CN109490241A - Quick dynamic Terahertz near field imaging system and its construction method based on photoconductive antenna array - Google Patents

Quick dynamic Terahertz near field imaging system and its construction method based on photoconductive antenna array Download PDF

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CN109490241A
CN109490241A CN201811495130.1A CN201811495130A CN109490241A CN 109490241 A CN109490241 A CN 109490241A CN 201811495130 A CN201811495130 A CN 201811495130A CN 109490241 A CN109490241 A CN 109490241A
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terahertz
antenna array
photoconductive antenna
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CN109490241B (en
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李璟文
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Jiangnan University
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    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3581Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using far infrared light; using Terahertz radiation

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Abstract

The invention discloses quick dynamic Terahertz near field imaging systems and its construction method based on photoconductive antenna array, the described method comprises the following steps: the micro Process of the design of probe unit structure, photoconductive antenna array that prepare optimization manufactures, realization carries out gate excitation to detection array using spatial light modulator and builds pulsed terahertz imaging system.Compared with prior art, the invention has the following advantages that (1) quick dynamic Terahertz near field imaging system of the present invention based on photoconductive antenna array realizes the photoconductive antenna array that THz wave efficiently detects, resolution ratio is better than λ/10, and unit signal-to-noise ratio is better than 70dB;(2) system carries out gate excitation to photoconductive antenna array using spatial light modulator, and combines multichannel phase lock amplifying technology, realizes a kind of dynamic, flexible, efficient, quick collecting method.

Description

Quick dynamic Terahertz near field imaging system and its structure based on photoconductive antenna array Construction method
Technical field
The invention belongs to THz imaging technologies, are related to a kind of terahertz imaging system, are specially based on photoconductive antenna The quick dynamic Terahertz near field imaging system and its construction method of array.
Background technique
THz imaging technology is grown up on the basis of time-domain spectroscopy system.Typical terahertz imaging Sample is usually placed in Terahertz system by system, by utilizing two-dimensional scanning platform mobile example or single point detector, To note down the transmission or reflection information of sample different location.Terahertz time-domain waveform is extracted to each pixel of sample, Sample image is rebuild by data processing.Since Hu et al. is for the first time using transmission-type Terahertz point by point scanning imaging technique to chip Since internal structure and leaf water content are imaged, THz imaging technology causes the extensive concern of people and obtains It rapidly develops.Since this method can be by phase lock amplifying technology noise reduction, high s/n ratio imaging may be implemented, and (signal-to-noise ratio reaches To 104Or higher).However, since traditional Terahertz single-point imaging system generallys use the measurement method of point-by-point mechanical scanning, Sweep time is long, and acquisition speed is slow.Imaging time depends on sample size and scanning step.Our research works in early period It finds in work, when one target having a size of 8mm × 8mm is imaged using the single point detector based on the method, needs Time-consuming 10h or more (scanning step: 250 μm).Therefore, this method is unfavorable for carrying out object to be measured dynamic measurement or in real time prison Control.In addition, during the scanning process, the power swing or sample to be tested physical state or chemistry of laser source and THz source are special The variation of property, can all influence imaging results, this undoubtedly limits the imaging mode in the application in the fields such as industry monitoring.
Imaging technique based on compression sensing (Compressive sensing) can significantly improve the figure of single point detector As acquiring speed, and signal-to-noise ratio with higher.Using the theory, can by algorithm by a sparse picture signal from It is rebuild in the measurement result of height lack sampling.Therefore, it can be rebuild from a small amount of measured value much smaller than the total pixel of image Original image, significantly shortening imaging time.Single pixel camera based on the theory most early in visible light wave range propose, and then in It is expanded by Chan to terahertz wave band within 2008.The system generally carries out sparse adopt to target image using multiple random mask plates Sample, and sampled value is measured using single point detector, target image is rebuild using algorithm later.Initially, the sparse sampling of sample by Several groups metal mask plate before being applied to sample is realized, but requires manual switching mask plate due to measuring every time, time-consuming to take Power.In recent years, this method receives very big concern, researcher propose it is a variety of can switching at runtime mask plate realization side Formula, such as the spatial light modulator based on Meta Materials and the light-operated Terahertz amplitude modulator of silicon substrate, have greatly pushed the field Further development.
