CN109481380A - A kind of sleep mask and preparation method thereof without preservative - Google Patents
A kind of sleep mask and preparation method thereof without preservative Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The present invention provides a kind of sleep mask without preservative, facial mask is prepared by following parts by weight component, 10-15 parts of sodium hyaluronates, 10-15 parts of Fructus Cucumidis sativi extracts, 3-5 parts of vitamin Es, 3-5 parts of Salvia root P.Es, 3-5 parts of Baical Skullcap root P.Es, 3-5 parts of phellodendron extracts, 3-5 parts of shrubby sophora extracts, 1-3 parts of white tea extracting solutions, 1-3 parts of collagen extracts, 10-15 parts of adlay extracts, 3-5 parts of thickeners, 15-20 parts of chitosans and 15-25 parts of deionized waters, above-mentioned parts by weight component passes through ultrasonic disperse, water surface facial mask is prepared in the last dissolution of spray drying, sleep mask has moisturizing, whitening and raising skin elasticity, trophic factors rate of release can be controlled simultaneously, improve skin assimilation effect.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of without the sleep mask of preservative and its preparation side
Method.
Background technique
Facial mask is more favored as skin care item to obtain female consumer, it can overcome the disadvantages that makeup removing and washes one's face still insufficient clear
Clean work cooperates other essential ingredients to realize other maintenance functions on this basis, for example, replenishing water and preserving moisture, whitening and anti-aging,
Sage Extract.Disposable sleep mask will not generate solid waste rubbish, be suitable for because its is easy to use, during the journey and extensively by
To the favor of people.Existing facial mask is to be uniformly mixed trophic factors and moisture to be prepared into emulsifying liquid, is applied on the face.But
Contain preservative in existing face mask cream, preservative has harmful effect to Skin Cell, thin using may result in skin for a long time
Born of the same parents' canceration；Trophic factors rate of release is uneven in face mask cream, and first quick release is presented, then as the reduction of trophic factors amount,
Rate of release slowly reduces, so deposited overlong time, will lead to nutrient and be sucked back by facial mask, influence assimilation effect.
A kind of float stone cosmetic membrane cream and its preparation side are disclosed in the Chinese patent of Publication No. CN201610585123.5
Method uses polyvinyl alcohol in the patent, has stronger irritation effect to skin；Patent CN1985796A discloses one kind
Black slime facial mask, consisting of: glycerol stearate monoglyceride, fatty alcohol, isobutyl palmitate, saualane, silicone oil, VE, sweet
Oil, panthenol, marine algae extract, black mud dry powder, preservative etc..The facial mask has effects that whitening, crease-resistant, nti-freckle and moisturizing.It should
Glycerol monoglyceride, silicone oil for containing in patent etc. have irritation effect to skin, and wherein silicone oil is it is verified that have carcinogenic
It acts on and forbids using in cosmetics.Patent CN103690464A discloses one kind by seaweed, kaolin, honey, alginic acid
The mud cream skin makeup facial mask that sodium, starch, pearl powder, talcum powder, Aloe gel juice, bentonite and olive oil are constituted.It is sliding in the facial mask
Mountain flour also has carcinogenesis.In addition, the above existing patent is not described in detail the control of facial mask trophic factors rate of release, because
This needs designs a kind of pure natural, uniform facial mask of trophic factors rate of release.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of sleep masks without preservative, so that facial mask has
Very high water lock moisture-retaining capacity, and the rate of release of trophic factors can be controlled.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At: 10-15 parts of sodium hyaluronates, 10-15 parts of Fructus Cucumidis sativi extracts, 3-5 parts of vitamin Es, 3-5 parts of Salvia root P.Es, 3-5 parts of radix scutellariaes mention
Take object, 3-5 part phellodendron extract, 3-5 parts of shrubby sophora extracts, 1-3 parts of white tea extracting solutions, 1-3 parts of collagens, the 10-15 parts of heart of a lotus seeds
Benevolence extract, 3-5 part thickener, 15-20 parts of chitosans and 15-25 parts of deionized waters.
