CN109349416A - A method of albumen powder is made using South Pole squama shrimp - Google Patents
A method of albumen powder is made using South Pole squama shrimp Download PDFInfo
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- CN109349416A CN109349416A CN201811461141.8A CN201811461141A CN109349416A CN 109349416 A CN109349416 A CN 109349416A CN 201811461141 A CN201811461141 A CN 201811461141A CN 109349416 A CN109349416 A CN 109349416A
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- solution
- south pole
- albumen powder
- dried
- squama
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- 239000000843 powder Substances 0.000 title claims abstract description 36
- 238000000034 method Methods 0.000 title claims abstract description 24
- 241000238557 Decapoda Species 0.000 title claims abstract description 19
- 241000239366 Euphausiacea Species 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 8
- 238000004140 cleaning Methods 0.000 claims abstract description 4
- 235000012054 meals Nutrition 0.000 claims abstract description 4
- 238000010298 pulverizing process Methods 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims description 22
- 229920001184 polypeptide Polymers 0.000 claims description 21
- 102000004196 processed proteins & peptides Human genes 0.000 claims description 21
- 108090000765 processed proteins & peptides Proteins 0.000 claims description 21
- 238000004519 manufacturing process Methods 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000012460 protein solution Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 9
- 102000004190 Enzymes Human genes 0.000 claims description 6
- 108090000790 Enzymes Proteins 0.000 claims description 6
- 108091005804 Peptidases Proteins 0.000 claims description 6
- 239000004365 Protease Substances 0.000 claims description 6
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 6
- 230000009849 deactivation Effects 0.000 claims description 6
- 230000007935 neutral effect Effects 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000001976 enzyme digestion Methods 0.000 claims description 5
- 235000013601 eggs Nutrition 0.000 claims description 4
- 230000007071 enzymatic hydrolysis Effects 0.000 claims description 4
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims description 4
- 102000004169 proteins and genes Human genes 0.000 claims description 4
- 108090000623 proteins and genes Proteins 0.000 claims description 4
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 claims description 3
- 102000002322 Egg Proteins Human genes 0.000 claims description 3
- 108010000912 Egg Proteins Proteins 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 235000014103 egg white Nutrition 0.000 claims description 3
- 210000000969 egg white Anatomy 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 230000003068 static effect Effects 0.000 claims description 3
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 abstract description 4
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 abstract description 4
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 abstract description 2
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 abstract description 2
- 229940024606 amino acid Drugs 0.000 abstract description 2
- 150000001413 amino acids Chemical class 0.000 abstract description 2
- 229910001424 calcium ion Inorganic materials 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052742 iron Inorganic materials 0.000 abstract description 2
- -1 iron ion Chemical class 0.000 abstract description 2
- 235000019192 riboflavin Nutrition 0.000 abstract description 2
- 229960002477 riboflavin Drugs 0.000 abstract description 2
- 239000002151 riboflavin Substances 0.000 abstract description 2
- 229960003080 taurine Drugs 0.000 abstract description 2
- 239000011573 trace mineral Substances 0.000 abstract 1
- 235000013619 trace mineral Nutrition 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 description 3
- 238000000926 separation method Methods 0.000 description 2
- 241000238424 Crustacea Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical group Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 210000004885 white matter Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/04—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from fish or other sea animals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/04—Animal proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/30—Working-up of proteins for foodstuffs by hydrolysis
- A23J3/32—Working-up of proteins for foodstuffs by hydrolysis using chemical agents
- A23J3/34—Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes
- A23J3/341—Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes of animal proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Zoology (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Marine Sciences & Fisheries (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
A method of albumen powder is made using South Pole squama shrimp, it is characterized in that the method the following steps are included: (1) raw material pretreatment: by squama shrimp carry out cleaning dry, (2) it dries and crushes: being put into dryer after drying, it is dried, shell after drying is put into pulverizer and carries out smashing processing, smashed powder is sieved, 120 mesh screens fine powder below is collected.Remaining crushing continues pulverization process; obtain krill meal; the protein content of krill be about 80% itself because marine; it is accompanied by the content of the various trace elements such as calcium ion, iron ion, taurine, riboflavin, amino acid; and the less expensive of krill; yield is also bigger, is easier to obtain on raw material.
Description
Technical field:
This hair is related to a kind of method using South Pole squama shrimp production albumen powder, belongs to the manufacture technology field of health care product.
Background technique
Krill is a kind of ocean for being distributed in antarctic waters without vertebra crustacean, and reserves are 6 .5~1,000,000,000
Ton.Protein content is up to 65~75% in krill dry weight.Krill Argine Monohydrochloride forms reasonable, essential amino acid
Content is high, is the huge animal protein resource treasure-house of the mankind, and carries out the important source material of protein higher value application.
Albumen powder is common health care product powder, but health care product is many kinds of now, and also type is also very for manufacture albumen powder
More, the raw material of the albumen powder of price is also universal also somewhat expensive, and the raw material of cheap albumen powder is also cheap, but product
Matter is without so perfect, and other microelements in protein are also fewer, basic reason be the selection of raw material not
It is so perfect.
