CN109349416A - A method of albumen powder is made using South Pole squama shrimp - Google Patents

A method of albumen powder is made using South Pole squama shrimp Download PDF

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Publication number
CN109349416A
CN109349416A CN201811461141.8A CN201811461141A CN109349416A CN 109349416 A CN109349416 A CN 109349416A CN 201811461141 A CN201811461141 A CN 201811461141A CN 109349416 A CN109349416 A CN 109349416A
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CN
China
Prior art keywords
solution
south pole
albumen powder
dried
squama
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Pending
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CN201811461141.8A
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Chinese (zh)
Inventor
刘宇
姜维
胡世伟
李世杰
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Zhejiang Ocean University ZJOU
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Zhejiang Ocean University ZJOU
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Priority to CN201811461141.8A priority Critical patent/CN109349416A/en
Publication of CN109349416A publication Critical patent/CN109349416A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/04Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from fish or other sea animals
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00Working-up of proteins for foodstuffs
    • A23J3/04Animal proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00Working-up of proteins for foodstuffs
    • A23J3/30Working-up of proteins for foodstuffs by hydrolysis
    • A23J3/32Working-up of proteins for foodstuffs by hydrolysis using chemical agents
    • A23J3/34Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes
    • A23J3/341Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes of animal proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Zoology (AREA)
  • Polymers & Plastics (AREA)
  • Food Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Nutrition Science (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Marine Sciences & Fisheries (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

A method of albumen powder is made using South Pole squama shrimp, it is characterized in that the method the following steps are included: (1) raw material pretreatment: by squama shrimp carry out cleaning dry, (2) it dries and crushes: being put into dryer after drying, it is dried, shell after drying is put into pulverizer and carries out smashing processing, smashed powder is sieved, 120 mesh screens fine powder below is collected.Remaining crushing continues pulverization process; obtain krill meal; the protein content of krill be about 80% itself because marine; it is accompanied by the content of the various trace elements such as calcium ion, iron ion, taurine, riboflavin, amino acid; and the less expensive of krill; yield is also bigger, is easier to obtain on raw material.

