CN109369276A - A kind of liquid is containing humic acid water-soluble fertilizer and preparation method thereof - Google Patents
A kind of liquid is containing humic acid water-soluble fertilizer and preparation method thereof Download PDFInfo
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- CN109369276A CN109369276A CN201811515902.3A CN201811515902A CN109369276A CN 109369276 A CN109369276 A CN 109369276A CN 201811515902 A CN201811515902 A CN 201811515902A CN 109369276 A CN109369276 A CN 109369276A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
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Abstract
The invention discloses a kind of liquid containing humic acid water-soluble fertilizer and preparation method thereof, each weight of material part are as follows: 8-13 parts of urea ammonium nitrate solution, 8-14 parts of ammonium polyphosphate, 14-20 parts of potassium tripolyphosphate, 7-11 parts of mineral resources potassium fulvate, 1-3 parts of nonionic surfactant, 0.05-0.2 parts of endophyte source extract Cyclic dipeptides, 0.1-0.3 parts of organic silicon defoamer, 0.2-0.6 parts of IDHA iron, 0.1-0.5 parts of glycerine, 0.1-0.5 parts of xanthan gum, 36.9-61.45 parts of water.This method is: xanthan gum being added in 6 parts of water in reaction kettle, stirs evenly and stands 24 hours, remaining water, potassium fulvate, surfactant, defoaming agent is then added, is heated to 50 DEG C, stirs 5min；Urea ammonium nitrate solution, ammonium polyphosphate, potassium tripolyphosphate, IDHA iron etc. are added in above-mentioned solution, it is to be dissolved completely after, add Cyclic dipeptides, glycerine, be heated to 50 DEG C, stir 5min, be cooled to room temperature, can pack.Present invention process is simple, and product is suitble to the requirement of current drip irrigation equipment, and using effect is good, can be widely popularized.
Description
Technical field
The invention belongs to the technical fields of fertilizer, are related to water-soluble fertilizer, and in particular to a kind of liquid is fertile containing humic acid water-soluble
Material and its preparation method and application.
Background technique
Refer to containing humic acid water-soluble fertilizer with the humic acid of ratio needed for suitable plant growth, it is big to add appropriate nitrogen, phosphorus, potassium
Liquid or solid water-soluble fertilizer made of the microelements such as secondary element or zinc, boron, iron, molybdenum, manganese, copper.
It is easy to appear crystallization or flocculation phenomenon when existing liquid is stored containing humic acid water-soluble fertilizer on the market, influence
Using effect.Its nutrient form majority is unreasonable simultaneously, lays particular stress on amidonitrogen, and the absorption rate of inorganic nutrients is not high, and lacks
Weary enough microelement supplements, be easy to cause waste and fruit quality low.
Endophyte of plant refers to that those move in the various of health plant in the certain phase of its history of life or whole stages
Fungi or bacterium inside tissue and organ, including endogenetic fungus, endogenetic bacteria and endogeny rayungus.Can secrete antibiotic,
The metabolites such as toxin, these metabolites can induce plant generation system induction of resistance (ISR).Therefore, plant is applied
Endophyte of plant plays biological control effect, has both reduced pollution of the chemical pesticide fertilizer to environment, has in turn ensured the production of plant
Measure quality.
Paecilomyces varioti bacteria strain SJ1 is a kind of endophyte separated from wild sea-buckthorn, and endophyte source Cyclic dipeptides are then
The endophyte of plant secondary metabolites with superelevation bioactivity generated from endophyte fermentation, is piperazinedione class chemical combination
Object, feature structure are to be condensed by two amino acid by peptide bond, the stabilization hexatomic ring skeleton structure having, due to its spy
Different chemical structure makes it become an important functional group in pharmaceutical chemistry, shows multiple biological activities and pharmacology is living
Property, increasingly cause the very big concern of people.It can be used as signaling molecule and participate in the metabolic process of life entity, there is plant growth tune
It saves agent, improve the functions such as immune function and anti-disease activity.
Endophyte source Cyclic dipeptides have several main advantage functions: 1. high activities: nanogram level just has fine effect, at low cost；2.
High function: growth-promoting, improves utilization rate of fertilizer significant effect at disease-resistant, degeneration-resistant, salt resistance；3. resistance to high salt: solving microbial inoculum in fertilizer with high salt
In viability problems；4. height adapts to: non-living body biology, high temperature resistant, effect be not affected by environment；5. high safety: inducer source
In natural ecological system, meet organic food requirement；6. high production: farmer is directly benefited, and promotes and is easy.
