CN109512751A - A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract - Google Patents
A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract Download PDFInfo
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- CN109512751A CN109512751A CN201710844611.8A CN201710844611A CN109512751A CN 109512751 A CN109512751 A CN 109512751A CN 201710844611 A CN201710844611 A CN 201710844611A CN 109512751 A CN109512751 A CN 109512751A
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- semen phaseoli
- phaseoli radiati
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The invention discloses a kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract, the toothpaste containing Semen phaseoli radiati extract contains the Semen phaseoli radiati extract that total weight percent is 0.1%~3.2%, the Semen phaseoli radiati extract is mung bean chromocor extract, the general flavone for being 30%~50% containing weight percent in the mung bean chromocor extract, the toothpaste containing Semen phaseoli radiati extract includes following components by its weight percent: Semen phaseoli radiati extract 0.1%~3.2%, nanometer calcium carbonate 40%~50%, honeysuckle 8%~12%, TianXing grass 3%~7%, silica 1 %~5%, propylene glycol 3%~10%, laruyl alcohol sodium sulfovinate 1%-3%, xanthan gum 0.5%~1%, cellulose gum 1%~2%, sorbierite 1~4%, peppermint oil 1%~2%, vitamin C 0.1%~0.4%, glycerol 0.3%~1.0%, remaining is deionized water.Water-based paint prepared by the present invention has heat-clearing inflammation relieving, swelling and pain relieving, antibacterial bacteriostatic, dispels oral peculiar smell and other effects, and preparation method is simple, and the technological process of production is easy to operate, is suitble to large-scale promotion.
Description
Technical field
The invention belongs to filed of daily-use chemical industry more particularly to a kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract.
Background technique
Toothpaste is dental care products necessary to daily life, and major function is cleaning oral cavity, usually by rubbing agent, moisturizing
Agent, surfactant, thickener, sweetener, preservative, active additive and pigment, essence etc. mix.With people
Oral health consciousness continuous enhancing, people propose more requirements, various drug teeth with health care function to toothpaste
Cream is used and is given birth to.Although traditional Chinese herbal toothpaste has certain inhibition oral cavity harmful bacteria, pure and fresh oral cavity, takes care of one's teeth
Function, taking care of one's teeth, the effect is unsatisfactory, although the medicated toothpaste effect after addition chemicals is significantly improved, but
It will cause certain influence to human health.Currently, also being compared using application of the natural plant extracts in terms of oral health
It is less.
Mung bean is the most common beans species, not only has good edible value, also has extraordinary medical value, tool
Have sweet in flavor, cold in nature, has the characteristics that clearing heat and detoxicating, antibacterial bacteriostatic, certain ingredients in mung bean directly have bacteriostasis.Pass through suppression
Bacterium test confirms that testa mungo extracting solution has inhibiting effect to staphylococcus.According to related research, tannin contained by mung bean can solidify
Microorganism plasm, can produce antibacterial activity.The bioactive substances such as flavone compound, phytosterol in mung bean may
There is a degree of inhibitory anti-virus to act on.
Chinese patent CN102727407A discloses a kind of health-care toothpaste containing pepper extract, in the health-care toothpaste
The pepper extract for being 0.1-3.5% containing mass fraction, the pepper extract are to be no less than 30% containing mass fraction
The extract of pepper volatile oil；Toothpaste additive is composed of the following components in parts by mass: 0.1-3.5 parts of pepper extract, fourth
Fragrant phenol 0.1-2.5 parts；The pepper extract and eugenol of antibacterial and analgesic activity have been used in pepper Healthy toothpaste of the present invention,
There is no the pure natural antibacterial agent of any toxic side effect to human body, safety is significantly better than synthetic antibacterial agents.But the health care of the invention
It is added with sldium lauryl sulfate and saccharin sodium in toothpaste, adverse effect may be caused to human body, and antibacterial bacteriostatic effect is bad.
