CN109432132A - A kind of concocting method of long-nosed pit viper meat medicine materical crude slice - Google Patents
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice Download PDFInfo
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- CN109432132A CN109432132A CN201811418711.5A CN201811418711A CN109432132A CN 109432132 A CN109432132 A CN 109432132A CN 201811418711 A CN201811418711 A CN 201811418711A CN 109432132 A CN109432132 A CN 109432132A
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- 241000271897 Viperidae Species 0.000 title claims abstract description 97
- 238000000034 method Methods 0.000 title claims abstract description 32
- 239000003814 drug Substances 0.000 title claims abstract description 29
- 235000013372 meat Nutrition 0.000 title claims abstract description 26
- 239000011259 mixed solution Substances 0.000 claims abstract description 30
- 235000019991 rice wine Nutrition 0.000 claims abstract description 28
- 235000021419 vinegar Nutrition 0.000 claims abstract description 28
- 239000000052 vinegar Substances 0.000 claims abstract description 28
- 210000000988 bone and bone Anatomy 0.000 claims abstract description 13
- 238000002224 dissection Methods 0.000 claims abstract description 3
- 238000001035 drying Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 16
- 238000005520 cutting process Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 210000002615 epidermis Anatomy 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 2
- 238000010025 steaming Methods 0.000 description 12
- 238000002474 experimental method Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 241000271039 Agkistrodon Species 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 2
- 235000017491 Bambusa tulda Nutrition 0.000 description 2
- 241001330002 Bambuseae Species 0.000 description 2
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 2
- 210000001015 abdomen Anatomy 0.000 description 2
- 239000011425 bamboo Substances 0.000 description 2
- 230000036461 convulsion Effects 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 235000014101 wine Nutrition 0.000 description 2
- 206010008190 Cerebrovascular accident Diseases 0.000 description 1
- 206010010904 Convulsion Diseases 0.000 description 1
- 241001505404 Deinagkistrodon acutus Species 0.000 description 1
- 206010019468 Hemiplegia Diseases 0.000 description 1
- 241000237903 Hirudo Species 0.000 description 1
- 208000004044 Hypesthesia Diseases 0.000 description 1
- 241001261543 Orthriophis moellendorffi Species 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 208000005392 Spasm Diseases 0.000 description 1
- 208000006011 Stroke Diseases 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 208000034783 hypoesthesia Diseases 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 231100000862 numbness Toxicity 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 206010039073 rheumatoid arthritis Diseases 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/58—Reptiles
- A61K35/583—Snakes; Lizards, e.g. chameleons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Chemical & Material Sciences (AREA)
- Public Health (AREA)
- Life Sciences & Earth Sciences (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Pain & Pain Management (AREA)
- Rheumatology (AREA)
- Biomedical Technology (AREA)
- Neurology (AREA)
- Neurosurgery (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps: (1) take long-nosed pit viper, the bored profit 40-60min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of the yellow rice wine and vinegar is (3-5): 1；The mass ratio of long-nosed pit viper and mixed solution is (10-14): 1；(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, and 5-7min is steamed at 0.01-0.015Mpa, 105-110 DEG C, are taken out long-nosed pit viper, are scaled；(3) continue to steam 15-20min, take out long-nosed pit viper, bone, dissection, it is dry to get.The present invention can shorten the production cycle, and can be easy cutting of boning of scaling, and remove thoroughly lossless long-nosed pit viper epidermis and meat, and ethanol soluble extractives content is high, in addition bored profit is carried out to long-nosed pit viper using vinegar and yellow rice wine mixing to steam, can reduce the bad smell of long-nosed pit viper, improve patient and take mouthfeel.
Description
Technical field
The invention belongs to Chinese medicine production technical fields, and in particular to a kind of concocting method of long-nosed pit viper meat medicine materical crude slice.