Mineral resources potassium fulvate is that the residuum of animals and plants was formed, molecular weight by edaphon conversion in several ten million years
It is generally arrived between tens of thousands of several hundred, can directly be decomposed and utilize by plant after applying to soil, can be retained with fertilizer conservation, increase soil
In crumb structure, improve yield improving quality, the resistance for improving plant, promote root is flourishing, adjusts pH value of soil etc., it is right
P elements in activating soil also have preferable effect.Mineral resources potassium fulvate or a kind of broad-spectrum plant growth regulator simultaneously,
Can promote plant growth, especially can suitable control plant leaf surface stomata openness, reduce rising, play an important role to drought resisting,
The effects of being improved anti-adversity ability, volume increase and improving quality.
Grape belongs to a kind of relatively high fruit of nutritive value, while fructose also rich in, amino acid, fruit in fruit
Acid, vitamin B1、B2、B6, C, P, flavonoids, resveratrol and mineral calcium, phosphorus, potassium, iron etc., have good nutrition to human body
Effect, can also effectively mitigate the symptoms such as neurasthenia, excessive fatigue, and flavonoids, which can also play, removes free radical, anti-oxidant
Effect.Nutrient is supplemented to grape, so to the strongest feature of the absorbability of nutrient in leaf stretching period and full-bloom stage using grape
It is relatively good method for increasing afterwards for plant absorption.
Summary of the invention
That the object of the present invention is to provide a kind of Storage periods is long, nutrient content is high, effectively facilitate plant growth, improve yield and
The liquid of quality contains humic acid water-soluble fertilizer, and provides the preparation method containing humic acid water-soluble fertilizer and on wine-growing
Application.The present invention is by carrying out inorganic nutrients ingredient, microelement, endophyte of plant metabolite and mineral resources potassium fulvate
Collocation, functionally mutually support, supplements necessary nutrient to plant, so that the yield and quality of plant is improved, but its
Middle performance leading role is endophyte metabolite and mineral resources potassium fulvate, passes through endophyte metabolite and mineral resources fulvic acid
The addition of potassium and the strict control of consumption proportion, so that the utilization rate of fertilizer improves, effective fertilizer composition smoothly discharges, is easy to
Plant absorption, and then improve the yield and quality.
The present invention implements that the water-soluble fertilizer of multiple nutrient formulas can be produced, such as: nitrogen content 60g/L, phosphorus content 180g/L,
Potassium content 120g/L, humic acid content 40g/L, fe 5g/L；Nitrogen content 80g/L, phosphorus content 100g/L, potassium content 120g/
L, humic acid content 40g/L etc..
The present invention be realize its purpose the technical solution adopted is that:
A kind of liquid contains humic acid water-soluble fertilizer, according to parts by weight, including urea ammonium nitrate solution 8-13
Part, 8-14 parts of ammonium polyphosphate, 14-20 parts of potassium tripolyphosphate, 7-11 parts of mineral resources potassium fulvate, nonionic surfactant
1-3 parts, 0.05-0.2 parts of endophyte source extract Cyclic dipeptides, 0.1-0.3 parts of organic silicon defoamer, 0.2-0.6 parts of IDHA iron, third
0.1-0.5 parts of triol, 0.1-0.5 parts of xanthan gum, 36.9-61.45 parts of water.
A kind of liquid contains humic acid water-soluble fertilizer, according to parts by weight, including urea ammonium nitrate solution 10-12
Part, 10-12 parts of ammonium polyphosphate, 15-18 parts of potassium tripolyphosphate, 7-10 parts of mineral resources potassium fulvate, non-ionic surface active
1-2 parts of agent, 0.05-0.1 parts of endophyte source extract Cyclic dipeptides, 0.1-0.2 parts of organic silicon defoamer, 0.4-0.6 parts of IDHA iron,
0.4-0.5 parts of glycerine, 0.1-0.2 parts of xanthan gum, 44.4-55.95 parts of water.
A kind of liquid contains humic acid water-soluble fertilizer, according to parts by weight, including urea ammonium nitrate solution 10.4
Part, 11 parts of ammonium polyphosphate, 17 parts of potassium tripolyphosphate, 7 parts of mineral resources potassium fulvate, 2 parts of nonionic surfactant, interior life
0.05 part of bacterium source extract Cyclic dipeptides, 0.1 part of organic silicon defoamer, 0.5 part of IDHA iron, 0.5 part of glycerine, 0.2 part of xanthan gum,
51.15 parts of water.
A kind of liquid contains humic acid water-soluble fertilizer, which is characterized in that urine
Nitrogenous 32% in plain ammonium nitrate solution, nitrogenous 17-18%, phosphorous 58-59%, pH value 6.2-7.0, trimerization in ammonium polyphosphate
Phosphorous 46-47%, 51-52% containing potassium in potassium phosphate, 10-12% containing potassium, 50-60% containing humic acid in mineral resources potassium fulvate, nonionic
Surfactant is one or more of peregal, NP-10, alkyl phenol polyoxyethylene ether, IDHA iron iron content 8%.
