1;
(2) after the powder that (1) step prepares being mixed with triethyl citrate, glycerine, mix with essence again, both perfuming agent is obtained after Homogeneous phase mixing, each composition in the mass percent of perfuming agent is: acrylic ester compound 20% ~ 50%, essence 2% ~ 10%, triethyl citrate 1% ~ 5%, calcium carbonate 3% ~ 10%, glycerine 10% ~ 25%, each composition sum is 100%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410076159.1A CN103865649B (en) | 2014-03-04 | 2014-03-04 | A kind of perfuming agent for dried flower and preparation method thereof |
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| CN201410076159.1A CN103865649B (en) | 2014-03-04 | 2014-03-04 | A kind of perfuming agent for dried flower and preparation method thereof |
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| CN103865649A CN103865649A (en) | 2014-06-18 |
| CN103865649B true CN103865649B (en) | 2015-11-04 |
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| CN107372474A (en) * | 2017-08-16 | 2017-11-24 | 河南科技学院 | A kind of dried flower color preserving agent, preparation method and color-retention method |
| CN112472859A (en) * | 2020-12-08 | 2021-03-12 | 华东理工大学 | Fragrance aromatherapy candle with twelve fragrances and lasting fragrance |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1784210A (en) * | 2003-05-07 | 2006-06-07 | 弗门尼舍有限公司 | Sprayable perfume with an improved tenacity |
| FR2902655A1 (en) * | 2006-06-23 | 2007-12-28 | Oreal | Topical cosmetic composition with long-lasting skin cooling and refreshing effect, comprises cooling agent and film-forming polymer in aqueous alcohol |
| CN101679914A (en) * | 2007-06-01 | 2010-03-24 | 可泰克斯有限合伙公司 | Method for formulating odoriferous active ingredients in order to protect same and to increase the persistence thereof |
| CN102395423A (en) * | 2009-04-17 | 2012-03-28 | 巴斯夫欧洲公司 | Carrier system for fragrances |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1784210A (en) * | 2003-05-07 | 2006-06-07 | 弗门尼舍有限公司 | Sprayable perfume with an improved tenacity |
| FR2902655A1 (en) * | 2006-06-23 | 2007-12-28 | Oreal | Topical cosmetic composition with long-lasting skin cooling and refreshing effect, comprises cooling agent and film-forming polymer in aqueous alcohol |
| CN101679914A (en) * | 2007-06-01 | 2010-03-24 | 可泰克斯有限合伙公司 | Method for formulating odoriferous active ingredients in order to protect same and to increase the persistence thereof |
| CN102395423A (en) * | 2009-04-17 | 2012-03-28 | 巴斯夫欧洲公司 | Carrier system for fragrances |
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