Background technique
Long-nosed pit viper is the hirudo leech of Viperidae animal long-noded pit viper Agkistrodon acutus (G ü enther), sweet in flavor, salty, property
Temperature, return liver warp.There is the effect of wind-dispelling, dredging collateral and relieving convulsion.Clinically it is usually used in rheumatoid arthritis stubborn, pruitus, apoplexy deviation of the mouth with numbness and paralysis,
Hemiplegia, the card such as twitch spasm.Long-nosed pit viper is used as medicine first recorded in Lei Gong's Treatise on Preparation and Broiling of Materia Medica, and the name of long-nosed pit viper comes across " herbal guiding principle earliest
Mesh ", release one of name as agkistrodon, 1963 version " Chinese Pharmacopoeia " be still rectification of name with agkistrodon, long-nosed pit viper is infused with bracket white
Flower snake name after, 1977 version " Chinese Pharmacopoeia " using long-nosed pit viper as rectify name, use till today.Long-nosed pit viper mostly captures in summer, two season of autumn, splits
Its abdomen removes internal organ, cleans, struts abdomen with bamboo chip, be coiled into the shape of a disc, and removes bamboo chip after dry.It is distributed mainly on China
Southern area, including Guangdong, Guangxi, Fujian, Hunan, Jiangxi, Yunnan, Guizhou, zhejiang and other places.Long-nosed pit viper is rare and expensive from ancient times
Weight currently belongs to Provincial Key protection wildlife species, and long-nosed pit viper medicinal material mainly originates in Zhejiang at present, based on cultivation.
From 1985 version " Chinese Pharmacopoeia ", three kinds of long-nosed pit viper, long-nosed pit viper meat and wine long-nosed pit viper medicine materical crude slice specifications were recorded under long-nosed pit viper.
It makes a general survey of long-nosed pit viper meat and processes Historic Evolution, it is most representational concocting method that wine, which moistens method,.It is recorded from version Chinese Pharmacopoeia in 1963
Long-nosed pit viper rises so far, is all made of the processing of profit method.Each province and city prepared slices of Chinese crude drugs concocted specification mostly uses profit method, also has and is processed using steaming method
Record also clearly recorded steaming method if Shandong Province's prepared slices of Chinese crude drugs concocted specification (2012) except recording profit method.But it is above to record
Lack specific technological parameter and operation standard, brings very big difficulty to medicine materical crude slice manufacturing enterprise.
Summary of the invention
The object of the invention is that providing a kind of concocting method of long-nosed pit viper meat medicine materical crude slice to solve the deficiencies in the prior art.
The purpose of the present invention is what is realized with following technical proposals:
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 40-60min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of the yellow rice wine and vinegar is
(3-5):1；The mass ratio of long-nosed pit viper and mixed solution is (10-14): 1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.01-0.015Mpa,
5-7min is steamed at 105-110 DEG C, is taken out long-nosed pit viper, is scaled；
(3) continue to steam 15-20min, take out long-nosed pit viper, bone, dissection, it is dry to get.
The degree of yellow rice wine is 14-20 ° in the step (1), and the degree of vinegar is 3.5-5 °.
The long-nosed pit viper disk diameter is 17-34cm.
Drying temperature is 70-80 DEG C in the step (3), and drying is to water content less than 12%.
The step (3) is cut into the section of 20-35mm.
A kind of long-nosed pit viper meat medicine materical crude slice, it is to be prepared using such as any one of claim 1-5 method.
Long-nosed pit viper meat medicine materical crude slice provided by the invention uses after first bored profit with certain high pressure steaming, first steams a period of time and scales
It is further continued for the method for steaming and then boning, the production cycle can be shortened, and cutting of boning of scaling can be easy, and is removed thorough
Lossless long-nosed pit viper epidermis and meat, and ethanol soluble extractives content is high, in addition carries out bored profit to long-nosed pit viper using vinegar and yellow rice wine mixing and steams
System can reduce the bad smell of long-nosed pit viper, improves patient and takes mouthfeel.
Specific embodiment
Embodiment 1
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 40-60min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is (3-
5):1；The mass ratio of long-nosed pit viper and mixed solution is (10-14): 1；Long-nosed pit viper selects size similar, disk diameter 17-34cm, no corruption hair
Mould long-nosed pit viper, the degree of yellow rice wine used are 14-20 °, and the degree of vinegar is 3.5-5 °；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.01-0.015Mpa,
5-7min is steamed at 105-110 DEG C, then takes out long-nosed pit viper, is scaled；
(3) continue to steam 15-20min, take out long-nosed pit viper, bone, be cut into 20-35mm sections, dry, drying temperature is 70-80 DEG C, is done
It is dry to water content less than 12% to get.