Another mode that can significantly improve terahertz imaging speed is using array Detection Techniques.It is relatively common Be the sampling technique based on electrooptic effect and the Detection Techniques based on photoconductive antenna.Wherein, electro optic sampling technology is using electricity Luminescent crystal (such as ZnTe) and area array CCD camera are as detection device.This method is not necessarily to carry out two-dimensional scanning energy directly to sample The shortcomings that extracting entire sample two-dimensional signal, therefore single point detector point by point scanning can be overcome to take long time, significantly improves Image taking speed, and sample can be monitored in real time.However, in practical applications, since system passes through CCD to Terahertz figure As information is acquired, lock-in amplifier noise reduction can not be utilized, therefore the signal-to-noise ratio of system is received and greatly limited, this is also hindered Its further industrial development is hindered.
The imaging technique of array based on photoconductive antenna can use phase lock amplifying technology and obtain high s/n ratio, while can To realize fast imaging.It is typically achieved in that and multiple photoconductive antenna units is integrated in same semiconductor core on piece, lead to Cross by femto-second laser pulse focus to antenna element gap it is carried out high speed gate excitation (Optical gating), Ke Yishi Existing Sample Scan imaging.Herrmann et al. succeeded in developing 8 channel terahertz imaging arrays in 2002 for the first time.In the system In, in order to realize the gate excitation to array element, the femtosecond laser source after expanding is focused to entire aerial array area by author Domain, only about 5% laser energy are efficiently used by array element gap, and extra laser energy causes high background and makes an uproar Sound, therefore limit it and further develop.Then, Pradarutti et al. proposes to carry out femtosecond laser using microlens array Then beam splitting and the electrode gap for focusing to each antenna element respectively are come using multichannel phase lock-in detecting technology while reading 16 The data in a channel.System signal-to-noise ratio with higher (suitable with individual antenna).However, since microlens array prepares work Skill is complicated, and with aerial array alignment difficulties, spatial resolution is restricted to~500 μm.
Further, since THz wave wavelength is longer, limited by diffraction effect, point of traditional far field terahertz imaging system Resolution is its wavelength magnitude, constrains the application of THz imaging technology to a certain extent.Therefore, develop near field detection imaging Technology is particularly important for obtaining higher imaging resolution.Report relatively common at present has based on probe-type, aperture The Near-Field Radar Imaging means of method and high order focusing light beam.
The processing of photoconductive antenna array is one of key technology of terahertz imaging.Terahertz photoconductive antenna most earlier than It is proposed by Auston and Grischkowsky et al. the eighties in last century, and goes so far as now, having become one kind at present Commonplace terahertz sources, detection means.THz wave transmitting and detection based on this means are required to swash by femtosecond It rises to realize.For different femtosecond excitation source categories and its operation wavelength (such as 800nm, 1550nm and 1030nm), lining Bottom material and micro fabrication are different.Under normal circumstances, photoconductive antenna may act as terahertz transmitter, while It can be used as receiver.But the working efficiency to be optimal, different operating modes to the selection of antenna material characteristic and Processing technology has different requirements.For example, terahertz transmitter generally requires base material with high electron mobility, and terahertz Hereby receiver generally requires extremely short carrier lifetime and high resistivity.Current terahertz time-domain system generallys use near-infrared Titanium sapphire laser device as laser source.For the operation wavelength (800nm), relatively common base material has radiation injury Silicon on sapphire or low-temperature epitaxy GaAs.Compared with silicon on sapphire, the GaAs material of low-temperature epitaxy has shorter load It flows the sub- service life, broader frequency and higher signal strength, therefore, is more advantageous to and carries out THz wave detection.To being at present Only, researcher has conducted extensive research the photoconductive antenna of different structure, such as dipole-type (Dipole), bow-tie type (Bowtie), screw type (Spiral antenna) etc..However, due to lacking a kind of flexible, efficient, quick array gate Mode of excitation, the most structure designs for being confined to single-point type antenna element of current research report (and photoconductive antenna of business) And performance study.
Summary of the invention
The technical issues of solution: it for overcome the deficiencies in the prior art, obtains a kind of with high-resolution, high s/n ratio Photoconductive exploring antenna array, and explore its array dynamic optical gate excitation technique based on spatial light modulator;Pass through Using multichannel lock-in amplifier parallel acquisition data, high s/n ratio, quick Terahertz Near-Field Radar Imaging are realized, the present invention provides Quick dynamic Terahertz near field imaging system and its construction method based on photoconductive antenna array.
