CN109432225A - A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum - Google Patents
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum Download PDFInfo
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- CN109432225A CN109432225A CN201811335173.3A CN201811335173A CN109432225A CN 109432225 A CN109432225 A CN 109432225A CN 201811335173 A CN201811335173 A CN 201811335173A CN 109432225 A CN109432225 A CN 109432225A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
- A61K31/19—Carboxylic acids, e.g. valproic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
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Abstract
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum, this method is processed using wine or vinegar toast, and its step are as follows: the fresh Solanum nigrum for preparatory processing of learning from else's experience, appropriate yellow rice wine or rice vinegar is added to mix thoroughly, it is bored, it sets in frying container, with surface is fried with slow fire into dark brown, takes out, cool to obtain the final product.The invention also discloses a kind of to carry out the method that the prepared slices of Chinese crude drugs of fresh Solanum nigrum process in such a way that wine steams or vinegar steams.The processing of black nightshade fresh fruit is carried out by the method for the invention, the fresh Solanum nigrum prepared slices of Chinese crude drugs can be effectively improved takes compliance, reduce the adverse reaction taken, improve after fresh Solanum nigrum prepared slices of Chinese crude drugs water decocts or water extract after active principle the rate of transform, and improve be prepared into Solanum nigrum granule after active principle content.The prepared slices of Chinese crude drugs that fresh Solanum nigrum is processed with the method for the present invention can be used for processing the fresh Solanum nigrum prepared slices of Chinese crude drugs, be also used as preparing fresh Solanum nigrum Chinese medicinal granule raw material.
Description
Technical field
The present invention relates to a kind of concocting method of prepared slices of Chinese crude drugs, especially a kind of prepared slices of Chinese crude drugs processing side of fresh Solanum nigrum
Method.
Background technique
Chinese patent document CN2013 1 0110440.8 discloses " a kind of processing method and extraction of black nightshade fresh fruit
Composition granule and purposes ", the patent document provide plant of Solanaceae black nightshadeSolanum nigrum L.Fruit black nightshade fresh fruit or few flower
Black nightshadeSolanum photeinocarpum Nakamura et OdashimaThe processing method and extract of fruit black nightshade fresh fruit
Particle and purposes.And disclose following technical scheme: (1) winning 6~August prematurity Solanum nigrum, Solanum nigrum color dark green, blueness
Yellow;A small amount of fruit is taken before picking, and equimultiple water is added, homogenate is broken, after filtering, filtrate dark green to brown-green, and do not go out
Existing rufous, rosiness;(2) it after Solanum nigrum after picking, decontamination and carpopodium, selects and does not damage pericarp, be precipitated without juice, character
Full fruit is 7~2kgcm through the detection hardness of fruit-1It is cleaned, is drained with water;(3) processing of step (2) is taken to obtain net
Fruit is set in boiling water 0.5~10 minute, is taken out, and ventilating and cooling drains;Or cold water is cooling, taking-up drains;(4) step (2) are taken
Or (3) handle obtained fruit, set at shady and cool ventilation 0.5~10, or be dried with circulating air, be fruit dehydration 5%~
50%;(5) step (2) is taken to drain rear fruit, or without mildew, fruit after unabroken dehydration after taking step (4) to handle, by weight
Volume ratio 1:0.5~10 are measured, 0.5~10L white wine is added in every 1 kilogram of fruit or edible alcohol impregnates, and white wine alcoholic strength V/V is
20%~65%, edible alcohol concentration is 15%~85%, and soaking time is 0.5 day or more;It (6) should be in clean environment, in batches
Lift face device takes step (5) treated fruit, drains liquid, remaining wine part is gone in ventilation, to be processed;Mobile phone, which all impregnates, uses white wine
Or edible alcohol, ethyl alcohol is recycled, relative density 1.01~1.08 is concentrated into, concentrate is taken uniformly to be sprayed on fruit to be processed,
It is gently mixed and dries in spray, 40~80 DEG C of drying temperature, until there is not dripping phenomenon, i.e., without obvious moisture in fruit surface
Obtain finished product Solanum nigrum.
The technology has obtained applications well on fresh black nightshade fruit product.But there is also following several for fresh black nightshade fruit product
A problem:
1, pan-fried juice is drunk or is made after extracting particle and takes after the directly edible perhaps water of fresh black nightshade fruit product decocts, and taste is bitter
It is puckery, pungent, take poor compliance.
