CN109332630A - Preparation method for ADC12 alloy semi-solid blank - Google Patents
Preparation method for ADC12 alloy semi-solid blank Download PDFInfo
- Publication number
- CN109332630A CN109332630A CN201811250967.XA CN201811250967A CN109332630A CN 109332630 A CN109332630 A CN 109332630A CN 201811250967 A CN201811250967 A CN 201811250967A CN 109332630 A CN109332630 A CN 109332630A
- Authority
- CN
- China
- Prior art keywords
- alloy
- adc12 alloy
- adc12
- preparation
- solid blank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D17/00—Pressure die casting or injection die casting, i.e. casting in which the metal is forced into a mould under high pressure
- B22D17/007—Semi-solid pressure die casting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/04—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
- C22F1/043—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with silicon as the next major constituent
Abstract
The invention discloses a kind of preparation methods, especially disclose a kind of preparation method for ADC12 alloy semi-solid blank, belong to non-ferrous metal forging and stamping manufacturing technology field.A kind of spheroidal structure can be effectively controlled ADC12 alloy is provided, realizes that ADC12 alloy stablizes the preparation method for ADC12 alloy semi-solid blank of batch machining.The preparation method obtains the ADC12 alloy semi-solid blank by water cooled copper mould pressurization or water quenching after isothermal processes based on the predeformation ADC12 alloy after alloy grain breaking deformation.
Description
Technical field
The present invention relates to a kind of preparation methods, more particularly, to a kind of preparation side for ADC12 alloy semi-solid blank
Method belongs to non-ferrous metal forging and stamping manufacturing technology field.
Background technique
ADC12 alloy has fabulous casting character and comprehensive mechanical property, is highly suitable for high-pressure casting molding, is vapour
One of most widely used alloy in vehicle field.But since ingredient is close to al-si eutectic point, apparent viscosity is lower under molten state, pressure
It is easy volume gas in type casting moulding, is mingled with, causes casting compactness to decline, cannot further be heat-treated raising mechanical property.
Semi-solid processing forming technique be use microstructure for subsphaeroidal crystal grain be suspended in the semi-solid blank of liquid phase into
The molding technique of row.The semi-solid blank of subsphaeroidal solid phase exponentially declines with the increase apparent viscosity of shear rate, so that
Forming process slurry fluid stable, forming force are low, volume gas, be mingled with it is less.The key of the forming technique, which is to be prepared, to be had
The semi-solid blank of bulb tissue.It, can be by carrying out mechanical stirring or electricity in alloy solid-liquid two-phase temperature range under normal condition
The Strong shears effect such as magnetic stirring obtains spheroidal structure, but only about 10 DEG C of ADC12 alloy solid-liquid temperature range to be crushed dendrite, it is difficult to
Stable batch machining is carried out by traditional approach.
Summary of the invention
The technical problems to be solved by the present invention are: providing a kind of spheroidal structure that can be effectively controlled ADC12 alloy, realize
ADC12 alloy stablizes the preparation method for ADC12 alloy semi-solid blank of batch machining.
Used technical solution is to solve above-mentioned technical problem: a kind of system for ADC12 alloy semi-solid blank
Preparation Method, the preparation method is based on the predeformation ADC12 alloy after alloy grain breaking deformation, after isothermal processes
The ADC12 alloy semi-solid blank is obtained by water cooled copper mould pressurization or water quenching.
Further, dicing treatment is first carried out before carrying out at isothermal to predeformation ADC12 alloy, the pre- change after stripping and slicing
The volume for the ADC12 alloy semi-solid blank that the volume and needs of shape ADC12 alloy obtain is adapted.
The preferred mode of the above solution is that carrying out isothermal processes again after the completion of stripping and slicing, the design parameter of isothermal processes is,
Between 480 DEG C~550 DEG C, soaking time requires to select isothermal treatment temperatures interval selection according to corresponding solid rate
Between 10~500min.
Further, the use forging method for the predeformation ADC12 alloy that alloy grain is crushed obtains.
The preferred mode of the above solution is that the forging and stamping when forging obtains the broken predeformation ADC12 alloy of alloy grain
Than between 2~4.
The preferred mode of the above solution is that forging and stamping temperature control is between 200-300 DEG C.