Chinese patent CN105001722A discloses a kind of toothpaste and preparation method thereof containing Notogineng Extract, the invention
The every 1ml for being 0.07%~1.2% with total weight percent in toothpaste is equivalent to the Radix Notoginseng liquid extract of 0.8~2g of raw medicine object；
It is other composition by rubbing agent 30%~55%, wetting agent 15%~30%, adhesive 0.6%~1.5%, foaming agent 2%~
2.7%, remaining is deionized water and a small amount of essence.The preparation method of toothpaste is that Radix Notoginseng liquid extract, wetting agent are put into deionization
Deionized water solution made of stirring in water is mixed with rubbing agent, adhesive, foaming agent, is stirred, simultaneously vacuum outgas of milling；It is added
Essence, stirs, mills and vacuum outgas, acquisition lotion of toothpaste, the toothpaste of invention preparation also have prevention and treatment periodontal in addition to cleaning the teeth
The efficacy of drugs such as scorching, gingivitis and bleeding gums, canker sore, but its antibacterial and bacteriostasis is bad.
Summary of the invention
The purpose of the present invention is to overcome the shortcomings of the existing technology, provides a kind of toothpaste containing Semen phaseoli radiati extract, this is answered
New approaches are provided with the preparation for toothpaste, the toothpaste of preparation has antibacterial bacteriostatic, clearing heat and detoxicating, swelling and pain relieving, refreshes the mind
The characteristics of；Another object of the present invention is to provide a kind of preparation method of environment-friendly water-soluble anti-corrosion of metal paint, this method
With easy to operate, preparation convenience, characteristic at low cost, it is suitable for industrialization large-scale production.
To realize the purpose, the technical scheme adopted by the invention is as follows: a kind of toothpaste containing Semen phaseoli radiati extract contains always
The Semen phaseoli radiati extract that weight percent is 0.1%~3.2%, the Semen phaseoli radiati extract are mung bean chromocor extract, the mung bean
The general flavone for being 30%~50% containing weight percent in chromocor extract.
Further, the toothpaste containing Semen phaseoli radiati extract includes following components by its weight percent: mung bean extracts
Object 0.1%~3.2%, nanometer calcium carbonate 40%~50%, honeysuckle 8%~12%, TianXing grass 3%~7%, silica
1%~5%, propylene glycol 3%~10%, laruyl alcohol sodium sulfovinate 1%-3%, xanthan gum 0.5%~1%, cellulose gum 1%~
2%, sorbierite 1~4%, peppermint oil 1%~2%, vitamin C 0.1%~0.4%, glycerol 0.3%~1.0%, remaining is to go
Ionized water；
Further, the toothpaste containing Semen phaseoli radiati extract includes following components by its weight percent: mung bean extracts
Object 1.0%~2.1%, nanometer calcium carbonate 42%~47%, honeysuckle 9%~10%, TianXing grass 4%~6%, silica
2%~4%, propylene glycol 5%~8%, laruyl alcohol sodium sulfovinate 1.5%-2.5%, xanthan gum 0.7%~0.9%, cellulose gum
1.3%~1.8%, sorbierite 2~3%, peppermint oil 1.2%~1.6%, vitamin C 0.2%~0.3%, glycerol 0.5%~
0.8%, remaining is deionized water；
Further, the toothpaste containing Semen phaseoli radiati extract includes following components by its weight percent: mung bean mentions
Take object 1.6%, nanometer calcium carbonate 45%, honeysuckle 10%, TianXing grass 5%, silica 3%, propylene glycol 7%, laruyl alcohol sulphur
Acid esters sodium 2%, xanthan gum 0.8%, cellulose gum 1.5%, sorbierite 3%, peppermint oil 1.4%, vitamin C 0.25%, glycerol
0.7%, remaining is deionized water.
Further, the preparation step of the Semen phaseoli radiati extract are as follows:
Step S10, takes Green Gram Seed, and 5~8 times of water is added by its weight, and squeezing keeps it heavy at juice, squeezeding juice standing
It forms sediment, the first filtrate and filter residue is obtained by filtration；
Filter residue ethyl alcohol is extracted twice, filtrate is stood and the second filtrate is obtained by filtration by step S20；
Wherein, mung bean is first squeezed into juice and carries out ethyl alcohol extraction to it again by above-mentioned steps, is improved extraction efficiency, is reduced
The machine cost of subsequent concentration.
