CN112472859A - Fragrance aromatherapy candle with twelve fragrances and lasting fragrance - Google Patents
Fragrance aromatherapy candle with twelve fragrances and lasting fragrance Download PDFInfo
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- CN112472859A CN112472859A CN202011442664.5A CN202011442664A CN112472859A CN 112472859 A CN112472859 A CN 112472859A CN 202011442664 A CN202011442664 A CN 202011442664A CN 112472859 A CN112472859 A CN 112472859A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
- A61L9/02—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air by heating or combustion
- A61L9/03—Apparatus therefor
- A61L9/035—Apparatus therefor emanating multiple odours
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
Abstract
The invention discloses a fragrance aromatherapy candle with twelve fragrance and lasting fragrance, which is prepared from the following components in parts by weight: mixing 95 parts of beeswax and 5 parts of dodecaperfume; the twelve perfume is prepared from the following components in percentage by mass: 5-10% of essence, 1-2% of a fragrance fixing agent, 0.5% of a flavoring agent and the balance of ethanol; the essence is twelve flower fragrances corresponding to the flower blossoming in May-Chang-Dou, and is selected from at least one of orchid, gardenia, litchi flower, sophora flower, peony, pomegranate flower, jasmine flower, lotus flower, jujube flower, sweet osmanthus flower, chrysanthemum flower and plum blossom; the fixative consists of isobutyric acid phenoxyethyl ester and benzyl alcohol in a mass ratio of (0.5-4) to 1; the flavoring agent is citrate polyether. The fragrance aromatherapy candle provided by the invention has the fragrance type corresponding to the specific flowery odour of twelve months, so that the specific pungent odor of the candle can be covered, and different enjoyment of the candle in different months in sense is endowed.
Description
Technical Field
The invention belongs to the technical field of daily-use chemical industry, and particularly relates to a fragrance aromatherapy candle with twelve fragrance and lasting fragrance.
Background
Perfume, which is one of cosmetics, is widely used in life, can emit a long-lasting and pleasant fragrance, is a liquid in which essence, a fragrance-retaining agent and ethanol are mixed, and can be mainly divided into three different forms, namely alcohol solution, emulsion and slurry. The perfume is also classified into various types according to the fragrance of the essence used in the perfume. The quality of the fragrance of the essence is a main factor of the quality of the perfume, and the design and the type selection of the fragrance type of the essence for the perfume are the key of the perfume.
The candle is traditionally used as a lighting tool, and nowadays, along with the continuous improvement of living standard, the candle is endowed with new significance, and the aromatherapy candle also starts to enter people's life, bringing new brilliance. The scented candle has the characteristic of fresh and pleasant fragrance. The scented candle belongs to one of the artistic candles, is beautiful in color, contains natural plant essential oil, and emits pleasant faint scent when burning. Therefore, in the aspect of fragrance type, the scented candle is diversified; in terms of fragrance, the scented candle is required to have a lasting fragrance effect.
In view of the above, there is a need to develop a perfume with various fragrance types and lasting fragrance, which is prepared by twelve flower fragrances corresponding to the blossoming in changan december, and can effectively remove the pungent odor of the candle itself, so that the perfume is well applied to the scented candle.
Disclosure of Invention
The first object of the invention is to provide a fragrance aromatherapy candle which has a twelve-fragrance and a lasting fragrance.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the invention provides a fragrance aromatherapy candle with twelve fragrance and lasting fragrance, which is prepared from the following components in parts by weight: mixing 95 parts of beeswax and 5 parts of dodecaperfume;
the twelve perfume is prepared from the following components in percentage by mass: 5-10% of essence, 1-2% of a fragrance fixing agent (the ratio of phenoxy ethyl isobutyrate to benzyl alcohol), 0.5% of a flavoring agent and the balance of ethanol;
the essence is twelve flower fragrances corresponding to the flower blossoming in May-Chang-Dou, and is selected from at least one of orchid, gardenia, litchi flower, sophora flower, peony, pomegranate flower, jasmine flower, lotus flower, jujube flower, sweet osmanthus flower, chrysanthemum flower and plum blossom;
the fixative consists of isobutyric acid phenoxyethyl ester and benzyl alcohol in a mass ratio of (0.5-4) to 1;
the flavoring agent is citrate polyether.