2, there are the adverse reactions such as gastric acid, gasteremphraxis, stomach cold in the part user of fresh black nightshade fruit product.
3, fresh Solanum nigrum product water decocts or water extracts, and active principle solasonine adds solamargine total transfer rate not
Height causes the effective dose of fresh black nightshade fruit product big.
Summary of the invention
The technical problem to be solved by the present invention is to be directed to the foot of the prior art, a kind of new fresh Solanum nigrum Chinese medicine drink is provided
The concocting method of piece.
The technical problem to be solved by the present invention is to realized through the following technical scheme.The present invention is a kind of fresh black nightshade
The prepared slices of Chinese crude drugs concocting method of fruit, its main feature is that: this method is processed using wine or vinegar toast, and its step are as follows: preparatory processing of learning from else's experience
Fresh Solanum nigrum adds appropriate yellow rice wine or rice vinegar to mix thoroughly, bored, sets in frying container, with surface is fried with slow fire into dark brown, takes
Out, it cools to obtain the final product.
The prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum of the present invention, further preferred technical solution is: wine toast
When the yellow rice wine that is added of the fresh Solanum nigrum of every 100kg be 10~20kg.The alcoholic strength v/v for the yellow rice wine being added is 15%~20%.Vinegar toast
When the rice vinegar that is added of the fresh Solanum nigrum of every 100kg be 20kg~30kg.The rice vinegar total acid content is with Acetometer >=5.0g/
100ml。
The present invention also provides the prepared slices of Chinese crude drugs concocting methods of another fresh Solanum nigrum, its main feature is that: this method uses wine
It steams or vinegar steams, its step are as follows: the fresh Solanum nigrum for preparatory processing of learning from else's experience adds yellow rice wine or white wine or rice vinegar or alimentary acetic acid to mix thoroughly,
It moisturizing, sets and steam in container, wine is exhausted by fresh Solanum nigrum or fresh Solanum nigrum surface is in yellowish-brown with being steam heated to, it takes out,
It slightly dries in the air, mixes back steaming liquid, then dry in the air to sixty percent dry, be drying to obtain.
The prepared slices of Chinese crude drugs concocting method of above-described fresh Solanum nigrum, further preferred technical solution is: when wine steams
The yellow rice wine or white wine 20kg~30kg that every fresh Solanum nigrum of 100kg is added.The alcoholic strength v/v for the yellow rice wine being added is 15%~20%,
The alcoholic strength v/v for the white wine being added is 20%~70%.Vinegar every fresh Solanum nigrum of 100kg is added when steaming rice vinegar or alimentary acetic acid are
20kg~30kg.The rice vinegar or alimentary acetic acid total acid content is with Acetometer >=5.0g/100ml.
Fresh Solanum nigrum described in the method for the present invention is plant of Solanaceae black nightshadeSolanum nigrum L.Immature fruit
Or S. photeinocarpumSolanum photeinocarpum Nakamura et OdashimaImmature fruit.
" the fresh Solanum nigrum of preparatory processing " described in the method for the present invention, can be according to disclosed in the prior art any one
Kind method is not influenced the preliminary working method of its composition.It is preferably public according to Chinese patent literature CN2013101104408 institute
Documented method carries out preparatory processing in " processing method and extract particles and purposes of a kind of black nightshade fresh fruit " opened, i.e., with
Processing method documented by lower 1 or 2 schemes:
1, the processing method of black nightshade fresh fruit chooses plant of Solanaceae black nightshadeSolanum nigrumL or S. photeinocarpumS. photeinocarpum Nakamura et OdashimaPrematurity Solanum nigrum is processed, and its step are as follows:
(1) 6~August prematurity Solanum nigrum, Solanum nigrum color viridescent, bluish yellow color are won;The hardness of fruit is 7~2Kg cm-1;It adopts
A small amount of fruit is taken before plucking, and equimultiple water is added, homogenate is broken, after filtering, filtrate dark green to brown-green, and do not occur reddish brown
Color, rosiness;
(2) it after Solanum nigrum after picking, decontamination and carpopodium, selects and does not damage pericarp, be precipitated without juice, the full fruit of shape, warp
The detection hardness of fruit is 7~2Kg cm-1;It is cleaned with water, drains, obtain Solanum nigrum.