Preferably, above-mentioned facial mask is prepared by following parts by weight component, 12 parts of sodium hyaluronates, 12 parts of Fructus Cucumidis sativi extracts,
4 parts of vitamin Es, 4 parts of Salvia root P.Es, 4 parts of Baical Skullcap root P.Es, 4 parts of phellodendron extracts, 4 parts of shrubby sophora extracts, 2 parts of white teas mention
Take liquid, 2 parts of collagens, 13 parts of adlay extracts, 4 parts of thickeners, 17 parts of chitosans and 20 parts of deionized waters.
Preferably, the preparation method of above-mentioned cucumber, white tea and adlay extract extract includes the following steps: new cadmium yellow
Melon, white tea and adlay independently use broken wall mode to grind, and obtain independent liquid mixture, each liquid mixture mistake
Filter obtains filtrate and filter residue, and the respective filter residue, which is adopted, to be washed with deionized, and respective cleaning solution is uniformly mixed with respective filtrate；
Reduced pressure cleaning solution and the mixed liquor of filtrate are until moisture content in mixture is less than 15%, and whole operation process is in nothing
It is carried out in bacterium laboratory.
Preferably, the preparation method of above-mentioned Salvia root P.E, Baical Skullcap root P.E and phellodendron extract include the following steps: by
Fresh salvia miltiorrhiza, radix scutellariae and Cortex Phellodendri independently use broken wall mode to grind, and obtain independent liquid mixture；Each liquid is mixed
It closes object to filter after alcohol extracting, obtains filtrate and filter residue, cleaning solution is collected and mixed with filtrate through ethanol washing by the filter residue
It is even；Until moisture content in mixture is less than 5%, whole operation process exists for reduced pressure cleaning solution and the mixed liquor of filtrate
It is carried out in aseptic experiment room.
Preferably, above-mentioned alcohol extracting and ethanol washing step are all made of ethyl alcohol.
Wherein, the preparation method of the above-mentioned sleep mask without preservative includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
The invention has the benefit that
The present invention using Fructus Cucumidis sativi extract, sodium hyaluronate, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract,
Shrubby sophora extract, white tea extracting solution, adlay extract, collagen, adlay extract, thickener, chitosan and deionized water,
Have the function of moisturizing, water lock, whitening by the facial mask that ultrasonication is prepared and increases skin elasticity.Nutriment passes through super
Raw even action disperses within the system portion, and various trophic factors are adsorbed on chitosan by the suction-operated of chitosan.By
In suction-operated of the chitosan to trophic factors, when facial mask is applied on the face, the absorption between trophic factors and chitosan is utilized
With desorption equilibrium as buffering, trophic factors slow release can be realized, will not generate facial mask suck-back and receive nutrition inside skin
It happens.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with implementation of the invention
Example, technical scheme in the embodiment of the invention is clearly and completely described.Based on the embodiments of the present invention, this field
Those of ordinary skill's every other embodiment obtained without creative efforts, belongs to protection of the present invention
Range.
Embodiment 1
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At 10 parts of sodium hyaluronates, 10 parts of Fructus Cucumidis sativi extracts, 3 parts of vitamin Es, 3 parts of Salvia root P.Es, 3 parts of Baical Skullcap root P.Es, 3 portions of Cortex Phellodendris
Extract, 3 parts of shrubby sophora extracts, 1 part of white tea extracting solution, 1 part of collagen, 10 parts of adlay extracts, 3 parts of thickeners, 15 parts
Chitosan and 15 parts of deionized waters.
Wherein, the preparation method of Fructus Cucumidis sativi extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Ramulus et Folium Mussaendae Pubescentis extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of adlay extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Baical Skullcap root P.E includes the following steps: to grind fresh Scutellaria baicalensis with broken wall mode, obtains
To independent liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, and filter residue is washed through ethyl alcohol
It washs, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until moisture contains in mixture
Until amount is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Salvia root P.E includes the following steps: independently to use broken wall mode to grind fresh salvia miltiorrhiza
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Alcohol washing, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to water in mixture
Until point content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of phellodendron extract includes the following steps: independently to use broken wall mode to grind fresh Cortex Phellodendri
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Ethanol washing is washed, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of above-mentioned sleep mask includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
Embodiment 2
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At 15 parts of sodium hyaluronates, 15 parts of Fructus Cucumidis sativi extracts, 5 parts of vitamin Es, 5 parts of Salvia root P.Es, 5 parts of Baical Skullcap root P.Es, 5 portions of Cortex Phellodendris
Extract, 5 parts of shrubby sophora extracts, 3 parts of white tea extracting solutions, 3 parts of collagens, 15 parts of adlay extracts, 5 parts of thickeners, 20 parts
Chitosan and 25 parts of deionized waters.