The beneficial effects of the present invention are: the application is based on the predeformation ADC12 alloy after alloy grain breaking deformation,
The ADC12 alloy semi-solid blank is obtained by water cooled copper mould pressurization or water quenching after isothermal processes.In the above-mentioned of the application
In technical solution, due to having isothermal processes and water cooled copper mould pressurization or water quenching, so as to adequately by traditional plastic processing
Technology is used for the preparation of ADC12 alloy semi-solid blank in conjunction with isothermal preservation and controlling technology, on the one hand can overcome the alloy
Solid-liquid temperature range is narrow to be difficult to the shortcomings that liquid is directly processed, on the other hand also can more stable realization continuously prepare, fit
Close batch production.Its principle is that traditional Technology of Plastic Processing is distorted alloy grain, and there are huge distortion for intercrystalline
Can, at a proper temperature heat preservation distortion can be released be easy so that crystal boundary preferentially melt, rounding, thus formed spherical shape
Grain.Above-mentioned technology is exactly adequately utilized in the application, combines both, and both can be effectively controlled the ball of ADC12 alloy
Shape tissue, and ADC12 alloy may be implemented and stablize batch machining.
Detailed description of the invention
Fig. 1 be the present invention relates to ADC12 alloy raw element tree arborescent structure；
Fig. 2 be the present invention relates to ADC12 alloy spherical microstructure of semisolid.
Specific embodiment
In order to solve the above technical problems existing in the prior art, one kind provided by the invention can be effectively controlled ADC12
The spheroidal structure of alloy realizes that ADC12 alloy stablizes the preparation method for ADC12 alloy semi-solid blank of batch machining.
The preparation method passes through water based on the predeformation ADC12 alloy after alloy grain breaking deformation after isothermal processes
Cold copper mold pressurization or water quenching obtain the ADC12 alloy semi-solid blank.The application is with pre- after alloy grain breaking deformation
Based on deforming ADC12 alloy, the ADC12 alloy semi-solid is obtained by water cooled copper mould pressurization or water quenching after isothermal processes
Blank.In the above-mentioned technical proposal of the application, due to having isothermal processes and water cooled copper mould pressurization or water quenching, so as to abundant
The preparation that traditional Technology of Plastic Processing is used for ADC12 alloy semi-solid blank in conjunction with isothermal preservation and controlling technology, one
Aspect can overcome the alloy solid-liquid temperature range is narrow to be difficult to the shortcomings that liquid is directly processed, on the other hand also can be more stable
Realization continuously prepare, it is suitable for mass production.Its principle is that traditional Technology of Plastic Processing is distorted alloy grain, brilliant
There are huge distortion energy for intergranular, and heat preservation distortion, which can be released, at a proper temperature is easy so that crystal boundary preferentially melts, is round
Integralization, to form spheric granules.Above-mentioned technology is exactly adequately utilized in the application, combines both, Ji Nengyou
The spheroidal structure of effect control ADC12 alloy, and ADC12 alloy may be implemented and stablize batch machining.
In above embodiment, in order to control the spheroidal structure of ADC12 alloy to greatest extent, improves plastic processing and walk sequence
Final product quality, the application to predeformation ADC12 alloy carry out isothermal at before first carry out dicing treatment, the predeformation after stripping and slicing
The volume for the ADC12 alloy semi-solid blank that the volume and needs of ADC12 alloy obtain is adapted.Meanwhile also isothermal is kept the temperature
And the parameter of forging and stamping has carried out the control of more refinement matter, specifically: isothermal processes are carried out again after the completion of stripping and slicing, isothermal processes
Design parameter is that between 480 DEG C~550 DEG C, soaking time requires isothermal treatment temperatures interval selection according to corresponding solid rate
Selection is between 10~500min.
Correspondingly, process equipment is simple, at low cost since forging technology is most traditional metal plastic deformation technique
It is honest and clean, with short production cycle, it is very suitable for the predeformation of alloy.Therefore the broken predeformation ADC12 alloy of the application alloy grain
It is obtained using forging method.Ratio of forging reduction when forging obtains the broken predeformation ADC12 alloy of alloy grain is between 2~4；
Temperature control is forged and pressed between 200-300 DEG C.
The present invention combines traditional forging deformation technique and Semi-solid Blank Production, realizes ADC12
The efficient preparation of the effectively controllable semi-solid blank of the high-quality spheroidal structure of alloy, further promotes and applies for the alloy and opens up
New approaches.
The present invention is described in detail combined with specific embodiments below.
Embodiment 1
The present embodiment is related to a kind of preparation method for forging predeformation ADC12 alloy semi-solid blank；The method includes
Following steps:
200 DEG C of ADC12 alloy is subjected to forging predeformation under 2 ratio of forging reduction.Then by the predeformation alloy 480
DEG C heat-treatment furnace keeps the temperature 500min, then quenches in water, then is made the semi-solid blank for having spheroidal structure, it is specific as Fig. 1,
Shown in Fig. 2, Fig. 1 is original dendrite tissue, and Fig. 2 is spherical microstructure of semisolid.
