CN109382053A - More transmittance process integrating devices - Google Patents
More transmittance process integrating devices Download PDFInfo
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- CN109382053A CN109382053A CN201811339802.XA CN201811339802A CN109382053A CN 109382053 A CN109382053 A CN 109382053A CN 201811339802 A CN201811339802 A CN 201811339802A CN 109382053 A CN109382053 A CN 109382053A
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- reaction kettle
- autoclave body
- transmittance process
- hole
- annulus
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/10—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
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Abstract
More transmittance process integrating devices, it is related to ultrasonic technology application apparatus field, it mainly include autoclave body, autoclave body upper end is equipped with feed inlet, lower end is equipped with discharge port, two parts up and down are broadly divided into inside autoclave body, its middle and upper part is divided, autoclave body upper end center is equipped with axis, axis lower end is equipped with rotor, rotor is located inside autoclave body, inner wall of kettle is equipped with horn-like aggregate bin, the small mouth down of aggregate bin, autoclave body inner lower point mainly includes stirring main shaft, stirring main shaft is attached across autoclave body bottom center, bottom center is equipped with positive tetragonal body ultrasonic transmission device in autoclave body, it connects stirring main shaft and is equipped with stirrer paddle, the inner wall of autoclave body inner lower point is equipped with connecting rod, connecting rod connects cylinder.The configuration of the present invention is simple, design rationally, are divided into kettle using liquid and being mixed three times, and sufficiently, effect is obvious for stirring.
Description
Technical field:
The present invention relates to chemical industry transmittance process apparatus fields, and in particular to a kind of collection for having a variety of mixing and heat transfer type
At device, including be stirred, ultrasonic mixing, percussion flow mixing, hypergravity mixing, microwave heating, wall-type heat exchange and directly
Heat exchange.
Background technique:
Traditional agitated reactor is the device for being industrially widely used in mixing and chemically reacting, and mostly interval is grasped
Make, momentum transmitting, heat transfer and mass transfer process can be suitable for.Agitated reactor is influenced very big by equipment volume
Interphase mass transfer and diabatic process inside consersion unit are difficult to reach ideal effect in a very short period of time, especially by microcosmic
Chemical reaction process and the strong Process of absorption or liberation of heat chemical reaction process for mixing control are particularly evident.If stirring cannot carry out in time
Heat transfer or mass transfer are adjusted, and will lead in system that temperature field and concentration field are out of control, this is to chemical reaction process and consersion unit
Serious danger when all.Hypergravity equipment and impact-flow equipment be then preferably can be realized the consersion unit quickly mixed, but
Disadvantage is that residence time of material is short, it is suitable for quickly mixing and reaction process.In addition to this, ultrasonic wave, which mixes, is also
Extremely effective mixed media is usually used in material dispersion, mixing and chemical reaction and strengthens.Under the premise of meeting reaction mixing,
Temperature is also an important factor for influencing chemical reaction.It is that reaction system heats and to strengthen chemical synthesis common that microwave, which has become,
Technological means.The chemical effect that ultrasonic wave and microwave have can accelerate chemical reaction rate, and have choosing to specific reaction
Selecting property.But dissipation and loss due to ultrasonic wave and microwave in the medium, ultrasonic wave and microwave are difficult to set large volume reaction
Standby internal heat transfer and mass transport process control effectively, industrially as just the means of a kind of auxiliary mixing and heating, skill
Art application above has significant limitation.For complicated mixed process or chemical reaction process, the differential responses stage
Mixing requires also to be not quite similar, and single hybrid mode is difficult to meet, thus needs to increase corresponding number of devices, so as to cause
Process flow is longer, and energy consumption increases.
Summary of the invention:
The technical problem to be solved by the present invention lies in overcoming the defects of the prior art, provide it is a kind of have a variety of mixing and
The integrating device of heat transfer meets momentum transmitting, the requirement of heat transfer and mass transfer process, different transmittance process is facilitated to combine
Between flexible switching.
The technical problems to be solved by the invention are realized using following technical scheme.
More transmittance process integrating devices, it is characterised in that: including
Reaction kettle；
Filler rotor, the filler rotor are located in the reaction kettle；
Driving source, the driving source are motor, and the motor provides power for the filler rotor；
Rabbling mechanism, the rabbling mechanism are located in reaction kettle, and the driving source provides power for rabbling mechanism；
Ultrasonic-microwave emitter, the ultrasonic-microwave emitter are located in reaction kettle；
Wherein filler rotor is located at reaction kettle inner top, and rabbling mechanism is located at middle part in reaction kettle, ultrasonic-microwave transmitting
Device is located at bottom in reaction kettle；Wherein filler rotor is divided into several layers rotating mechanism, and several layers rotating mechanism is that several layers are same
The inner and outer wall of heart annulus composition, annulus is reticular structure, and outer layer annulus, to internal layer annulus, the mesh of inner and outer wall is not
Disconnected to increase, annulus top and bottom is plate structure, and wherein the top and bottom edge of annulus is equipped with ring, and adjacent annulus passes through
Spring connection, both ends of the spring are connected on ring.