Wherein, the preparation method of Fructus Cucumidis sativi extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Ramulus et Folium Mussaendae Pubescentis extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of adlay extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Baical Skullcap root P.E includes the following steps: to grind fresh Scutellaria baicalensis with broken wall mode, obtains
To independent liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, and filter residue is washed through ethyl alcohol
It washs, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until moisture contains in mixture
Until amount is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Salvia root P.E includes the following steps: independently to use broken wall mode to grind fresh salvia miltiorrhiza
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Alcohol washing, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to water in mixture
Until point content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of phellodendron extract includes the following steps: independently to use broken wall mode to grind fresh Cortex Phellodendri
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Ethanol washing is washed, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of above-mentioned sleep mask includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
Embodiment 3
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At 11 parts of sodium hyaluronates, 11 parts of Fructus Cucumidis sativi extracts, 4 parts of vitamin Es, 4 parts of Salvia root P.Es, 4 parts of Baical Skullcap root P.Es, 4 portions of Cortex Phellodendris
Extract, 4 parts of shrubby sophora extracts, 2 parts of white tea extracting solutions, 2 parts of collagens, 11 parts of adlay extracts, 4 parts of thickeners, 16 parts
Chitosan and 17 parts of deionized waters.
Wherein, the preparation method of Fructus Cucumidis sativi extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Ramulus et Folium Mussaendae Pubescentis extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of adlay extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Baical Skullcap root P.E includes the following steps: to grind fresh Scutellaria baicalensis with broken wall mode, obtains
To independent liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, and filter residue is washed through ethyl alcohol
It washs, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until moisture contains in mixture
Until amount is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Salvia root P.E includes the following steps: independently to use broken wall mode to grind fresh salvia miltiorrhiza
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Alcohol washing, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to water in mixture
Until point content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of phellodendron extract includes the following steps: independently to use broken wall mode to grind fresh Cortex Phellodendri
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Ethanol washing is washed, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of above-mentioned sleep mask includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
Embodiment 4
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At 12 parts of sodium hyaluronates, 12 parts of Fructus Cucumidis sativi extracts, 4 parts of vitamin Es, 4 parts of Salvia root P.Es, 4 parts of Baical Skullcap root P.Es, 4 portions of Cortex Phellodendris
Extract, 4 parts of shrubby sophora extracts, 2 parts of white tea extracting solutions, 2 parts of collagens, 12 parts of adlay extracts, 4 parts of thickeners, 19 parts
Chitosan and 19 parts of deionized waters.
Wherein, the preparation method of Fructus Cucumidis sativi extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Ramulus et Folium Mussaendae Pubescentis extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of adlay extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Baical Skullcap root P.E includes the following steps: to grind fresh Scutellaria baicalensis with broken wall mode, obtains
To independent liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, and filter residue is washed through ethyl alcohol
It washs, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until moisture contains in mixture
Until amount is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Salvia root P.E includes the following steps: independently to use broken wall mode to grind fresh salvia miltiorrhiza
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Alcohol washing, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to water in mixture
Until point content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of phellodendron extract includes the following steps: independently to use broken wall mode to grind fresh Cortex Phellodendri
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Ethanol washing is washed, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of above-mentioned sleep mask includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
Embodiment 5
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At 13 parts of sodium hyaluronates, 13 parts of Fructus Cucumidis sativi extracts, 4 parts of vitamin Es, 4 parts of Salvia root P.Es, 4 parts of Baical Skullcap root P.Es, 4 portions of Cortex Phellodendris
Extract, 4 parts of shrubby sophora extracts, 2 parts of white tea extracting solutions, 2 parts of collagens, 13 parts of adlay extracts, 4 parts of thickeners, 18 parts
Chitosan and 21 parts of deionized waters.