Embodiment 2
The present embodiment is related to a kind of preparation method for forging predeformation ADC12 alloy semi-solid blank；The method includes
Following steps:
300 DEG C of ADC12 alloy is carried out forging predeformation under 3 ratio of forging reduction.Then by the predeformation alloy 550
DEG C heat preservation 10min, is then quickly transferred to copper mold pressurization cooling, is then made and has the semi-solid blank of spheroidal structure.
Embodiment 3
The present embodiment is related to a kind of preparation method for forging predeformation ADC12 alloy semi-solid blank；The method includes
Following steps:
200 DEG C of ADC12 alloys are carried out the open die forging predeformation that forging ratio is about 4 in forging press.Then by the pre- change
Shape alloy keeps the temperature 100min in 500 DEG C of isothermals, is then quickly transferred to cold water quenching, then the semisolid of spheroidal structure is prepared
Blank.
Claims (6)
1. a kind of preparation method for ADC12 alloy semi-solid blank, it is characterised in that: the preparation method is with alloy crystalline substance
Based on predeformation ADC12 alloy after grain breaking deformation, institute is obtained by water cooled copper mould pressurization or water quenching after isothermal processes
The ADC12 alloy semi-solid blank stated.
2. the preparation method according to claim 1 for ADC12 alloy semi-solid blank, it is characterised in that: to pre-
Deformation ADC12 alloy carries out first carrying out dicing treatment before at isothermal, and the volume of the predeformation ADC12 alloy after stripping and slicing is obtained with needs
The volume of the ADC12 alloy semi-solid blank obtained is adapted.
3. the preparation method according to claim 2 for ADC12 alloy semi-solid blank, it is characterised in that: stripping and slicing is complete
Cheng Houzai carries out isothermal processes, and the design parameter of isothermal processes is,
For isothermal treatment temperatures interval selection between 480 DEG C~550 DEG C, soaking time requires selection 10 according to corresponding solid rate
Between~500min.
4. the preparation method according to claim 1 for ADC12 alloy semi-solid blank, it is characterised in that: alloy is brilliant
The use forging method of the broken predeformation ADC12 alloy of grain obtains.
5. the preparation method according to claim 4 for ADC12 alloy semi-solid blank, it is characterised in that: forging
Ratio of forging reduction when the predeformation ADC12 alloy that acquisition alloy grain is crushed is between 2~4.
6. the preparation method according to claim 5 for ADC12 alloy semi-solid blank, it is characterised in that: forging and stamping temperature
Degree control is between 200-300 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811250967.XA CN109332630B (en) | 2018-10-25 | 2018-10-25 | Preparation method of semi-solid blank for ADC12 alloy |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811250967.XA CN109332630B (en) | 2018-10-25 | 2018-10-25 | Preparation method of semi-solid blank for ADC12 alloy |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109332630A true CN109332630A (en) | 2019-02-15 |
| CN109332630B CN109332630B (en) | 2021-03-30 |
Family
ID=65312084
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811250967.XA Active CN109332630B (en) | 2018-10-25 | 2018-10-25 | Preparation method of semi-solid blank for ADC12 alloy |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109332630B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110643913A (en) * | 2019-10-31 | 2020-01-03 | 成都先进金属材料产业技术研究院有限公司 | Preparation method of aluminum alloy semi-solid structure for pre-deformation vehicle |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102284536A (en) * | 2011-05-30 | 2011-12-21 | 哈尔滨工业大学 | Preparation device and method of light-alloy semisolid blanks by equal-channel reciprocating extrusion and spheroidization |
| CN104525829A (en) * | 2014-12-26 | 2015-04-22 | 西安交通大学 | Radial forging strain-induced semi-solid state process for manufacturing aluminum alloy crankshaft of air condition compressor |
| CN104561852A (en) * | 2014-12-26 | 2015-04-29 | 西安交通大学 | Process for preparing semi-solid state aluminum alloy scroll plate by radial forging strain induction method |
| CN104624914A (en) * | 2014-12-26 | 2015-05-20 | 西安交通大学 | Semisolid process for manufacturing engine aluminum alloy cam shaft through radial forging strain provocation method |
| CN104726809A (en) * | 2015-02-06 | 2015-06-24 | 西安交通大学 | Radial forging type strain-induced semi-solid integral die forging process of blade |
| CN107012415A (en) * | 2017-04-20 | 2017-08-04 | 哈尔滨工业大学 | A kind of preparation method of wrought aluminium alloy high solid fractions semi solid slurry applied to semi-solid die casting |
-
2018