2, a kind of processing method of black nightshade fresh fruit, its step are as follows:
(1) 6~August prematurity Solanum nigrum, Solanum nigrum color viridescent, bluish yellow color are won;The hardness of fruit is 7~2Kg cm-1;It adopts
A small amount of fruit is taken before plucking, and equimultiple water is added, homogenate is broken, after filtering, filtrate dark green to brown-green, and do not occur reddish brown
Color, rosiness;
(2) it after Solanum nigrum after picking, decontamination and carpopodium, selects and does not damage pericarp, be precipitated without juice, the full fruit of shape, warp
The detection hardness of fruit is 7~2Kg cm-1;It is cleaned, is drained with water;
(3) the net fruit for taking the processing of step (2) to obtain is set in boiling water 0.5~10 minute, is taken out, is drained;Or it sets in cold water again
0.5~20 minute, taking-up drained;
(4) step (2) or (3) are taken treated fruit, set at shady and cool ventilation 0.5 ~ 10, or be dried with circulating air,
Make fruit dehydration 5%~50%;
(5) step (2) is taken to drain rear fruit, or without mildew, fruit after unabroken dehydration after taking step (4) to handle, by weight
Volume ratio 1:0.5~10 are measured, 0.5~10L white wine is added in every 1 kilogram of fruit or edible alcohol impregnates, and white wine alcoholic strength V/V is
20~65 %, edible alcohol concentration are 15%~85%.Soaking time is 0.5 day or more;
(6) should be in clean grade environment, lift face device takes step (5) treated fruit in batches, drains liquid, ventilation is gone residual
Remaining wine part is to be processed;Collect all impregnate use white wine or edible alcohols, recycle ethyl alcohol, be concentrated into relative density 1.01~
1.08, it takes concentrate to be uniformly sprayed on fruit to be processed, is gently mixed and dries in spray, 40~80 DEG C of drying temperature, until
There is not dripping phenomenon without obvious moisture to get finished product Solanum nigrum in fruit surface.
Compared with prior art, the method for the present invention has the beneficial effect that: carrying out black nightshade fresh fruit big gun by the method for the invention
System, can effectively improve the fresh Solanum nigrum prepared slices of Chinese crude drugs takes compliance, reduces the adverse reaction taken, improves fresh Solanum nigrum
Prepared slices of Chinese crude drugs water decoct after or water extract after active principle the rate of transform, and improve be prepared into Solanum nigrum granule after have
Imitate the content of component.The prepared slices of Chinese crude drugs that fresh Solanum nigrum is processed with the method for the present invention can be used for processing the fresh Solanum nigrum prepared slices of Chinese crude drugs,
It is also used as preparing fresh Solanum nigrum Chinese medicinal granule raw material.
Specific embodiment
The specific technical solution of the present invention described further below, in order to which those skilled in the art is further understood that
The present invention, without constituting the limitation to its right.
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: embodiment 1 carries out wine toast with yellow rice wine, its step are as follows: learning from else's experience
The fresh Solanum nigrum of preparatory processing, adding alcoholic strength v/v is that 18% yellow rice wine is mixed thoroughly, bored, is set in frying container, with being fried with slow fire surface
At dark brown, takes out, cool.The fresh Solanum nigrum yellow rice wine 15kg of every 100kg preliminary working.
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: embodiment 2 carries out vinegar toast with rice vinegar, its step are as follows: learning from else's experience
The fresh Solanum nigrum of preparatory processing, aggregation acid content is mixed thoroughly with Acetometer >=5.0g/100ml rice vinegar, bored, sets frying container
It is interior, it fries to fruit surface dark brown, takes out, cool.Vinegar every 100kg fresh Solanum nigrum when processing, with rice vinegar 20kg.
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: embodiment 3 is steamed with wine and is processed, its step are as follows: learning from else's experience preliminary
The fresh Solanum nigrum of processing, adding alcoholic strength v/v is that 15% yellow rice wine is mixed thoroughly, moisturizes, sets and steam in container, with being steam heated to wine quilt
Fresh Solanum nigrum exhausts or fresh Solanum nigrum surface is in yellowish-brown, takes out, slightly dries in the air, mix back steaming liquid, then dries in the air to sixty percent dry, drying.Wine
Every 100kg fresh Solanum nigrum when steaming, with yellow rice wine 30kg.