The preparation method of the fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps: melting the mixed beeswax in a water-proof manner, placing a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted mixed dense wax into the mold, adding the prepared twelve-fragrance perfume when the surrounding changes thin white, uniformly shaking, standing and solidifying to obtain the fragrance candle with twelve fragrance and lasting fragrance;
the preparation method of the twelve-fragrance perfume comprises the following steps: uniformly mixing phenoxy ethyl isobutyrate and benzyl alcohol to obtain a fixative, diluting essence with ethanol to obtain light perfume, dripping the prepared fixative and flavoring agent into the light perfume, uniformly mixing, standing, keeping out of the sun, and aging to obtain the twelve-fragrance perfume.
The mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is preferably 1:1, 1:2, 2:1, 3:2, 4: 1.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 5% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 6% of essence, 1% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 7% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 8% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 9% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 10% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 5% of essence, 2% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 6% of essence, 2% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 7% of essence, 2% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 8% of essence, 2% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 9% of essence, 2% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
The twelve-fragrance perfume is prepared from the following components in percentage by mass: 10% of essence, 2% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
Due to the adoption of the technical scheme, the invention has the following advantages and beneficial effects:
the fragrance aromatherapy candle with lasting fragrance provided by the invention uses the twelve fragrances which are prepared by using twelve flowerings blooming corresponding to Changan December, and the twelve fragrances are harmless and nontoxic, have elegant and fresh fragrance, have lasting and pleasant fragrance and special fragrance of twelve months, are mild and not irritant, and can endow the fragrance with enjoyment in different months in sense organs while ensuring the fragrance of the twelve fragrances; but also can prolong the effectiveness of the perfume and endow the perfume with sensory enjoyment in different hours; when the scented candle is manufactured, the twelve-fragrance perfume is added, so that the unique pungent smell of the candle can be covered, and meanwhile, the twelve-fragrance perfume can be kept for a long time for long-time storage and use.
The perfume fixative (the proportion of the isobutyric acid phenoxyethyl ester and the benzyl alcohol) and the flavoring agent used in the twelve-spice perfume provided by the invention do not influence the color, the fragrance, the state and the like of the light perfume.
The fragrance aromatherapy candle with twelve fragrance and lasting fragrance provided by the invention uses the fragrance type which is the specific fragrance corresponding to twelve months, not only can cover the specific pungent taste of the candle, but also endows the candle with different enjoyment in different months in sense, the fragrance is elegant and fresh, the fragrance is mild and non-irritating, nerves can be relieved, air can be purified, and peculiar smell can be eliminated; after the compounded fragrance fixing agent is added, the scented candle can keep fragrance for a long time and can be stored and used for a long time.
Detailed Description
In order to more clearly illustrate the invention, the invention is further described below in connection with preferred embodiments. It is to be understood by persons skilled in the art that the following detailed description is illustrative and not restrictive, and is not to be taken as limiting the scope of the invention.
The essence used in the examples of the present invention was purchased from international essence and flavor (china) limited (IFF); phenoxyethyl isobutyrate was purchased from Kyowa high chemical Co., Ltd; benzyl alcohol was purchased from the national pharmaceutical group. Ortho-dichlorobenzene (100ppm) was purchased from the pharmaceutical groups; citric acid was purchased from shanghai runjie chemical agents, ltd; benzoic acid was purchased from national pharmaceutical group; diethylene glycol monobutyl ether was purchased from the national pharmaceutical group.
Example 1
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
and (3) putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared orchid perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with orchid fragrance.
Preparing orchid perfume: 5% of essence (orchid), 1% of fragrance fixative (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 1:1), 0.5% of fragrance enhancer (citrate polyether), and the balance of ethanol; uniformly mixing 0.5g of isobutyric acid phenoxyethyl ester and 0.5g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 1:1) to obtain a fixative, diluting 5g of orchid essence into light perfume by using 93.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 2
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense candle into the mold, adding 5g of prepared gardenia perfume when the surrounding changes thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with the fragrance of gardenia.
Preparing gardenia perfume: 6% of essence (gardenia), 1% of fragrance fixing agent (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 1:2), 0.5% of fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.33g of isobutyric acid phenoxyethyl ester and 0.67g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 1:2) to obtain a fixative, diluting 6g of gardenia essence into light perfume by using 92.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 3
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
and (3) putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense candle into the mold, adding 5g of prepared litchi flower perfume when the surrounding is changed to be thin white, uniformly shaking, standing and solidifying to obtain the fragrance candle with litchi flower fragrance.