A kind of preparation method of the liquid containing humic acid water-soluble fertilizer, comprising the following steps:
A. 0.2 part of xanthan gum is added in 6 parts of water in a kettle, stirs evenly and stands 24 hours.
B. remaining water, 7 parts of mineral resources potassium fulvates, 2 portions of nonionic surfactants, 0.1 part of organic silicon defoamer is added, adds
Heat stirs 5min to 50 DEG C.
C. 10.4 parts of urea ammonium nitrate solutions, 11 parts of ammonium polyphosphates, 17 parts of potassium tripolyphosphate, 0.5 part of IDHA iron are added, it is molten
After solution is complete, 0.05 part of endophyte source extract Cyclic dipeptides, 0.5 part of glycerine are added, are heated to 50 DEG C, stir 5 minutes, stand
It 30 minutes, can pack.
A kind of application of liquid containing humic acid water-soluble fertilizer on wine-growing.The present invention also provides above-mentioned water containing humic acid
Application of the molten fertilizer on wine-growing.According to grape different cultivars and resident time, it is proposed that mu amount of application 60-80kg is bloomed
Phase application is primary, and the application of young fruit expanding stage is primary, and fructescence application is primary；Foliage-spray better effect.
The beneficial effects of the present invention are: liquid of the present invention contain humic acid water-soluble fertilizer, can promote plant growth,
Increase yield, improve quality, convenience, fertilizer efficiency height is administered simultaneously, is conducive to promote the use of.In addition to particularly suitable for grape, this hair
The bright humic acid water-soluble fertilizer that contains may be equally applicable to other fruit, can also play a degree of raising fruit sugar
Degree and mouthfeel, the purpose for increasing yield and quality.
The effect of each ingredient is as follows in the present invention:
Contain amidonitrogen, nitrate nitrogen and ammonium nitrogen in urea ammonium nitrate solution, nitrogen form is comprehensive, and nutrient effect is higher, more
Persistently, and not it will lead to soil acidification, while production technology compares traditional synthesis process of urea, decreases the energy and disappears
Consumption.
Endophyte source Cyclic dipeptides are the endophyte of plant secondary metabolites with superelevation bioactivity, can be used as signaling molecule
And the metabolic process of life entity is participated in, and there is plant growth regulator, improve the functions such as immune function and anti-disease activity, it is high
Active, high function.
Ammonium polyphosphate nutrient content is high, and dissolubility is good, be not easy in the soil liquid calcium, magnesium, iron, aluminium plasma reaction and
Phosphate radical is set to fail.Ammonium polyphosphate also has the function of chelated metal ions, improves the activity of microelement.Ammonium polyphosphate applies
After soil, hydrolysis is generated under the action of enzyme, orthophosphates is the final product of Quadrafos hydrolysis.Usual plant only inhales
The phosphorus for receiving orthophosphates form, since some in polyphosphoric acid is orthophosphoric acid, ammonium polyphosphate is a kind of rapid long-acting knot
The phosphate fertilizer of conjunction.
Mineral resources potassium fulvate is a kind of broad-spectrum plant growth regulator, can promote plant growth, especially can suitable control plant
The openness of object blade face stomata reduces transpiration, plays an important role to drought resisting, be improved anti-adversity ability, volume increase and improving quality etc.
Effect.
Existing liquid is exactly crystallization and flocculation containing problem maximum existing for humic acid water-soluble fertilizer, after crystallization and flocculation
The fertilizer efficiency containing humic acid water-soluble fertilizer have a greatly reduced quality, using difficulty, or even cause to fail.In face of the problem, existing solution
Scheme is to be adjusted with with matching or reducing the content of humic acid, but more manufacturers are not find this at all
A problem, just thinks that the shelf-life fails, and does not take any measure.Existing solution, taking makes with with the mode matched
It with very inconvenient, and reduce nutrient content and can reduce fertilizer efficiency, be hindered absorbing and releasing for effective component, influence to plant
The growth of object, therefore existing solution is not applicable.The present invention to solve this problem, have passed through long-term exploration and research,
By controlling the collocation of each raw material, in conjunction with the dosage control to each component, peregal/NP-10/ alkylphenol-polyethenoxy is being added
It, can be in the degree for not influencing product nutrient content by the mutual support between component functionally in the case where ether and glycerine
The lower significant crystallization reduced containing humic acid water-soluble fertilizer and flocculation phenomenon, it is easy to use, the release of nutrient is not influenced, it will not
Irrigation equipment is impacted, very good solution prior art open question.
Water-soluble fertilizer of the present invention also has the advantage that
1, fertilizer efficiency period is 20 days or more.
2, the shelf-life of water-soluble fertilizer of the present invention is up to 1 year or more, nodeless mesh and flocculation phenomenon.
3, endophyte source extract Cyclic dipeptides used in the present invention, promotion plant root development affine with soil and plant
Effect, while there is antiacid, strengthening root, growth promoting, the big remarkable efficacy of beautiful fruit four to soil and plant.