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 50~80:1, dry, obtains mung bean general flavone and mentions
Take object；
Further, the method that the ethyl alcohol extracts is to add 3~6 times of ethyl alcohol to extract twice by its weight, every time 1.5
Hour, Extracting temperature is 40~60 DEG C.
Wherein, above-mentioned Semen phaseoli radiati extract only uses water and ethyl alcohol as Extraction solvent, does not introduce toxic organic solvents, obtains
Contain extractive of general flavone in Semen phaseoli radiati extract, have the function of antibacterial bacteriostatic, in addition may also contain other tannin energy contained
Microorganism plasm is solidified, can produce antibacterial activity, makes the antibacterial action enhancing of toothpaste obtained.
The present invention contains the preparation method of the toothpaste of Semen phaseoli radiati extract, and steps are as follows:
Step S10, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, is obtained
First mixture；
Step S20 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture, add by step S30
Thermal agitation mixes 3~8 minutes, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S40, and Semen phaseoli radiati extract, gold and silver is added
Colored and TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste；
Wherein, traditional Chinese medicine ingredients honeysuckle and TianXing grass are added in toothpaste, the swelling and pain relieving of toothpaste can be improved in honeysuckle
Effect, TianXing grass have wind and heat eliminating, and the effect of analgesic, the two, which is mixed addition, can greatly promote honeysuckle swelling and pain relieving
Effect improves the health-care effect of toothpaste.
Further, heating temperature is 50~65 DEG C in the step S30；
Further, it in the step S40, is added before honeysuckle and TianXing grass, is crushed into powder after first drying the two,
150 meshes are crossed, the mixing fine powders of honeysuckle and TianXing grass are obtained.
Beneficial effects of the present invention:
1. Semen phaseoli radiati extract prepared by the present invention has effects that clearing heat and detoxicating, antibacterial bacteriostatic, refreshes the mind, can also have
Effect alleviates the symptoms such as oral peculiar smell；
2. the toothpaste prepared by the present invention containing Semen phaseoli radiati extract has heat-clearing inflammation relieving, resists because being added with Semen phaseoli radiati extract
Bacterium is antibacterial, dispels oral peculiar smell and other effects, also added with honeysuckle and TianXing grass, improves the effect of its swelling and pain relieving, special needle
To because the gum caused by reasons such as get angry is red and swollen, toothache symptom, effect of releiving is obvious；
3. in the toothpaste of the invention containing Semen phaseoli radiati extract, the extraction process unharmful substance of Semen phaseoli radiati extract has day
So feature of health；The preparation method of toothpaste is easy, and low manufacture cost works well, and is suitble to large-scale promotion production.
Other than objects, features and advantages described above, there are also other objects, features and advantages by the present invention.
Below with reference to specific embodiment, the present invention is described in further detail.
Specific embodiment
The present invention is described in detail with reference to embodiments, but the present invention can be defined by the claims and cover
Multitude of different ways implement.
Embodiment 1
A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract
Raw material of toothpaste composition containing Semen phaseoli radiati extract:
Semen phaseoli radiati extract 1.6g, nanometer calcium carbonate 45g, honeysuckle 10g, TianXing grass 5g, silica 3g, propylene glycol 7g,
It is laruyl alcohol sodium sulfovinate 2g, xanthan gum 0.8g, cellulose gum 1.5g, sorbierite 3g, peppermint oil 1.4g, vitamin C 0.25g, sweet
Oily 0.7g, deionized water 18.75g；
The preparation step of the Semen phaseoli radiati extract are as follows:
Step S10, takes Green Gram Seed, and 7 times of water is added by its weight, and squeezing makes its precipitating, mistake at juice, squeezeding juice standing
Filter obtains the first filtrate and filter residue；
Filter residue is added 4 times of ethyl alcohol to extract twice by step S20 by its weight, and 1.5 hours every time, Extracting temperature was 50 DEG C,
Filtrate is stood and the second filtrate is obtained by filtration；
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 65:1, dry, obtains the extraction of mung bean general flavone
Object, the general flavone for being 50% containing weight percent in the Semen phaseoli radiati extract.