Preparing litchi flower perfume: 7% of essence (litchi flower), 1% of fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 2:1), 0.5% of fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.67g of isobutyric acid phenoxyethyl ester and 0.33g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 2:1) to obtain a fixative, diluting 7g of litchi essence into light perfume by using 91.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly stirring and mixing by magnetic force, standing in a dark place, and aging for 1 h.
Example 4
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared sophora flower perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with the fragrance of sophora flower.
Preparing sophora flower perfume: 8% of essence (sophora flower), 1% of fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 3:1), 0.5% of fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.75g of isobutyric acid phenoxyethyl ester and 0.25g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 3:1) to obtain a fixative, diluting 8g of sophora flower essence into light perfume by using 90.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 5
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared peony perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with peony fragrance.
Preparing peony perfume: 9% of essence (peony), 1% of perfume fixative (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 3:2), 0.5% of flavoring agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.6g of isobutyric acid phenoxyethyl ester and 0.4g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 3:2) to obtain a fixative, diluting 9g of peony essence into light perfume by 89.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 6
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense candle into the mold, adding 5g of prepared pomegranate flower perfume when the surrounding changes thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with the pomegranate flower fragrance.
Preparing pomegranate flower perfume: 10% of essence (pomegranate flower), 1% of fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 4:1), 0.5% of fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.8g of isobutyric acid phenoxyethyl ester and 0.2g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 4:1) to obtain a fixative, diluting 10g of pomegranate flower essence into light perfume by using 88.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 7
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense candle into the mold, adding 5g of prepared jasmine perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with the fragrance of jasmine.
Preparing jasmine flower perfume: 5% of essence (jasmine), 1% of fragrance fixing agent (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 1:1), 0.5% of fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.5g of isobutyric acid phenoxyethyl ester and 0.5g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 1:1) to obtain a fixative, diluting 5g of jasmine essence into light perfume by using 93.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 8
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
and putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared lotus perfume when the surrounding is changed to be thin white, uniformly shaking, standing and solidifying to obtain the fragrance candle with lotus fragrance.
Preparing the lotus perfume: 6% of essence (lotus), 2% of fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 1:2), 0.5% of fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 0.66g of isobutyric acid phenoxyethyl ester and 1.34g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 1:2) to obtain a fixative, diluting 6g of lotus essence into light perfume by using 91.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 9
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared jujube flower perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with jujube flower fragrance.
Preparing jujube flower perfume: 7% of essence (jujube flower), 2% of a fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 2:1), 0.5% of a fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 1.34g of isobutyric acid phenoxyethyl ester and 0.66g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 2:1) to obtain a fixative, diluting 7g of jujube essence into light perfume by using 90.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 10
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense candle into the mold, adding 5g of prepared sweet osmanthus perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with sweet osmanthus fragrance.
Preparing sweet osmanthus perfume: 8% of essence (sweet osmanthus), 2% of a fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 3:1), 0.5% of a fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 1.5g of isobutyric acid phenoxyethyl ester and 0.5g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 3:1) to obtain a fixative, diluting 8g of osmanthus essence into light perfume by 89.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by a dropper, uniformly stirring and mixing by magnetic force, standing in a dark place, and aging for 1 h.
Example 11
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
and putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared chrysanthemum perfume when the surrounding is changed into thin white, uniformly shaking, standing and solidifying to obtain the fragrance candle with chrysanthemum fragrance.
Preparing chrysanthemum perfume: 9% of essence (chrysanthemum), 2% of a fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 3:2), 0.5% of a fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 1.2g of isobutyric acid phenoxyethyl ester and 0.8g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 3:2) to obtain a fixative, diluting 9g of chrysanthemum essence into light perfume by using 88.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Example 12
A preparation method of a fragrance aromatherapy candle with twelve fragrance and lasting fragrance comprises the following steps:
putting 95g of mixed beeswax into a heat-resistant glassware, melting the mixed beeswax in a water-proof manner, putting a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted dense wax into the mold, adding 5g of prepared plum blossom perfume when the surrounding is changed to be thin white, shaking uniformly, standing and solidifying to obtain the fragrance candle with plum blossom fragrance.