4, the control of the ratio of each nutritional ingredient of the raw materials used in the present invention, to meet the needs of plant is to nutrient, simultaneously
The nitrogen nutrient of three kinds of forms is arranged in pairs or groups mutually, so that cooperating more preferably between the effective component of fertilizer, is conducive to effective component and is continued surely
Fixed release meets the needs of plant different growing stages are to nutrient, prevents supersaturation and starvation, but also can be improved
20% or more the utilization rate of nitrogen improves 25% or more the utilization rate of phosphorus, improves 15% or more the utilization rate of potassium.Below with reference to embodiment
A kind of liquid provided by the invention is described in detail containing humic acid water-soluble fertilizer and preparation method thereof, but cannot be it
Be interpreted as limiting the scope of the present invention.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below.
IDHA iron of the present invention is purchased from Shijiazhuang Jackization for the known trace-element fertilizer that can be commercially available
Work Co., Ltd etc. contains Fe8% in the IDHA iron.Urea ammonium nitrate solution of the present invention, ammonium polyphosphate, potassium tripolyphosphate,
Mineral resources potassium fulvate, endophyte source Cyclic dipeptides, the known raw material that can be respectively commercially available, wherein the urea ammonium nitrate
Nitrogenous solution is 32%；Nitrogenous 18-19% in the ammonium polyphosphate, phosphorous 58-59%；Phosphorous 46- in the potassium tripolyphosphate
47%, 51-52% containing potassium；10-12% containing potassium, 50-70% containing humic acid in the potassium fulvate.Above-mentioned raw materials are purchased from Shandong Hua Lu
Hengsheng chemical inc, Yunnan Yuntianhua Co., Ltd., Hangzhou Lan Hong Chemical Co., Ltd., the rotten plant of Shandong innovation
The flourishing biological Co., Ltd etc. in sour Science and Technology Co., Ltd., Shandong.
One, specific embodiment
Embodiment 1-7 each provides a kind of liquid containing humic acid water-soluble fertilizer, and formula is specifically shown in Table 1.
Table 1 (units/kg)
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 | |
| Urea ammonium nitrate solution | 11 | 8 | 10.4 | 9.5 | 10 | 12 | 12.5 |
| Ammonium polyphosphate | 13 | 13 | 11 | 9 | 9.5 | 9.5 | 10 |
| Potassium tripolyphosphate | 16 | 14.5 | 17 | 18 | 15 | 15 | 14 |
| Mineral resources potassium fulvate | 8 | 7 | 7 | 7.5 | 7 | 8 | 8.5 |
| Glycerine | 0.4 | 0.2 | 0.5 | - | 0.3 | 0.2 | 0.1 |
| Peregal | 1.5 | 1 | - | 2 | - | 1 | 0.5 |
| OP-10 | - | - | - | - | 1 | 1 | 0.5 |
| Alkyl phenol polyoxyethylene ether | - | 1 | 2 | - | 1 | - | 1 |
| Organic silicon defoamer | - | 0.1 | 0.1 | - | - | 0.1 | 0.1 |
| IDHA iron | 0.9 | 0.5 | 0.5 | 0.3 | - | - | 0.3 |
| Endophyte source Cyclic dipeptides | 0.08 | 0.05 | 0.05 | 0.1 | 0.05 | 0.06 | 0.08 |
| Xanthan gum | 0.2 | 0.3 | 0.3 | 0.2 | 0.3 | - | 0.3 |
| Water | 49.22 | 54.35 | 51.15 | 53 | 55.85 | 53.14 | 52.12 |
Embodiment 8-14 each provides the liquid of a kind of raising vintage and quality containing humic acid water-soluble fertilizer, formula tool
Body is shown in Table 2.
Table 2 (units/kg)
| Embodiment 8 | Embodiment 9 | Embodiment 10 | Embodiment 11 | Embodiment 12 | Embodiment 13 | Embodiment 14 | |
| Urea ammonium nitrate solution | 11.5 | 11 | 13 | 10.5 | 12 | 9.6 | 8 |
| Ammonium polyphosphate | 8 | 13 | 9 | 9 | 10 | 11.4 | 8 |
| Potassium tripolyphosphate | 14.5 | 14.5 | 18.5 | 15 | 15.5 | 16 | 14 |
| Mineral resources potassium fulvate | 8.5 | 7 | 10.5 | 9 | 9.5 | 8.5 | 7 |
| Glycerine | 0.2 | 0.2 | 0.5 | 0.1 | 0.3 | 0.2 | 0.1 |
| Peregal | 1 | 1 | 1.5 | 1 | 0.8 | 1 | 0.5 |
| OP-10 | 1 | 0.5 | 0.5 | - | 0.2 | 1 | 0.5 |
| Alkyl phenol polyoxyethylene ether | 1 | 0.5 | - | 1 | - | 0.5 | 1 |
| Organic silicon defoamer | 0.15 | 0.1 | 0.2 | 0.2 | - | 0.12 | 0.1 |
| IDHA iron | 0.4 | 0.3 | 0.3 | 0.5 | - | 0.32 | 0.2 |
| Endophyte source Cyclic dipeptides | 0.05 | 0.08 | 0.08 | 0.12 | 0.1 | 0.06 | 0.05 |
| Xanthan gum | 0.3 | 0.2 | 0.2 | 0.2 | 0.1 | - | 0.1 |
| Water | 53.4 | 51.62 | 45.72 | 53.48 | 51.5 | 51.3 | 60.45 |
Preparation of the fluid present invention containing humic acid water-soluble fertilizer can be prepared by traditional technique, and more preferably selection is with the present invention
Preparation method, it is specific as follows:
Specifically includes the following steps:
1) xanthan gum is added in 6 parts of water in a kettle, stirs evenly and stands 24 hours.
