CN109349405A - A kind of moistening lung to arrest cough ointment and preparation method - Google Patents
A kind of moistening lung to arrest cough ointment and preparation method Download PDFInfo
- Publication number
- CN109349405A CN109349405A CN201811283100.4A CN201811283100A CN109349405A CN 109349405 A CN109349405 A CN 109349405A CN 201811283100 A CN201811283100 A CN 201811283100A CN 109349405 A CN109349405 A CN 109349405A
- Authority
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- Prior art keywords
- orange peel
- water
- dried orange
- radix glycyrrhizae
- ointment
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- 206010011224 Cough Diseases 0.000 title claims abstract description 18
- 210000004072 lung Anatomy 0.000 title claims abstract description 18
- 239000002674 ointment Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 235000021552 granulated sugar Nutrition 0.000 claims abstract description 13
- 241000234435 Lilium Species 0.000 claims abstract description 12
- 241000220324 Pyrus Species 0.000 claims abstract description 12
- 235000021017 pears Nutrition 0.000 claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 10
- 239000002562 thickening agent Substances 0.000 claims abstract description 10
- 239000004615 ingredient Substances 0.000 claims abstract description 8
- 238000011049 filling Methods 0.000 claims abstract description 7
- 238000013329 compounding Methods 0.000 claims abstract description 5
- 235000000346 sugar Nutrition 0.000 claims abstract description 5
- 244000068988 Glycine max Species 0.000 claims abstract description 3
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 3
- 235000009508 confectionery Nutrition 0.000 claims abstract description 3
- 235000013325 dietary fiber Nutrition 0.000 claims abstract description 3
- 238000002156 mixing Methods 0.000 claims abstract description 3
- 230000003068 static effect Effects 0.000 claims abstract description 3
- 230000001954 sterilising effect Effects 0.000 claims abstract description 3
- 239000007788 liquid Substances 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 5
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 4
- MTJGVAJYTOXFJH-UHFFFAOYSA-N 3-aminonaphthalene-1,5-disulfonic acid Chemical compound C1=CC=C(S(O)(=O)=O)C2=CC(N)=CC(S(O)(=O)=O)=C21 MTJGVAJYTOXFJH-UHFFFAOYSA-N 0.000 claims description 2
- VTAJIXDZFCRWBR-UHFFFAOYSA-N Licoricesaponin B2 Natural products C1C(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2)C(O)=O)C)(C)CC2)(C)C2C(C)(C)CC1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O VTAJIXDZFCRWBR-UHFFFAOYSA-N 0.000 claims description 2
- OBIOZWXPDBWYHB-UHFFFAOYSA-N Nobiletin Natural products C1=CC(OC)=CC=C1C1=C(OC)C(=O)C2=C(OC)C(OC)=C(OC)C(OC)=C2O1 OBIOZWXPDBWYHB-UHFFFAOYSA-N 0.000 claims description 2
- 239000000084 colloidal system Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 claims description 2
- 229960004949 glycyrrhizic acid Drugs 0.000 claims description 2
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 claims description 2
- 239000001685 glycyrrhizic acid Substances 0.000 claims description 2
- 235000019410 glycyrrhizin Nutrition 0.000 claims description 2
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 230000002706 hydrostatic effect Effects 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims description 2
- MRIAQLRQZPPODS-UHFFFAOYSA-N nobiletin Chemical compound C1=C(OC)C(OC)=CC=C1C1=CC(=O)C2=C(OC)C(OC)=C(OC)C(OC)=C2O1 MRIAQLRQZPPODS-UHFFFAOYSA-N 0.000 claims description 2
- 238000003825 pressing Methods 0.000 claims description 2
- 238000007789 sealing Methods 0.000 claims description 2
- 239000013049 sediment Substances 0.000 claims description 2
- 229910001220 stainless steel Inorganic materials 0.000 claims description 2
- 239000010935 stainless steel Substances 0.000 claims description 2
- 235000005979 Citrus limon Nutrition 0.000 claims 1
- 244000131522 Citrus pyriformis Species 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 235000013399 edible fruits Nutrition 0.000 claims 1