Embodiment 2
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 60min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is 4:1；Long-nosed pit viper
Mass ratio with mixed solution is 12:1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, at 0.01Mpa, 105 DEG C
7min is steamed, long-nosed pit viper is taken out, scales；
(3) continue to steam 20min, take out long-nosed pit viper, bone, cut 20-35mm sections, dry, drying temperature is 75 DEG C, dry to aqueous
Amount less than 12% to get.
Embodiment 3
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 50min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is 5:1；Long-nosed pit viper
Mass ratio with mixed solution is 12:1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, at 0.01Mpa, 105 DEG C
7min is steamed, long-nosed pit viper is taken out, scales；
(3) continue to steam 15min, take out long-nosed pit viper, bone, cut 20-35mm sections, dry, drying temperature is 70 DEG C, dry to aqueous
Amount less than 12% to get.
Embodiment 4
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 40min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is 3:1；Long-nosed pit viper
Mass ratio with mixed solution is 14:1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.015Mpa, 110 DEG C
Under steam 5min, take out long-nosed pit viper, scale；
(3) continue to steam 20min, take out long-nosed pit viper, bone, cut 20-35mm sections, dry, drying temperature is 75 DEG C, dry to aqueous
Amount less than 12% to get.
Embodiment 5
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 50min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is 3:1；Long-nosed pit viper
Mass ratio with mixed solution is 10:1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.015Mpa, 108 DEG C
Under steam 6min, take out long-nosed pit viper, scale；
(3) continue to steam 18min, take out long-nosed pit viper, bone, cut 20-35mm sections, dry, drying temperature is 75 DEG C, dry to aqueous
Amount less than 12% to get.
Embodiment 6
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 60min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is 5:1；Long-nosed pit viper
Mass ratio with mixed solution is 12:1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.015Mpa, 105 DEG C
Under steam 6min, take out long-nosed pit viper, scale；
(3) continue to steam 20min, take out long-nosed pit viper, bone, cut 20-35mm sections, dry, drying temperature is 80 DEG C, dry to aqueous
Amount less than 12% to get.
Embodiment 7
A kind of concocting method of long-nosed pit viper meat medicine materical crude slice, comprising the following steps:
(1) long-nosed pit viper is taken, the bored profit 50min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of yellow rice wine and vinegar is 4:1；Long-nosed pit viper
Mass ratio with mixed solution is 12:1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.010Mpa, 107 DEG C
Under steam 7min, take out long-nosed pit viper, scale；
(3) continue to steam 18min, take out long-nosed pit viper, bone, cut 20-35mm sections, dry, drying temperature is 75 DEG C, dry to aqueous
Amount less than 12% to get.
Test example
It is found by preliminary experiment, the ratio of yellow rice wine and vinegar is affected to medicine materical crude slice bad smell, and steaming temperature steams pressure and steams
Time, complexity of boning, ethanol soluble extractives content were affected, therefore this experiment is with yellow rice wine and vinegar to complexity of scaling
Ratio a, steaming time b, steaming temperature c and steam pressure d be investigation factor, to scale, complexity A(total score 20 is divided；Hold
Easily scale 20 points；It is easier to scale 10 points；It is difficult to scale 0 point), complexity of boning B(total score 20 divides, is easy to bone 20 points；It is easier to
Bone 10 points, be difficult to bone 0 point), cutting complexity C(total score 20 divide, be easy cutting 20 divide；It can cut, 10 points；It is difficult cutting,
0 point), ethanol soluble extractives content D(take sample 3.00g, it is accurately weighed, according to Chinese Pharmacopoeia ethanol soluble extractives measuring method-heat
The measurement of leaching method；Ethanol soluble extractives content is greater than 15%, 20 points；Ethanol soluble extractives content is greater than 13%, 10 points；Alcohol-soluble leaches
Object content is greater than 11%, 5 points；Ethanol soluble extractives content is less than 10%, 0 point) and the deep or light E(total score 20 of bad smell divide；It is slightly stench
Taste 20 divides；There is a bad smell, 10 points；Bad smell is dense, and 0 point) it is Score index, so that it is determined that the processing procedure of long-nosed pit viper meat medicine materical crude slice
Parameter.Orthogonal test factor level table is shown in Table 1, the results are shown in Table 2.
