CN205495570U - Inside and outside circulating ultrasonic wave - microwave stirring reation kettle - Google Patents
Inside and outside circulating ultrasonic wave - microwave stirring reation kettle Download PDFInfo
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- CN205495570U CN205495570U CN201620151183.1U CN201620151183U CN205495570U CN 205495570 U CN205495570 U CN 205495570U CN 201620151183 U CN201620151183 U CN 201620151183U CN 205495570 U CN205495570 U CN 205495570U
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- kettle
- cauldron
- main shaft
- microwave
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Abstract
The utility model provides circulating ultrasonic wave inside and outside one kind microwave stirring reation kettle, relate to ultrasonic wave technique application apparatus field, it is main including the cauldron body, cauldron body upper end is equipped with the feed inlet, the lower end of the stocker is provided with a discharging cylinder, two parts about the internal portion of cauldron mainly divide into, wherein top mainly includes, cauldron body upper end center is equipped with the axle, the axle lower extreme is equipped with the rotor, the rotor is located the internal portion of cauldron, be equipped with the collecting hopper of loudspeaker form on the internal wall of cauldron, the little mouth down of collecting hopper, the internal troops under one's command's part of cauldron is main including the stirring main shaft, the cauldron body bottom center of passing is connected to the stirring main shaft, the internal end center of cauldron is equipped with positive tetragonal body ultrasonic emission device, be equipped with stirring paddle leaf on the connection stirring main shaft, be equipped with the connecting rod on the inner wall of the internal troops under one's command's part of cauldron, the drum is connected to the connecting rod. The utility model discloses simple structure, reasonable in design utilizes liquid to be divided into the cubic in the cauldron and mixes the stirring, and the stirring is abundant, and the effect is obvious.
Description
Technical field:
This utility model relates to ultrasonic-microwave-microwave technique application apparatus field, is specifically related to internal and external circulation type ultrasonic-microwave-microwave stirred autoclave.
Background technology:
Ultrasonic-microwave and microwave have important effect in chemosynthesis, and its chemical effect can be accelerated chemical reaction velocity and specific reaction is had selectivity.When ultrasonic-microwave is propagated in media as well, due to the interaction of ultrasonic-microwave Yu medium, make medium generation physics and the change of chemistry, thus produce a series of mechanics, calorifics, electromagnetic and chemical ultrasonic effect.The mechanism of ultrasonic-microwave can facilitate the emulsifying of liquid, the liquefaction of gel and the dispersion of solid；The minute bubbles that ultrasonic cavitation is formed can constantly move with the vibration of surrounding medium, grow up or vanish suddenly.When vanishing, surrounding liquid pours bubble suddenly and produces high temperature, high pressure, produces shock wave simultaneously；The effect of ultrasonic-microwave can promote occur or accelerate some chemical reaction.Hydrogen peroxide is produced after the purest distilled water is sonicated；Dissolved with the water of nitrogen sonicated after produce nitrous acid；Can variable color or fade after the aqueous solution of dyestuff is sonicated.Ultrasonic-microwave also can accelerate many hydrolysis of chemical substance, decomposition and polymerization process.Photochemistry and electrochemical process are also had a significant effect by ultrasonic-microwave.After various aminoacid are sonicated with the aqueous solution of other organic substances, characteristic absorption spectrum band disappears and in uniform general absorption, this shows that cavitation makes molecular structure there occurs change.Under the effect of microwave high-frequency electric field, polar molecule is the most quickly orientated and rotates and frictional heat；Internal ion vibrates under microwave action and also can convert vibrational energy into heat；General molecule makes energy of thermal motion increase after also absorbing microwave energy；Reactant molecule will be deformed and vibrate, and then affects the generation etc. of chemical reaction.
Owing to some thermo-responsive degree reacted are different, in other courses of reaction then can endothermic heat of reaction or exothermic heat of reaction, the most unavoidably there is heat transfer process in this.If stirring can not be dispelled the heat in time or reaction heat cannot regulate and cause temperature control in system, chemical reaction process and equipment all can produce serious danger.The microwave of common band stirring or ultrasonic-microwave device, for the control of device internal heat, are all had no idea to realize, application are had certain restriction.
Utility model content:
Technical problem to be solved in the utility model is to overcome the defect of prior art, it is provided that a kind of internal and external circulation type ultrasonic-microwave-microwave stirred autoclave.
Technical problem to be solved in the utility model realizes by the following technical solutions.
nullInternal and external circulation type ultrasonic-microwave stirred autoclave，Mainly include kettle，Kettle upper end is provided with charging aperture，Lower end is provided with discharging opening，It is characterized in that: inside described kettle, be broadly divided into upper and lower two parts，Wherein upper part mainly includes，Kettle upper end center is provided with axle，Axle upper end is provided with belt pulley I，Belt pulley I connects motor I，Motor I is positioned at kettle upper end，Axle lower end is provided with rotor，Rotor is positioned at inside kettle，Described inner wall of kettle is provided with trumpet-shaped aggregate bin，The little mouth down of aggregate bin，Described kettle inner lower is divided and is mainly included stirring main shaft，Stirring main shaft is attached across autoclave body bottom center，Stirring main shaft lower end is provided with belt pulley II，Belt pulley II connects motor II，Described kettle inner bottom center is provided with positive tetragonal body ultrasonic-microwave discharger，Connect stirring main shaft and be provided with stirrer paddle，The inwall that kettle inner lower is divided is provided with connecting rod，Connecting rod connects cylinder.