Technical solution: the construction method of the quick dynamic Terahertz near field imaging system based on photoconductive antenna array, institute State method the following steps are included:
Step 1, the probe unit structure design of preparation optimization
Research and analyse photoconductive antenna substrate material properties, different antennae structure and size and excitation laser pulse characteristic Influence to terahertz detection performance, and is carried out by numerical simulation and is tested for it using Finite-Difference Time-Domain Method and electromagnetic simulation software Card;
The micro Process manufacture of step 2, photoconductive antenna array
According to excitation optical source wavelength and the operating mode of antenna element, selects antenna material or determine its production technology, obtain There must be the semiconductor material of short carrier lifetime and high resistivity characteristic;In addition, selection antenna electrode material or its determining life Production. art forms good Ohmic contact with base material;Finally, utilizing photoetching, the method patterned metal electrode of etching;
Step 3, realization carry out gate excitation to detection array using spatial light modulator
According to system requirements, selective transmission formula or reflection type liquid crystal spatial light modulator, and research and utilization its carry out photoelectricity Lead antenna array efficiently gates the feasibility of excitation: expanding first to femtosecond pulse, then utilizes space light modulation Device is split incident beam, modulates, and finally focuses to probe unit gap respectively;Under the influence of control signals, right Detection array carries out simultaneously, partially or successively sequentially gate excitation;The number of research and utilization low noise amplifier and lock-in amplifier According to acquisition technique, it is ready for subsequent realization terahertz imaging;
Step 4 builds pulsed terahertz imaging system
Use titanium sapphire mode locking femto-second laser for excitaton source, and be classified as pumping pulse and detection using beam splitter Pulse, the former is incident on terahertz emission generation device after time delay system and generates terahertz pulse, the pulse by Sample to be tested is focused to after a pair of of parabolic mirror, the latter divides it after optical beam-expanding, by spatial light modulator Beam, modulation simultaneously focus to photoconductive antenna cell gap respectively, so that Terahertz antenna array unit be driven to measure;Benefit Data acquisition is realized with low noise preamplifier and multichannel lock-in amplifier, and pumping is adjusted by control time delay system Time delay between pulse and direct impulse detects the entire time domain waveform of terahertz pulse, by data processing, rebuild to Sample terahertz image.
Preferably, antenna described in step 1 is dipole antenna, and structure is I shape or H-shaped.
Preferably, in step 2 antenna material select low-temperature epitaxy GaAs;Base material selects semi-insulated arsenic Gallium, for the gallium arsenide film layer of 1 μ m-thick of 200-300 DEG C of growth.
Preferably, the spacing range between detection array and sample is 500um-3mm.
The quick dynamic Terahertz near field imaging system based on photoconductive antenna array that the building of any of the above method obtains.
The utility model has the advantages that (1) quick dynamic Terahertz near field imaging system of the present invention based on photoconductive antenna array Realize the photoconductive antenna array that THz wave efficiently detects, resolution ratio is better than λ/10, and unit signal-to-noise ratio is better than 70dB;(2) institute It states system and gate excitation is carried out to photoconductive antenna array using spatial light modulator, and combine multichannel phase lock amplifying technology, Realize a kind of dynamic, flexible, efficient, quick collecting method;(3) system can be further realized based on Sparse Array The quick terahertz imaging of column and compressive sensing theory.It, can be by algorithm by a sparse picture signal using the theory It is rebuild from the measurement result of height lack sampling, it can rebuild original from a small amount of measured value much smaller than the total pixel of image Beginning image, significantly shortening imaging time.The system passes through simultaneous shot and acquires in photoconductive antenna array specific position too Hertz imaging unit, then rebuilds target image using algorithm, to realize high speed terahertz imaging.
Detailed description of the invention
Fig. 1 is the quick dynamic Terahertz near field imaging system construction method of the present invention based on photoconductive antenna array Technology Roadmap;
Fig. 2 is photoconductive antenna unit design drawing, and (a) is H-shaped dipole antenna, is (b) I shape dipole antenna, (c) is Simplified antenna element processing technology schematic diagram;Wherein, L is dipole length, g is gap, w is electrode width (L=80um, g =5um, w=20um), D is electrode width, and l is that gap p is electrode pad size;
Fig. 3 is the photoconductive antenna array gate schematic diagram based on transmissive spatial optical modulator;
Fig. 4 is Terahertz near field imaging system schematic diagram.
Specific embodiment
Following embodiment further illustrates the contents of the present invention, but should not be construed as limiting the invention.Without departing substantially from In the case where spirit of that invention and essence, to modification made by the method for the present invention, step or condition and replaces, belong to the present invention Range.Unless otherwise specified, the conventional means that technological means used in embodiment is well known to those skilled in the art.
