CN109399930A - Happy gloss firing and preparation method thereof - Google Patents
Happy gloss firing and preparation method thereof Download PDFInfo
- Publication number
- CN109399930A CN109399930A CN201811517189.6A CN201811517189A CN109399930A CN 109399930 A CN109399930 A CN 109399930A CN 201811517189 A CN201811517189 A CN 201811517189A CN 109399930 A CN109399930 A CN 109399930A
- Authority
- CN
- China
- Prior art keywords
- parts
- happy
- green body
- glaze
- component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000010304 firing Methods 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 229910052751 metal Inorganic materials 0.000 claims abstract description 21
- 239000002184 metal Substances 0.000 claims abstract description 21
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 12
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 6
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 claims abstract description 6
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910001950 potassium oxide Inorganic materials 0.000 claims abstract description 6
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910001948 sodium oxide Inorganic materials 0.000 claims abstract description 6
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims abstract description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 7
- 238000000498 ball milling Methods 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 238000005034 decoration Methods 0.000 abstract description 3
- NOTVAPJNGZMVSD-UHFFFAOYSA-N potassium oxide Chemical compound [K]O[K] NOTVAPJNGZMVSD-UHFFFAOYSA-N 0.000 abstract 1
- 238000002485 combustion reaction Methods 0.000 description 4
- 229910052573 porcelain Inorganic materials 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000000465 moulding Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a kind of happy gloss firing and preparation method thereof, the component and each component mass parts contained in glaze used in happy gloss firing is as follows: line borate: 66-68 parts；Aluminum oxide: 7-9 parts；Zirconium silicate: 15-17 parts；Magnesia: 15-17 parts；Potassium oxide: 3-5 parts；Sodium oxide molybdena: 3-5 parts.The black tone of deep or light different rich variation can be presented in the present invention, and surface forms the metal film with shining property, and ice crack effect, has fine decoration function.
Description
Technical field
The present invention relates to a kind of happy gloss firings and preparation method thereof.
Background technique
Currently, the moulding of porcelain billet is the basis of quality product in porcelain industry, the allotment of glaze and process for calcining make
Porcelain is more bright and colourful, and the porcelain billet of same moulding often because of the difference of glaze, and generates different shadows to the vision of consumer
It rings.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the deficiencies of existing technologies, a kind of happy gloss firing is provided, it presents dense
The black tone of light different rich variation, and surface forms the metal film with shining property, and ice crack effect, has fine
Decoration function.
In order to solve the above technical problems, containing in glaze used in it the technical scheme is that a kind of happy gloss firing
Some components and each component mass parts are as follows:
Line borate: 66-68 parts；
Aluminum oxide: 7-9 parts；
Zirconium silicate: 15-17 parts；
Magnesia: 15-17 parts；
Potassium oxide: 3-5 parts；
Sodium oxide molybdena: 3-5 parts.
The present invention also provides a kind of preparation method of happy gloss firing, the step of method in contain:
S1: it stocks up according to each component and each component mass parts；
S2: according to material: ball: mass ratio=1:1:1.7 of water, wet ball grinding 16~19 hours, the glaze sieving after ball milling
With remove iron, then be tuned into glaze slip；
S3: the biscuiting green body of the biscuiting at 800 DEG C~1100 DEG C of temperature environment is taken, is imposed on the biscuiting green body using glaze slip
Afterwards, it is aglow that green body is fired in the happy firing that temperature is 900 DEG C~1100 DEG C, and aglow green body is put into organic combustion built in one
In the metal bucket of substance, metal bucket is then covered into bung, smoulders 15~30 minutes, green body is pressed from both sides out from metal bucket, is placed in cold in water
But to finished product.
After above-mentioned technical proposal, happy gloss firing of the invention not only makes green body suction carbon, is in due to rapidly restoring
The black tone of existing deep or light different rich variation, and muffle painting is set off into obtain more floridity, but also the metal of glaze inner part point in terms of another
Oxide is reduced into pure metal, and the metal film with shining property is formed on surface, and rather brilliance is dazzled rotten, due to rapidly
Cooling, be easy to cause the ice crack effect of glaze, have good decoration function.
Specific embodiment
In order that the present invention can be more clearly and readily understood, below according to specific embodiment, to the present invention make into
One step detailed description.
Embodiment one
A kind of happy gloss firing, the component and each component mass parts contained in glaze used in it are as follows:
Line borate: 66 parts；
Aluminum oxide: 7 parts；
Zirconium silicate: 15 parts；
Magnesia: 15 parts；
Potassium oxide: 3 parts；
Sodium oxide molybdena: 3 parts.