2) it is proportionally added into remaining water, mineral resources potassium fulvate, nonionic surfactant, organic silicon defoamer, is heated to
50 DEG C, stir 5min.
3) it is proportionally added into urea ammonium nitrate solution, ammonium polyphosphate, potassium tripolyphosphate, IDHA iron, after dissolution completely, is added
Endophyte source extract Cyclic dipeptides, glycerine are heated to 50 DEG C, stir 5 minutes, stand 30 minutes, can pack.
Two, application effect
The investigation that liquid described in embodiment 1-14 applies fertilizer to grape containing humic acid water-soluble fertilizer.
1) analysis is measured to growing area soil, investigates the Yantai Longkou City town Lan Gao grape growing region soil nutrient shape
Condition, soil sampling measurement analysis respectively, on the whole, soil organic matter content is relatively low, and phosphorus, potassium content are relatively low, and soil is slightly acidified.
2) apply fertilizer field trial, and grape variety ruby applies fertilizer 20kg described in embodiment 1-14 per acre every time.
Application test one:
In March, 2016 applies more than 20 mu of fertilizer described in embodiment 1-14, altogether in 3, the Yantai Longkou City town Lan Gao peasant household field
Application 3 times, first time mu apply 20kg, florescence application, and punching is applied；Second mu is applied 15kg, the application of young fruit expanding stage, blade face spray
It applies；Third time mu applies 20kg, the application of fruit picking maturity period, foliage-spray.It compares totally 2 plot: applying reference examples 1 in first plot
Fertilizer (double treasured 14-6-30 a great number of elements water-soluble fertilizers), method of administration is identical；Second plot application 2 fertilizer of reference examples is (existing
Non-present invention contain humic acid water-soluble fertilizer), method of administration is identical.Specific yield increase effect is shown in Table 3.
3 yield increase effect contrast table of table
| Processing | Per mu yield (kg) | Yield increases (%) |
| Embodiment 1 | 2901.8 | 10.5 |
| Embodiment 2 | 2852.8 | 8.7 |
| Embodiment 3 | 2995.7 | 14.1 |
| Embodiment 4 | 2908.3 | 10.8 |
| Embodiment 5 | 2892.7 | 10.3 |
| Embodiment 6 | 2913.6 | 10.98 |
| Embodiment 7 | 2921.8 | 11.3 |
| Embodiment 8 | 2928.4 | 11.5 |
| Embodiment 9 | 2935.7 | 11.8 |
| Embodiment 10 | 2941.8 | 12.1 |
| Embodiment 11 | 2872.8 | 9.4 |
| Embodiment 12 | 2965.7 | 12.96 |
| Embodiment 13 | 2971.8 | 13.2 |
| Embodiment 14 | 2982.8 | 13.6 |
| Reference examples 1 | 2625.4 | --- |
| Reference examples 2 | 2732.5 | 4.1 |
From the table of comparisons it is found that compared with 1 fertilizer of reference examples, the grape of application embodiment 1-14 fertilizer is average to increase production 11.5% per acre
More than, wherein product effect described in embodiment 3 is best, reaches 14.1%.
Application test two:
Manure trial is carried out in the Yantai Longkou City town the Lan Gao village Zhu Sha grape-planting regions, is divided into 3 processing in March, 2017,
Processing one: mu applies fertilizer 60kg described in the embodiment of the present invention, and first time mu applies 25kg, florescence application, and punching is applied；Second mu is applied
15kg, the application of young fruit expanding stage, foliage-spray；Third time mu applies 20kg, the application of fruit picking maturity period, foliage-spray.Processing two: it applies
The fertilizer described in reference examples 3 (the containing humic acid water-soluble fertilizer of existing non-present invention), illustrates, 70kg/ mus according to application；Processing
Three: fertilizer described in application reference examples 4 (extra large champion 16-6-24 seaweed punching fertilising), 60kg/ mus.Growth period co-administers four times.Specifically
Yield increase effect is shown in Table 4.