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: embodiment 4 is steamed with wine and is processed, its step are as follows: learning from else's experience preliminary
The fresh Solanum nigrum of processing, adding alcoholic strength v/v is that 35% white wine is mixed thoroughly, moisturizes, sets and steam in container, with being steam heated to wine quilt
Fresh Solanum nigrum exhausts or fresh Solanum nigrum surface is in yellowish-brown, takes out, slightly dries in the air, mix back steaming liquid, then dries in the air to sixty percent dry, drying.Wine
Every 100kg fresh Solanum nigrum when steaming, with white wine 20kg.
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: embodiment 5 is steamed with vinegar and is processed, its step are as follows: learning from else's experience preliminary
The fresh Solanum nigrum of processing, aggregation acid content are mixed thoroughly with the rice vinegar of Acetometer about 5g/100ml, moisturize, set and steam in container, with steaming
Vapour is heated to that acetic acid is exhausted by fresh Solanum nigrum or fresh Solanum nigrum surface is in yellowish-brown, takes out, slightly dries in the air, mix back steaming liquid, then dry in the air to
Sixty percent is dry, dry.Vinegar every 100kg fresh Solanum nigrum when steaming, with rice vinegar 30kg.
A kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: embodiment 6 is steamed with vinegar and is processed, its step are as follows: learning from else's experience preliminary
The fresh Solanum nigrum of processing, aggregation acid content are mixed thoroughly with the alimentary acetic acid of Acetometer about 10g/100ml, moisturize, set and steam in container,
Acetic acid is exhausted by fresh Solanum nigrum or fresh Solanum nigrum surface is in yellowish-brown with being steam heated to, and is taken out, is slightly dried in the air, mix back steaming liquid, then
It dries in the air to sixty percent dry, drying.Vinegar every 100kg fresh Solanum nigrum when steaming, with alimentary acetic acid 20kg.
Embodiment 7, a kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum: with the fresh Solanum nigrum of preparatory processing
(method of record disclosed in CN2013101104408 is processed, similarly hereinafter) is compared with 4 kinds of Solanum nigrum prepared slices of Chinese crude drugs characters:
Comparison is taken as can be seen that be obviously reduced by the method for the present invention treated Solanum nigrum bitter taste and acid below
Compliance significantly improves.
Embodiment 8, wine steam the Solanum nigrum prepared slices of Chinese crude drugs and take adverse reaction observation
Occur patient 23 of the adverse reactions such as gastric acid stomach cold to the fresh Solanum nigrum of preliminary working is taken, the wine for using embodiment 3 instead steams dragon
Certain herbaceous plants with big flowers fruit continuously takes 5, observes user's adverse reaction, as a result 9 do not occur adverse reaction, and 11 gastric acid stomach colds etc. are bad
Reaction is obviously reduced, and 3 private prosecution adverse reactions are without change.It is fresh to be substantially less than preliminary working for wine steaming Solanum nigrum adverse reaction as the result is shown
Solanum nigrum.
Embodiment 9, the fresh Solanum nigrum of preparatory processing and the 4 kinds of Solanum nigrum prepared slices of Chinese crude drugs (record of embodiment 1,2,3 and 5) methanol
Extraction method and water reflux extraction active principle recovery rate compare, the method is as follows:
It is measured according to high performance liquid chromatography (2015 editions general rules 0512 of Chinese Pharmacopoeia);
Chromatographic condition and system suitability test are using octadecylsilane chemically bonded silica as filler;With acetonitrile -2mmol/L
Na2HPO4 aqueous solution (33:67) is mobile phase;Detection wavelength is 203nm;Number of theoretical plate should be not less than by the calculating of solasonine peak
3000。
The preparation of reference substance solution takes solasonine, solamargine reference substance appropriate, and respectively plus every 1ml is made in methanol
Solution containing 1.0mg to get.
The preparation of test solution
1,5 kinds of sample methanol extract the preparation of test solution
The fresh Solanum nigrum of preliminary working, wine toast Solanum nigrum, vinegar toast Solanum nigrum, wine steaming Solanum nigrum, vinegar is taken to steam Solanum nigrum and (be followed successively by embodiment
1,2,3 and 5 record) etc. five kinds of samples be ground into coarse powder respectively after 80 DEG C are dried under reduced pressure 24 hours, respectively take about 4g precision to claim
It is fixed, it sets in stuffed conical flask, methanol 100ml is added in precision, and weighed weight, is let cool, then weighed 2 hours of heating and refluxing extraction
Weight is supplied the weight of less loss with methanol, is shaken up, and filtration takes subsequent filtrate to obtain the final product.
