CN109354956A - A kind of insulating mold coating and preparation method - Google Patents

A kind of insulating mold coating and preparation method Download PDF

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Publication number
CN109354956A
CN109354956A CN201811209565.5A CN201811209565A CN109354956A CN 109354956 A CN109354956 A CN 109354956A CN 201811209565 A CN201811209565 A CN 201811209565A CN 109354956 A CN109354956 A CN 109354956A
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China
Prior art keywords
parts
component
ratio
copies
heat
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CN201811209565.5A
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Chinese (zh)
Inventor
李友柱
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Tianjin Miyi Science & Technology Co Ltd
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Tianjin Miyi Science & Technology Co Ltd
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Priority to CN201811209565.5A priority Critical patent/CN109354956A/en
Publication of CN109354956A publication Critical patent/CN109354956A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • C09D133/06Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09D133/08Homopolymers or copolymers of acrylic acid esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The present invention provides a kind of insulating mold coating and preparation methods, it is related to paint field, including component A, B component and C component, component A includes xylene solution, butyl acetate solution, benzoyl peroxide, methyl methacrylate, butyl acrylate and ring sila oxygen alkane, B component includes 803 heat-insulating powders and shell powder, and C component is silane coupling agent, and the present invention realizes film forming speed block, facilitate construction, while obtained coating film forming adhesive force is strong, heat-insulation and heat-preservation is excellent.

