CN109431837A - A kind of moisturizing beauty paper handkerchief and preparation method thereof - Google Patents
A kind of moisturizing beauty paper handkerchief and preparation method thereof Download PDFInfo
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- CN109431837A CN109431837A CN201811423055.8A CN201811423055A CN109431837A CN 109431837 A CN109431837 A CN 109431837A CN 201811423055 A CN201811423055 A CN 201811423055A CN 109431837 A CN109431837 A CN 109431837A
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- paper handkerchief
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Paper (AREA)
Abstract
The present invention discloses a kind of moisturizing beauty paper handkerchief, it is related to daily necessities field, lack beauty and health care function based on existing paper product, antibacterial effect is poor, and the problem of condensation phenomenon easily occurs for emulsion compositions during the preparation process and propose, the present invention includes paper handkerchief and emulsion compositions, the emulsion compositions are mainly by moisturizer 30%-50%, sodium hyaluronate 0.01%-0.1%, γ-aminobutyric acid 0.01%-0.1%, surfactant 1%-5%, nano zine oxide 1%-10%, softening agent 5%-20%, deionized water 20%-40% composition, the present invention also provides the preparation methods of above-mentioned flexible towelette, the following steps are included: preparing emulsion compositions, coating, curing；The beneficial effects of the present invention are: preparation process is simple, cost is relatively low, and flexible towelette obtained has good hydrophily, absorbability, moisture retention, pliability and fluffy sense are preferable, there is preferable fungistatic effect, have the function of certain skin beauty and health care simultaneously, there is enhancing skin elasticity, anti-aging function.
Description
Technical field
The present invention relates to daily necessities fields, and in particular to a kind of moisturizing beauty paper handkerchief and preparation method thereof.
Background technique
With the improvement of living standards and to the deep understanding that ambient enviroment adverse factor adversely affects human body, people's
Consciousness of keeping a public place clean is gradually increased, and paper has become necessity for people's lives.
On manpower, the scurf etc. of dust and human body in the sweat and air of people together forms dirt.In dirt
On have accumulated a large amount of microorganism, wherein just having some may be sex pheromone, these bring people's health certain
It threatens.Especially some frequent carry out outdoor activists, due to the limitation of sanitary condition, dirt is more on hand skin, gathers above
A large amount of microorganism is collected, wherein may have some is pathogenic microorganism.And in daily life common paper hardness compared with
Greatly, and after the symptoms such as dry skin are easily caused, existing paper handkerchief has a single function, paper is easily layered, while paper
Antibacterial effect is poor, easily goes mouldy, and during the preparation process, and easily there is a phenomenon where condensations for emulsion compositions.
Summary of the invention
The problem to be solved by the present invention is that existing paper handkerchief antibacterial effect is poor, lack beauty and health care function, and making
Condensation phenomenon easily occurs for emulsion compositions during standby.
The present invention adopts the following technical solutions solves above-mentioned technical problem:
A kind of moisturizing beauty paper handkerchief, including paper handkerchief and emulsion compositions, the emulsion compositions are mainly by moisturizer 30%-
50%, sodium hyaluronate 0.01%-0.1%, γ-aminobutyric acid 0.01%-0.1%, surfactant 1%-5%, nano zine oxide
1%-10%, softening agent 5%-20%, deionized water 20%-40% composition.
It preferably, further include 0.1% defoaming agent in the emulsion compositions.
Preferably, the defoaming agent is polyethers defoaming agent or organic silicon defoaming agent.
Preferably, the moisturizer is polyhydroxy alcohols.
Preferably, the softening agent is polysiloxanes.
Preferably, the surfactant is neopelex, sodium cetanesulfonate, polyoxyethylene polyols
One of ether, polyoxyethylene aliphatic alcohol ether, polyoxyethylene nonylphenol ether are a variety of.
The present invention also provides a kind of preparation methods of moisturizing beauty paper handkerchief, comprising the following steps:
(1) sodium hyaluronate and deionized water are added in reaction kettle, stirring is configured to colloidal sol, adds moisturizer, γ-ammonia
Base butyric acid, surfactant, softening agent, nano zine oxide, defoaming agent, stirring, are configured to emulsion compositions；
(2) the emulsion compositions addition prepared in step (1) is applied on paper handkerchief, the rate of sizing is the 10%- of paper handkerchief
30%；
(3) paper handkerchief after coating is wound, and cures its naturally osmotic, made in paper handkerchief internal moisture and air
Moisture reaches balance, then is cut, packed to get moisturizing beauty paper handkerchief is arrived.
Preferably, the moisturizer is polyhydroxy alcohols.
Preferably, the softening agent is polysiloxanes.
Preferably, the surfactant is neopelex, sodium cetanesulfonate, polyoxyethylene polyols
One of ether, polyoxyethylene aliphatic alcohol ether, polyoxyethylene nonylphenol ether are a variety of.
Preferably, every square metre of the paper obtained is evenly distributed with the gamma-amino fourth of 2-10mg sodium hyaluronate, 2-10mg
Acid, 0.1-0.5g polysiloxanes, 0.2-0.6g polyhydroxy alcohols, 0.02-0.1g surfactant.
The beneficial effects of the present invention are:
(1) preparation process of the invention is simple, and cost is relatively low, and paper handkerchief obtained has good hydrophily, absorbability,
Pliability and fluffy sense are preferable simultaneously；
(2) bacteriostatic agent used in preparation process of the present invention is nano zine oxide, nano zine oxide and other Emulsion combinations
Object intermiscibility is preferable, and paper handkerchief has good antibacterial effect, inhibits fungi, prevents from going mouldy；
(3) moisturizing beauty paper handkerchief moisture retention prepared by the present invention is good and is not easy to be layered, and can prevent chapped skin, have simultaneously
Skin beauty and health care function has enhancing skin elasticity, anti-aging function.
Specific embodiment
The present invention is described in further details below with reference to embodiment.
Test material and reagent as used in the following examples etc., unless otherwise specified, commercially obtain,
Middle nano zine oxide can also be commercially available from domestic and international market.
Embodiment 1
The different ratio of emulsion compositions is as shown in table 1 in moisturizing beauty paper handkerchief:
| It is formulated (%) | One | Two | Three |
| Sodium hyaluronate | 0.050 | 0.025 | 0.050 |
| γ-aminobutyric acid | 0.050 | 0.050 | 0.050 |
| Polysiloxanes | 10 | 12 | 12 |
| Glycerine | 50 | 50 | 50 |
| Polyoxyethylene glycerol ether | 3 | 3 | 3 |
| Nano zine oxide | 3 | 3 | 3 |
| Defoaming agent | 0.1 | 0.1 | 0.1 |
| Water | 33.8 | 31.825 | 31.8 |
Sodium hyaluronate and γ-aminobutyric acid have the function of improve paper handkerchief hydrophily and absorbability, make paper handkerchief humidity-preserving type compared with
It is good, especially have beauty and health care function.
Due to there is surfactant in emulsion compositions, rear extended meeting generates many foams, therefore need to attach defoaming agent.
Embodiment 2
A kind of preparation method of moisturizing beauty paper handkerchief, comprising the following steps:
(1) 0.01% solid sodium hyaluronate and 49.79% deionized water are added in reaction kettle, stir 12h, is configured to transparent
Homogeneous sol after, add 0.1% γ-aminobutyric acid, 5% polyoxyethylene polyols ether, 10% polysiloxanes, 30% the third
Triol, 5% nano zine oxide, 0.1% polyethers defoaming agent stir 1h, are configured to emulsion compositions；Due to emulsion compositions
In have a surfactant, rear extended meeting generates many foams, therefore need to attach defoaming agent；
(2) the emulsion compositions addition prepared in step (1) is applied on paper handkerchief, the rate of sizing is the 20% of paper handkerchief；
(3) paper handkerchief after coating is wound, and makes the curing of its naturally osmotic for 24 hours, make paper handkerchief internal moisture and air
In moisture reach balance, then cut, packed to get to moisturizing beauty paper handkerchief.
Wherein, the coating method of emulsion compositions is the prior art.
Embodiment 3
A kind of preparation method of moisturizing beauty paper handkerchief, comprising the following steps:
(1) 0.01% solid sodium hyaluronate and 46.79% deionized water are added in reaction kettle, stir 12h, is configured to transparent
Homogeneous sol after, add 0.1% γ-aminobutyric acid, 5% polyoxyethylene polyols ether, 10% polysiloxanes, 30% the third
Triol, 8% nano zine oxide, 0.1% polyethers defoaming agent stir 1h, are configured to emulsion compositions；
(2) the emulsion compositions addition prepared in step (1) is applied on paper handkerchief, the rate of sizing is the 10% of paper handkerchief；
(3) paper handkerchief after coating is carried out, winding, and makes the curing of its naturally osmotic for 24 hours, make paper handkerchief internal moisture and air
In moisture reach balance, then cut, packed to get to moisturizing beauty paper handkerchief.
Wherein, the coating method of emulsion compositions is the prior art.
The range of viscosities of emulsion compositions is conducive to the coating of emulsion compositions between 30mPas-100mPas,
Since sodium hyaluronate colloidal sol has very high viscosity, 1% sodium hyaluronate dissolved adhesiveness can reach 300mPas, therefore can be by adjusting
The dosage of deionized water adjusts the viscosity of emulsion compositions.
The bacteriostasis rate of product in embodiment 2 and embodiment 3 is detected, submitted sample and control sample are cut into
50mm × 50mm size is detected according to GB T 31402-2015 plastics frosting Anti-microbial Performance Tests method.
Testing result is as shown in table 2:
As can be seen from Table 2, when containing 5% or 8% nano zine oxide in paper handkerchief, paper handkerchief obtained has good anti-
Bacterium effect.The selection of bacteriostatic agent should consider fungistatic effect, also to consider the compatibility with emulsion compositions, prevent colloidal sol
Condensation.A variety of bacteriostatic agents, such as polyhexamethylene guanide, Bronopol, isothiazolinone are used in experimentation, it is above-mentioned antibacterial
There is condensation phenomenon after mixing with the sol solution containing sodium hyaluronate in agent, in the present embodiment with nano zine oxide its with contain glass
The emulsion compositions compatibility of uric acid colloidal sol is preferable, while having very strong fungistatic effect to bacterium, moreover it is possible to inhibit fungi, make paper
Towel is not susceptible to go mouldy, and wherein the partial size of nano zine oxide is 15nm.
Embodiment 4
The influence of polysiloxanes, glycerine, polyoxyethylene glycerol ether content to product physical property in emulsion compositions:
Table 3 is influence of the polysiloxane level to product physical property
From table 3 it is observed that polysiloxane level influences the pliability and intensity of paper handkerchief, when its content is greater than 14%
When, the lateral tensile index of paper will be less than 1.2Nm/g, and paper is easily broken in use；When content is less than 6%
When, pliability will be greater than 56mN, while paper handkerchief can seem stiffening and coarse；Therefore, polysiloxane level should be in 6%- in paper handkerchief
Between 14%.When content is between 10%-12%, the pliability of paper handkerchief will in 40mN hereinafter, and lateral tensile index will be big
In 1.5Nm/g.
Table 4 is influence of the glycerol content to product physical property
By the processed obtained paper handkerchief of sili-cone surfaces, the hydroxyl value on paper fibre element surface itself can reduce, make
Hyarogen-bonding weakens between obtaining cellulosic molecule, and the adsorption capacity between each layer paper handkerchief can reduce, and paper handkerchief is easy layering；Polyalcohol
Hyarogen-bonding is easily formed between hydroxyl and hydrone, therefore polynary alcohol and water has fabulous compatibility and water imbibition, potentially acts as
Moisturizer；Polyalcohol can absorb the moisture in environment, and saves it in the surface of paper, and paper is made to have damp, soft and moist
Property gets a promotion；Meanwhile polyalcohol, in paper surface, the hydroxyl value of paper surface increases naturally, the absorption between each layer paper handkerchief
Power will be improved, and paper is made to be not easy to be layered.
When glycerine is when paper surface content is less than 30%, paper hygroscopicity is poor, soft and moist property is bad, and easily layering；When
Glycerine is excessive in paper surface content, and when more than 60%, adsorption capacity rises and is closely adsorbed on one between each layer paper handkerchief
It rises, so that paper handkerchief loses original fluffy sense.
Table 5 is influence of the polyoxyethylene glycerol ether to product physical property
Since polysiloxane soft agent reduces the surface tension of paper fibre element, so that water is not easy to spread in paper surface
The hydrophily of exhibition, paper reduces, and therefore, surfactant is added in the lotion containing polysiloxane soft agent, and add poly-
The effect of ethylene oxide glycerin ether is best.
When the content of polyoxyethylene glycerol ether is less than 1%, the hydrophilicity of paper handkerchief cannot preferably improve, and be more than
When 4%, the absorption speed of paper handkerchief is without improved space.
The above is only the preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-described embodiment,
It is within the scope of the invention with present inventive concept without the various process programs of substantial differences.
Claims (10)
1. a kind of moisturizing beauty paper handkerchief, including paper handkerchief and emulsion compositions, it is characterised in that: the emulsion compositions are mainly by protecting
Humectant 30%-50%, it sodium hyaluronate 0.01%-0.1%, γ-aminobutyric acid 0.01%-0.1%, surfactant 1%-5%, receives
Rice zinc oxide 1%-10%, softening agent 5%-20%, deionized water 20%-40% composition.
2. moisturizing beauty paper handkerchief according to claim 1, it is characterised in that: further include 0.1% in the emulsion compositions
Defoaming agent.
3. moisturizing beauty paper handkerchief according to claim 1, it is characterised in that: the moisturizer is polyhydroxy alcohols.
4. moisturizing beauty paper handkerchief according to claim 1, it is characterised in that: the softening agent is polysiloxanes.