Each sample prepares 3 parts of test solutions in parallel.
2, the preparation of 5 kinds of sample water refluxing extraction test solutions
The fresh Solanum nigrum of preliminary working, wine toast Solanum nigrum, vinegar toast Solanum nigrum, wine is taken to steam five kinds of samples such as Solanum nigrum, vinegar steaming Solanum nigrum, point
Not after 80 DEG C are dried under reduced pressure 24 hours, it is ground into coarse powder, respectively takes about 4g accurately weighed, sets in round-bottomed flask respectively, water is added to return
Stream extracts 2 times, and 10 times of water are added in volume ratio by weight every time, extract 1 hour every time, merge No. 2 extracting solutions, are concentrated, and water-bath is steamed
It is dry, methanol dissolution is added, sets 100ml volumetric flask constant volume, shakes up, filters, takes subsequent filtrate to obtain the final product.
Each samples prepare 3 parts of test solutions in parallel.
Measuring method is accurate respectively to draw reference substance solution and each 10 μ l of test solution, injects high performance liquid chromatograph, note
Enter liquid chromatograph, measurement to get.Three parts of parallel samples are averaged.
Detection data shows that, through wine toast, vinegar toast, wine steam, vinegar steams the Solanum nigrum after four kinds of techniques process, solasonine adds Australia
The water recovery rate of continent solamargine active principle is all remarkably higher than the fresh Solanum nigrum of preparatory processing.
Claims (10)
1. a kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum, it is characterised in that: this method is processed using wine or vinegar toast, and step is such as
Under: the fresh Solanum nigrum for preparatory processing of learning from else's experience adds appropriate yellow rice wine or rice vinegar to mix thoroughly, bored, sets in frying container, with being fried with slow fire
It takes out, cools at dark brown in surface to obtain the final product.
2. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 1, it is characterised in that: wine every 100kg when processing
The yellow rice wine that fresh Solanum nigrum is added is 10~20kg.
3. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 1 or 2, it is characterised in that: the Huang being added
The alcoholic strength v/v of wine is 15%~20%.
4. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 1, it is characterised in that: vinegar every 100kg when processing
The rice vinegar that fresh Solanum nigrum is added is 20kg~30kg.
5. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 1 or 4, it is characterised in that: the rice vinegar
Total acid content is with Acetometer >=5.0g/100ml.
6. a kind of prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum, it is characterised in that: this method is steamed using wine or vinegar steams, and step is such as
Under: the fresh Solanum nigrum for preparatory processing of learning from else's experience adds yellow rice wine or white wine or rice vinegar or alimentary acetic acid to mix thoroughly, moisturizes, sets and steam in container,
Wine is exhausted by fresh Solanum nigrum or fresh Solanum nigrum surface is in yellowish-brown with being steam heated to, and is taken out, is slightly dried in the air, mix back steaming liquid, then dry in the air
It is dry to sixty percent, it is drying to obtain.
7. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 6, it is characterised in that: wine every 100kg when steaming
The yellow rice wine or white wine 20kg~30kg that fresh Solanum nigrum is added.
8. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 6 or 7, it is characterised in that: the Huang being added
The alcoholic strength v/v of wine is 15%~20%, and the alcoholic strength v/v for the white wine being added is 20%~70%.
9. the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum according to claim 6, it is characterised in that: vinegar every 100kg when steaming
The rice vinegar or alimentary acetic acid that fresh Solanum nigrum is added are 20kg~30kg.
10. according to claim 1 or the prepared slices of Chinese crude drugs concocting method of fresh Solanum nigrum described in 9, it is characterised in that: the rice vinegar
Or alimentary acetic acid total acid content is with Acetometer >=5.0g/100ml.
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Citations (1)
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CN104083522A (en) * | 2013-04-01 | 2014-10-08 | 张锦超 | Processing method of fresh solanum nigrum fruit, solanum nigrum fruit extract particles and use of solanum nigrum fruit extract particles |
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CN104083522A (en) * | 2013-04-01 | 2014-10-08 | 张锦超 | Processing method of fresh solanum nigrum fruit, solanum nigrum fruit extract particles and use of solanum nigrum fruit extract particles |
Non-Patent Citations (1)
Title |
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龚千锋: "《中药炮制学》", 31 August 2016 * |
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Application publication date: 20190308 |