Description

A kind of insulating mold coating and preparation method
Technical field
The present invention relates to paint field more particularly to a kind of insulating mold coating and preparation methods.
Background technique
Existing conventional insulation material has the products such as mineral wool, mineral rock wool and asbestos, but such material is made into guarantor The process of warm plate is more complicated, and installation period is longer;Conventional thermal barrier thermal insulation coatings are mostly function of heat reflection coating, only to red Outer heat radiation has a certain effect, but poor to conduction heat-insulation and heat-preservation, and in addition above-mentioned material pulls open method adhesive force test result It generally can only achieve 3-5MPa, be fixed on wall and metal epidermis is easy to fall off, there are certain risk hidden danger;Therefore how to make Heat preserving and insulating material can be convenient for constructing and strong adsorption force after constructing, thermal and insulating performance is excellent becomes art technology Personnel's urgent problem to be solved.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the deficiencies in the prior art, a kind of insulation is provided Coating, the insulating mold coating is convenient for construction, and coating strong adsorption force, thermal and insulating performance are excellent.
The present invention is to be achieved by the following technical programs: a kind of insulating mold coating, by ratio of weight and the number of copies, including 60-75 parts of component As, 65-70 parts of B components and 24-40 parts of C components, by ratio of weight and the number of copies, component A include 15-25 parts of dimethylbenzene Solution, 15-25 parts of butyl acetate solution, 1-3 parts of benzoyl peroxides, 8-12 parts of methyl methacrylates, 10-15 parts of acrylic acid Butyl ester and 7-11 parts of ring sila oxygen alkane, B component include 803 heat-insulating powder of 10-13 part and 20-25 parts of shell powder, and C component is silane Coupling agent.
According to the above technical scheme, it is preferable that silane coupling agent is silane coupling A-Link 600.
According to the above technical scheme, it is preferable that the mesh number of shell powder is 150-300 mesh.
According to the above technical scheme, it is preferable that shell powder is walnut shell powder.
A kind of preparation method of insulating mold coating, steps are as follows:
It prepares component A: by ratio of weight and the number of copies, choosing 15-25 parts of xylene solutions and 15-25 parts of butyl acetate solution are thrown Enter in mixing drum, is uniformly mixed, obtains mixed solution;It measures 8-12 part mixed solutions to be put into reaction kettle, heating and by temperature Maintain 105-120 DEG C;By ratio of weight and the number of copies, 1-3 parts of benzoyl peroxides, 10 parts of methyl methacrylates, 10-15 parts are chosen Butyl acrylate and 7-11 parts of ring sila oxygen alkane are placed in mixing drum, are then measured 8-12 parts of mixed solutions and are dissolved, to Dissolution complete and after mixing evenly, lysate is slowly added dropwise in reaction kettle, be added after the completion of heat preservation 1-2h;Choose 1-2 parts Benzoyl peroxide is dissolved and is stirred evenly using remaining mixed solution, and lysate is slowly added dropwise in reaction kettle, dimension Temperature is held at 105-120 DEG C, cooling after the time is 4-6h obtains component A;
B component: by ratio of weight and the number of copies, 803 heat-insulating powder of 10-13 part and 20-25 parts of shell powder is chosen, 200-400 mesh is utilized Electric sieve screening is stand-by;
Coating preparation: it by ratio of weight and the number of copies, chooses in 60-75 parts of component A investment a mixing bowls, under 200 revs/min of speed 65-70 parts of B components and 24-40 parts of C components are added, disperse 40-80 minutes under 800 revs/min of speed, final filtration obtains Coating.
The beneficial effects of the present invention are: the coating film forming speed block that the present invention obtains, facilitates construction;The painting generated after construction Layer has guarantor strong with adhesive force, heat-insulated after obtained coating film forming using particulate the third ring sila oxygen alkane resin as film-forming resin The excellent performance of warm nature.
Detailed description of the invention
Fig. 1 shows the coating performance figure of embodiment according to the present invention.
Specific embodiment
In order to make those skilled in the art more fully understand technical solution of the present invention, with reference to the accompanying drawing and most The present invention is described in further detail for good embodiment.
Embodiment 1:
As shown, a kind of insulating mold coating, by ratio of weight and the number of copies, including 60 parts of component As, 70 parts of B components and 35 Part C component, by ratio of weight and the number of copies, component A include 20 parts of xylene solutions, 20 parts of butyl acetate solution, 1 part of benzoyl peroxide first Acyl, 10 parts of methyl methacrylates, 12 parts of butyl acrylates and 9 parts of ring sila oxygen alkane, B component include 12 part of 803 heat-insulating powder And 21 parts of shell powder, C component are silane coupling agent, the coating film forming speed block that the present invention obtains facilitates construction;And after constructing The coating of generation has after obtained coating film forming with adhesive force using particulate the third ring sila oxygen alkane resin as film-forming resin By force, the excellent performance of heat-insulation and heat-preservation.
Embodiment 12:
A kind of insulating mold coating, by ratio of weight and the number of copies, including 65 parts of component As, 68 parts of B components and 35 parts of C components, it presses Weight fraction ratio, component A include 20 parts of xylene solutions, 20 parts of butyl acetate solution, 1 part of benzoyl peroxide, 10 parts of methyl Methyl acrylate, 12 parts of butyl acrylates and 9 parts of ring sila oxygen alkane, B component include 12 part of 803 heat-insulating powder and 21 parts of shells Powder, C component are silane coupling agent.
Embodiment 3:
A kind of insulating mold coating, by ratio of weight and the number of copies, including 75 parts of component As, 65 parts of B components and 35 parts of C components, it presses Weight fraction ratio, component A include 20 parts of xylene solutions, 20 parts of butyl acetate solution, 1 part of benzoyl peroxide, 10 parts of methyl Methyl acrylate, 12 parts of butyl acrylates and 9 parts of ring sila oxygen alkane, B component include 12 part of 803 heat-insulating powder and 21 parts of shells Powder, C component are silane coupling agent.
According to above-described embodiment, it is preferable that silane coupling agent is silane coupling A-Link 600.
According to above-described embodiment, it is preferable that the mesh number of shell powder is 200 mesh, screens the shell powder of suitable diameter.
According to above-described embodiment, it is preferable that shell powder is walnut shell powder, and walnut powder can effectively improve heat-proof quality.
A kind of preparation method of insulating mold coating, steps are as follows:
It prepares component A: pressing volume parts ratio, choose 15-25 parts of xylene solutions and 15-25 parts of butyl acetate solution are thrown Enter in mixing drum, is uniformly mixed, obtains mixed solution;It measures 8-12 part mixed solutions to be put into reaction kettle, heating and by temperature Maintain 105-120 DEG C;By ratio of weight and the number of copies, 1-3 parts of benzoyl peroxides, 10 parts of methyl methacrylates, 10-15 parts are chosen Butyl acrylate and 7-11 parts of ring sila oxygen alkane are placed in mixing drum, are then measured 8-12 parts of mixed solutions and are dissolved, to Dissolution complete and after mixing evenly, lysate is slowly added dropwise in reaction kettle, be added after the completion of heat preservation 1-2h;Choose 1-2 parts Benzoyl peroxide is dissolved and is stirred evenly using remaining mixed solution, and lysate is slowly added dropwise in reaction kettle, dimension Temperature is held at 105-120 DEG C, cooling after the time is 4-6h obtains component A;
B component: by ratio of weight and the number of copies, 803 heat-insulating powder of 10-13 part and 20-25 parts of shell powder is chosen, 200-400 mesh is utilized Electric sieve screening is stand-by;
Coating preparation: it by ratio of weight and the number of copies, chooses in 60-75 parts of component A investment a mixing bowls, under 200 revs/min of speed 65-70 parts of B components and 24-40 parts of C components are added, disperse 40-80 minutes under 800 revs/min of speed, final filtration obtains Coating.
Form of construction work:
Form of construction work includes two kinds, respectively sprays and brushes.
High-pressure airless spraying gun, spray gun pressure 100kg or more, jet size 0.36mm or more, spray angle are used when spraying 40°/70°;
When in precoating and small area coating using brushing, but defined thickness of dry film must be reached, heat preservation coating suggestion It is more than 2mm thickness;Recoating interval (25 DEG C) minimum 8h, maximum is without limitation.
The beneficial effects of the present invention are: the coating film forming speed block that the present invention obtains, facilitates construction;The painting that the present invention generates Layer has guarantor strong with adhesive force, heat-insulated after obtained coating film forming using particulate the third ring sila oxygen alkane resin as film-forming resin The excellent performance of warm nature.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered It is considered as protection scope of the present invention.