The inner and outer wall of the annulus is equipped with several recess, and the recess of inner and outer wall is combined together shape
At a hole, ring is located at the bottom and top edge of recess, and spring is located in the hole for combining and being formed.
Using centrifugal force, the liquid on rotor is thrown away, by net, small water droplet is dropped to by flood, is remixed, multilayer separation
Recombination, mixed effect is more preferable, meanwhile, it for the stronger liquid of viscosity, gets rid of online to partially remaining in after online, reduces net
Hole size, excessively remains in annulus, and annulus weight increases, and decline, the small mesh of outer layer is abandoned, and the big mesh of internal layer is exposed,
Continue to rotate, after the drying of outer layer residual liquid, outer layer annulus receives spring tension, and it is automatic to rise, continue multilayer separation recombination.
The driving source is motor and agitating shaft.
Preferably, motor uses servo motor.
The rabbling mechanism packet false bottom axial flow type dasher and radial type dasher.
Preferably, radial type dasher selects oblique leaf dasher, six straight leaves to open turbine dasher；Axis
Flow pattern dasher selects three leaves push type, compound hinged joint paddle, two-fold leaf paddle or the stirring of leafy unlatching turbine paddle
Device.
Water conservancy diversion percussion device is equipped in the reaction kettle, middle and lower part is arranged in kettle in the water conservancy diversion percussion device, by leading
Flow the positive hexagonal honeycomb water conservancy diversion shock layer composition between cylinder and cylinder and kettle wall；Guide shell material is metal, and outer layer applies
Cover anticorrosion polytetrafluoroethylene material.
Preferably, draft tube diameter and kettle diameter ratio are 0.618~0.8.
The inner wall of kettle is equipped with horn-like aggregate bin, the small mouth down of aggregate bin.
The ultrasonic-microwave emitter is uniformly distributed in reactor bottom central stirring shaft surrounding, preferably sets
4~8 groups are set, convenient for super body wave and microwave reflection to reaction kettle lower central, makes full use of the energy of ultrasonic wave and microwave.
The lower end of the reaction kettle is equipped with hole I, and the upper end of reaction kettle is equipped with hole II, and hole I is connect with hole II by pipeline,
Pipeline is equipped with pump, and pipeline is equipped with dividing wall type heat exchanger, conducts heat convenient for kettle liquid.
The pump is located on the pipeline outside reaction kettle.
The pipeline of the connecting hole II extends in filler rotor.
The feed inlet of the reaction kettle is equipped with pipeline and is connected on the extensional pipeline in hole II.
The present invention has rational design, and structure is simple, and integration degree is high, can be realized material be stirred, ultrasound, hit,
It is centrifuged four kinds of different mixed forms and microwave heating and the two different form of heat transfer of septate heat transfer.
It is mixed that axial flow type dasher driving liquid in bottom recycles the shock realized on fluid orthogonal direction in reaction kettle
It closing, radial type dasher provides the ultrasonic mixing of kettle liquid for the mixing on fluid levels direction, bottom ultrasonic unit,
It can be realized and cooperateed between stirring and ultrasound, improve micromixing effect；Solution-air or specific may be implemented in top filler rotor
The mixing of stage liquid-liquid phase with react, microcosmic mixed effect is obvious.
Bottom microwave device can quick liquid in heating kettle, and realized in big volume reaction unit by ultrasound and stirring
Circulation in heat is realized in the requirement of portion's liquid phase homogeneous heating.Pump pumps out hydrothermal solution outside kettle, carries out heat friendship with dividing wall type heat exchanger
It changes, to achieve the purpose that adjust liquidus temperature in kettle.Heat exchange fluid is pumped into top filler rotor and gas and can carry out directly
Heat exchange, which perhaps reacts, to be achieved the purpose that adjust pressure or reaction in kettle, to realize heat outer loop process.
Integration degree is high by the present invention, and operation can be switched between a variety of hybrid modes and heating method, is avoided
The switching of differential responses stage material between different devices, shortens process flow, can satisfy multiphase flow mixing with it is anti-
The requirement answered.In addition, the intermediate product of different phase can also facilitate the separation and receipts of intermediate product in different location sample tap
Collection.