4 yield increase effect contrast table of table
| Processing | Per mu yield (kg) | Yield increases (%) |
| Embodiment 1 | 3089.1 | 14.2 |
| Embodiment 2 | 2994.4 | 10.8 |
| Embodiment 3 | 3252.8 | 20.3 |
| Embodiment 4 | 3058.6 | 13.1 |
| Embodiment 5 | 3094.4 | 10.7 |
| Embodiment 6 | 3154.8 | 16.7 |
| Embodiment 7 | 3108.6 | 14.9 |
| Embodiment 8 | 3097.2 | 14.5 |
| Embodiment 9 | 3085.7 | 14.1 |
| Embodiment 10 | 2996.2 | 10.8 |
| Embodiment 11 | 3072.4 | 13.6 |
| Embodiment 12 | 2994.3 | 10.7 |
| Embodiment 13 | 3082.6 | 13.98 |
| Embodiment 14 | 2908.8 | 14.9 |
| Reference examples 3 | 2704.5 | --- |
| Reference examples 4 | 2795.4 | 3.4 |
Compared with reference examples 3, the grape growing way for applying embodiment 1-14 fertilizer is good, and fruit is beautiful full, in good taste, fruit fragrance
Strong, wherein product effect described in embodiment 3 is best, and yield increases by 16.6%.
Three, to the influence of grape quality
Impact effect of 5 present invention of table to grape quality
| Preparation method | Soluble adhesion molecule % | Organic acid % | Sugar/acid |
| Embodiment 1 | 16.18 | 0.85 | 19.04 |
| Embodiment 2 | 16.39 | 0.86 | 19.06 |
| Embodiment 3 | 18.53 | 0.73 | 25.38 |
| Embodiment 4 | 15.72 | 0.85 | 15.55 |
| Embodiment 5 | 17.25 | 0.86 | 18.49 |
| Embodiment 6 | 16.97 | 0.86 | 19.73 |
| Embodiment 7 | 17.38 | 0.85 | 20.45 |
| Embodiment 8 | 16.15 | 0.86 | 18.78 |
| Embodiment 9 | 16.69 | 0.86 | 19.41 |
| Embodiment 10 | 16.17 | 0.85 | 19.02 |
| Embodiment 11 | 18.13 | 0.86 | 21.08 |
| Embodiment 12 | 16.98 | 0.86 | 19.74 |
| Embodiment 13 | 16.28 | 0.85 | 19.15 |
| Embodiment 14 | 17.37 | 0.81 | 21.44 |
| Reference product | 14.55 | 0.98 | 14.85 |
By upper table 5 it is found that water-soluble fertilizer of the present invention is obviously improved the quality of grape, nutritive value is higher, to grape
Application effect can be seen that application effect of the Soluble adhesion molecule of grape, sugar/acid than being all larger than reference product, illustrate application originally
Invention water-soluble fertilizer improves the quality of grape fruit, and every per mu yield may be up to 2852kg or more, than applying the prior art
At least volume increase 8.7%.
The present invention has also done the application effect experiment black to the huge peak of kind and kind autumn simultaneously, likewise, to the red earth
11% or more yield volume increase, the yield volume increase 13% or more black to the autumn, is obviously improved the quality of two kinds of grapes, soluble
Total sugar content promotes 5.5% or more, and for sugar/acid than promoting 4.3% or more, organic acid content reduces by 0.1% or more.
Applying water-soluble fertilizer of the invention makes the quality of grape get a promotion, and mouthfeel is more preferable, increases the benefit of grape
And income, the unexpected client feedback through fruit juice factory, active constituent content is high in grape berry, and utility value is big, to food
There is critically important progress meaning in market, health market, can create bigger income；With health care and the hair of medicine
Exhibition, more and more people are concerned about in the utility value of grape berry, and through detecting, unexpected grape berry essential ingredient is obtained
To raising, especially former blue and white element and linoleic content are promoted, this will have field of medicaments and healthy diet aspect
Push meaning.By taking the ruby grape of above-mentioned experiment, kyoto grape and Qiu Hei grape as an example, by colorimetric determination grape pip
The content of procyanidine is as follows:
1) kyoto grape for applying water-soluble fertilizer of the present invention, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 100-130mg/
g；The kyoto grape for applying double treasured 14-6-30 a great number of elements water-soluble fertilizers, extra large champion 16-6-32 seaweed punching fertilising, through detecting, Portugal
The content of grape seed procyanidins reaches 89-91mg/g；Apply the Portugal Ju Feng containing humic acid water-soluble fertilizer of existing non-present invention
Grape, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 90-93mg/g；Kyoto grape commercially, through detecting, Portugal
The content of grape seed procyanidins is up to 88.4 ± 3.1mg/g.