Wherein, the preparation method of Fructus Cucumidis sativi extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Ramulus et Folium Mussaendae Pubescentis extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of adlay extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Baical Skullcap root P.E includes the following steps: to grind fresh Scutellaria baicalensis with broken wall mode, obtains
To independent liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, and filter residue is washed through ethyl alcohol
It washs, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until moisture contains in mixture
Until amount is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Salvia root P.E includes the following steps: independently to use broken wall mode to grind fresh salvia miltiorrhiza
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Alcohol washing, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to water in mixture
Until point content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of phellodendron extract includes the following steps: independently to use broken wall mode to grind fresh Cortex Phellodendri
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Ethanol washing is washed, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of above-mentioned sleep mask includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
Embodiment 6
The present invention provides a kind of sleep mask without preservative, the facial mask prepared by following parts by weight component and
At 14 parts of sodium hyaluronates, 14 parts of Fructus Cucumidis sativi extracts, 4 parts of vitamin Es, 4 parts of Salvia root P.Es, 4 parts of Baical Skullcap root P.Es, 4 portions of Cortex Phellodendris
Extract, 4 parts of shrubby sophora extracts, 2 parts of white tea extracting solutions, 2 parts of collagens, 14 parts of adlay extracts, 4 parts of thickeners, 18 parts
Chitosan and 23 parts of deionized waters.
Wherein, the preparation method of Fructus Cucumidis sativi extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Ramulus et Folium Mussaendae Pubescentis extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of adlay extract includes the following steps: to grind fresh cucumber using broken wall mode,
Liquid mixture is obtained, filtrate and filter residue is obtained by filtration in liquid mixture, the respective filter residue, which is adopted, to be washed with deionized, will
Respective cleaning solution is uniformly mixed with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to moisture content in mixture
Until 15%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Baical Skullcap root P.E includes the following steps: to grind fresh Scutellaria baicalensis with broken wall mode, obtains
To independent liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, and filter residue is washed through ethyl alcohol
It washs, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until moisture contains in mixture
Until amount is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of Salvia root P.E includes the following steps: independently to use broken wall mode to grind fresh salvia miltiorrhiza
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Alcohol washing, cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure up to water in mixture
Until point content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of phellodendron extract includes the following steps: independently to use broken wall mode to grind fresh Cortex Phellodendri
It crushes, obtains liquid mixture；Liquid mixture filters after ethyl alcohol extracts, and obtains filtrate and filter residue, the filter residue is through second
Ethanol washing is washed, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 5%, whole operation process carries out in aseptic experiment room.
Wherein, the preparation method of above-mentioned sleep mask includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng
Extract, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are obtained
Mixed liquor A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, then sets mixed liquid B
Ultrasonic disperse is carried out in ultrasonic disperse instrument, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving,
Obtain facial mask lotion.
The face mask cream prepared and the face mask cream sold on the market are applied on plastic plate, measurement smear after 5min,
The residual moisture of face mask cream when 10min, 20min and 30min, i.e. moisturizing rate, as shown in table 1.As shown in Table 1, the present invention provides
High face mask cream moisturizing rate is due to the face mask cream sold on the market.
Moisture preserving time when 1 embodiment 1-6 of table is placed in air
According to previous embodiment, invention is explained in detail, those skilled in the art should understand that: its
It is still possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is equal
Replacement；And these are modified or replaceed, technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution
Spirit and scope.
Claims (6)
1. a kind of sleep mask without preservative, which is characterized in that the facial mask is prepared by following parts by weight component:
10-15 parts of sodium hyaluronates, 10-15 parts of Fructus Cucumidis sativi extracts, 3-5 parts of vitamin Es, 3-5 parts of Salvia root P.Es, 3-5 parts of Baical Skullcap root P.Es,
3-5 parts of phellodendron extracts, 3-5 parts of shrubby sophora extracts, 1-3 parts of white tea extracting solutions, 1-3 parts of collagens, 10-15 parts of adlays are extracted
Object, 3-5 part thickener, 15-20 parts of chitosans and 15-25 parts of deionized waters.
2. the sleep mask according to claim 1 without preservative, which is characterized in that the facial mask is by following parts by weight
Array point is prepared: 12 parts of sodium hyaluronates, 12 parts of Fructus Cucumidis sativi extracts, 4 parts of vitamin Es, 4 parts of Salvia root P.Es, 4 parts of radix scutellariaes extract
Object, 4 parts of phellodendron extracts, 4 parts of shrubby sophora extracts, 2 parts of white tea extracting solutions, 2 parts of collagens, 13 parts of adlay extracts, 4 parts of increasings
Thick dose, 17 parts of chitosans and 20 parts of deionized waters.