- 239000003814 drug Substances 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 244000025254 Cannabis sativa Species 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
Invent a kind of moistening lung to arrest cough ointment and preparation method, moistening lung to arrest cough ointment is made of the ingredient of following weight proportion: fresh pears 0.4 ~ 0.6%, Loquat-Shaped Cake 0.08 ~ 0.12%, Radix Glycyrrhizae 0.2 ~ 0.4%, dried orange peel 0.4 ~ 0.8%, lily 2.5 ~ 3.5%, white granulated sugar 12.5 ~ 13.0%, compounding thickener 0.31 ~ 0.34%, citric acid 0.004 ~ 0.006%, surplus is water.The ingredient of its best weight ratio is fresh pears 0.5%, Loquat-Shaped Cake 0.1%, Radix Glycyrrhizae 0.3%, dried orange peel 0.65%, lily 3.0%, white granulated sugar 12.8%, compounding thickener 0.325%, citric acid 0.005%, and surplus is water.It is extracted by static pressure such as the water lift-off heart, super-pressure, supercritical CO2Extraction, molten candy sugar, mixing, soybean dietary fiber, it is filling, sterilizing and etc. obtain product.Moistening lung to arrest cough ointment of the invention has been broken mostly using Chinese medicine as the moistening lung to arrest cough traditional product of primary raw material, has accomplished that color is various.
Description
Technical field
The present invention relates to a kind of ointment and preparation method, especially a kind of moistening lung to arrest cough ointment and preparation method.
Background technique
The product of moistening lung to arrest cough at present, which is mostly slightly mentioned with Chinese herbal medicine, to be mixed, herbal cuisine effect of seldom composite food and medium-height grass
The fine extraction of medicine can make product mouthfeel finer and smoother smooth.
Summary of the invention
The purpose of the present invention is invent a kind of moistening lung to arrest cough ointment and preparation method thereof.
Moistening lung to arrest cough ointment of the invention, it is characterised in that be made of the ingredient of following weight proportion: fresh pears 0.4 ~
0.6%, Loquat-Shaped Cake 0.08 ~ 0.12%, Radix Glycyrrhizae 0.2 ~ 0.4%, dried orange peel 0.4 ~ 0.8%, lily 2.5 ~ 3.5%, white granulated sugar 12.5 ~
13.0%, thickener 0.31 ~ 0.34%, citric acid 0.004 ~ 0.006% are compounded, surplus is water.
The ingredient of the best weight ratio of moistening lung to arrest cough ointment of the present invention are as follows: fresh pears 0.5%, Loquat-Shaped Cake 0.1%, Radix Glycyrrhizae
0.3%, dried orange peel 0.65%, lily 3.0%, white granulated sugar 12.8%, compounding thickener 0.325%, citric acid 0.005%, surplus is water.
The preparation method of moistening lung to arrest cough ointment of the invention, it is characterised in that the following steps are included:
(1) the water lift-off heart: the fresh pears of cleaned Loquat-Shaped Cake, chopping are put into together by formula ratio and are extracted in pot, are added 10 ~ 12 times
The water of medicinal material amount is extracted using circulation and boils extraction twice, and 1 hour every time, extracting solution the screen to filtrate more than 120 mesh was dense
It is reduced to the one third of original volume, sediment is centrifuged off and obtains concentrate, cooling is stored in freezer after cooling, and 2 ~ 8 DEG C of preservations are standby
With；
(2) superelevation isostatic cool pressing is extracted: cleaned Radix Glycyrrhizae is weighed by formula ratio, the water of 5 times of medicinal material amounts is added, and to be placed in superelevation cold
Equal static pressure extract in pot, with the hydrostatic pressure of 120 ~ 125MPa on mixed liquor under room temperature, and under a predetermined
It is kept for 1 hour, effective component is made to reach rapid release after balance, removed filter residue with the screen to filtrates more than 120 mesh and obtain Radix Glycyrrhizae filter