Description

A method of albumen powder is made using South Pole squama shrimp
Technical field:
This hair is related to a kind of method using South Pole squama shrimp production albumen powder, belongs to the manufacture technology field of health care product.
Background technique
Krill is a kind of ocean for being distributed in antarctic waters without vertebra crustacean, and reserves are 6 .5~1,000,000,000 Ton.Protein content is up to 65~75% in krill dry weight.Krill Argine Monohydrochloride forms reasonable, essential amino acid Content is high, is the huge animal protein resource treasure-house of the mankind, and carries out the important source material of protein higher value application.
Albumen powder is common health care product powder, but health care product is many kinds of now, and also type is also very for manufacture albumen powder More, the raw material of the albumen powder of price is also universal also somewhat expensive, and the raw material of cheap albumen powder is also cheap, but product Matter is without so perfect, and other microelements in protein are also fewer, basic reason be the selection of raw material not It is so perfect.
Summary of the invention:
To solve the above-mentioned problems, the present invention provides a kind of method using South Pole squama shrimp production albumen powder
, certainly protein complex process, the lower disadvantage of purity are extracted in sorting in the prior art, and a kind of of proposition utilizes South Pole squama The method of shrimp production albumen powder.Aiming at the shortcomings in the prior art, a kind of side using South Pole squama shrimp production albumen powder is provided Method, the method the following steps are included:
A method of using South Pole squama shrimp make albumen powder, the method the following steps are included:
(1) pretreatment of raw material: squama shrimp is subjected to cleaning and is dried.
(2) it dries and crushes: being put into dryer after drying, dried, the shell after drying is put into pulverizer and carries out powder Essence processing, smashed powder is sieved, and collects 120 mesh screens fine powder below.Remaining crushing continues at crushing Reason, obtains krill meal
(3) adjust pH value: PH regulator, which is added, will adjust pH value between 7.0-8.0,
(4) it digests: being incorporated as the marine products of solution quality 0.2-0.3% after neutral solution is mixed with water 1:2-3 in mass ratio Product protease, 50-55 DEG C of water enzyme digestion 6-8 h, during which and is stirred continuously, 85-90 DEG C of enzyme deactivations 10-15 is risen to after stirring Min is cooled to 40-50 DEG C;
(5) left undisturbed overnight under the conditions of solution is put into 4 DEG C will be digested after cooling
(6) solution after static removes upper oil, and is filtered with three layers of gauze;Obtain krill polypeptide egg White matter solution.(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, is centrifuged under the conditions of 6000-10000 rpm/min 5-10 min takes upper layer polypeptide protein solution;
(8) polypeptide protein solution is spray-dried, and rear ground 50-99 mesh standard sieve obtains polypeptide egg after spray-dried White powder.
As preferred: it is between 7.5 that the step (3), which is added PH regulator and will adjust pH value,.
As preferred: the step (4) is incorporated as solution quality after mixing neutral solution with water 1:3 in mass ratio 0.3% marine product protease, 55 DEG C of 8 h of water enzyme digestion, during which and is stirred continuously, and 90 DEG C of enzyme deactivation 8min are risen to after stirring, cold But to 45 DEG C;
As preferred: (6) three layers of filtered through gauze of the step, wherein interbed is enzymatic hydrolysis liquid layer.
As preferred: step (7) centrifuge separation: enzymolysis liquid is centrifuged at a high speed, 8000rpm/min condition Lower centrifugation 8min takes upper layer polypeptide protein solution;
As preferred: step (8) the polypeptide protein solution is spray-dried, rear ground 80 target after spray-dried Quasi- sieve obtains polypeptide albumen powder.
The present invention solves the deficiencies in the prior art using bright, from the krill selected in ocean on raw material, the egg of krill White matter content be about 80% itself because marine, it is a variety of micro- to be accompanied by calcium ion, iron ion, taurine, riboflavin, amino acid etc. The content of secondary element, and the less expensive of krill, yield is also bigger, is easier to obtain on raw material.
Specific embodiment
Below with reference to specific implementation example, the present invention is described in detail:
A method of using South Pole squama shrimp make albumen powder, the method the following steps are included:
(1) pretreatment of raw material: squama shrimp is subjected to cleaning and is dried.
(2) it dries and crushes: being put into dryer after drying, dried, the shell after drying is put into pulverizer and carries out powder Essence processing, smashed powder is sieved, and collects 120 mesh screens fine powder below.Remaining crushing continues at crushing Reason, obtains krill meal
(3) adjust pH value: PH regulator, which is added, will adjust pH value between 7.0-8.0,
(4) it digests: being incorporated as the marine products of solution quality 0.2-0.3% after neutral solution is mixed with water 1:2-3 in mass ratio Product protease, 50-55 DEG C of water enzyme digestion 6-8 h, during which and is stirred continuously, 85-90 DEG C of enzyme deactivations 10-15 is risen to after stirring Min is cooled to 40-50 DEG C;
(5) left undisturbed overnight under the conditions of solution is put into 4 DEG C will be digested after cooling
(6) solution after static removes upper oil, and is filtered with three layers of gauze;Obtain krill polypeptide egg White matter solution.(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, is centrifuged under the conditions of 6000-10000 rpm/min 5-10 min takes upper layer polypeptide protein solution;
(8) polypeptide protein solution is spray-dried, and rear ground 50-99 mesh standard sieve obtains polypeptide egg after spray-dried White powder.
As a preferred embodiment: it is between 7.5 that the step (3), which is added PH regulator and will adjust pH value,.
As a preferred embodiment: the step (4) is incorporated as solution after mixing neutral solution with water 1:3 in mass ratio The marine product protease of quality 0.3%, 55 DEG C of 8 h of water enzyme digestion, during which and is stirred continuously, and 90 DEG C of enzyme deactivations are risen to after stirring 8min is cooled to 45 DEG C;
As a preferred embodiment: (6) three layers of filtered through gauze of the step, wherein interbed is enzymatic hydrolysis liquid layer.
As a preferred embodiment: step (7) centrifuge separation: enzymolysis liquid is centrifuged at a high speed, 8000rpm/ It is centrifuged 8min under the conditions of min, takes upper layer polypeptide protein solution;
As a preferred embodiment: step (8) the polypeptide protein solution is spray-dried, rear ground after spray-dried 80 mesh standard sieves obtain polypeptide albumen powder.