Claims (5)

1. a kind of insulating mold coating, which is characterized in that by ratio of weight and the number of copies, including 60-75 parts of component As, 65-70 parts of B components And 24-40 parts of C components, by ratio of weight and the number of copies, the component A includes 15-25 parts of xylene solutions, 15-25 parts of butyl acetates Solution, 1-3 part benzoyl peroxide, 8-12 parts of methyl methacrylates, 10-15 parts of butyl acrylates and 7-11 parts of ring silas Oxygen alkane, the B component include 803 heat-insulating powder of 10-13 part and 20-25 parts of shell powder, and the C component is silane coupling agent.
2. a kind of insulating mold coating according to claim 1, which is characterized in that the silane coupling agent is silane coupled Agent A-Link 600.
3. a kind of insulating mold coating according to claim 1, which is characterized in that the mesh number of the shell powder is 150-300 Mesh.
4. a kind of insulating mold coating according to claim 3, which is characterized in that the shell powder is walnut shell powder.
5. a kind of preparation method of insulating mold coating as described in claim 1, which is characterized in that steps are as follows:
It prepares component A: pressing volume parts ratio, choose 15-25 part xylene solutions and 15-25 parts of butyl acetate solution put into the In one mixing drum, it is uniformly mixed, obtains mixed solution;It measures 8-12 part mixed solutions to be put into reaction kettle, heating and by temperature Maintain 105-120 DEG C;By ratio of weight and the number of copies, 1-3 parts of benzoyl peroxides, 8-12 parts of methyl methacrylates, 10-15 are chosen Part butyl acrylate and 7-11 parts of ring sila oxygen alkane are placed in the second mixing drum, and it is molten then to measure 8-12 parts of mixed solutions progress Solution, it is to be dissolved complete and after mixing evenly, lysate is slowly added dropwise in reaction kettle, be added after the completion of heat preservation 1-2h;It chooses 1-2 parts of benzoyl peroxides are dissolved and are stirred evenly using remaining mixed solution, and lysate is slowly added dropwise into reaction kettle In, maintain temperature at 105-120 DEG C, cooling after the time is 4-6h obtains component A;
B component: by ratio of weight and the number of copies, 803 heat-insulating powder of 10-13 part and 20-25 parts of shell powder is chosen, 200-400 mesh electric sieve is utilized Screening is stand-by;
Coating preparation: it by ratio of weight and the number of copies, chooses in 60-75 parts of component A investment a mixing bowls, is added under 200 revs/min of speed 65-70 parts of B components and 24-40 parts of C components disperse 40-80 minutes under 800 revs/min of speed, and final filtration is applied Material.
CN201811209565.5A 2018-10-17 2018-10-17 A kind of insulating mold coating and preparation method Pending CN109354956A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116355527A (en) * 2023-03-20 2023-06-30 河南联防科技防火材料有限公司 Intumescent inorganic environment-friendly fireproof coating and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009153195A1 (en) * 2008-06-20 2009-12-23 Wacker Chemie Ag Nanoparticulate silicone organo copolymers and use thereof in coating means
CN103059313A (en) * 2012-12-17 2013-04-24 中山大桥化工集团有限公司 Method for preparing organosilicon modified acrylic resin
CN106366713A (en) * 2016-08-26 2017-02-01 安徽钰锦生态木材料有限公司 Delicate-fragrant-type environment-friendly wall surface coating
CN106519873A (en) * 2016-12-06 2017-03-22 广西德骏门窗幕墙有限公司 Glass thermal insulation paint and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009153195A1 (en) * 2008-06-20 2009-12-23 Wacker Chemie Ag Nanoparticulate silicone organo copolymers and use thereof in coating means
CN103059313A (en) * 2012-12-17 2013-04-24 中山大桥化工集团有限公司 Method for preparing organosilicon modified acrylic resin
CN106366713A (en) * 2016-08-26 2017-02-01 安徽钰锦生态木材料有限公司 Delicate-fragrant-type environment-friendly wall surface coating
CN106519873A (en) * 2016-12-06 2017-03-22 广西德骏门窗幕墙有限公司 Glass thermal insulation paint and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
马莺等: "《野生食用植物资源加工技术》", 30 June 2009 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116355527A (en) * 2023-03-20 2023-06-30 河南联防科技防火材料有限公司 Intumescent inorganic environment-friendly fireproof coating and preparation method thereof

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Application publication date: 20190219

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