CN109330945A - A kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients - Google Patents

A kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients Download PDF

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Publication number
CN109330945A
CN109330945A CN201811446313.4A CN201811446313A CN109330945A CN 109330945 A CN109330945 A CN 109330945A CN 201811446313 A CN201811446313 A CN 201811446313A CN 109330945 A CN109330945 A CN 109330945A
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parts
chinese medicine
traditional chinese
medicine ingredients
containing traditional
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CN201811446313.4A
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孙丽丽
翟颖敏
谷智媛
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Yantai Bafang Cultural Media Co Ltd
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Yantai Bafang Cultural Media Co Ltd
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Priority to CN201811446313.4A priority Critical patent/CN109330945A/en
Publication of CN109330945A publication Critical patent/CN109330945A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00—Formulations or additives for perfume preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients, raw material including following parts by weight: 30-50 parts of Radix Paeoniae Alba, 10-20 parts of Radix Codonopsis, 10-20 parts of Semen sesami nigrum, 1-3 parts of triethyl citrate, 1-3 parts of salicylic acid benzyl ester, 0.5-2 parts of lilial, 20-30 parts of dipropylene glycol, 2-6 parts of dihydrojasmonate, 0.2-0.8 parts of leaf-alcohol, 0.02-0.08 parts of sodium alginate, 2-5 parts of distilled water, fragrance of the present invention is pure and fresh pleasant, smell with pleasant, and preparation method is simple, raw material is prepared to be easy to get, cost is relatively low, it is with good economic efficiency, and the moisturizing perfume produced by the present invention containing traditional Chinese medicine ingredients, the fragrance residence time is long, fragrance more lasting stability, soothing effect is significant, by adding Radix Paeoniae Alba, Radix Codonopsis , substantially increase lasting fragrance and soothing effect.