5. moisturizing beauty paper handkerchief according to claim 1, it is characterised in that: the surfactant is detergent alkylate sulphur
Sour sodium, sodium cetanesulfonate, polyoxyethylene polyols ether, polyoxyethylene aliphatic alcohol ether, one in polyoxyethylene nonylphenol ether
Kind is a variety of.
6. preparing the preparation method of moisturizing beauty paper handkerchief according to any one of claims 1 to 5, it is characterised in that: including with
Lower step:
(1) sodium hyaluronate and deionized water are added in reaction kettle, stirring is configured to colloidal sol, adds moisturizer, gamma-amino fourth
Acid, surfactant, softening agent, nano zine oxide, defoaming agent, stirring, are configured to emulsion compositions；
(2) the emulsion compositions addition prepared in step (1) is applied on paper handkerchief, the rate of sizing is the 10%-30% of paper handkerchief；
(3) paper handkerchief after coating is wound, and cures its naturally osmotic, make the moisture in paper handkerchief internal moisture and air
Reach balance, then is cut, packed to get moisturizing beauty paper handkerchief is arrived.
7. the preparation method of moisturizing beauty paper handkerchief according to claim 6, it is characterised in that: the moisturizer is polyhydroxy
Alcohols.
8. the preparation method of moisturizing beauty paper handkerchief according to claim 6, it is characterised in that: the softening agent is poly- silicon oxygen
Alkane.
9. the preparation method of moisturizing beauty paper handkerchief according to claim 6, it is characterised in that: the surfactant is ten
One of dialkyl benzene sulfonic acids sodium, sodium cetanesulfonate, polyoxyethylene polyols ether, polyoxyethylene aliphatic alcohol ether are more
Kind.
10. the preparation method of moisturizing beauty paper handkerchief according to claim 6, it is characterised in that: the paper handkerchief obtained is every
It is more square metre to be evenly distributed with 2-10mg sodium hyaluronate, the γ-aminobutyric acid of 2-10mg, 0.1-0.5g polysiloxanes, 0.2-0.6g
Hydroxy alcohols, 0.02-0.1g surfactant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811423055.8A CN109431837A (en) | 2018-11-27 | 2018-11-27 | A kind of moisturizing beauty paper handkerchief and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811423055.8A CN109431837A (en) | 2018-11-27 | 2018-11-27 | A kind of moisturizing beauty paper handkerchief and preparation method thereof |
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| CN109431837A true CN109431837A (en) | 2019-03-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811423055.8A Pending CN109431837A (en) | 2018-11-27 | 2018-11-27 | A kind of moisturizing beauty paper handkerchief and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114182571A (en) * | 2020-09-15 | 2022-03-15 | 刘训林 | Pearl amino acid paper towel and preparation method thereof |
| CN114345492A (en) * | 2021-12-27 | 2022-04-15 | 深圳市金阳盛城市服务集团有限公司 | Intelligent garbage treatment equipment and garbage treatment method |
| CN114983833A (en) * | 2021-07-31 | 2022-09-02 | 铜陵天天纸品科技有限公司 | Wet and smooth cream paper and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103061204A (en) * | 2012-10-26 | 2013-04-24 | 福建恒安集团有限公司 | Soft paper subjected to surface preparation |
| CN103417154A (en) * | 2013-07-26 | 2013-12-04 | 广州联庄科技有限公司 | Mobile-phone antibacterial cleaning wet tissue |
| CN105951506A (en) * | 2016-05-19 | 2016-09-21 | 唐山冀东石墨烯科技发展有限公司 | Antibacterial paper and preparation method thereof |
-
2018
- 2018-11-27 CN CN201811423055.8A patent/CN109431837A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103061204A (en) * | 2012-10-26 | 2013-04-24 | 福建恒安集团有限公司 | Soft paper subjected to surface preparation |
| CN103417154A (en) * | 2013-07-26 | 2013-12-04 | 广州联庄科技有限公司 | Mobile-phone antibacterial cleaning wet tissue |
| CN105951506A (en) * | 2016-05-19 | 2016-09-21 | 唐山冀东石墨烯科技发展有限公司 | Antibacterial paper and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114182571A (en) * | 2020-09-15 | 2022-03-15 | 刘训林 | Pearl amino acid paper towel and preparation method thereof |
| CN114983833A (en) * | 2021-07-31 | 2022-09-02 | 铜陵天天纸品科技有限公司 | Wet and smooth cream paper and preparation method thereof |
| CN114983833B (en) * | 2021-07-31 | 2023-12-01 | 铜陵天天纸品科技有限公司 | Wet-slip cream paper and preparation method thereof |
| CN114345492A (en) * | 2021-12-27 | 2022-04-15 | 深圳市金阳盛城市服务集团有限公司 | Intelligent garbage treatment equipment and garbage treatment method |
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