CN109444367A - The flow path system of petroleum, animals and plants oil content in a kind of all automatic measurement water - Google Patents
The flow path system of petroleum, animals and plants oil content in a kind of all automatic measurement water Download PDFInfo
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- CN109444367A CN109444367A CN201811466469.9A CN201811466469A CN109444367A CN 109444367 A CN109444367 A CN 109444367A CN 201811466469 A CN201811466469 A CN 201811466469A CN 109444367 A CN109444367 A CN 109444367A
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- Prior art keywords
- mechanical arm
- animals
- petroleum
- water
- flow path
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 55
- 241001465754 Metazoa Species 0.000 title claims abstract description 20
- 239000003208 petroleum Substances 0.000 title claims abstract description 14
- 238000005259 measurement Methods 0.000 title claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 33
- 239000003921 oil Substances 0.000 claims abstract description 26
- 238000010790 dilution Methods 0.000 claims abstract description 11
- 239000012895 dilution Substances 0.000 claims abstract description 11
- 239000012535 impurity Substances 0.000 claims abstract description 10
- 239000012528 membrane Substances 0.000 claims abstract description 10
- 239000002699 waste material Substances 0.000 claims abstract description 10
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052919 magnesium silicate Inorganic materials 0.000 claims abstract description 8
- 235000019792 magnesium silicate Nutrition 0.000 claims abstract description 8
- 239000000391 magnesium silicate Substances 0.000 claims abstract description 8
- 230000002572 peristaltic effect Effects 0.000 claims abstract description 8
- 238000001179 sorption measurement Methods 0.000 claims abstract description 8
- 239000003153 chemical reaction reagent Substances 0.000 claims description 21
- 238000004140 cleaning Methods 0.000 claims description 9
- 238000012545 processing Methods 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 6
- 230000008569 process Effects 0.000 abstract description 4
- 235000013311 vegetables Nutrition 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 6
- 230000008901 benefit Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1826—Organic contamination in water
- G01N33/1833—Oil in water
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The present invention relates to the flow path systems of petroleum, animals and plants oil content in a kind of all automatic measurement water, including controller and by the chain-type turntable of controller control, three-mechanical arm water sample processor, peristaltic pump, 8 logical syringe pumps, different densities liquid separator, impurity, moisture membrane filter separator, waste liquid separator, adsorption of magnesium silicate device and automatically with mark, dilution device；The adsorption process of automation vegetable and animals oils may be implemented, so that instrument can petroleum-type, animals and plants oils in automatic measurement water.Instrument flow path system is also added into automatic preparation standard curve system, automatic dilution function and automatic collection waste liquid function.
Description
Technical field
The present invention relates to measuring device field, petroleum in specifically a kind of all automatic measurement water, animals and plants oil content
Flow path system.
Background technique
Now, full-automation measures petroleum-type in water, the instrument of animals and plants oil content emerges one after another, and every kind of automation is surveyed
The instrument of oil content has oneself unique full-automatic flow path system in amount water.It is directed to existing full-automatic oil content analyzer
The flow path system of device, each producer can have its advantage and deficiency.Oils instrument is surveyed to different manufacturers according to our companies
Solution.It was found that existing oil content analyzer flow path system largely uses the design scheme of fixed sample bottle, so that sample digit is general
It is less, and can not infinitely expand sample position；Some uses extraction agent carbon tetrachloride and directly extracts measurement in sample bottle, makes
It must be unable to measure seriously polluted water sample, especially the stirring serious water sample of extracting and emulsifying；Some instruments are gone using anhydrous sodium sulfate
Except the water in carbon tetrachloride, cause water removal effect in carbon tetrachloride bad；Some instruments can only measure total oil content in water, nothing
Method measures petroleum class and zoology and botany oil class.
Summary of the invention
Technical problem to be solved by the invention is to provide petroleum in a kind of all automatic measurement water, animals and plants oil content
Flow path system, to solve defect existing in the prior art.