Liquid is stored in freezer, saves backup at 2 ~ 8 DEG C, and glycyrrhizic acid content is up to 73.09% in the Radix Glycyrrhizae filtrate；
(3) supercritical CO2Extraction: cleaned dried orange peel is weighed by formula ratio and is placed in supercritical CO2In extraction equipment, with liquid CO2
As spe medium, extracted 2 hours under conditions of 35 DEG C of temperature, pressure 30MPa, CO2Flow velocity is to obtain dried orange peel in 20kg/ hours
Dried orange peel extract is stored in freezer by extract, and 2 ~ 8 DEG C save backup, and Nobiletin and orange peel element are total in the dried orange peel extract
Content reaches 45.23mg/g；
(4) molten candy sugar: white granulated sugar is weighed by formula ratio and is placed in ingredients pot, the water of formula ratio is added, boils molten sugar, cooling is put
Cool to 55 ~ 60 DEG C, it is spare to obtain 50 DEG C of liquid glucose for the quantitative weight to formula ratio white granulated sugar and water；
(5) it mixes: the dried orange peel of Radix Glycyrrhizae filtrate, step (3) acquisition that the extraction concentrate of step (1) acquisition, step (2) are obtained
The liquid glucose that extract, step (4) obtain compounds thickener mixing with the citric acid of formula ratio and after immersion 30 minutes, obtains
Mixed liquor；
(6) soybean dietary fiber: cleaned lily is weighed by formula ratio and is sent into progress first time ultramicro grinding in colloid mill, is made
The granularity of material is down to 25 μm and is carried out second hereinafter, being re-fed into high pressure homogenizer together with the mixed liquor that step (5) obtains
Feed liquid is pulverized to obtain, makes the granularity of feed liquid at 2 μm or less；
(7) filling, sterilizing: feed liquid will be obtained from step (6) and is heated to 85 ~ 95 DEG C by heater, infused by stainless steel pipes
Enter quantitative hot filling in automatic filling machine, sterilizes after sealing, product can be obtained.
Moistening lung to arrest cough ointment of the invention has been broken mostly using Chinese medicine as the moistening lung to arrest cough traditional product of primary raw material, with
Fresh pears, Loquat-Shaped Cake are primary raw material, are equipped with the fine extract of Radix Glycyrrhizae, dried orange peel and lily, and processing technology is fine and smooth, efficient, environmentally friendly,
Formula is unique, and taste is smooth soft, has accomplished that color is various.
Specific embodiment
Embodiment 1
Formula: it fresh pears 0.5kg, Loquat-Shaped Cake 0.1kg, Radix Glycyrrhizae 0.3kg, dried orange peel 0.65kg, lily 3.0kg, white granulated sugar 12.8kg, answers
With thickener 0.325kg, citric acid 0.005kg and water 82.32kg.
Embodiment 2
Formula: it fresh pears 0.4kg, Loquat-Shaped Cake 0.08kg, Radix Glycyrrhizae 0.2kg, dried orange peel 0.4kg, lily 2.5kg, white granulated sugar 12.5kg, answers
With thickener 0.31kg, citric acid 0.004kg and water 83.606kg.
Embodiment 3
Formula: it fresh pears 0.6kg, Loquat-Shaped Cake 0.12kg, Radix Glycyrrhizae 0.4kg, dried orange peel 0.8kg, lily 3.5kg, white granulated sugar 13.0kg, answers
With thickener 0.34kg, citric acid 0.006kg and water 81.234kg.
Instant moistening lung to arrest cough ointment can be made in the formula of all embodiments according to above-mentioned preparation method.It is industrial when carrying out
It, can expanding production according to the ratio when metaplasia produces.
Claims (3)
1. a kind of moistening lung to arrest cough ointment, it is characterised in that: be made of the ingredient of following weight proportion: fresh pears 0.4 ~ 0.6%, Pi
Rake fruit 0.08 ~ 0.12%, Radix Glycyrrhizae 0.2 ~ 0.4%, dried orange peel 0.4 ~ 0.8%, lily 2.5 ~ 3.5%, white granulated sugar 12.5 ~ 13.0%, compounding increase
Thick dose 0.31 ~ 0.34%, citric acid 0.004 ~ 0.006%, surplus are water.