Wherein, above-mentioned Semen phaseoli radiati extract only uses water and ethyl alcohol as Extraction solvent, does not introduce toxic organic solvents, obtains
Contain extractive of general flavone in Semen phaseoli radiati extract, have the function of antibacterial bacteriostatic, in addition may also contain other tannin energy contained
Microorganism plasm is solidified, can produce antibacterial activity, makes the antibacterial action enhancing of toothpaste obtained.
The toothpaste containing Semen phaseoli radiati extract is prepared via a method which:
Step S10 is crushed into powder after drying honeysuckle and TianXing grass, cross 150 meshes, obtain honeysuckle and TianXing grass
Mixing fine powders；
Step S20, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, is obtained
First mixture；
Step S30 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture, add by step S40
Thermal agitation mixes 5 minutes, and heating temperature is 58 DEG C, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S50, and Semen phaseoli radiati extract, gold and silver is added
Colored and TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste.
Embodiment 2
A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract
Raw material of toothpaste composition containing Semen phaseoli radiati extract:
Semen phaseoli radiati extract 2.1g, nanometer calcium carbonate 50g, honeysuckle 8g, TianXing grass 6g, silica 2g, propylene glycol 8g, the moon
Cinnamic alcohol sodium sulfovinate 3g, xanthan gum 1.0g, cellulose gum 1.3g, sorbierite 2g, peppermint oil 2g, vitamin C 0.1g, glycerol
0.5g, deionized water 14g；
The preparation step of the Semen phaseoli radiati extract are as follows:
Step S10, takes Green Gram Seed, and 5 times of water is added by its weight, and squeezing makes its precipitating, mistake at juice, squeezeding juice standing
Filter obtains the first filtrate and filter residue；
Filter residue is added 6 times of ethyl alcohol to extract twice by step S20 by its weight, and 1.5 hours every time, Extracting temperature was 60 DEG C,
Filtrate is stood and the second filtrate is obtained by filtration；
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 80:1, dry, obtains the extraction of mung bean general flavone
Object, the general flavone for being 60% containing weight percent in the Semen phaseoli radiati extract.
Wherein, above-mentioned Semen phaseoli radiati extract only uses water and ethyl alcohol as Extraction solvent, does not introduce toxic organic solvents, obtains
Contain extractive of general flavone in Semen phaseoli radiati extract, have the function of antibacterial bacteriostatic, in addition may also contain other tannin energy contained
Microorganism plasm is solidified, can produce antibacterial activity, makes the antibacterial action enhancing of toothpaste obtained.
The toothpaste containing Semen phaseoli radiati extract is prepared via a method which:
Step S10 is crushed into powder after drying honeysuckle and TianXing grass, cross 150 meshes, obtain honeysuckle and TianXing grass
Mixing fine powders；
Step S20, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, is obtained
First mixture；
Step S30 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture, add by step S40
Thermal agitation mixes 8 minutes, and heating temperature is 65 DEG C, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S50, and Semen phaseoli radiati extract, gold and silver is added
Colored and TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste.
Embodiment 3
A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract
Raw material of toothpaste composition containing Semen phaseoli radiati extract:
Semen phaseoli radiati extract 3.2g, nanometer calcium carbonate 40g, honeysuckle 12g, TianXing grass 7g, silica 5g, propylene glycol 10g,
Laruyl alcohol sodium sulfovinate 1g, xanthan gum 0.7g, cellulose gum 2.0g, sorbierite 1g, peppermint oil 1.6g, vitamin C 0.4g, glycerol
1.0g, deionized water 15.1g；The preparation step of the Semen phaseoli radiati extract are as follows:
Step S10, takes Green Gram Seed, and 8 times of water is added by its weight, and squeezing makes its precipitating, mistake at juice, squeezeding juice standing
Filter obtains the first filtrate and filter residue；
Filter residue is added 3 times of ethyl alcohol to extract twice by step S20 by its weight, and 1.5 hours every time, Extracting temperature was 60 DEG C,
Filtrate is stood and the second filtrate is obtained by filtration；
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 50:1, dry, obtains the extraction of mung bean general flavone
Object, the general flavone for being 40% containing weight percent in the Semen phaseoli radiati extract.