The technical scheme to solve the above technical problems is that
The flow path system of petroleum, animals and plants oil content in a kind of all automatic measurement water, including controller and pass through control
It is the chain-type turntable of device control, three-mechanical arm water sample processor, peristaltic pump, 8 logical syringe pumps, different densities liquid separator, miscellaneous
Matter, moisture membrane filter separator, waste liquid separator, adsorption of magnesium silicate device and automatic with mark, dilution device；Described three is mechanical
Arm water sample processor includes for adding the first mechanical arm of organic reagent toward the sample bottle on the chain-type turntable of lower section, for stirring
Mix the second mechanical arm of extraction and for extracting the third mechanical arm that clear water carries out cleaning and organic reagent is collected；Described three is mechanical
Arm water sample processor is successively connected to different densities liquid separator, impurity, moisture membrane filter separator, the impurity, moisture
Membrane filter separator is connected to syringe pump and different densities liquid separator respectively, and the liquid passes through 8 logical injections after processing
To analysis system, petroleum in water, animals and plants oil content is calculated to liquid in the analysis system for pump and pipeline；
Further, there is the third mechanical arm pipeline to be connected to pure water bottle, and the pure water bottle connect use with cleaning pump
It is cleaned in pipeline；There is the third mechanical arm pipeline to be connected to different densities liquid separator, be provided on pipeline
Organic reagent is delivered to different densities liquid separator by peristaltic pump；
Further, it is provided on the pipeline of the analysis system front end automatic with mark, dilution system；
The beneficial effects of the present invention are: using the Chain drum kinematic system of independent design, so that the sample of instrument can nothing
Limit circulation makees sample, and sample digit can infinitely be added according to customer demand, fundamentally solve the limitation of sample digit.And
And instrument uses three mechanical water sample processing systems, it will be in the addition of organic reagent in water sample, the stirring extraction and water sample of water sample
The separation of organic reagent and water, which efficiently separates, comes, and allows instrument to handle three water samples simultaneously, and do not interfere with each other, thus
Substantially reduce the processing time of water sample.The flow path system also uses the separator of two kinds of different densities liquid, so as to
A small amount of organic reagent and a large amount of water samples optimization to be separated.Flow path system incorporates magnesium silicate column, keeps total oil automatic
It after change is measured, can automate into magnesium silicate column, so that the adsorption process of automation vegetable and animals oils is realized, so that instrument can
Petroleum-type, animals and plants oils in automatic measurement water.Instrument flow path system is also added into automatic preparation standard curve system, from
Dynamic dilution function and automatic collection waste liquid function.
Detailed description of the invention
Fig. 1 is schematic structural view of the invention；
The reference numerals are as follows:
1, chain-type turntable, 2, three-mechanical arm water sample processor, 21, cleaning pump, 3, different densities liquid separator, 4, miscellaneous
Matter, moisture membrane filter separator, 5, waste liquid separator, 6, adsorption of magnesium silicate device, 7, automatic with mark, dilution device, 8, point
Analysis system, 9, pure water bottle, 10, waste collection bottle, 11, peristaltic pump, 12,8 channel injections pump；
Specific embodiment
The principle and features of the present invention will be described below with reference to the accompanying drawings, and the given examples are served only to explain the present invention, and
It is non-to be used to limit the scope of the invention.
As shown in Figure 1, in a kind of all automatic measurement water petroleum, animals and plants oil content flow path system, including controller
And it is close by the chain-type turntable 1 of controller control, three-mechanical arm water sample processor 2, peristaltic pump 11,8 logical syringe pumps 12, difference
Spend liquid separator 3, impurity, moisture membrane filter separator 4, waste liquid separator 5, adsorption of magnesium silicate device 6 and it is automatic with mark,
Dilution device 7；The three-mechanical arm water sample processor 2 includes for organic toward the sample bottle addition on lower section chain-type turntable 1
The first mechanical arm of reagent, for stirring the second mechanical arm extracted and for extracting, clear water carries out cleaning and organic reagent is collected
Third mechanical arm；The three-mechanical arm water sample processor 2 is successively filtered with different densities liquid separator 3, impurity, moisture film
Separator 4 is connected to, and the impurity, moisture membrane filter separator 4 are connected to syringe pump and different densities liquid separator 3 respectively,
The liquid passes through 8 logical syringe pumps 12 and pipeline to analysis system 8 after processing, and the analysis system 8 calculates liquid
Petroleum, animals and plants oil content in must being discharged；
More specifically, there is the third mechanical arm pipeline to be connected to pure water bottle 9, and the pure water bottle 9 connects with cleaning pump 21
It connects for being cleaned to pipeline；There is the third mechanical arm pipeline to be connected to different densities liquid separator 3, set on pipeline
It is equipped with peristaltic pump 11 and organic reagent is delivered to different densities liquid separator 3；
More specifically, it is provided on the pipeline of 8 front end of analysis system automatic with mark, dilution system 7；
Specific work process:
1, chain-type turntable is accurately positioned at three-mechanical arm water sample processor, in the three-mechanical arm water sample processor, one
A mechanical arm carries out the addition of organic reagent, and a mechanical arm is stirred extraction, and a mechanical arm carries out extracting clear water progress
Cleaning and organic reagent are collected, and three-mechanical arm runs co-ordination of working in coordination simultaneously
2, three-mechanical arm processing is completed, and after waste liquid is excluded, organic reagent is collected into different densities liquid separating appts,
Carry out the layering of water and organic reagent.