2. moistening lung to arrest cough ointment according to claim 1, it is characterised in that: the ingredient of best weight ratio is fresh pears
0.5%, Loquat-Shaped Cake 0.1%, Radix Glycyrrhizae 0.3%, dried orange peel 0.65%, lily 3.0%, white granulated sugar 12.8%, compounding thickener 0.325%, lemon
Acid 0.005%, surplus is water.
3. a kind of preparation method of moistening lung to arrest cough ointment of any of claims 1 or 2, it is characterised in that the following steps are included:
(1) the water lift-off heart: the fresh pears of cleaned Loquat-Shaped Cake, chopping are put into together by formula ratio and are extracted in pot, are added 10 ~ 12
The water of times medicinal material amount is extracted using circulation and boils extraction twice, and 1 hour every time, extracting solution the screen to filtrate more than 120 mesh,
It is concentrated into the one third of original volume, concentrate must be extracted by being centrifuged off sediment, and cooling is stored in freezer after cooling, and 2 ~ 8 DEG C
It saves backup；
(2) superelevation isostatic cool pressing is extracted: cleaned Radix Glycyrrhizae is weighed by formula ratio, the water of 5 times of medicinal material amounts is added, and to be placed in superelevation cold
Equal static pressure extract in pot, with the hydrostatic pressure of 120 ~ 125MPa on mixed liquor under room temperature, and under a predetermined
It is kept for 1 hour, effective component is made to reach rapid release after balance, removed filter residue with the screen to filtrates more than 120 mesh and obtain Radix Glycyrrhizae filter
Liquid is stored in freezer, saves backup at 2 ~ 8 DEG C, and glycyrrhizic acid content is up to 73.09% in the Radix Glycyrrhizae filtrate；
(3) supercritical CO2Extraction: cleaned dried orange peel is weighed by formula ratio and is placed in supercritical CO2In extraction equipment, with liquid CO2
As spe medium, extracted 2 hours under conditions of 35 DEG C of temperature, pressure 30MPa, CO2Flow velocity is to obtain dried orange peel in 20kg/ hours
Dried orange peel extract is stored in freezer by extract, and 2 ~ 8 DEG C save backup, and Nobiletin and orange peel element are total in the dried orange peel extract
Content reaches 45.23mg/g；
(4) molten candy sugar: white granulated sugar is weighed by formula ratio and is placed in ingredients pot, the water of formula ratio is added, boils molten sugar, cooling is put
Cool to 55 ~ 60 DEG C, it is spare to obtain 50 DEG C of liquid glucose for the quantitative weight to formula ratio white granulated sugar and water；
(5) it mixes: the dried orange peel of Radix Glycyrrhizae filtrate, step (3) acquisition that the extraction concentrate of step (1) acquisition, step (2) are obtained
The liquid glucose that extract, step (4) obtain compounds thickener mixing with the citric acid of formula ratio and after immersion 30 minutes, obtains
Mixed liquor；
(6) soybean dietary fiber: cleaned lily is weighed by formula ratio and is sent into progress first time ultramicro grinding in colloid mill, is made
The granularity of material is down to 25 μm and is carried out second hereinafter, being re-fed into high pressure homogenizer together with the mixed liquor that step (5) obtains
Feed liquid is pulverized to obtain, makes the granularity of feed liquid at 2 μm or less；
(7) filling, sterilizing: feed liquid will be obtained from step (6) and is heated to 85 ~ 95 DEG C by heater, infused by stainless steel pipes
Enter quantitative hot filling in automatic filling machine, sterilizes after sealing, product can be obtained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811283100.4A CN109349405A (en) | 2018-10-31 | 2018-10-31 | A kind of moistening lung to arrest cough ointment and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811283100.4A CN109349405A (en) | 2018-10-31 | 2018-10-31 | A kind of moistening lung to arrest cough ointment and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109349405A true CN109349405A (en) | 2019-02-19 |
Family
ID=65347412
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811283100.4A Pending CN109349405A (en) | 2018-10-31 | 2018-10-31 | A kind of moistening lung to arrest cough ointment and preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109349405A (en) |
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Application publication date: 20190219 |