Described trumpet-shaped aggregate bin osculum is positioned at below rotor, and osculum diameter is less than the diameter of rotor, it is simple to aggregate bin collects the liquid that rotor produces.
The upper end nozzle of described cylinder is positioned at above aggregate bin osculum level, and ultrasonic-microwave can be along gathering materials the incoming cylinder interior of headwall
Described stirring main shaft is provided with straight leaf dasher.
The still wall lower end of described kettle is provided with hole I, and the still wall upper end of kettle is provided with hole II, and hole I is connected by pipeline with hole II, and pipeline is provided with pump, and pipeline is provided with condenser, it is simple to extraction re-starts mixing.
Described pump is positioned on the pipeline outside kettle.
The pipeline of described connecting hole II extends in rotor.
Described charging aperture is provided with pipeline and is connected on the extensional pipeline in hole II.
Described positive tetragonal body ultrasonic-microwave discharger is located on stirring main shaft, and rotatable transmitting boundary is wide, effective.
Described trumpet-shaped aggregate bin lower surface is provided with gripper shoe, and gripper shoe is perpendicular to trumpet-shaped aggregate bin lower surface, it is simple to being refracted in cylinder of super body ripple.
This utility model simple in construction, reasonable in design, liquid is utilized to be divided into four mix and blends in still, one time bottom flat leaf stirring paddle drives liquid to circulate the mixing realized on fluid orthogonal direction, the mixing on fluid levels direction of the middle hinged joint stirrer paddle in guide shell, and top filler rotor realizes gas-liquid mixed, bottom ultrasonic-microwave emitter provides can be with the ultrasonic mixing of the entirety of liquid in still, fully, mixed effect is obvious in stirring, and efficiency is high.Hydrothermal solution condensing unit outside pipe is realized heat exchange by pump and cools down by outer circulation, pumps into top rotor and carries out heat exchange with high-temperature gas, it is achieved pressure regulation in still.In bottom microwave device realizes still, the uniform of liquid heats, it is simple to the control of temperature.
Accompanying drawing illustrates:
Fig. 1 is structural representation of the present utility model；
1: kettle；2: charging aperture；3: discharging opening；4: axle；5: belt pulley I；6: motor I；7: filler rotor；8: aggregate bin；9: stirring main shaft；10: belt pulley II；11: motor II；12: positive tetragonal body ultrasonic-microwave discharger；13: hinged joint stirring paddle；14: connecting rod；15: guide shell；16: straight leaf stirring paddle；17: hole I；18: hole II；19: pump；20: condenser；21: gripper shoe.
Detailed description of the invention:
For the technological means making this utility model realize, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with being specifically illustrating, this utility model is expanded on further.
nullInternal and external circulation type ultrasonic-microwave microwave stirred autoclave as shown in Figure 1，Mainly include kettle 1，Kettle upper end is provided with charging aperture 2，Lower end is provided with discharging opening 3，Wherein it is broadly divided into upper and lower two parts inside kettle，Wherein upper part mainly includes，Kettle upper end center is provided with axle 4，Axle upper end is provided with belt pulley I 5，Belt pulley I connects motor I 6，Motor I is positioned at kettle upper end，Axle lower end is provided with rotor 7，Rotor is positioned at inside kettle，Wherein inner wall of kettle is provided with trumpet-shaped aggregate bin 8，The little mouth down of aggregate bin，Wherein kettle inner lower is divided and is mainly included stirring main shaft 9，Stirring main shaft is attached across autoclave body bottom center，Stirring main shaft lower end is provided with belt pulley II 10，Belt pulley II connects motor II 11，Wherein kettle inner bottom center is provided with positive tetragonal body ultrasonic-microwave discharger 12，Connect stirring main shaft and be provided with stirrer paddle 13，The inwall that kettle inner lower is divided is provided with connecting rod 14，Connecting rod connects cylinder 15.
The most trumpet-shaped aggregate bin osculum is positioned at below rotor, and osculum diameter is less than the diameter of rotor, it is simple to aggregate bin collects the liquid that rotor produces.
Wherein the upper end nozzle of cylinder is positioned at above aggregate bin osculum level, and ultrasonic-microwave can be along gathering materials the incoming cylinder interior of headwall
Wherein stirring main shaft is provided with straight leaf dasher 16.
Wherein the still wall lower end of kettle is provided with hole I 17, and the still wall upper end of kettle is provided with hole II 18, and hole I is connected by pipeline with hole II, and pipeline is provided with pump 19, and pipeline is provided with condenser 20, it is simple to extraction re-starts mixing.