3, the organic reagent after layering is separated by filtration by syringe pump after organic reagent layering by impurity moisture film and is
System extracts some volumes, injects analysis system.
4, after total oil is completed in analysis system analysis, the organic reagent after analysis is extracted, then passes through adsorption of magnesium silicate system
System, adsorbs vegetable and animals oils therein, then re-injects analysis system, read the content of petroleum-type, and then calculate animals and plants
The content of class
The present invention has the advantage that
In the process use waste collection and separation system, carry out the collection of organic reagent, thus make experimenter from
The murder by poisoning of organic reagent；In this flow path with mark system is matched, can accurately prepare required for being configured to highly concentrated solution
Concentration point；The flow path system has simultaneously, ultrahigh concentration water sample automatic dilution function, when measuring exceeded so as to meet,
Experimental data is accurately measured in automation.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and
Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (3)
1. the flow path system of petroleum, animals and plants oil content in a kind of all automatic measurement water, it is characterised in that: including controller and
Chain-type turntable, three-mechanical arm water sample processor, peristaltic pump, 8 logical syringe pumps, the different densities liquid point controlled by controller
From device, impurity, moisture membrane filter separator, waste liquid separator, adsorption of magnesium silicate device and automatically with mark, dilution device；Institute
Stating three-mechanical arm water sample processor includes for the first machinery toward the sample bottle addition organic reagent on the chain-type turntable of lower section
Arm, the second mechanical arm for stirring extraction and the third mechanical arm that cleaning and organic reagent collection are carried out for extracting clear water；
The three-mechanical arm water sample processor is successively connected to different densities liquid separator, impurity, moisture membrane filter separator, described
Impurity, moisture membrane filter separator are connected to syringe pump and different densities liquid separator respectively, and the liquid leads to after processing
8 logical syringe pumps and pipeline are crossed to analysis system, petroleum in water, animals and plants oils is calculated to liquid in the analysis system
Content.
2. the flow path system of petroleum, animals and plants oil content in a kind of all automatic measurement water according to claim 1, special
Sign is: the third mechanical arm have pipeline be connected to pure water bottle, the pure water bottle connect with cleaning pump for pipeline into
Row cleaning；There is the third mechanical arm pipeline to be connected to different densities liquid separator, and peristaltic pump will be provided on pipeline to be had
Machine reagent is delivered to different densities liquid separator.
3. the flow path system of petroleum, animals and plants oil content in a kind of all automatic measurement water according to claim 2, special
Sign is: being provided on the pipeline of the analysis system front end automatic with mark, dilution system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811466469.9A CN109444367B (en) | 2018-12-06 | 2018-12-06 | Flow path system for fully automatically measuring oil content, animal and vegetable oil content in water |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811466469.9A CN109444367B (en) | 2018-12-06 | 2018-12-06 | Flow path system for fully automatically measuring oil content, animal and vegetable oil content in water |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109444367A true CN109444367A (en) | 2019-03-08 |
| CN109444367B CN109444367B (en) | 2023-08-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811466469.9A Active CN109444367B (en) | 2018-12-06 | 2018-12-06 | Flow path system for fully automatically measuring oil content, animal and vegetable oil content in water |
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| CN (1) | CN109444367B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110376359A (en) * | 2019-07-28 | 2019-10-25 | 赵健 | It is a kind of for detecting the detection device of oil density |
Citations (9)
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|---|---|---|---|---|
| JPH10142234A (en) * | 1996-11-13 | 1998-05-29 | Horiba Ltd | Oil content measuring device |
| CN201399261Y (en) * | 2009-04-16 | 2010-02-10 | 泰安市科瑞光学仪器有限公司 | Full-automatic extraction apparatus |
| CN104345035A (en) * | 2014-11-13 | 2015-02-11 | 天津市能谱科技有限公司 | Full automatic infrared oil content analyzer |
| CN105181922A (en) * | 2015-09-18 | 2015-12-23 | 上海昂林科学仪器有限公司 | Device for measuring animal and plant oil |
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| CN205216279U (en) * | 2015-05-26 | 2016-05-11 | 德清县同福楼食品有限公司 | Take oil water separator of density detector |
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-
2018
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| JPH10142234A (en) * | 1996-11-13 | 1998-05-29 | Horiba Ltd | Oil content measuring device |
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| CN104345035A (en) * | 2014-11-13 | 2015-02-11 | 天津市能谱科技有限公司 | Full automatic infrared oil content analyzer |
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Cited By (1)
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| CN110376359A (en) * | 2019-07-28 | 2019-10-25 | 赵健 | It is a kind of for detecting the detection device of oil density |
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| CN109444367B (en) | 2023-08-08 |
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