Description

A kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients
Technical field
The present invention relates to cosmetic field, specifically a kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients.
Background technique
Perfume is the alcoholic solution of essence, then plus the mixture of the formation such as fixastive in right amount.With the strong fragrance of fragrance, Main function is to be sprayed on the positions such as the hem, handkerchief and hairline, distributes pleasant fragrance, is important one of cosmetics.Perfume Middle essence dosage is higher, and generally 15%~25%, concentration of alcohol is 75%~85%, and 5% water energy, which is added, sends out fragrance thoroughly.Ten From the second half in nineth century, perfume manufacturing technology comparative maturity, the way of distillation of early stage is replaced by volatile solvent, especially people Work synthetic perfume is born in France, and perfume is no longer limited to natural essence, this rapidly develops perfumes industry.
However perfume on the market can only often provide the smell of fragrance, not have moisturizing function.
Summary of the invention
The purpose of the present invention is to provide a kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients, it is above-mentioned to solve The problem of being proposed in background technique.
To achieve the above object, the invention provides the following technical scheme:
A kind of moisturizing perfume containing traditional Chinese medicine ingredients, the raw material including following parts by weight: 30-50 parts of Radix Paeoniae Alba, Radix Codonopsis 10- 20 parts, 10-20 parts of Semen sesami nigrum, 1-3 parts of triethyl citrate, 1-3 parts of salicylic acid benzyl ester, 0.5-2 parts of lilial, dipropylene glycol 20- 30 parts, 2-6 parts of dihydrojasmonate, 0.2-0.8 parts of leaf-alcohol, 0.02-0.08 parts of sodium alginate, 2-5 parts of distilled water.
As a further solution of the present invention: the raw material including following parts by weight: 35-45 parts of Radix Paeoniae Alba, Radix Codonopsis 12-18 Part, 12-18 parts of Semen sesami nigrum, 1.5-2.5 parts of triethyl citrate, 1.5-2.5 parts of salicylic acid benzyl ester, 0.8-1.8 parts of lilial, dipropyl 22-28 parts of glycol, 3-5 parts of dihydrojasmonate, 0.4-0.6 parts of leaf-alcohol, 0.03-0.07 parts of sodium alginate, distilled water 2.5-4.5 part.
As the present invention further scheme: the raw material including following parts by weight: 40 parts of Radix Paeoniae Alba, 15 parts of Radix Codonopsis, black 15 parts of sesame, 2 parts of triethyl citrate, 2 parts of salicylic acid benzyl ester, 1.5 parts of lilial, 25 parts of dipropylene glycol, dihydro jasmone acid first 4 parts of ester, 0.5 part of leaf-alcohol, 0.05 part of sodium alginate, 4 parts of distilled water.
A kind of preparation method of the moisturizing perfume containing traditional Chinese medicine ingredients, which comprises the following steps: (1) will be white Chinese herbaceous peony, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) it will be crushed in Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum investment pulverizer, obtain mixture； (3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 35-38MPa, 35-45 DEG C of extraction temperature, Obtain essential oil of traditional Chinese medicine；(4) sodium alginate is put into distilled water, stirring is completely dissolved to sodium alginate, and it is molten to obtain sodium alginate Liquid；(5) triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, microwave shakes 20-40min, obtains Mixed liquor A；(6) essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydrojasmonate, leaf-alcohol are put into reaction kettle, Heated sealed stirring, heating temperature are 55-65 DEG C, obtain semi-finished product；(7) semi-finished product are poured into sealing container, is aged 60-80 It to get.
As further scheme of the invention: in step (3), extracting pressure 36MPa.
As further scheme of the invention: in step (3), extraction temperature is 40 DEG C.
As further scheme of the invention: in step (5), microwave shakes the time for 30min.
As further scheme of the invention: in step (6), heating temperature is 60 DEG C.
As further scheme of the invention: in step (7), digestion time is 70 days.
Compared with prior art, the beneficial effects of the present invention are: fragrance of the present invention is pure and fresh pleasant, the gas with pleasant Taste, and preparation method is simple, prepares raw material and is easy to get, cost is relatively low, with good economic efficiency, and it is produced by the present invention containing The moisturizing perfume of traditional Chinese medicine ingredients, containing Chinese medicine natural component, the fragrance residence time is long, fragrance more lasting stability, soothing effect Significantly, by adding Radix Paeoniae Alba, Radix Codonopsis, lasting fragrance and soothing effect are substantially increased.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of moisturizing perfume containing traditional Chinese medicine ingredients, including following raw material: Radix Paeoniae Alba 30g, Radix Codonopsis 10g, Semen sesami nigrum 10g, lemon Lemon triethylenetetraminehexaacetic acid ester 1g, salicylic acid benzyl ester 1g, lilial 0.5g, dipropylene glycol 20g, dihydrojasmonate 2g, leaf-alcohol 0.2g, sea Mosanom 0.02g, distilled water 2g.
A kind of preparation method of the moisturizing perfume containing traditional Chinese medicine ingredients, which comprises the following steps: (1) will be white Chinese herbaceous peony, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) it will be crushed in Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum investment pulverizer, obtain mixture； (3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 35MPa, is obtained by 35 DEG C of extraction temperature Medicine essential oil；(4) sodium alginate is put into distilled water, stirring is completely dissolved to sodium alginate, obtains sodium alginate soln；(5) Triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, microwave shakes 20min, obtains mixed liquor A； (6) essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydrojasmonate, leaf-alcohol are put into reaction kettle, heated sealed Stirring, heating temperature are 55 DEG C, obtain semi-finished product；(7) semi-finished product are poured into sealing container, be aged 60 days to get.
Embodiment 2
A kind of moisturizing perfume containing traditional Chinese medicine ingredients, including following raw material: Radix Paeoniae Alba 50g, Radix Codonopsis 20g, Semen sesami nigrum 20g, lemon Lemon triethylenetetraminehexaacetic acid ester 3g, salicylic acid benzyl ester 3g, lilial 2g, dipropylene glycol 30g, dihydrojasmonate 6g, leaf-alcohol 0.8g, seaweed Sour sodium 0.08g, distilled water 5g.