3. the sleep mask according to claim 1 without preservative, which is characterized in that the cucumber, white tea and adlay
The preparation method of extract includes the following steps: independently to use broken wall mode to grind fresh cucumber, white tea and adlay, obtain
To independent liquid mixture, filtrate and filter residue is obtained by filtration in each liquid mixture, and the respective filter residue uses deionization
Respective cleaning solution is uniformly mixed by water washing with respective filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until mixture
Until middle moisture content is less than 15%, whole operation process carries out in aseptic experiment room.
4. the sleep mask according to claim 1 without preservative, which is characterized in that the Salvia root P.E, radix scutellariae
The preparation method of extract phellodendron extract includes the following steps: fresh salvia miltiorrhiza, radix scutellariae and Cortex Phellodendri independently using broken wall side
Formula is ground, and obtains independent liquid mixture；Each liquid mixture filters after alcohol extracting, obtains filtrate and filter
Slag, the filter residue are washed through alcohol, and cleaning solution is collected and is uniformly mixed with filtrate；The mixed liquor of cleaning solution and filtrate is concentrated under reduced pressure until
Until moisture content is less than 5% in mixture, whole operation process carries out in aseptic experiment room.
5. the sleep mask according to claim 4 without preservative, which is characterized in that it is equal that the alcohol extracting and alcohol wash step
Using ethyl alcohol.
6. the preparation method of the sleep mask according to claim 1 without preservative, which is characterized in that the preparation side
Method includes the following steps:
(1) by sodium hyaluronate, Fructus Cucumidis sativi extract, vitamin E, Salvia root P.E, Baical Skullcap root P.E, phellodendron extract, kuh-seng are extracted
Object, white tea extracting solution, collagen, adlay extract, portions of de-ionized water mixing, stirring at normal temperature 30-45min are mixed
Liquid A is stand-by；
(2) it adds chitosan into mixed liquor A, stirring at normal temperature 10min obtains mixed liquid B, is then placed in mixed liquid B super
Ultrasonic disperse is carried out in sound separating apparatus, jitter time 20min-30min obtains solution C；
(3) solution C is spray-dried, obtains chitosan microball；
(4) by step (3) chitosan microball and thickener mix be placed in remaining deionized water, stirring and dissolving obtains
Facial mask lotion.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811535852.5A CN109481380A (en) | 2018-12-15 | 2018-12-15 | A kind of sleep mask and preparation method thereof without preservative |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811535852.5A CN109481380A (en) | 2018-12-15 | 2018-12-15 | A kind of sleep mask and preparation method thereof without preservative |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103315925A (en) * | 2012-03-20 | 2013-09-25 | 董根荣 | Chinese medicine facial mask possessing whitening and moisturizing efficacy, and preparation method thereof |
| CN106176280A (en) * | 2016-07-21 | 2016-12-07 | 东华大学 | A kind of preparation method of chitosan microball moisturizing antibacterial facial mask |
| CN106474025A (en) * | 2015-08-27 | 2017-03-08 | 李尧 | Moisture saver mask |
| CN106511116A (en) * | 2016-12-28 | 2017-03-22 | 芜湖凯奥尔环保科技有限公司 | Tencel mask containing traditional Chinese medicine content and preparation method thereof |
-
2018
- 2018-12-15 CN CN201811535852.5A patent/CN109481380A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103315925A (en) * | 2012-03-20 | 2013-09-25 | 董根荣 | Chinese medicine facial mask possessing whitening and moisturizing efficacy, and preparation method thereof |
| CN106474025A (en) * | 2015-08-27 | 2017-03-08 | 李尧 | Moisture saver mask |
| CN106176280A (en) * | 2016-07-21 | 2016-12-07 | 东华大学 | A kind of preparation method of chitosan microball moisturizing antibacterial facial mask |
| CN106511116A (en) * | 2016-12-28 | 2017-03-22 | 芜湖凯奥尔环保科技有限公司 | Tencel mask containing traditional Chinese medicine content and preparation method thereof |
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Application publication date: 20190319 |