Wherein, above-mentioned Semen phaseoli radiati extract only uses water and ethyl alcohol as Extraction solvent, does not introduce toxic organic solvents, obtains
Contain extractive of general flavone in Semen phaseoli radiati extract, have the function of antibacterial bacteriostatic, in addition may also contain other tannin energy contained
Microorganism plasm is solidified, can produce antibacterial activity, makes the antibacterial action enhancing of toothpaste obtained.
The toothpaste containing Semen phaseoli radiati extract is prepared via a method which:
Step S10 is crushed into powder after drying honeysuckle and TianXing grass, cross 150 meshes, obtain honeysuckle and TianXing grass
Mixing fine powders；
Step S20, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, is obtained
First mixture；
Step S30 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture, add by step S40
Thermal agitation mixes 6 minutes, and heating temperature is 50 DEG C, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S50, and Semen phaseoli radiati extract, gold and silver is added
Colored and TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste.
Embodiment 4
A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract
Raw material of toothpaste composition containing Semen phaseoli radiati extract:
Semen phaseoli radiati extract 1.0g, nanometer calcium carbonate 42g, honeysuckle 9g, TianXing grass 3g, silica 1 g, propylene glycol 3g, the moon
Cinnamic alcohol sodium sulfovinate 1.5g, xanthan gum 0.8g, cellulose gum 1.8g, sorbierite 3g, peppermint oil 1.2g, vitamin C 0.3g, glycerol
0.3g, deionized water 15.1g；
The preparation step of the Semen phaseoli radiati extract are as follows:
Step S10, takes Green Gram Seed, and 6 times of water is added by its weight, and squeezing makes its precipitating, mistake at juice, squeezeding juice standing
Filter obtains the first filtrate and filter residue；
Filter residue is added 5 times of ethyl alcohol to extract twice by step S20 by its weight, and 1.5 hours every time, Extracting temperature was 70 DEG C,
Filtrate is stood and the second filtrate is obtained by filtration；
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 70:1, dry, obtains the extraction of mung bean general flavone
Object, the general flavone for being 55% containing weight percent in the Semen phaseoli radiati extract.
Wherein, above-mentioned Semen phaseoli radiati extract only uses water and ethyl alcohol as Extraction solvent, does not introduce toxic organic solvents, obtains
Contain extractive of general flavone in Semen phaseoli radiati extract, have the function of antibacterial bacteriostatic, in addition may also contain other tannin energy contained
Microorganism plasm is solidified, can produce antibacterial activity, makes the antibacterial action enhancing of toothpaste obtained.
The toothpaste containing Semen phaseoli radiati extract is prepared via a method which:
Step S10 is crushed into powder after drying honeysuckle and TianXing grass, cross 150 meshes, obtain honeysuckle and TianXing grass
Mixing fine powders；
Step S20, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, is obtained
First mixture；
Step S30 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture, add by step S40
Thermal agitation mixes 7 minutes, and heating temperature is 55 DEG C, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S50, and Semen phaseoli radiati extract, gold and silver is added
Colored and TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste.
Embodiment 5
A kind of toothpaste and preparation method thereof containing Semen phaseoli radiati extract
Raw material of toothpaste composition containing Semen phaseoli radiati extract:
Semen phaseoli radiati extract 0.1g, nanometer calcium carbonate 47g, honeysuckle 12g, TianXing grass 4g, silica 4g, propylene glycol 5g,
It is laruyl alcohol sodium sulfovinate 2.5g, xanthan gum 0.5g, cellulose gum 1.0g, sorbierite 4g, peppermint oil 1.0g, vitamin C 0.2g, sweet
Oily 0.8g, deionized water 17.9g；
The preparation step of the Semen phaseoli radiati extract are as follows:
Step S10, takes Green Gram Seed, and 6 times of water is added by its weight, and squeezing makes its precipitating, mistake at juice, squeezeding juice standing
Filter obtains the first filtrate and filter residue；
Filter residue is added 6 times of ethyl alcohol to extract twice by step S20 by its weight, and 1.5 hours every time, Extracting temperature was 50 DEG C,
Filtrate is stood and the second filtrate is obtained by filtration；
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 85:1, dry, obtains the extraction of mung bean general flavone
Object, the general flavone for being 62% containing weight percent in the Semen phaseoli radiati extract.