Summary of the invention:
To solve the above-mentioned problems, the present invention provides a kind of method using South Pole squama shrimp production albumen powder
, certainly protein complex process, the lower disadvantage of purity are extracted in sorting in the prior art, and a kind of of proposition utilizes South Pole squama
The method of shrimp production albumen powder.Aiming at the shortcomings in the prior art, a kind of side using South Pole squama shrimp production albumen powder is provided
Method, the method the following steps are included:
A method of using South Pole squama shrimp make albumen powder, the method the following steps are included:
(1) pretreatment of raw material: squama shrimp is subjected to cleaning and is dried.
(2) it dries and crushes: being put into dryer after drying, dried, the shell after drying is put into pulverizer and carries out powder
Essence processing, smashed powder is sieved, and collects 120 mesh screens fine powder below.Remaining crushing continues at crushing
Reason, obtains krill meal
(3) adjust pH value: PH regulator, which is added, will adjust pH value between 7.0-8.0,
(4) it digests: being incorporated as the marine products of solution quality 0.2-0.3% after neutral solution is mixed with water 1:2-3 in mass ratio
Product protease, 50-55 DEG C of water enzyme digestion 6-8 h, during which and is stirred continuously, 85-90 DEG C of enzyme deactivations 10-15 is risen to after stirring
Min is cooled to 40-50 DEG C;
(5) left undisturbed overnight under the conditions of solution is put into 4 DEG C will be digested after cooling
(6) solution after static removes upper oil, and is filtered with three layers of gauze;Obtain krill polypeptide egg
White matter solution.(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, is centrifuged under the conditions of 6000-10000 rpm/min
5-10 min takes upper layer polypeptide protein solution;
(8) polypeptide protein solution is spray-dried, and rear ground 50-99 mesh standard sieve obtains polypeptide egg after spray-dried
White powder.
As preferred: it is between 7.5 that the step (3), which is added PH regulator and will adjust pH value,.
As preferred: the step (4) is incorporated as solution quality after mixing neutral solution with water 1:3 in mass ratio
0.3% marine product protease, 55 DEG C of 8 h of water enzyme digestion, during which and is stirred continuously, and 90 DEG C of enzyme deactivation 8min are risen to after stirring, cold
But to 45 DEG C;
As preferred: (6) three layers of filtered through gauze of the step, wherein interbed is enzymatic hydrolysis liquid layer.
As preferred: step (7) centrifuge separation: enzymolysis liquid is centrifuged at a high speed, 8000rpm/min condition
Lower centrifugation 8min takes upper layer polypeptide protein solution;
As preferred: step (8) the polypeptide protein solution is spray-dried, rear ground 80 target after spray-dried
Quasi- sieve obtains polypeptide albumen powder.
The present invention solves the deficiencies in the prior art using bright, from the krill selected in ocean on raw material, the egg of krill
White matter content be about 80% itself because marine, it is a variety of micro- to be accompanied by calcium ion, iron ion, taurine, riboflavin, amino acid etc.
The content of secondary element, and the less expensive of krill, yield is also bigger, is easier to obtain on raw material.
Specific embodiment
Below with reference to specific implementation example, the present invention is described in detail:
A method of using South Pole squama shrimp make albumen powder, the method the following steps are included:
(1) pretreatment of raw material: squama shrimp is subjected to cleaning and is dried.
(2) it dries and crushes: being put into dryer after drying, dried, the shell after drying is put into pulverizer and carries out powder
Essence processing, smashed powder is sieved, and collects 120 mesh screens fine powder below.Remaining crushing continues at crushing
Reason, obtains krill meal
(3) adjust pH value: PH regulator, which is added, will adjust pH value between 7.0-8.0,
(4) it digests: being incorporated as the marine products of solution quality 0.2-0.3% after neutral solution is mixed with water 1:2-3 in mass ratio
Product protease, 50-55 DEG C of water enzyme digestion 6-8 h, during which and is stirred continuously, 85-90 DEG C of enzyme deactivations 10-15 is risen to after stirring
Min is cooled to 40-50 DEG C;
(5) left undisturbed overnight under the conditions of solution is put into 4 DEG C will be digested after cooling
(6) solution after static removes upper oil, and is filtered with three layers of gauze;Obtain krill polypeptide egg
White matter solution.(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, is centrifuged under the conditions of 6000-10000 rpm/min
5-10 min takes upper layer polypeptide protein solution;
(8) polypeptide protein solution is spray-dried, and rear ground 50-99 mesh standard sieve obtains polypeptide egg after spray-dried
White powder.
As a preferred embodiment: it is between 7.5 that the step (3), which is added PH regulator and will adjust pH value,.
As a preferred embodiment: the step (4) is incorporated as solution after mixing neutral solution with water 1:3 in mass ratio
The marine product protease of quality 0.3%, 55 DEG C of 8 h of water enzyme digestion, during which and is stirred continuously, and 90 DEG C of enzyme deactivations are risen to after stirring
8min is cooled to 45 DEG C;
As a preferred embodiment: (6) three layers of filtered through gauze of the step, wherein interbed is enzymatic hydrolysis liquid layer.