Detailed description of the invention:
Fig. 1 is the structural diagram of the present invention；
Fig. 2 is filler rotor structure schematic diagram of the invention；
1: autoclave body；2: feed inlet；3: discharge port；4: axis；5: belt pulley I；6: motor I；7: filler rotor；8: aggregate bin；
9: stirring main shaft；10: belt pulley II；11: motor II；12: positive tetragonal body ultrasonic-microwave emitter；13: hinged joint stirring
Paddle；14: connecting rod；15: guide shell；16: axial flow type dasher；17: hole I；18: hole II；19: pump；20: condenser；21:
Support plate；22: annulus；23: ring；24: spring；25: recess.
Specific embodiment:
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Conjunction is specifically illustrating, and the present invention is further explained.
Internal and external circulation type ultrasonic-microwave stirred autoclave as shown in Figure 1 includes mainly autoclave body 1, and autoclave body upper end is equipped with
Feed inlet 2, lower end are equipped with discharge port 3, and two parts up and down are wherein broadly divided into inside autoclave body, and middle and upper part, which is divided, mainly includes,
Autoclave body upper end center is equipped with axis 4, and axis upper end is equipped with belt pulley I 5, and belt pulley I connects motor I 6, and motor I is located at autoclave body upper end, axis
Lower end is equipped with rotor 7, and rotor is located inside autoclave body, and wherein inner wall of kettle is equipped with horn-like aggregate bin 8, aggregate bin osculum court
Under, wherein autoclave body inner lower point mainly includes stirring main shaft 9, and stirring main shaft is attached across autoclave body bottom center, stirring main shaft
Lower end is equipped with belt pulley II 10, and belt pulley II connects motor II 11, and wherein bottom center is micro- equipped with positive tetragonal body ultrasonic wave-in autoclave body
Wave transmitting device 12, connection stirring main shaft are equipped with stirrer paddle 13, and the inner wall of autoclave body inner lower point is equipped with connecting rod 14,
Connecting rod connects cylinder 15.
Wherein horn-like aggregate bin osculum is located at below rotor, and osculum diameter is less than the diameter of rotor, convenient for gathering materials
Bucket collects the liquid that rotor produces.
Wherein the upper end nozzle of cylinder is located at the horizontal top of aggregate bin osculum, and ultrasonic-microwave can be incoming along the headwall that gathers materials
Cylinder interior
Wherein stirring main shaft is equipped with straight leaf dasher 16.
Wherein the kettle wall lower end of autoclave body is equipped with hole I 17, and the kettle wall upper end of autoclave body is equipped with hole II 18, and hole I and hole II pass through pipe
Road connection, pipeline are equipped with pump 19, and pipeline is equipped with condenser 20, re-start mixing convenient for extracting.
Wherein pump is located on the pipeline outside autoclave body.
Wherein the pipeline of connecting hole II extends in rotor.
Its middle charging aperture is equipped with pipeline and is connected on the extensional pipeline in hole II.
Wherein positive tetragonal body ultrasonic-microwave emitter is located in stirring main shaft, and rotatably transmitting range is wide, effect
It is good.
Wherein horn-like aggregate bin lower surface is equipped with support plate 21, and support plate is perpendicular to horn-like aggregate bin following table
Face, convenient for being refracted into cylinder for super body wave.
Embodiment 2: such as Fig. 1-2, on the basis of embodiment 1, wherein filler rotor is located at reaction kettle inner top, blender
Structure is located at middle part, ultrasonic-microwave emitter in reaction kettle and is located at bottom in reaction kettle, and several persons are driven by the same driving source
It is dynamic；Wherein filler rotor is divided into several layers rotating mechanism, and several layers rotating mechanism is that several layers concentric circles 22 forms, annulus it is interior
Wall and outer wall are reticular structure, and outer layer annulus, to internal layer annulus, the mesh of inner and outer wall constantly increases, at the top of annulus and bottom
Portion is plate structure, and wherein the top and bottom edge of annulus is equipped with ring 23, and adjacent annulus is connected by spring 24, spring two
End is connected on ring.
The inner and outer wall of the annulus is equipped with several recess 25, and the recess of inner and outer wall is combined together
A hole is formed, ring is located at the bottom and top edge of recess, and spring is located in the hole for combining and being formed.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (9)
- Transmittance process integrating device more than 1., it is characterised in that: includingReaction kettle；Filler rotor, the filler rotor are located in the reaction kettle；Driving source, the driving source are motor, and the motor provides power for the filler rotor；Rabbling mechanism, the rabbling mechanism are located in reaction kettle, and the driving source provides power for rabbling mechanism；Ultrasonic-microwave emitter, the ultrasonic-microwave emitter are located in reaction kettle；Wherein filler rotor is located at reaction kettle inner top, and rabbling mechanism is located at middle part, ultrasonic-microwave emitter in reaction kettle The bottom in reaction kettle, wherein filler rotor is divided into several layers rotating mechanism, and several layers rotating mechanism is several layers concentric circles The inner and outer wall of ring composition, annulus is reticular structure, and outer layer annulus, to internal layer annulus, the mesh of inner and outer wall constantly increases Greatly, annulus top and bottom is plate structure, and wherein the top and bottom edge of annulus is equipped with ring, and adjacent annulus passes through spring Connection, both ends of the spring are connected on ring.