Claims (6)

1. a kind of method using South Pole squama shrimp production albumen powder, it is characterised in that the method the following steps are included:
(1) pretreatment of raw material: squama shrimp is subjected to cleaning and is dried;
(2) it dries and crushes: being put into dryer after drying, dried, the shell after drying is put into pulverizer and carries out at smashing Reason, smashed powder is sieved, and collects 120 mesh screens fine powder below, remaining crushing continues pulverization process, Obtain krill meal
(3) adjust pH value: PH regulator, which is added, will adjust pH value between 7.0-8.0,
(4) it digests: being incorporated as the marine products of solution quality 0.2-0.3% after neutral solution is mixed with water 1:2-3 in mass ratio Product protease, 50-55 DEG C of water enzyme digestion 6-8 h, during which and is stirred continuously, 85-90 DEG C of enzyme deactivations 10-15 is risen to after stirring Min is cooled to 40-50 DEG C;
(5) left undisturbed overnight under the conditions of solution is put into 4 DEG C will be digested after cooling
(6) solution after static removes upper oil, and is filtered with three layers of gauze;Obtain krill polypeptide egg White matter solution;(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, is centrifuged under the conditions of 6000-10000 rpm/min 5-10 min takes upper layer polypeptide protein solution;
(8) polypeptide protein solution is spray-dried, and rear ground 50-99 mesh standard sieve obtains polypeptide egg after spray-dried White powder.
2. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step (3) it is between 7.5 that PH regulator, which is added, and will adjust pH value.
3. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step (4) the marine product protease of solution quality 0.3%, 55 DEG C of water are incorporated as after mixing neutral solution with water 1:3 in mass ratio Bath 8 h of enzymatic hydrolysis, during which and are stirred continuously, 90 DEG C of enzyme deactivation 8min are risen to after stirring, are cooled to 45 DEG C.
4. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step (6) three layers of filtered through gauze, wherein interbed is enzymatic hydrolysis liquid layer.
5. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step (7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, 8min is centrifuged under the conditions of 8000rpm/min, takes upper layer polypeptide protein Matter solution.
6. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step (8) polypeptide protein solution is spray-dried, and rear ground 80 mesh standard sieve obtains polypeptide albumen powder after spray-dried.
CN201811461141.8A 2018-12-01 2018-12-01 A method of albumen powder is made using South Pole squama shrimp Pending CN109349416A (en)

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CN201811461141.8A CN109349416A (en) 2018-12-01 2018-12-01 A method of albumen powder is made using South Pole squama shrimp

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CN201811461141.8A CN109349416A (en) 2018-12-01 2018-12-01 A method of albumen powder is made using South Pole squama shrimp

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114431414A (en) * 2022-03-02 2022-05-06 成都国酿食品股份有限公司 Fermented bean curd compound seasoning, preparation method thereof and fermented bean curd

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104357206A (en) * 2014-11-18 2015-02-18 董寰 Method for preparing phospholipid-rich Antarctic krill oil by water enzyme process
CN104388176A (en) * 2014-11-10 2015-03-04 大连工业大学 Method for preparing euphausia superba oil, microcapsule of euphausia superba oil and low-fluorine euphausia superba peptide by using aqueous enzymatic method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104388176A (en) * 2014-11-10 2015-03-04 大连工业大学 Method for preparing euphausia superba oil, microcapsule of euphausia superba oil and low-fluorine euphausia superba peptide by using aqueous enzymatic method
CN104357206A (en) * 2014-11-18 2015-02-18 董寰 Method for preparing phospholipid-rich Antarctic krill oil by water enzyme process

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114431414A (en) * 2022-03-02 2022-05-06 成都国酿食品股份有限公司 Fermented bean curd compound seasoning, preparation method thereof and fermented bean curd
CN114431414B (en) * 2022-03-02 2023-12-29 成都国酿食品股份有限公司 Fermented bean curd composite seasoning, preparation method thereof and fermented bean curd

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Application publication date: 20190219

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