As a preferred embodiment: step (7) centrifuge separation: enzymolysis liquid is centrifuged at a high speed, 8000rpm/
It is centrifuged 8min under the conditions of min, takes upper layer polypeptide protein solution;
As a preferred embodiment: step (8) the polypeptide protein solution is spray-dried, rear ground after spray-dried
80 mesh standard sieves obtain polypeptide albumen powder.
Claims (6)
1. a kind of method using South Pole squama shrimp production albumen powder, it is characterised in that the method the following steps are included:
(1) pretreatment of raw material: squama shrimp is subjected to cleaning and is dried;
(2) it dries and crushes: being put into dryer after drying, dried, the shell after drying is put into pulverizer and carries out at smashing
Reason, smashed powder is sieved, and collects 120 mesh screens fine powder below, remaining crushing continues pulverization process,
Obtain krill meal
(3) adjust pH value: PH regulator, which is added, will adjust pH value between 7.0-8.0,
(4) it digests: being incorporated as the marine products of solution quality 0.2-0.3% after neutral solution is mixed with water 1:2-3 in mass ratio
Product protease, 50-55 DEG C of water enzyme digestion 6-8 h, during which and is stirred continuously, 85-90 DEG C of enzyme deactivations 10-15 is risen to after stirring
Min is cooled to 40-50 DEG C;
(5) left undisturbed overnight under the conditions of solution is put into 4 DEG C will be digested after cooling
(6) solution after static removes upper oil, and is filtered with three layers of gauze;Obtain krill polypeptide egg
White matter solution;(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, is centrifuged under the conditions of 6000-10000 rpm/min
5-10 min takes upper layer polypeptide protein solution;
(8) polypeptide protein solution is spray-dried, and rear ground 50-99 mesh standard sieve obtains polypeptide egg after spray-dried
White powder.
2. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step
(3) it is between 7.5 that PH regulator, which is added, and will adjust pH value.
3. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step
(4) the marine product protease of solution quality 0.3%, 55 DEG C of water are incorporated as after mixing neutral solution with water 1:3 in mass ratio
Bath 8 h of enzymatic hydrolysis, during which and are stirred continuously, 90 DEG C of enzyme deactivation 8min are risen to after stirring, are cooled to 45 DEG C.
4. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step
(6) three layers of filtered through gauze, wherein interbed is enzymatic hydrolysis liquid layer.
5. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step
(7) it is centrifugated: enzymolysis liquid being centrifuged at a high speed, 8min is centrifuged under the conditions of 8000rpm/min, takes upper layer polypeptide protein
Matter solution.
6. a kind of method using South Pole squama shrimp production albumen powder according to claim 1, it is characterised in that the step
(8) polypeptide protein solution is spray-dried, and rear ground 80 mesh standard sieve obtains polypeptide albumen powder after spray-dried.
Priority Applications (1)
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CN201811461141.8A CN109349416A (en) | 2018-12-01 | 2018-12-01 | A method of albumen powder is made using South Pole squama shrimp |
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CN201811461141.8A CN109349416A (en) | 2018-12-01 | 2018-12-01 | A method of albumen powder is made using South Pole squama shrimp |
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Family
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CN201811461141.8A Pending CN109349416A (en) | 2018-12-01 | 2018-12-01 | A method of albumen powder is made using South Pole squama shrimp |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114431414A (en) * | 2022-03-02 | 2022-05-06 | 成都国酿食品股份有限公司 | Fermented bean curd compound seasoning, preparation method thereof and fermented bean curd |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104357206A (en) * | 2014-11-18 | 2015-02-18 | 董寰 | Method for preparing phospholipid-rich Antarctic krill oil by water enzyme process |
CN104388176A (en) * | 2014-11-10 | 2015-03-04 | 大连工业大学 | Method for preparing euphausia superba oil, microcapsule of euphausia superba oil and low-fluorine euphausia superba peptide by using aqueous enzymatic method |
-
2018
- 2018-12-01 CN CN201811461141.8A patent/CN109349416A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104388176A (en) * | 2014-11-10 | 2015-03-04 | 大连工业大学 | Method for preparing euphausia superba oil, microcapsule of euphausia superba oil and low-fluorine euphausia superba peptide by using aqueous enzymatic method |
CN104357206A (en) * | 2014-11-18 | 2015-02-18 | 董寰 | Method for preparing phospholipid-rich Antarctic krill oil by water enzyme process |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114431414A (en) * | 2022-03-02 | 2022-05-06 | 成都国酿食品股份有限公司 | Fermented bean curd compound seasoning, preparation method thereof and fermented bean curd |
CN114431414B (en) * | 2022-03-02 | 2023-12-29 | 成都国酿食品股份有限公司 | Fermented bean curd composite seasoning, preparation method thereof and fermented bean curd |
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Application publication date: 20190219 |
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