- 2. more transmittance process integrating devices according to claim 1, it is characterised in that: the inner wall of the annulus and outer Wall is equipped with several recess, and the recess of inner and outer wall is combined together to form a hole, and ring is located at the bottom of recess And top edge, spring are located in the hole for combining and being formed.
- 3. more transmittance process integrating devices according to claim 1, it is characterised in that: the driving source be motor and Agitating shaft.
- 4. more transmittance process integrating devices according to claim 1, it is characterised in that: the rabbling mechanism packet false bottom Portion's axial flow type dasher and radial type dasher.
- 5. more transmittance process integrating devices according to claim 1, it is characterised in that: bottom centre in the reaction kettle It is filled equipped with 4 groups of equally distributed ultrasonic-microwave emitters convenient for super body wave and microwave reflection to reaction kettle lower central Divide the energy using ultrasonic wave and microwave.
- 6. more transmittance process integrating devices according to claim 1, it is characterised in that: the lower end of the reaction kettle is set There is hole I, the upper end of reaction kettle is equipped with hole II, and hole I is connect with hole II by pipeline, and pipeline is equipped with pump, and pipeline is equipped with partition Formula heat exchanger conducts heat convenient for kettle liquid.
- 7. more transmittance process integrating devices according to claim 6, it is characterised in that: the pump is located at outside reaction kettle On the pipeline in portion.
- 8. more transmittance process integrating devices according to claim 1, it is characterised in that: the pipeline of connecting hole II extends to In filler rotor.
- 9. more transmittance process integrating devices according to claim 1, it is characterised in that: the feed inlet of reaction kettle is equipped with Pipeline is connected on the extensional pipeline in hole II.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811339802.XA CN109382053B (en) | 2018-11-12 | 2018-11-12 | Multi-transmission process integrated device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811339802.XA CN109382053B (en) | 2018-11-12 | 2018-11-12 | Multi-transmission process integrated device |
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| Publication Number | Publication Date |
|---|---|
| CN109382053A true CN109382053A (en) | 2019-02-26 |
| CN109382053B CN109382053B (en) | 2020-12-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811339802.XA Active CN109382053B (en) | 2018-11-12 | 2018-11-12 | Multi-transmission process integrated device |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101372522A (en) * | 2007-08-24 | 2009-02-25 | 北京化工大学 | Method and apparatus for removing polymer volatile component |
| CN101890250A (en) * | 2010-07-20 | 2010-11-24 | 浙江工业大学 | Super-gravity revolving bed provided with multi-layer cylindrical rotary liquid distributor |
| CN104710062A (en) * | 2015-03-03 | 2015-06-17 | 中北大学 | Device for degrading waste water containing high-concentration nitrobenzene through air stripping-ozone/ultrasound oxidation and treatment method of device |
| WO2016038480A1 (en) * | 2014-09-09 | 2016-03-17 | Hindustan Petroleum Corporation Ltd. | Rotating packed bed assembly |
| CN105617962A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Inner-and-outer-circulation-type ultrasonic-microwave stirring reaction kettle |
| CN107686742A (en) * | 2017-09-27 | 2018-02-13 | 北京化工大学 | A kind of method that residual hydrogenation reaction is carried out in supergravity reactor |
-
2018
- 2018-11-12 CN CN201811339802.XA patent/CN109382053B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101372522A (en) * | 2007-08-24 | 2009-02-25 | 北京化工大学 | Method and apparatus for removing polymer volatile component |
| CN101890250A (en) * | 2010-07-20 | 2010-11-24 | 浙江工业大学 | Super-gravity revolving bed provided with multi-layer cylindrical rotary liquid distributor |
| WO2016038480A1 (en) * | 2014-09-09 | 2016-03-17 | Hindustan Petroleum Corporation Ltd. | Rotating packed bed assembly |
| CN104710062A (en) * | 2015-03-03 | 2015-06-17 | 中北大学 | Device for degrading waste water containing high-concentration nitrobenzene through air stripping-ozone/ultrasound oxidation and treatment method of device |
| CN105617962A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Inner-and-outer-circulation-type ultrasonic-microwave stirring reaction kettle |
| CN107686742A (en) * | 2017-09-27 | 2018-02-13 | 北京化工大学 | A kind of method that residual hydrogenation reaction is carried out in supergravity reactor |
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| Publication number | Publication date |
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| CN109382053B (en) | 2020-12-25 |
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