A kind of preparation method of the moisturizing perfume containing traditional Chinese medicine ingredients, which comprises the following steps: (1) will be white Chinese herbaceous peony, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) it will be crushed in Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum investment pulverizer, obtain mixture； (3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 38MPa, is obtained by 45 DEG C of extraction temperature Medicine essential oil；(4) sodium alginate is put into distilled water, stirring is completely dissolved to sodium alginate, obtains sodium alginate soln；(5) Triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, microwave shakes 40min, obtains mixed liquor A； (6) essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydrojasmonate, leaf-alcohol are put into reaction kettle, heated sealed Stirring, heating temperature are 65 DEG C, obtain semi-finished product；(7) semi-finished product are poured into sealing container, be aged 80 days to get.
Embodiment 3
A kind of moisturizing perfume containing traditional Chinese medicine ingredients, including following raw material: Radix Paeoniae Alba 35g, Radix Codonopsis 12g, Semen sesami nigrum 12g, lemon Lemon triethylenetetraminehexaacetic acid ester 1.5g, salicylic acid benzyl ester 1.5g, lilial 0.8g, dipropylene glycol 22g, dihydrojasmonate 3g, leaf-alcohol 0.4g, sodium alginate 0.03g, distilled water 2.5g.
A kind of preparation method of the moisturizing perfume containing traditional Chinese medicine ingredients, which comprises the following steps: (1) will be white Chinese herbaceous peony, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) it will be crushed in Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum investment pulverizer, obtain mixture； (3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 37MPa, is obtained by 38 DEG C of extraction temperature Medicine essential oil；(4) sodium alginate is put into distilled water, stirring is completely dissolved to sodium alginate, obtains sodium alginate soln；(5) Triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, microwave shakes 25min, obtains mixed liquor A； (6) essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydrojasmonate, leaf-alcohol are put into reaction kettle, heated sealed Stirring, heating temperature are 58 DEG C, obtain semi-finished product；(7) semi-finished product are poured into sealing container, be aged 68 days to get.
Embodiment 4
A kind of moisturizing perfume containing traditional Chinese medicine ingredients, including following raw material: Radix Paeoniae Alba 45g, Radix Codonopsis 18g, Semen sesami nigrum 18g, lemon Lemon triethylenetetraminehexaacetic acid ester 2.5g, salicylic acid benzyl ester 2.5g, lilial 1.8g, dipropylene glycol 28g, dihydrojasmonate 5g, leaf-alcohol 0.6g, sodium alginate 0.07g, distilled water 4.5g.
A kind of preparation method of the moisturizing perfume containing traditional Chinese medicine ingredients, which comprises the following steps: (1) will be white Chinese herbaceous peony, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) it will be crushed in Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum investment pulverizer, obtain mixture； (3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 37MPa, is obtained by 38 DEG C of extraction temperature Medicine essential oil；(4) sodium alginate is put into distilled water, stirring is completely dissolved to sodium alginate, obtains sodium alginate soln；(5) Triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, microwave shakes 35min, obtains mixed liquor A； (6) essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydrojasmonate, leaf-alcohol are put into reaction kettle, heated sealed Stirring, heating temperature are 58 DEG C, obtain semi-finished product；(7) semi-finished product are poured into sealing container, be aged 75 days to get.
Embodiment 5
A kind of moisturizing perfume containing traditional Chinese medicine ingredients, including following raw material: Radix Paeoniae Alba 40g, Radix Codonopsis 15g, Semen sesami nigrum 15g, lemon Lemon triethylenetetraminehexaacetic acid ester 2g, salicylic acid benzyl ester 2g, lilial 1.5g, dipropylene glycol 25g, dihydrojasmonate 4g, leaf-alcohol 0.5g, sea Mosanom 0.05g, distilled water 4g.
A kind of preparation method of the moisturizing perfume containing traditional Chinese medicine ingredients, which comprises the following steps: (1) will be white Chinese herbaceous peony, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) it will be crushed in Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum investment pulverizer, obtain mixture； (3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 36MPa, is obtained by 40 DEG C of extraction temperature Medicine essential oil；(4) sodium alginate is put into distilled water, stirring is completely dissolved to sodium alginate, obtains sodium alginate soln；(5) Triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, microwave shakes 30min, obtains mixed liquor A； (6) essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydrojasmonate, leaf-alcohol are put into reaction kettle, heated sealed Stirring, heating temperature are 60 DEG C, obtain semi-finished product；(7) semi-finished product are poured into sealing container, be aged 70 days to get.
Comparative example 1
In addition to without Radix Paeoniae Alba, remaining its raw material and preparation process and embodiment 5 are unanimously.
Comparative example 2
In addition to without Radix Codonopsis, remaining its raw material and preparation process and embodiment 5 are unanimously.
Comparative example 3
In addition to without Radix Paeoniae Alba, Radix Codonopsis, remaining its raw material and preparation process and embodiment 5 are unanimously.
Comparative example 4
Essential oil of traditional Chinese medicine will be obtained after Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum extraction, essential oil of traditional Chinese medicine and remaining each raw material is directly stirred mixed It closes to get the additive amount and embodiment 5 of each raw material are consistent.
Moisturizing perfume containing traditional Chinese medicine ingredients made from Example 1-5, comparative example 1-4, do the measurement of fragrance residence time, Soothing effect measurement, measuring method is that 180 skin quality are close, age identical young woman is divided into 9 groups, is sprayed to the back of the hand Perfume, measurement result are as shown in the table:
Table 1: perfume test result record sheet
It is fragrant by upper surface it is known that the moisturizing perfume produced by the present invention containing traditional Chinese medicine ingredients, the fragrance residence time is long Taste more lasting stability, soothing effect is significant, by adding Radix Paeoniae Alba, Radix Codonopsis, substantially increases lasting fragrance and moisturizing effect Fruit.
The preferred embodiment of the patent is described in detail above, but this patent is not limited to above-mentioned embodiment party Formula within the knowledge of one of ordinary skill in the art can also be under the premise of not departing from this patent objective Various changes can be made.