Wherein, above-mentioned Semen phaseoli radiati extract only uses water and ethyl alcohol as Extraction solvent, does not introduce toxic organic solvents, obtains
Contain extractive of general flavone in Semen phaseoli radiati extract, have the function of antibacterial bacteriostatic, in addition may also contain other tannin energy contained
Microorganism plasm is solidified, can produce antibacterial activity, makes the antibacterial action enhancing of toothpaste obtained.
The toothpaste containing Semen phaseoli radiati extract is prepared via a method which:
Step S10 is crushed into powder after drying honeysuckle and TianXing grass, cross 150 meshes, obtain honeysuckle and TianXing grass
Mixing fine powders；
Step S20, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, is obtained
First mixture；
Step S30 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture, add by step S40
Thermal agitation mixes 10 minutes, and heating temperature is 45 DEG C, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S50, and Semen phaseoli radiati extract, gold and silver is added
Colored and TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste.
Experimental example
1. subjects
It chooses 100 subjects to test, selection criteria is chosen by the diagnostic criteria that medical treatment is routinely assert, subject year
Age at 20~55 years old, male to female ratio 1:1.
2. application method
Subject is divided into 5 groups, every group includes 10 males, and 10 women contain mung bean with prepared by Examples 1 to 5
The toothpaste of extract is daily sooner or later respectively using primary, 3~4 minutes every time, during use, is not added with other medicines, altogether using 7~
15 days.
3. test result
Test criterion of therapeutical effect is divided into three kinds, and a, effect are obvious: symptom disappears；B, effectively: symptom improves；C, invalid: without bright
Effective fruit.Efficacy result is shown in Table 1.
The test result of toothpaste of the table 1. containing Semen phaseoli radiati extract
Test result shows the toothpaste containing Semen phaseoli radiati extract of the preparation of the embodiment of the present invention 1~5 for gum redness
Effective percentage is greater than 85%, is greater than 65% to the effective percentage of oral peculiar smell, it is seen that the remission of gum redness is acted on obviously, but
General to the therapeutic effect of oral peculiar smell, this is primarily due to oral peculiar smell and is not only to be generated by breeding bacterium in oral cavity, also
Some patientss are since gastrointestinal system disorder causes.It can thus be seen that the toothpaste prepared by the present invention containing Semen phaseoli radiati extract
Have the effects that swelling and pain relieving, antibacterial bacteriostatic and remove oral peculiar smell, and preparation method is simple, the technological process of production is easily grasped
Make, is suitble to large-scale promotion.
The above is only a preferred embodiment of the present invention and experimental example, is not intended to restrict the invention, for this field
Technical staff for, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made
What modification, equivalent replacement, improvement etc., should be included within the protection scope of invention.
Claims (9)
1. a kind of toothpaste containing Semen phaseoli radiati extract, which is characterized in that the toothpaste containing Semen phaseoli radiati extract contains total weight
The Semen phaseoli radiati extract that percentage is 0.1%~3.2%, the Semen phaseoli radiati extract are mung bean chromocor extract, the mung bean flavones
The general flavone for being 30%~50% containing weight percent in extract.
2. the toothpaste according to claim 1 containing Semen phaseoli radiati extract, which is characterized in that described containing Semen phaseoli radiati extract
Toothpaste includes following components by its weight percent: Semen phaseoli radiati extract 0.1%~3.2%, nanometer calcium carbonate 40%~50%, gold
Honeysuckle flower 8%~12%, TianXing grass 3%~7%, silica 1 %~5%, propylene glycol 3%~10%, laruyl alcohol sodium sulfovinate
1%-3%, xanthan gum 0.5%~1%, cellulose gum 1%~2%, sorbierite 1~4%, peppermint oil 1%~2%, vitamin
C0.1%~0.4%, glycerol 0.3%~1.0%, remaining is deionized water.