As known from Table 2, as a result best for a2b2c2d1, i.e. the ratio of yellow rice wine and vinegar is 4:1,105 DEG C of steaming temperature, is steamed
Pressing pressure 0.1Mpa, steaming time 30min be it is best, verification test comprehensive score be 92, and the experiment proved that, steaming 5-
It can be easy to scale when 7min, scale again when steaming 30min and be easy to damage epidermis, therefore, finally determination first steams 5-7min,
Taking-up is further continued for steaming 15-20min after scaling.
Claims (6)
1. a kind of concocting method of long-nosed pit viper meat medicine materical crude slice, it is characterised in that the following steps are included:
(1) long-nosed pit viper is taken, the bored profit 40-60min of mixed solution of yellow rice wine and vinegar is added in decaptitating；The volume ratio of the yellow rice wine and vinegar is
(3-5):1；The mass ratio of long-nosed pit viper and mixed solution is (10-14): 1；
(2) long-nosed pit viper and mixed solution after taking bored profit, are placed in high-pressure bottle, are heated with vapor, in 0.01-0.015Mpa,
5-7min is steamed at 105-110 DEG C, is taken out long-nosed pit viper, is scaled；
(3) continue to steam 15-20min, take out long-nosed pit viper, bone, dissection, it is dry to get.
2. the concocting method of long-nosed pit viper meat medicine materical crude slice as described in claim 1, it is characterised in that the degree of yellow rice wine in the step (1)
It is 14-20 °, the degree of vinegar is 3.5-5 °.
3. the concocting method of the long-nosed pit viper meat medicine materical crude slice as described in claim 1, it is characterised in that the long-nosed pit viper disk diameter is 17-34cm.
4. the concocting method of long-nosed pit viper meat medicine materical crude slice as described in claim 1, it is characterised in that drying temperature in the step (3)
It is 70-80 DEG C, drying is to water content less than 12%.
5. the concocting method of long-nosed pit viper meat medicine materical crude slice as described in claim 1, it is characterised in that the step (3) is cut into 20-35mm
Section.
6. a kind of long-nosed pit viper meat medicine materical crude slice, it is characterised in that it is to be prepared using such as any one of claim 1-5 method.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115154499A (en) * | 2022-06-20 | 2022-10-11 | 江西大自然制药有限公司 | Preparation method of agkistrodon medicinal liquor |
Citations (2)
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|---|---|---|---|---|
| CN1899354A (en) * | 2006-07-14 | 2007-01-24 | 河南中医学院 | Method for processing dogwood fruit wite white spirit |
| CN108186708A (en) * | 2018-03-19 | 2018-06-22 | 北京杏林药业有限责任公司 | A kind of wine-prepared fructus corni processing procedure |
-
2018
- 2018-11-26 CN CN201811418711.5A patent/CN109432132A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1899354A (en) * | 2006-07-14 | 2007-01-24 | 河南中医学院 | Method for processing dogwood fruit wite white spirit |
| CN108186708A (en) * | 2018-03-19 | 2018-06-22 | 北京杏林药业有限责任公司 | A kind of wine-prepared fructus corni processing procedure |
Non-Patent Citations (1)
| Title |
|---|
| 国家药典委员会: "蕲蛇", 《中国药典2015年版》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115154499A (en) * | 2022-06-20 | 2022-10-11 | 江西大自然制药有限公司 | Preparation method of agkistrodon medicinal liquor |
| CN115154499B (en) * | 2022-06-20 | 2023-07-21 | 江西大自然制药有限公司 | Preparation method of agkistrodon medicated wine |
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