Contain in the step of preparation method of the happy gloss firing, method:
S1: it stocks up according to each component and each component mass parts；
S2: according to material: ball: mass ratio=1:1:1.7 of water, wet ball grinding 16 hours, the glaze after ball milling was sieved and removes
Iron, then it is tuned into glaze slip；
S3: the biscuiting green body of the biscuiting at 800 DEG C~1100 DEG C of temperature environment is taken, is imposed on the biscuiting green body using glaze slip
Afterwards, it is aglow that green body is fired in the happy firing that temperature is 900 DEG C~1100 DEG C, and aglow green body is put into organic combustion built in one
In the metal bucket of substance, metal bucket is then covered into bung, smoulders 15 minutes, green body is pressed from both sides out from metal bucket, is placed in water and is cooled to
Finished product.
Embodiment two
A kind of happy gloss firing, the component and each component mass parts contained in glaze used in it are as follows:
Line borate: 68 parts；
Aluminum oxide: 9 parts；
Zirconium silicate: 17 parts；
Magnesia: 17 parts；
Potassium oxide: 5 parts；
Sodium oxide molybdena: 5 parts.
Contain in the step of preparation method of the happy gloss firing, method:
S1: it stocks up according to each component and each component mass parts；
S2: according to material: ball: mass ratio=1:1:1.7 of water, wet ball grinding 19 hours, the glaze after ball milling was sieved and removes
Iron, then it is tuned into glaze slip；
S3: the biscuiting green body of the biscuiting at 800 DEG C~1100 DEG C of temperature environment is taken, is imposed on the biscuiting green body using glaze slip
Afterwards, it is aglow that green body is fired in the happy firing that temperature is 900 DEG C~1100 DEG C, and aglow green body is put into organic combustion built in one
In the metal bucket of substance, metal bucket is then covered into bung, smoulders 30 minutes, green body is pressed from both sides out from metal bucket, is placed in water and is cooled to
Finished product.
Embodiment three
A kind of happy gloss firing, the component and each component mass parts contained in glaze used in it are as follows:
Line borate: 67 parts；
Aluminum oxide: 8 parts；
Zirconium silicate: 16 parts；
Magnesia: 16 parts；
Potassium oxide: 4 parts；
Sodium oxide molybdena: 4 parts.
Contain in the step of preparation method of the happy gloss firing, method:
S1: it stocks up according to each component and each component mass parts；
S2: according to material: ball: mass ratio=1:1:1.7 of water, wet ball grinding 17 hours, the glaze after ball milling was sieved and removes
Iron, then it is tuned into glaze slip；
S3: the biscuiting green body of the biscuiting at 800 DEG C~1100 DEG C of temperature environment is taken, is imposed on the biscuiting green body using glaze slip
Afterwards, it is aglow that green body is fired in the happy firing that temperature is 900 DEG C~1100 DEG C, and aglow green body is put into organic combustion built in one
In the metal bucket of substance, metal bucket is then covered into bung, smoulders 20 minutes, green body is pressed from both sides out from metal bucket, is placed in water and is cooled to
Finished product.
The happy gloss firing that three above embodiment is prepared, by it has been observed that its glaze presents deep or light black
Tone, surface also forms the metal film with shining property, and glaze also has ice crack effect, reaches design requirement.
Particular embodiments described above has carried out further in detail the purpose of the present invention, technical scheme and beneficial effects
It describes in detail bright, it should be understood that the above is only a specific embodiment of the present invention, is not intended to restrict the invention, it is all
Within the spirit and principles in the present invention, any modification, equivalent substitution, improvement and etc. done should be included in guarantor of the invention
Within the scope of shield.
Claims (2)
1. a kind of happy gloss firing, which is characterized in that the component and each component mass parts contained in glaze used in it is as follows:
Line borate: 66-68 parts；
Aluminum oxide: 7-9 parts；
Zirconium silicate: 15-17 parts；
Magnesia: 15-17 parts；
Potassium oxide: 3-5 parts；
Sodium oxide molybdena: 3-5 parts.