Preparing plum blossom perfume: 10% of essence (plum blossom), 2% of a fragrance fixing agent (the mass ratio of isobutyric acid phenoxyethyl ester to benzyl alcohol is 4:1), 0.5% of a fragrance increasing agent (citrate polyether), and the balance of ethanol; uniformly mixing 1.6g of isobutyric acid phenoxyethyl ester and 0.4g of benzyl alcohol (the mass ratio of the isobutyric acid phenoxyethyl ester to the benzyl alcohol is 4:1) to obtain a fixative, diluting 10g of plum blossom essence into light perfume by using 87.5g of ethanol, dripping the prepared fixative and 0.5g of flavoring agent into the light perfume by using a dropper, uniformly mixing by magnetic stirring, standing in a dark place, and aging for 1 h.
Comparative example 1
The same procedure as in example 1 was repeated except that the fragrance fixative was not contained as compared with example 1.
Comparative example 2
The same procedure as in example 1 was repeated except that benzoic acid as an odorant was contained in the composition in comparison with example 1.
Comparative example 3
The same procedure as in example 1 was repeated except that the composition contained diethylene glycol monobutyl ether as an odorant in example 1.
Comparative example 4
The same procedure as in example 1 was repeated except that the same procedure was carried out in example 1.
The prepared scented candles were tested for fragrance retention by two methods:
(1) sensory evaluation
Sensory evaluation of smell was performed on the aromatherapy candles obtained in examples 1 to 12 and comparative examples 1 to 4, specifically as follows:
placing the scented candle at a ventilated place, and comparing the fragrance intensity of the scented candle at intervals of one hour at the early stage for 1 hour, 2 hours and 3 hours …; and then comparing the strength of the smelling aroma at intervals of 6h, 24h and 48h ….
Sensory evaluation results of the aromatherapy candles obtained in examples 1 to 12 and comparative examples 1 to 4 are shown in the following table:
TABLE 1
For example 4, no dodecane was added, so the scented candle had only the taste of mixed beeswax.
(2) Headspace solid phase microextraction-gas chromatography
The fragrance retaining effect of the dodecahedron in the aromatherapy candles obtained in examples 1 to 12 and comparative examples 1 to 4 is judged by detecting the fragrance release concentration after 8 hours by headspace solid phase microextraction-gas chromatography, and the specific steps are as follows:
adding 5mL of prepared twelve-spice perfume with lasting fragrance into 50mL of deionized water, adding citric acid to adjust the pH value of the solution to 3.1, standing for 12h, adding deionized water to adjust the pH value of the solution to 4.0-4.2, soaking a piece of 12 x 12cm cotton cloth in the solution, stirring for 10min, standing for 5min to promote the fragrance fixing agent and the fragrance substance to be adsorbed on the cotton cloth, naturally drying overnight, ventilating and standing for 8 h. Then, 2mL of an acidic aqueous solution having a pH of 4.5 was uniformly sprayed on cotton cloth, the cotton cloth was cut into fine pieces and placed in a 20mL headspace bottle, and 20. mu.L of o-dichlorobenzene (100ppm) was added as an internal standard, and the bottle was sealed to conduct a solid phase microextraction.
The evaluation results of the twelve-fragrance perfumes proposed in examples 1 to 12 and comparative examples 1 to 4 are shown in the following table:
TABLE 2
From the above results, it can be seen that the fragrance-retaining time of example 8 is longest, the fragrance concentration detected after 8h is the greatest, and the fragrance-retaining property of the perfume is better than that of other perfume alone by using phenoxyethyl isobutyrate and benzyl alcohol as perfume fixatives at a suitable mass ratio. When the ratio of phenoxyethyl isobutyrate to benzyl alcohol as the fragrance fixing agent is 1:2 and the content of phenoxyethyl isobutyrate in the whole solution is 2%, the fragrance retaining effect is best.
The prepared twelve-fragrance perfume with the longest fragrance retention time and the largest fragrance concentration detected after 8 hours is selected to prepare the aromatherapy candle, so that the unique pungent smell of the candle is covered, the fragrance is mild, elegant and fresh, the fragrance is retained for a long time, and the candle can be stored and used for a long time.
The twelve-fragrance perfume is prepared by adding the fragrance fixative isobutyric acid phenoxyethyl ester and benzyl alcohol with the content of 1:2 and the essence of 5 percent into the candle. The combustion performance test result shows that: the scented candle added with the twelve perfume releases fresh fragrance in the combustion process, is safe and reliable, has excellent performance, and can purify air; when not in use, the fragrance of the scented candle can be kept for a long time. The scented candle without the addition of the twelve perfume has no fresh fragrance in the combustion process and keeps the taste of part of raw materials (mixed beeswax); when not in use, the scented candle only has the original taste of the mixed beeswax.