Wherein pump is positioned on the pipeline outside kettle.
Wherein the pipeline of connecting hole II extends in rotor.
Wherein charging aperture is provided with pipeline and is connected on the extensional pipeline in hole II.
Wherein positive tetragonal body ultrasonic-microwave discharger is located on stirring main shaft, and rotatable transmitting boundary is wide, effective.
The most trumpet-shaped aggregate bin lower surface is provided with gripper shoe 21, and gripper shoe is perpendicular to trumpet-shaped aggregate bin lower surface, it is simple to being refracted in cylinder of super body ripple.
Of the present utility model ultimate principle, principal character and of the present utility model advantage have more than been shown and described.Skilled person will appreciate that of the industry; this utility model is not restricted to the described embodiments; described in above-described embodiment and description, principle of the present utility model is simply described; on the premise of without departing from this utility model spirit and scope; this utility model also has various changes and modifications, in the range of these changes and improvements both fall within claimed this utility model.This utility model claims scope and is defined by appending claims and equivalent thereof.
Claims (7)
1. an internal and external circulation type ultrasonic-microwave stirred autoclave, mainly includes that kettle, kettle upper end set
Charging aperture, lower end is had to be provided with discharging opening, it is characterised in that: it is broadly divided into upper and lower two inside described kettle
Individual part, wherein upper part mainly includes, kettle upper end center is provided with axle, and axle upper end is provided with belt pulley I,
Belt pulley I connects motor I, and motor I is positioned at kettle upper end, and axle lower end is provided with rotor, and rotor is positioned at still
Internal portion, described inner wall of kettle is provided with trumpet-shaped aggregate bin, the little mouth down of aggregate bin, described
Kettle inner lower is divided and is mainly included stirring main shaft, and stirring main shaft is attached across autoclave body bottom center, stirring
Main shaft lower end is provided with belt pulley II, and belt pulley II connects motor II, and described kettle inner bottom center is provided with positive four
Cube ultrasonic transmission device, connects stirring main shaft and is provided with stirrer paddle, and it is interior that kettle inner lower is divided
Wall is provided with connecting rod, and connecting rod connects cylinder.
2. according to a kind of internal and external circulation type ultrasonic-microwave stirred autoclave described in claim 1, its
It is characterised by: described trumpet-shaped aggregate bin osculum is positioned at below rotor, and osculum diameter is less than rotor
Diameter.
3. according to a kind of internal and external circulation type ultrasonic-microwave stirred autoclave described in claim 1, its
It is characterised by: the upper end nozzle of described cylinder is positioned at above aggregate bin osculum level.
4. according to a kind of internal and external circulation type ultrasonic-microwave stirred autoclave described in claim 1, its
It is characterised by: described stirring main shaft is provided with straight leaf dasher, before straight leaf dasher
Section is positioned at the lower end of cylinder barrel.
5. according to a kind of internal and external circulation type ultrasonic-microwave stirred autoclave described in claim 1, its
It is characterised by: described pump is positioned on the pipeline outside kettle.
6. according to a kind of internal and external circulation type ultrasonic-microwave stirred autoclave described in claim 1, its
It is characterised by: described positive tetragonal body ultrasonic transmission device is located on stirring main shaft.
7. according to a kind of internal and external circulation type ultrasonic-microwave stirred autoclave described in claim 1, its
It is characterised by: described trumpet-shaped aggregate bin lower surface is provided with gripper shoe, and gripper shoe is perpendicular to horn-like
Aggregate bin lower surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620151183.1U CN205495570U (en) | 2016-02-27 | 2016-02-27 | Inside and outside circulating ultrasonic wave - microwave stirring reation kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620151183.1U CN205495570U (en) | 2016-02-27 | 2016-02-27 | Inside and outside circulating ultrasonic wave - microwave stirring reation kettle |
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| Publication Number | Publication Date |
|---|---|
| CN205495570U true CN205495570U (en) | 2016-08-24 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620151183.1U Expired - Fee Related CN205495570U (en) | 2016-02-27 | 2016-02-27 | Inside and outside circulating ultrasonic wave - microwave stirring reation kettle |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105617962A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Inner-and-outer-circulation-type ultrasonic-microwave stirring reaction kettle |
-
2016
- 2016-02-27 CN CN201620151183.1U patent/CN205495570U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105617962A (en) * | 2016-02-27 | 2016-06-01 | 安徽海德石油化工有限公司 | Inner-and-outer-circulation-type ultrasonic-microwave stirring reaction kettle |
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| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 238251 Ma'anshan province and Anhui City, Wujiang province fine chemical base Patentee after: Anhui Haide Chemical Technology Co., Ltd. Address before: 238251 Ma'anshan province and Anhui City, Wujiang province fine chemical base Patentee before: Anhui haydite oil Chemical Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160824 Termination date: 20210227 |