2) the ruby grape for applying water-soluble fertilizer of the present invention, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 115-
130mg/g；The ruby grape of double treasured 14-6-30 a great number of elements water-soluble fertilizers, extra large champion 16-6-32 seaweed punching fertilising is applied,
Through detecting, the content of Proanthocyanidins from Grape Seeds reaches 103-105mg/g；Apply the fertile containing humic acid water-soluble of existing non-present invention
The ruby grape of material, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 105-108mg/g；Red treasured commercially
Stone grape, through detecting, the content of Proanthocyanidins from Grape Seeds is up to 102.4 ± 2.0mg/g.
3) the autumn black grape for applying water-soluble fertilizer of the present invention, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 150-
160mg/g；Apply double treasured 14-6-30 a great number of elements water-soluble fertilizers, extra large champion 16-6-32 seaweed punching fertilising or existing commercially available fertilizer
Autumn black grape, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 132-135mg/g；Apply containing for existing non-present invention
The autumn of humic acid water-soluble fertilizer black grape, through detecting, the content of Proanthocyanidins from Grape Seeds reaches 136-140mg/g；From the market
The autumn of purchase black grape, through detecting, the content of Proanthocyanidins from Grape Seeds is up to 131.7 ± 5.4mg/g.
It is found through above-mentioned detection, unexpectedly increases the nutritive value of grape pip, the content of grape pip procyanidin really
9% or more is promoted, the nutritive value and commodity value of grape is further substantially increased, improves the practical application of grape, into one
Step has expanded the application market of grape.
Chemical fertilizer is widely used, and makes the inorganic nutrients ion transit such as nitrogen, phosphorus, potassium of soil middle peasant's plant available
The salt of indissoluble causes soil hardening, and fertilizer efficiency reduces, and over time, reduces agriculture plant products, causes the low return of high investment, this is not
Meet the basic demand of agricultural development, water-soluble fertilizer of the present invention solves the above problem, and mineral resources potassium fulvate can will be in soil
The salt of indissoluble is changed into the ion that agriculture plant available utilizes, and alleviates soil hardening, discharges soil vitality, endophyte source Cyclic dipeptides
Plant resistance to environment stress can be enhanced, improve growth vigor.Meanwhile using same amount of water-soluble fertilizer of the present invention and existing commercially available fertilizer phase
Than for melon and fruit, the present invention is compared to existing commercially available 7% or more fertilizer volume increase.The present invention feelings few in water-soluble fertilizer amount of application
Under condition, still realize high volume increase, high synergy, high usage effect.
It is a kind of addition Cyclic dipeptides contain humic acid water-soluble fertilizer, the invention belongs to the technical fields of fertilizer, in parts by weight
Meter, including 8-13 parts of urea ammonium nitrate solution, 8-14 parts of ammonium polyphosphate, 14-20 parts of potassium tripolyphosphate, mineral resources potassium fulvate 7-11
Part, 1-3 parts of nonionic surfactant, 0.05-0.2 parts of endophyte source extract Cyclic dipeptides, organic silicon defoamer 0.1-0.3
Part, 0.2-0.6 parts of IDHA iron, 0.1-0.5 parts of glycerine, 0.1-0.5 parts of xanthan gum, 36.9-61.45 parts of water.The present invention also mentions
Supply that this contains the preparation method of humic acid water-soluble fertilizer and this contains the application of humic acid water-soluble fertilizer, present invention process is simple, former
Expect at low cost, product is suitble to the requirement of current drip irrigation equipment, and effect is good, can be widely popularized.The invention is particularly useful for fruit trees
Growth period absorbs nutrient, improves fruit pol, improves the yield and quality.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (6)
1. a kind of liquid contains humic acid water-soluble fertilizer, which is characterized in that according to parts by weight, including urea ammonium nitrate solution 8-13
Part, 8-14 parts of ammonium polyphosphate, 14-20 parts of potassium tripolyphosphate, 7-11 parts of mineral resources potassium fulvate, nonionic surfactant 1-3
Part, 0.05-0.2 parts of endophyte source extract Cyclic dipeptides, 0.1-0.3 parts of organic silicon defoamer, 0.2-0.6 parts of IDHA iron, the third three
0.1-0.5 parts of alcohol, 0.1-0.5 parts of xanthan gum, 36.9-61.45 parts of water.
2. a kind of liquid according to claim 1 contains humic acid water-soluble fertilizer, which is characterized in that according to parts by weight, packet
Include 10-12 parts of urea ammonium nitrate solution, 10-12 parts of ammonium polyphosphate, 15-18 parts of potassium tripolyphosphate, 7-10 parts of mineral resources potassium fulvate,
1-2 parts of nonionic surfactant, 0.05-0.1 parts of endophyte source extract Cyclic dipeptides, 0.1-0.2 parts of organic silicon defoamer,
0.4-0.6 parts of IDHA iron, 0.4-0.5 parts of glycerine, 0.1-0.2 parts of xanthan gum, 44.4-55.95 parts of water.