3. the toothpaste according to claim 1 containing Semen phaseoli radiati extract, which is characterized in that described containing Semen phaseoli radiati extract
Toothpaste includes following components by its weight percent: Semen phaseoli radiati extract 1.0%~2.1%, nanometer calcium carbonate 42%~47%, gold
Honeysuckle flower 9%~10%, TianXing grass 4%~6%, silica 2%~4%, propylene glycol 5%~8%, laruyl alcohol sodium sulfovinate
1.5%-2.5%, xanthan gum 0.7%~0.9%, cellulose gum 1.3%~1.8%, sorbierite 2~3%, peppermint oil 1.2%
~1.6%, vitamin C 0.2%~0.3%, glycerol 0.5%~0.8%, remaining is deionized water.
4. the toothpaste according to claim 1 containing Semen phaseoli radiati extract, which is characterized in that described containing Semen phaseoli radiati extract
Toothpaste includes following components by its weight percent: Semen phaseoli radiati extract 1.6%, nanometer calcium carbonate 45%, honeysuckle 10%, TianXing
Careless 5%, silica 3%, propylene glycol 7%, laruyl alcohol sodium sulfovinate 2%, xanthan gum 0.8%, cellulose gum 1.5%, sorb
Alcohol 3%, peppermint oil 1.4%, vitamin C 0.25%, glycerol 0.7%, remaining is deionized water.
5. the toothpaste according to claim 1 containing Semen phaseoli radiati extract, which is characterized in that the preparation of the Semen phaseoli radiati extract
Step are as follows:
Step S10, takes Green Gram Seed, and 5~8 times of water is added by its weight, and squeezing makes its precipitating, mistake at juice, squeezeding juice standing
Filter obtains the first filtrate and filter residue；
Filter residue ethyl alcohol is extracted twice, filtrate is stood and the second filtrate is obtained by filtration by step S20；
Second filtrate and the first filtrate are stirred 2 hours by step S30, obtain total filtrate after recycling ethyl alcohol；
Step S40, filtrate is decolourized, and is concentrated by volume for 50~80:1, dry, obtains the extraction of mung bean general flavone
Object.
6. the preparation method of Semen phaseoli radiati extract according to claim 5, which is characterized in that the method that the ethyl alcohol extracts
To add 3~6 times of ethyl alcohol to extract twice by its weight, 1.5 hours every time, Extracting temperature was 40~60 DEG C.
7. a kind of preparation method of the toothpaste as described in Claims 1 to 4 containing Semen phaseoli radiati extract, which is characterized in that containing green
The specific preparation step of the toothpaste of beans extract are as follows:
Step S10, nanometer calcium carbonate is dissolved in deionized water, and laruyl alcohol sodium sulfovinate is added while stirring, obtains first
Mixture；
Step S20 stirs evenly peppermint oil, sorbierite and mixed with propylene glycol, obtains the second mixture；
Silica, xanthan gum, cellulose gum and vitamin C are added sequentially in the first mixture by step S30, and heating is stirred
It mixes mixing 3~8 minutes, obtains third mixture；
Second mixture and third mixture are added in emulsion pot by step S40, and be added Semen phaseoli radiati extract, honeysuckle and
TianXing grass, ground and mixed, and vacuum outgas, obtain lotion of toothpaste.
8. preparation method according to claim 7, which is characterized in that heating temperature is 50~65 DEG C in the step S30.
9. preparation method according to claim 7, which is characterized in that in the step S40, honeysuckle and TianXing grass is added
Before, it is crushed into powder after first drying the two, crosses 150 meshes, obtain the mixing fine powders of honeysuckle and TianXing grass.
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Citations (3)
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| CN101879208A (en) * | 2010-04-27 | 2010-11-10 | 南京泽朗农业发展有限公司 | Method for extracting total flavonoids from mung bean shell |
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| CN101879208A (en) * | 2010-04-27 | 2010-11-10 | 南京泽朗农业发展有限公司 | Method for extracting total flavonoids from mung bean shell |
| KR101192161B1 (en) * | 2010-06-21 | 2012-10-17 | (주)에이씨티 | Cosmetic composition containing stabilized retinol in the mesoporous polymer bead and the nano emulsion |
| CN102895147A (en) * | 2012-09-25 | 2013-01-30 | 广州中汉口腔用品有限公司 | Toothpaste with anti-inflammation and anti-allergic effects and making technology thereof |
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