Claims (9)

1. a kind of moisturizing perfume containing traditional Chinese medicine ingredients, which is characterized in that the raw material including following parts by weight: Radix Paeoniae Alba 30-50 Part, 10-20 parts of Radix Codonopsis, 10-20 parts of Semen sesami nigrum, 1-3 parts of triethyl citrate, 1-3 parts of salicylic acid benzyl ester, 0.5-2 parts of lilial, two 20-30 parts of propylene glycol, 2-6 parts of dihydrojasmonate, 0.2-0.8 parts of leaf-alcohol, 0.02-0.08 parts of sodium alginate, distilled water 2-5 parts.
2. the moisturizing perfume according to claim 1 containing traditional Chinese medicine ingredients, which is characterized in that including following parts by weight Raw material: 35-45 parts of Radix Paeoniae Alba, 12-18 parts of Radix Codonopsis, 12-18 parts of Semen sesami nigrum, 1.5-2.5 parts of triethyl citrate, salicylic acid benzyl ester 1.5- 2.5 parts, 0.8-1.8 parts of lilial, 22-28 parts of dipropylene glycol, 3-5 parts of dihydrojasmonate, 0.4-0.6 parts of leaf-alcohol, sea 0.03-0.07 parts of mosanom, 2.5-4.5 parts of distilled water.
3. the moisturizing perfume according to claim 1 containing traditional Chinese medicine ingredients, which is characterized in that including following parts by weight Raw material: 40 parts of Radix Paeoniae Alba, 15 parts of Radix Codonopsis, 15 parts of Semen sesami nigrum, 2 parts of triethyl citrate, 2 parts of salicylic acid benzyl ester, 1.5 parts of lilial, two 25 parts of propylene glycol, 4 parts of dihydrojasmonate, 0.5 part of leaf-alcohol, 0.05 part of sodium alginate, 4 parts of distilled water.
4. a kind of preparation method of the moisturizing perfume according to claim 1 to 3 containing traditional Chinese medicine ingredients, feature exist In, comprising the following steps: (1) Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum are cleaned drained and standby；(2) Radix Paeoniae Alba, Radix Codonopsis, Semen sesami nigrum are put into powder It is crushed in broken machine, obtains mixture；(3) mixture is extracted, using carbon dioxide supercritical extraction, extracting pressure 35- 38MPa, obtains essential oil of traditional Chinese medicine by 35-45 DEG C of extraction temperature；(4) sodium alginate is put into distilled water, is stirred complete to sodium alginate Fully dissolved obtains sodium alginate soln；(5) triethyl citrate, salicylic acid benzyl ester, lilial, dipropylene glycol are mixed, Microwave shakes 20-40min, obtains mixed liquor A；(6) by essential oil of traditional Chinese medicine, sodium alginate soln, mixed liquor A, dihydro jasmone acid In methyl esters, leaf-alcohol investment reaction kettle, heated sealed stirring, heating temperature is 55-65 DEG C, obtains semi-finished product；(7) semi-finished product are fallen Enter in sealing container, be aged 60-80 days to get.
5. the preparation method of the moisturizing perfume according to claim 4 containing traditional Chinese medicine ingredients, which is characterized in that step (3) In, extracting pressure 36MPa.
6. the preparation method of the moisturizing perfume according to claim 4 containing traditional Chinese medicine ingredients, which is characterized in that step (3) In, extraction temperature is 40 DEG C.
7. the preparation method of the moisturizing perfume according to claim 4 containing traditional Chinese medicine ingredients, which is characterized in that step (5) In, microwave shakes the time for 30min.
8. the preparation method of the moisturizing perfume according to claim 4 containing traditional Chinese medicine ingredients, which is characterized in that step (6) In, heating temperature is 60 DEG C.
9. the preparation method of the moisturizing perfume according to claim 4 containing traditional Chinese medicine ingredients, which is characterized in that step (7) In, digestion time is 70 days.
CN201811446313.4A 2018-11-29 2018-11-29 A kind of moisturizing perfume and preparation method thereof containing traditional Chinese medicine ingredients Withdrawn CN109330945A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111297756A (en) * 2020-02-25 2020-06-19 刘燕 Essence with moistening and moisturizing and anti-allergy effects and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111297756A (en) * 2020-02-25 2020-06-19 刘燕 Essence with moistening and moisturizing and anti-allergy effects and preparation method thereof
CN111297756B (en) * 2020-02-25 2020-11-13 广东康容实业有限公司 Essence with moistening and moisturizing and anti-allergy effects and preparation method thereof

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