Although the present invention has been described with reference to a preferred embodiment, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (10)
1. The fragrance aromatherapy candle with twelve fragrance and lasting fragrance is characterized by being prepared from the following components in parts by weight: mixing 95 parts of beeswax and 5 parts of dodecaperfume;
the twelve perfume is prepared from the following components in percentage by mass: 5-10% of essence, 1-2% of a fragrance fixing agent, 0.5% of a flavoring agent and the balance of ethanol;
the essence is twelve flower fragrances corresponding to the flower blossoming in May-Chang-Dou, and is selected from at least one of orchid, gardenia, litchi flower, sophora flower, peony, pomegranate flower, jasmine flower, lotus flower, jujube flower, sweet osmanthus flower, chrysanthemum flower and plum blossom;
the fixative consists of isobutyric acid phenoxyethyl ester and benzyl alcohol in a mass ratio of (0.5-4) to 1;
the flavoring agent is citrate polyether.
2. The fragrance aromatherapy candle with a twelve fragrance and a lasting scent according to claim 1, wherein the preparation method of the fragrance aromatherapy candle with a twelve fragrance and a lasting scent comprises the steps of: melting the mixed beeswax in a water-proof manner, placing a wick into the bottom of a fragrance candle mold, straightening the wick, slowly pouring the melted mixed dense wax into the mold, adding the prepared twelve-fragrance perfume when the surrounding changes thin white, uniformly shaking, standing and solidifying to obtain the fragrance candle with twelve fragrance and lasting fragrance.
3. The scented candle of claim 1, wherein the scent having a twelve fragrance scent and a long lasting scent is produced by a process comprising the steps of: uniformly mixing phenoxy ethyl isobutyrate and benzyl alcohol to obtain a fixative, diluting essence with ethanol to obtain light perfume, dripping the prepared fixative and flavoring agent into the light perfume, uniformly mixing, standing, keeping out of the sun, and aging to obtain the twelve-fragrance perfume.
4. The fragrance aromatherapy candle having a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the mass ratio of phenoxyethyl isobutyrate to benzyl alcohol is 1:1, 1:2, 2:1, 3:2, 4: 1.
5. The fragrance aromatherapy candle with a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the twelve-note fragrance is prepared from the following components in percentage by mass: 5% of essence, 1% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol;
or the twelve-fragrance perfume is prepared from the following components in percentage by mass: 6% of essence, 1% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol.
6. The fragrance aromatherapy candle with a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the twelve-note fragrance is prepared from the following components in percentage by mass: 7% of essence, 1% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol;
or the twelve-fragrance perfume is prepared from the following components in percentage by mass: 8% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
7. The fragrance aromatherapy candle with a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the twelve-note fragrance is prepared from the following components in percentage by mass: 9% of essence, 1% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol;
or the twelve-fragrance perfume is prepared from the following components in percentage by mass: 10% of essence, 1% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
8. The fragrance aromatherapy candle with a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the twelve-note fragrance is prepared from the following components in percentage by mass: 5% of essence, 2% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol;
or the twelve-fragrance perfume is prepared from the following components in percentage by mass: 6% of essence, 2% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol.
9. The fragrance aromatherapy candle with a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the twelve-note fragrance is prepared from the following components in percentage by mass: 7% of essence, 2% of a fragrance fixing agent, 0.5% of a flavoring agent and the balance of ethanol;
or the twelve-fragrance perfume is prepared from the following components in percentage by mass: 8% of essence, 2% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol.
10. The fragrance aromatherapy candle with a twelve-note fragrance and a lasting fragrance according to claim 1, wherein the twelve-note fragrance is prepared from the following components in percentage by mass: 9% of essence, 2% of fragrance fixing agent, 0.5% of flavoring agent and the balance of ethanol;
or the twelve-fragrance perfume is prepared from the following components in percentage by mass: 10% of essence, 2% of perfume fixative, 0.5% of flavoring agent and the balance of ethanol.
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| CN202011442664.5A CN112472859A (en) | 2020-12-08 | 2020-12-08 | Fragrance aromatherapy candle with twelve fragrances and lasting fragrance |
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Cited By (1)
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| WO2024047365A1 (en) * | 2022-09-02 | 2024-03-07 | Reckitt & Colman (Overseas) Hygiene Home Limited | A method of manufacturing a scented candle |
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Application publication date: 20210312 |