2. a kind of preparation method of happy gloss firing as described in claim 1, it is characterised in that contain in the step of method:
S1: it stocks up according to each component and each component mass parts；
S2: according to material: ball: mass ratio=1:1:1.7 of water, wet ball grinding 16~19 hours, the glaze after ball milling was sieved and removes
Iron, then it is tuned into glaze slip；
S3: taking the biscuiting green body of the biscuiting at 800 DEG C~1100 DEG C of temperature environment, after being imposed on the biscuiting green body using glaze slip,
It is aglow that green body is fired in the happy firing that temperature is 900 DEG C~1100 DEG C, and aglow green body is put into organic combustible built in one
In the metal bucket of matter, metal bucket is then covered into bung, smoulders 15~30 minutes, green body is pressed from both sides out from metal bucket, is placed in water cooling
To finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811517189.6A CN109399930B (en) | 2018-12-12 | 2018-12-12 | Leshao glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811517189.6A CN109399930B (en) | 2018-12-12 | 2018-12-12 | Leshao glaze and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109399930A true CN109399930A (en) | 2019-03-01 |
| CN109399930B CN109399930B (en) | 2023-05-16 |
Family
ID=65458681
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811517189.6A Active CN109399930B (en) | 2018-12-12 | 2018-12-12 | Leshao glaze and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109399930B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3119445A1 (en) | 2021-02-03 | 2022-08-05 | Adam Pyrométrie | "RAKU" electric ceramic kiln on domestic power supply |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1083155A1 (en) * | 1999-09-08 | 2001-03-14 | Ferro Enamels (Japan) Limited | Method of manufacturing frit for ceramic glaze |
| CN1724477A (en) * | 2005-05-25 | 2006-01-25 | 广东全福陶瓷实业有限公司 | Manufacturing method of redyohen tenmoku ceramic and ceramic glaze used therefor |
| CN102249739A (en) * | 2011-05-26 | 2011-11-23 | 山西高陶瓷业有限责任公司 | Preparation method of carbon-golden metallic luster crystalline glaze |
| CN103044079A (en) * | 2012-12-14 | 2013-04-17 | 广东东宝集团有限公司 | Leadless ceramic glaze and preparation method thereof |
| JP2014166925A (en) * | 2013-02-28 | 2014-09-11 | Toto Ltd | Glaze composition capable of forming glaze layer having high diffuse reflection property and stain resistance, and member having glaze layer formed thereby |
| CN104945018A (en) * | 2014-12-23 | 2015-09-30 | 广西师范学院 | Earthy yellow raw glaze special for Nixing ceramics |
| CN105016782A (en) * | 2015-07-17 | 2015-11-04 | 广西师范学院 | Nixing pottery dedicated glossy grass green raw glaze and preparation method thereof |
| CN105036812A (en) * | 2015-07-28 | 2015-11-11 | 郏县宏大瓷业有限公司 | Glaze material for Jun red glaze and process for preparing Jun porcelain from glaze material |
| CN106986539A (en) * | 2017-05-18 | 2017-07-28 | 东北大学 | A kind of brown has Ceramic glaze material of snakeskin texture and preparation method thereof |
| CN107082566A (en) * | 2017-03-31 | 2017-08-22 | 华南理工大学 | Single-phase cordierite transparent wear glaze and preparation method thereof |
| CN107986624A (en) * | 2017-12-12 | 2018-05-04 | 李炜 | Classic individual layer furnace transmutation glaze and preparation method thereof |
-
2018
- 2018-12-12 CN CN201811517189.6A patent/CN109399930B/en active Active
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1083155A1 (en) * | 1999-09-08 | 2001-03-14 | Ferro Enamels (Japan) Limited | Method of manufacturing frit for ceramic glaze |
| CN1724477A (en) * | 2005-05-25 | 2006-01-25 | 广东全福陶瓷实业有限公司 | Manufacturing method of redyohen tenmoku ceramic and ceramic glaze used therefor |
| CN102249739A (en) * | 2011-05-26 | 2011-11-23 | 山西高陶瓷业有限责任公司 | Preparation method of carbon-golden metallic luster crystalline glaze |
| CN103044079A (en) * | 2012-12-14 | 2013-04-17 | 广东东宝集团有限公司 | Leadless ceramic glaze and preparation method thereof |
| JP2014166925A (en) * | 2013-02-28 | 2014-09-11 | Toto Ltd | Glaze composition capable of forming glaze layer having high diffuse reflection property and stain resistance, and member having glaze layer formed thereby |
| CN104945018A (en) * | 2014-12-23 | 2015-09-30 | 广西师范学院 | Earthy yellow raw glaze special for Nixing ceramics |
| CN105016782A (en) * | 2015-07-17 | 2015-11-04 | 广西师范学院 | Nixing pottery dedicated glossy grass green raw glaze and preparation method thereof |
| CN105036812A (en) * | 2015-07-28 | 2015-11-11 | 郏县宏大瓷业有限公司 | Glaze material for Jun red glaze and process for preparing Jun porcelain from glaze material |
| CN107082566A (en) * | 2017-03-31 | 2017-08-22 | 华南理工大学 | Single-phase cordierite transparent wear glaze and preparation method thereof |
| CN106986539A (en) * | 2017-05-18 | 2017-07-28 | 东北大学 | A kind of brown has Ceramic glaze material of snakeskin texture and preparation method thereof |
| CN107986624A (en) * | 2017-12-12 | 2018-05-04 | 李炜 | Classic individual layer furnace transmutation glaze and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3119445A1 (en) | 2021-02-03 | 2022-08-05 | Adam Pyrométrie | "RAKU" electric ceramic kiln on domestic power supply |
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| Publication number | Publication date |
|---|---|
| CN109399930B (en) | 2023-05-16 |
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Denomination of invention: Le Shao glaze and its preparation method Granted publication date: 20230516 Pledgee: Zhuzhou Branch of China Everbright Bank Co.,Ltd. Pledgor: HUNAN DEXING CERAMICS Co.,Ltd. Registration number: Y2024980014569 |