Embodiment 1
As shown in Figure 1, the construction method packet of the quick dynamic Terahertz near field imaging system based on photoconductive antenna array Include following steps:
The design of step 1, photoconductive antenna array
The detection performance (efficiency, bandwidth, resolution ratio, signal strength) of photoconductive antenna depend primarily on the following because Element: substrate material properties (such as carrier lifetime, dark resistivity, carrier mobility), antenna structure and size, and gate Laser characteristics (such as intensity, pulsewidth, focal position, spot size).Therefore, the selection of base material and its technique, day knot Structure, the design of size and the selection of operating mode are most important to the efficient terahertz detection of realization.
For the ease of realizing the array of photoconductive antenna and integrated, two different dipole antenna knots are mainly studied Structure, i.e. I shape and H-shaped, in Fig. 2 shown in (a) and (b).By studying its structure snd size (such as dipole length L, gap g, electricity Pole width w etc.) influence to Terahertz antenna detective bandwidth, efficiency and signal strength, realize the optimization design of electrode structure. The work mainly utilizes the Comsol for being based on Finite-Difference Time-Domain Method (Finite-difference time-domain, FDTD) Simulation softward and based on time-domain finite integration method electromagnetic simulation software (Computer simulation technology, CST it) completes.
The micro Process preparation of step 2, photoconductive antenna array
After completing The Optimal Design of Antenna Structure, photoconductive antenna array is prepared using micro-processing technology.Antenna material choosing With the GaAs of low-temperature epitaxy, which has shorter carrier lifetime and high resistivity under low temperature growth conditions, is to realize The ideal material of THz wave efficient detection.The technique is in molecular beam epitaxy (Molecular beam epitaxy, MBE) equipment Middle realization, substrate material select semi-insulated GaAs (Semi-insulating gallium arsenide, SI-GaAs), And the gallium arsenide film layer of about 1 μ m-thick is grown at cryogenic conditions (about 200-300 DEG C).Under cryogenic, it can grow non- The service life (subpicosecond magnitude) of carrier can be significantly reduced to form defect in stoichiometric compound.By adjusting annealing temperature Degree, optimizes the electrical resistivity property of GaAs material, to be conducive to the detection of THz wave.Finally metal is made in gallium arsenide surface Electrode.In order to form good Ohmic contact, Ti/Pt/Au electrode (50/100/ is sequentially depositing using electron beam evaporation process 200nm), finally, utilizing photoetching, the method patterned electrodes structure of etching.For the ease of subsequent device test lead, Wo Men Larger-size square pad is devised in electrode structure.The structure design of two kinds of antenna elements and its simplified processing flow As shown in Figure 2.
Step 3, the dynamic gate excitation technique research based on spatial light modulator
In order to realize fast imaging to sample to be tested using above-mentioned photoconductive antenna array, need to explore a kind of efficient battle array The gate excitation technique of column.The purpose is realized using German Holoeye LCD space light modulator.The modulator is a kind of dynamic State optical device is divided into transmission-type and two kinds reflective, and the two can meet project demand.Its working principle is that passing through utilization Applied voltage changes liquid crystal molecule and is directed toward, and controls its birefringent characteristic, to realize the modulation to incident light wave amplitude, phase. Spatial light modulator is made of many separate units (pixel), spatially lines up two-dimensional array structure, and each unit can be only It is vertical to receive electrical signal control.Therefore, which can be split incident excitation pulse, and carry out to its amplitude and phase It modulates respectively, finally focuses to probe unit gap respectively, and gate the unit.It under the influence of control signals, can be to spy Survey array carry out simultaneously, part or successively sequentially excite, to realize a kind of dynamic, flexible, efficient, quick imaging method. In Fig. 3, by taking transmission liquid crystal spatial light modulator as an example, its operating mode is illustrated.