3. a kind of liquid according to claim 1 contains humic acid water-soluble fertilizer, which is characterized in that according to parts by weight, packet
Include 10.4 parts of urea ammonium nitrate solution, 11 parts of ammonium polyphosphate, 17 parts of potassium tripolyphosphate, 7 parts of mineral resources potassium fulvate, non-ionic surface
2 parts of activating agent, 0.05 part of endophyte source extract Cyclic dipeptides, 0.1 part of organic silicon defoamer, 0.5 part of IDHA iron, glycerine 0.5
Part, 0.2 part of xanthan gum, 51.15 parts of water.
4. a kind of liquid according to claim 1 contains humic acid water-soluble fertilizer, which is characterized in that contain in urea ammonium nitrate solution
Nitrogen 32%, nitrogenous 17-18%, phosphorous 58-59%, pH value 6.2-7.0 in ammonium polyphosphate, phosphorous 46-47% in potassium tripolyphosphate,
51-52% containing potassium, 10-12% containing potassium, 50-60% containing humic acid in mineral resources potassium fulvate, nonionic surfactant be peregal,
One or more of NP-10, alkyl phenol polyoxyethylene ether, IDHA iron iron content 8%.
5. a kind of preparation method of liquid containing humic acid water-soluble fertilizer, which comprises the following steps:
A. 0.2 part of xanthan gum is added in 6 parts of water in a kettle, stirs evenly and stands 24 hours；
B. remaining water, 7 parts of mineral resources potassium fulvates, 2 portions of nonionic surfactants, 0.1 part of organic silicon defoamer is added, is heated to
50 DEG C, stir 5min；
C. 10.4 parts of urea ammonium nitrate solutions, 11 parts of ammonium polyphosphates, 17 parts of potassium tripolyphosphate, 0.5 part of IDHA iron are added, have dissolved
0.05 part of endophyte source extract Cyclic dipeptides, 0.5 part of glycerine are added in Quan Hou, are heated to 50 DEG C, stir 5 minutes, stand 30 points
Clock can be packed.
6. application of a kind of liquid containing humic acid water-soluble fertilizer on wine-growing as described in claim 1.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811515902.3A CN109369276A (en) | 2018-12-12 | 2018-12-12 | A kind of liquid is containing humic acid water-soluble fertilizer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811515902.3A CN109369276A (en) | 2018-12-12 | 2018-12-12 | A kind of liquid is containing humic acid water-soluble fertilizer and preparation method thereof |
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| CN109369276A true CN109369276A (en) | 2019-02-22 |
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ID=65373399
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| CN201811515902.3A Withdrawn CN109369276A (en) | 2018-12-12 | 2018-12-12 | A kind of liquid is containing humic acid water-soluble fertilizer and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111440023A (en) * | 2020-03-17 | 2020-07-24 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer containing humic acid |
| CN113307687A (en) * | 2021-06-21 | 2021-08-27 | 北京耕天下生物科技有限公司 | Liquid water-soluble fertilizer compounded by microalgae fermentation liquor and humic acid and production method thereof |
| CN113480342A (en) * | 2021-07-29 | 2021-10-08 | 兰州市冠涛科技有限责任公司 | Humic acid preparation process, and humic acid-containing base fertilizer and fertilizer prepared by process |
| CN114409467A (en) * | 2022-02-19 | 2022-04-29 | 陕西正宏生物科技有限公司 | Preparation method of water-soluble fertilizer |
| CN114874044A (en) * | 2022-04-13 | 2022-08-09 | 山东碧护生物科技有限公司 | Humic acid water-soluble fertilizer and production process thereof |
-
2018
- 2018-12-12 CN CN201811515902.3A patent/CN109369276A/en not_active Withdrawn
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111440023A (en) * | 2020-03-17 | 2020-07-24 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer containing humic acid |
| CN113307687A (en) * | 2021-06-21 | 2021-08-27 | 北京耕天下生物科技有限公司 | Liquid water-soluble fertilizer compounded by microalgae fermentation liquor and humic acid and production method thereof |
| CN113480342A (en) * | 2021-07-29 | 2021-10-08 | 兰州市冠涛科技有限责任公司 | Humic acid preparation process, and humic acid-containing base fertilizer and fertilizer prepared by process |
| CN114409467A (en) * | 2022-02-19 | 2022-04-29 | 陕西正宏生物科技有限公司 | Preparation method of water-soluble fertilizer |
| CN114874044A (en) * | 2022-04-13 | 2022-08-09 | 山东碧护生物科技有限公司 | Humic acid water-soluble fertilizer and production process thereof |
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Application publication date: 20190222 |