- 2018-10-25 CN CN201811250967.XA patent/CN109332630B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102284536A (en) * | 2011-05-30 | 2011-12-21 | 哈尔滨工业大学 | Preparation device and method of light-alloy semisolid blanks by equal-channel reciprocating extrusion and spheroidization |
| CN104525829A (en) * | 2014-12-26 | 2015-04-22 | 西安交通大学 | Radial forging strain-induced semi-solid state process for manufacturing aluminum alloy crankshaft of air condition compressor |
| CN104561852A (en) * | 2014-12-26 | 2015-04-29 | 西安交通大学 | Process for preparing semi-solid state aluminum alloy scroll plate by radial forging strain induction method |
| CN104624914A (en) * | 2014-12-26 | 2015-05-20 | 西安交通大学 | Semisolid process for manufacturing engine aluminum alloy cam shaft through radial forging strain provocation method |
| CN104726809A (en) * | 2015-02-06 | 2015-06-24 | 西安交通大学 | Radial forging type strain-induced semi-solid integral die forging process of blade |
| CN107012415A (en) * | 2017-04-20 | 2017-08-04 | 哈尔滨工业大学 | A kind of preparation method of wrought aluminium alloy high solid fractions semi solid slurry applied to semi-solid die casting |
Non-Patent Citations (1)
| Title |
|---|
| 王永飞等: "径向锻式应变诱发法制备半固态坯料的研究", 《稀有金属材料与工程》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110643913A (en) * | 2019-10-31 | 2020-01-03 | 成都先进金属材料产业技术研究院有限公司 | Preparation method of aluminum alloy semi-solid structure for pre-deformation vehicle |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109332630B (en) | 2021-03-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105268884B (en) | Method for forging superhigh-temperature soft core of steel ingot | |
| CN109338185A (en) | A kind of preparation method of high-strength 7 line aluminium alloy profile | |
| CN106890865B (en) | Major diameter AQ80M magnesium alloy cake materials squeeze forging and integrate forming technology | |
| CN101748251A (en) | Forging method of Cr12MoV cold work die steel module | |
| CN1329549C (en) | Heating technology for refining TiAl alloy ingot microscopic texture | |
| CN107099762A (en) | A kind of Hot Deformation Strengthening method of magnesium-rare earth | |
| CN110468361A (en) | A kind of preparation method of wrought superalloy fine grain bar | |
| CN111687369B (en) | Forging method of petroleum valve block for fracturing pump | |
| CN103469130A (en) | Thermal deformation strengthening method of rare-earth magnesium alloy | |
| CN102787263B (en) | Method for manufacturing aluminum alloy rivet rod for aerospace product | |
| CN102268621A (en) | Production method of aluminium alloy bar | |
| CN109332630A (en) | Preparation method for ADC12 alloy semi-solid blank | |
| CN1032962A (en) | Technology of equiaxial miniaturization of crystal microstructure of alpha+beta titanium alloys | |
| CN101250618A (en) | Grain ultra-refining method for Fe-32%Ni alloy | |
| CN1234883C (en) | Isothermal spheroidizing technique for H13 steel | |
| CN107974632B (en) | Austenite hot-work die steel and preparation method thereof | |
| CN104324968A (en) | Extrusion method of hollow aluminum sections | |
| CN111575561B (en) | Aluminum-lithium alloy for large-depth pressure-bearing shell and preparation method thereof | |
| CN109128078B (en) | Preparation method of isothermal semi-solid structure slurry of aluminum alloy die-casting billet | |
| CN102534293B (en) | High strength superfine crystalloid copper-germanium alloy and preparation method thereof | |
| CN104561489A (en) | Process for preparing semisolid steel blank by using radial forging strain induction method | |
| CN103173703A (en) | Process for improving age hardening effect of high-zinc deformed magnesium alloy | |
| CN109202031A (en) | The preparation method of the automobile-used alloy semi-solid blank of predeformation | |
| CN106566914A (en) | Heat treatment method for tool and mould steel obtained after electroslag remelting continuous directional solidification | |
| CN100360700C (en) | Composite preparation method for isothermal spherocrystallization semisolid blank from magnesium alloy by diameter variable curve extrusion pressing and shearing induction |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 610306 Chengdu City, Chengdu, Sichuan, China (Sichuan) free trade test zone, Chengdu City, Qingbaijiang District, xiangdao Boulevard, Chengxiang Town, No. 1509 (room 13, A District, railway port mansion), room 1319 Patentee after: Chengdu advanced metal material industry technology Research Institute Co.,Ltd. Address before: 610306 Chengdu City, Chengdu, Sichuan, China (Sichuan) free trade test zone, Chengdu City, Qingbaijiang District, xiangdao Boulevard, Chengxiang Town, No. 1509 (room 13, A District, railway port mansion), room 1319 Patentee before: CHENGDU ADVANCED METAL MATERIAL INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder |