CN109430296A - A kind of Chinese medicine composition for preventing and treating ginseng store pest - Google Patents
A kind of Chinese medicine composition for preventing and treating ginseng store pest Download PDFInfo
- Publication number
- CN109430296A CN109430296A CN201910015943.4A CN201910015943A CN109430296A CN 109430296 A CN109430296 A CN 109430296A CN 201910015943 A CN201910015943 A CN 201910015943A CN 109430296 A CN109430296 A CN 109430296A
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- China
- Prior art keywords
- chinese medicine
- medicine composition
- parts
- ginseng
- composition
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The present invention relates to a kind of for preventing and treating the Chinese medicine composition of ginseng store pest, and the composition includes the traditional Chinese medicinal components of following parts by weight: 1-3 parts of asarum, 2-4 parts of Chinese prickly ash, 1-3 parts of lemon, and the Chinese medicine composition is above-mentioned Chinese medicine supercritical extract；Chinese medicine composition of the invention has apparent insecticidal action, can be used for repellent, stifling, the non-residual toxicity of ginseng store pest, the prevention and treatment of suitable ginseng store pest, abundant raw material, simple production process, production cost is low, is expected to exploitation into green bio pesticide.
Description
Technical field
The invention belongs to Chinese medicine storage production technical fields more particularly to a kind of for preventing and treating in ginseng storage pest
Drug composition, the composition are Chinese medicine supercritical extracts.
Background technique
Ginseng is your thin invigorant medicinal material, and many pests are all liked with ginseng for food.According to more than ten a provinces and cities' investigation, people is endangered
The storage pest of ginseng has 2 mesh, and 13 sections, 19 kinds, wherein red flour beetle and lasioderma serricorne etc. are dominant population.Since pest is caused harm, make
Riddled with gaping wounds at ginseng, inside is eaten hollow, becomes disintegrating slag, powder, and larva can spin winding, agglomeration bunchiness, live on trees in or change
Pupa produces offspring, and ginseng is made to lose medical value completely, it is annual caused by economic loss reach several hundred million members.
The pest and disease damage of Chinese medicine storage at present uses long-term, excessive use based on the stifling chemical preventions such as sulphur, aluminum phosphate
Chemical pesticide causes the problems such as residual exceeded, the pest resistance to insecticide increase of agriculture and environmental pollution, and bring Chinese medicine safety problem also causes
Extensive concern.And antagonistic storage be can be risen using having special odor expelling parasite mildew-proof function medicinal material (fight medicinal material) and
Easily infested mouldy medicinal material (with storage medicinal material) coexists to reach the method for Vermins-proof mildew-proof, be Chinese medicine storage and maintenance classical way it
One, it is the accumulation of our people's long-term practical experience and summary.It is inspired by this, the research that people prevent and treat Chinese medicine storage pest is
It is gradually transferred to from natural plants and looks for pest-resistant ingredient, develop in Green Protection agent, meet the environmentally protective trend in the world
Trend has great importance to promotion traditional Chinese medicine sustainable development and internationalization.
Summary of the invention
The present invention is a kind of Chinese medicine composition, is made of, can use the Chinese medicine supercritical extract of asarum, Chinese prickly ash, lemon
In prevention and treatment ginseng store pest.
The purpose of the present invention is to provide a kind of Chinese medicine compositions for having fine control efficiency to main ginseng store pest.
The composition has efficient, low toxicity, low-residual, low cost, green safe characteristic, and is suitable for the anti-of ginseng store pest
It controls.
The object of the invention is also to provide the preparation methods of above-mentioned Chinese medicine composition, in this way, can be used for
Prevent and treat the stable pharmaceutical composition of significant effect, sophisticated technologies, the quality of ginseng store pest.
The object of the invention is also to provide the purposes of the prevention and treatment ginseng store pest of pharmaceutical composition among the above.
In order to achieve the above object, the present invention provides a kind of Chinese medicine composition, the composition includes following parts by weight
Traditional Chinese medicinal components: 1~3 part of asarum, 2~4 parts of Chinese prickly ash, 1~3 part of lemon, the Chinese medicine composition are faced by above-mentioned Chinese medicine is super
Boundary's extract composition.
The dosage form of above-mentioned Chinese medicine composition is preferably repellant and fumigant, and the acceptable auxiliary material is ethyl alcohol, described
The weight of acceptable auxiliary material accounts for the 20~95% of the drug weight.
The present invention provides the preparation methods of the Chinese medicine composition of prevention and treatment Associated With Stored Chinese Medicinal Materials pest, comprise the steps of:
The medicinal materials such as asarum, Chinese prickly ash and lemon are weighed respectively according to above-mentioned weight proportion, are crushed in postposition supercritical extraction reactor,
First extraction kettle, separating still are preheated, basin is cooled down, and when reaching predetermined temperature, opens CO2Gas cylinder is supplied gas, and is opened
High-pressure pump boosting starts the cycle over extraction when temperature, pressure reach predetermined value, when extraction fixedly separated pressure 5.0~
6.0MPa, 50 DEG C of separation temperature, discharging is added acceptable auxiliary material, is made smoked after constant temperature and pressure extracts 1h to get extract is arrived
Steam agent or repellant.
Preparation is placed in storage ginseng Chinese medicine by product of the present invention using simply.This product is a kind of Chinese medicine group
Object is closed, nature volatilization can be carried out, it is possible to reduce workload saves cost of labor, plays the role of Green Protection.
Specific embodiment
Illustrate goal of the invention and technical solution in order to apparent, is described in further detail by following embodiments.
Embodiment:
1, composition prescription:
Asarum 500g Chinese prickly ash 1000g lemon 500g
2, prepared by supercritical extract:
The above three tastes Chinese medicine crushes in postposition extraction kettle, first preheats to extraction kettle, separating still, and basin is cooled down,
When reaching predetermined temperature, CO is opened2Gas cylinder is supplied gas, and opens high-pressure pump boosting, when temperature, pressure reach predetermined value, is started
Cycling extraction, when extraction fixedly separated 5.0~6.0MPa of pressure, 50 DEG C of separation temperature, constant temperature and pressure extract after 1h discharging to get
It is spare to extract 300g.
3, prepared by fumigant:
Supercritical extract 10.0g beta-cyclodextrin 10.0g ethyl alcohol 20.0g
Supercritical extract 10.0g is taken, ethyl alcohol 20.0g is uniformly mixed, spare.Separately take beta-cyclodextrin 10.0g that 60g water is added
Above-mentioned supercritical extract solution is added in middle dissolution, continues to stir 12h, emulsion is made, bottle, be re-filled with a certain amount of pressure
Spray is made to get fumigant in contracting nitrogen and butane, sealing.
4, prepared by repellant:
- 40 5.0g gellan gum 1.0g ethyl alcohol 10.0g of supercritical extract 10.0g rilanit special
Supercritical extract 10.0g is taken, ethyl alcohol 10.0g is uniformly mixed with materials such as -40 5.0g of rilanit special, spare.
It separately takes gellan gum 1.0g that water 75g is added to heat (90~100 DEG C) dissolutions and colloidal solution is made, by means of supercritical extraction at 50~60 DEG C
Object mixed solution be added, mix, it is filling, it is to be solidified after to get arrive gel type solid repellant.
5, function and effect experimental study:
The test of 5.1 fumigation activities
Composition tests reference literature the method to the fumigation activity of red flour beetle and lasioderma serricorne[1]: select emergence one week
10 test worms are put into diameter 2.5cm by the adult of left and right, in the vial of high 5.5cm, prepare 5 not according to preliminary result
With the composition n-hexane dilution of concentration, 10 μ L dilution drop then is drawn on the filter paper in bottle cap, separately with liquid-transfering gun
It takes untreated filter paper that n-hexane is added dropwise to compare.Bottle cap is tightened after administration rapidly, sealing sealing is wound with sealed membrane, forms one
Confined space, bottleneck are coated with polytetrafluoroethylene (PTFE) (Floun), prevent from touching the filter paper containing medicament for examination insect.Red flour beetle by
In more sensitive to solvent, after delivering medicine on filter paper, needing to volatilize solvent is sealed again after 20s.Each concentration repeats 5
It is secondary, 10 test worms of each repetition.
It is (29 ± 1) DEG C that control group and processing group, which are placed in temperature, and relative humidity is the constant incubator of (75 ± 5) %
For 24 hours, the death condition of observation and record test worm calculates LC for middle culture50Value.LC50Value presses literature method[2]Using Probit (IBM
SPSS V20.0) analytical calculation.
Laboratory sample: the composition of the embodiment of the present invention；
Positive reference substance: bromomethane, hydrogen phosphide, DDVP；
It the results are shown in Table 1.
Fumigation activity of 1 composition of table to red flour beetle and lasioderma serricorne
The test of 5.2 repellent activities
Composition tests reference literature the method to the repellent activity of red flour beetle and lasioderma serricorne[3], it is 9cm by diameter
Circular filter paper from centre cut out be two halves, with liquid-transfering gun draw 500 μ L composition n-hexane dilutions, (setting 5 concentration be
78.63,15.73,3.15,0.63 and 0.13nL/cm2, 5 repetitions of each concentration) drop on wherein half filter paper, the other half
Use the processing of blank solvent n-hexane as control, after volatilizing naturally, being pasted onto culture dish bottom in opposite directions with solid gum, (ware wall is coated
Polytetrafluoroethylene (PTFE)), 20 test worms are poured into culture dish center, are closed the lid.Processing group and control group when observing and recording 2h and 4h
The distribution situation of test worm on filter paper calculates scattering ratio PR (%), and formula is as follows:
PR (%)=[(Nc-Nt)/(Nc+Nt)] × 100
Nc is the quantity of test worm on control group filter paper, and Nt is the quantity of test worm on processing group filter paper.
Laboratory sample: the composition of the embodiment of the present invention；
Positive reference substance: Metadelphene；
It the results are shown in Table 2.
2 composition of table is in 2h and 4h to the scattering ratio (PR% ± SE) of red flour beetle and lasioderma serricorne
Conclusion: the above experimental result shows that the present composition has ginseng storage pest red flour beetle and lasioderma serricorne etc.
There are preferable repellent and fumigation activity, prompts that there is fabulous control efficiency to ginseng storage pest.
In conclusion the invention has the following advantages that
1, the method for the present invention, abundant raw material, simple production process, production cost are low.
2, purposes of the present invention is the prevention and treatment of ginseng storage pest, to ginseng crude drug's storage pest red flour beetle and lasioderma serricorne
Etc. there is fabulous stifling and repellent action.
3, the present invention has the characteristic of efficient green safety, is expected to exploitation into Green Protection agent.
The foregoing describe the preferred embodiment for the present invention, and however, it is not to limit the invention.Those skilled in the art couple
Embodiment disclosed herein can carry out the improvements and changes without departing from scope and spirit.
Bibliography
[1]Wang CF,Yang K,Zhang HM,Cao J,Fang R,Liu ZL,Du SS,Wang YY,Deng ZW,
Zhou LG.Components and insecticidal activity against the maize weevils of
Zanthoxylum schinifolium fruits and leaves[J].Molecules, 2011,16(4):3077-
3088.
[2]Sakuma M.Probit analysis of preference data[J].Applied Entomology
and Zoology.1998,33:339-347
[3]Liu ZL,Yu M,Li XM,Wan T,Chu SS.Repellent activity of eight
essential oils of Chinese medicinal herbs to Blattella germanica L[J].Records
of Natural Products,2011,5(3):176-183。
Claims (3)
1. a kind of Chinese medicine composition, the composition includes the traditional Chinese medicinal components of following parts by weight: 1-3 parts of asarum, 2-4 parts of Chinese prickly ash, lemon
1-3 parts of lemon, the Chinese medicine composition is above-mentioned Chinese medicine supercritical extract.
2. the preparation method of Chinese medicine composition as described in claim 1, it is characterised in that comprise the steps of:
According to above-mentioned weight proportion weigh respectively asarum, Chinese prickly ash, lemon Chinese medicine, crush postposition extraction kettle in, first to extraction
Kettle, separating still are preheated, and basin is cooled down, and when reaching predetermined temperature, open CO2Gas cylinder is supplied gas, and opens high-pressure pump liter
Pressure starts the cycle over extraction when temperature, pressure reach predetermined value, when extraction fixedly separated pressure 5.0-6.0MPa, separation temperature
50 DEG C, discharging is added pharmaceutically acceptable auxiliary material, fumigant or drive is made after constant temperature and pressure extracts 1h to get extract is arrived
Keep away agent.
3. application of the Chinese medicine composition described in claim 1 in prevention and treatment ginseng store pest.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811007505 | 2018-08-31 | ||
| CN2018110075055 | 2018-08-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109430296A true CN109430296A (en) | 2019-03-08 |
Family
ID=65544006
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910015943.4A Pending CN109430296A (en) | 2018-08-31 | 2019-01-08 | A kind of Chinese medicine composition for preventing and treating ginseng store pest |
Country Status (1)
| Country | Link |
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| CN (1) | CN109430296A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113002999A (en) * | 2021-03-25 | 2021-06-22 | 生态环境部南京环境科学研究所 | Storage device and method for pseudo-ginseng medicinal materials |
Citations (3)
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|---|---|---|---|---|
| CN102640765A (en) * | 2012-04-18 | 2012-08-22 | 王振伟 | Green and novel crop pest repellent |
| CN104430580A (en) * | 2014-12-10 | 2015-03-25 | 甘肃惠森药业发展有限公司 | Traditional Chinese medicinal material stored pest repellent |
| CN104585253A (en) * | 2014-12-22 | 2015-05-06 | 广西中烟工业有限责任公司 | Traditional Chinese medicine composition for prevention and control of tobacco insect pests and preparation method as well as application thereof |
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2019
- 2019-01-08 CN CN201910015943.4A patent/CN109430296A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102640765A (en) * | 2012-04-18 | 2012-08-22 | 王振伟 | Green and novel crop pest repellent |
| CN104430580A (en) * | 2014-12-10 | 2015-03-25 | 甘肃惠森药业发展有限公司 | Traditional Chinese medicinal material stored pest repellent |
| CN104585253A (en) * | 2014-12-22 | 2015-05-06 | 广西中烟工业有限责任公司 | Traditional Chinese medicine composition for prevention and control of tobacco insect pests and preparation method as well as application thereof |
Non-Patent Citations (1)
| Title |
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| 韩群鑫 等: "几种中药材对赤拟谷盗的致死作用及其趋避性研究", 《植物保护》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113002999A (en) * | 2021-03-25 | 2021-06-22 | 生态环境部南京环境科学研究所 | Storage device and method for pseudo-ginseng medicinal materials |
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Application publication date: 20190308 |