Step 4 builds terahertz time-domain imaging system, completes the test of Terahertz Near-Field Radar Imaging
It uses Ti:Sapphire laser mode locking femto-second laser for excitation light source, builds terahertz imaging system, as shown in Figure 4.Femtosecond Laser pulse is divided into two-way coherent light: pumping pulse and direct impulse after beam splitter.The former passes through time delay system After be incident on terahertz transmitter and generate terahertz pulse, then by after a pair of of paraboloidal mirror through over-focusing to sample to be tested. To improve system signal noise ratio, the commercial high power photoconductive antenna of our uses of transmitter.Direct impulse is after expanding, by transmiting The photoconductive antenna array element gap for not adding bias voltage is modulated and is focused to respectively in the beam splitting of formula spatial light modulator, thus Excitation generates electronic-hole to (free carrier).At the same time, the terahertz pulse synchronously arrived at is used as and is added in antenna Bias field on unit, and carrier moving is driven, and photoelectric current is formed in antenna element.The signal passes through low noise electricity After stream amplifier amplification, it is phase locked amplifier acquisition.By using multichannel lock-in amplifier (Signal Recovery, Quick, high s/n ratio terahertz imaging may be implemented in 8Channel) parallel acquisition data.In addition, passing through research gate laser beam Intensity, facula position and size, photoproduction carrier concentration and spatial distribution in adjustable photoconduction base material, thus Further increase and optimize the detection efficient of photoconductive array.Finally, by the way that sample is abutted photoconductive antenna array, and optimize Cellular construction design, may be implemented Terahertz Near-Field Radar Imaging, to significantly provide its imaging resolution.Utilize three-dimensional mobile platform The spacing between detection array and sample is adjusted, influence of the different spacing to performances such as imaging resolutions can be studied, thus excellent Change imaging system.

Claims (5)

1. the construction method of the quick dynamic Terahertz near field imaging system based on photoconductive antenna array, which is characterized in that institute State method the following steps are included:
Step 1, the probe unit structure design of preparation optimization
Photoconductive antenna substrate material properties, different antennae structure and size and excitation laser pulse characteristic are researched and analysed to too The influence of hertz detection performance, and numerical simulation and verifying are carried out to it using Finite-Difference Time-Domain Method and electromagnetic simulation software;
The micro Process manufacture of step 2, photoconductive antenna array
According to excitation optical source wavelength and the operating mode of antenna element, selects antenna material or determine its production technology, had There is the semiconductor material of short carrier lifetime and high resistivity characteristic;In addition, selection antenna electrode material or determining its produce work Skill forms good Ohmic contact with base material;Finally, utilizing photoetching, the method patterned metal electrode of etching;
Step 3, realization carry out gate excitation to detection array using spatial light modulator
According to system requirements, selective transmission formula or reflection type liquid crystal spatial light modulator, and the photoconductive day of its progress of research and utilization Linear array efficiently gates the feasibility of excitation: expanding first to femtosecond pulse, then utilizes spatial light modulator pair Incident beam is split, modulates, and finally focuses to probe unit gap respectively;Under the influence of control signals, to detection Array carries out simultaneously, partially or successively sequentially gate excitation;The data of research and utilization low noise amplifier and lock-in amplifier are adopted Collection technology is ready for subsequent realization terahertz imaging;
Step 4 builds pulsed terahertz imaging system
It uses titanium sapphire mode locking femto-second laser for excitaton source, and is classified as pumping pulse and detection arteries and veins using beam splitter Punching, the former is incident on terahertz emission generation device after time delay system and generates terahertz pulse, and the pulse is by one To focusing to sample to be tested after parabolic mirror, the latter is split it after optical beam-expanding, by spatial light modulator, It modulates and focuses to photoconductive antenna cell gap respectively, so that Terahertz antenna array unit be driven to measure;Using low Noise preamplifier and multichannel lock-in amplifier realize data acquisition, adjust pumping pulse by control time delay system Time delay between direct impulse detects the entire time domain waveform of terahertz pulse, by data processing, rebuilds to test sample Product terahertz image.
2. the building of the quick dynamic Terahertz near field imaging system according to claim 1 based on photoconductive antenna array Method, which is characterized in that antenna described in step 1 is dipole antenna, and structure is I shape or H-shaped.
3. the building of the quick dynamic Terahertz near field imaging system according to claim 1 based on photoconductive antenna array Method, which is characterized in that antenna material selects the GaAs of low-temperature epitaxy in step 2;Base material selects semi-insulated arsenic Gallium, for the gallium arsenide film layer of 1 μ m-thick of 200-300 DEG C of growth.
4. the building of the quick dynamic Terahertz near field imaging system according to claim 1 based on photoconductive antenna array Method, which is characterized in that the spacing range between detection array and sample is 500um-3mm.
5. the quick dynamic Terahertz Near-Field Radar Imaging based on photoconductive antenna array that the building of claim 1-4 either method obtains System.
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