CN109330903A - A kind of clean oil packet water aqua type preparation method and applications - Google Patents
A kind of clean oil packet water aqua type preparation method and applications Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/585—Organosilicon compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
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- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a kind of clean oil packet water aqua type preparation method and applications, and Aqueous Phase Raw Material is uniformly mixed, and are heated to 80-100 DEG C, and sterilize 10-30min, are cooled to room temperature, additive are slowly added to be uniformly mixed spare；Water-in-oil emulsifier is added in oily phase raw material, it is uniformly mixed, it is spare (to be added if any solid or semisolid grease, then need appropriate heating and melting), then under high velocity agitation, the above-mentioned Aqueous Phase Raw Material that additive has been added is slowly added to emulsify in the oily phase raw material for having added emulsifier, homogeneous is carried out under vacuum condition, it is eventually adding preservative and essence, continuation stirs under vacuum, discharges and dispense after mixing evenly.The present invention is only added to the oil components of 10%-15%, and Water-In-Oil dosage form is allowed to be presented transparent quality, stability, sense of touch, usability more preferably, salubrious non-greasy while moisturizing is moistened.
Description
Technical field
The present invention relates to cosmetics processing technique field, relate particularly to a kind of clean oil packet water aqua type preparation method and
It is applied.
Background technique
The completion of skin metabolism function needs a large amount of moisture, and the Water Cycle that human body daily intakes to it is facial
Through very limited, not nearly enough required content.And skin water shortage will lead to the generation of many problems, as peeling, pore are coarse
Skin is helped to complete this important link of replenishing water and preserving moisture Deng, it is therefore desirable to all kinds of cosmetics.But skin is only given simply
Moisturizing, although the temporary moisturizing of skin can be allowed, but when dry weather, the moisture in skin is easy to distribute, but also can band
Original moisture in skin, do not play the role of replenishing water and preserving moisture not only, also make skin more and more dry.Oiliness raw material can be
Play the role of that moisture and air is isolated in cosmetics, plays the moist purpose of water lock.
Emulsification composition is roughly divided into oil-in-water type (O/W) and water-in-oil type (W/O), and then there is also Water-In-Oil oil-ins
(O/W/O), the multiple type such as water-in-oil type (W/O/W) in water.All the time, these are effectively used to skin care in cosmetic field
With emulsifiable paste, lotion, hair care emulsifiable paste etc..Wherein, with it is oily be mutually water-in-oil emulsified cosmetic that foreign minister, water phase are interior phase because can
Oil-soluble effective component, such as soothing oil, oil-soluble medicament, ultraviolet absorbing agent etc. to be effectively unfolded on the skin,
And becoming is suitable for dosage form as cosmetics, at this point, it is more excellent compared with oil-in-water type.In addition, oil-in-water dosage form one
As it is frivolous and ventilative, but skin can only temporarily be allowed to play the role of moisturizing, moisturizing persistence is bad, in comparison, Water-In-Oil
Dosage form can be in the air-permeable protective film of skin surface one layer of water-insoluble of formation after smearing, and water lock moisturizing effect is more preferable.
In current preparation process, majority is the oil gelation by making to constitute foreign minister in water-in-oil emulsified cosmetic,
Water droplet is fixed, the frequency of collisions between particle is reduced, is stabilized with this to realize, existing necessarily causes viscosity to get higher (i.e. thickness
Double infection is strong) the case where.Therefore, water-in-oil emulsified cosmetic is difficult to take into account lowering viscousity and stabilisation, it is difficult to while improving warp
When stability and coating when ductility, use sense of touch.Up to now, in order to realize low viscosity and stable water-in-oil emulsion
Cosmetics have carried out various trials.For example, Patent Document 1 discloses by the high powder of oil absorption and the different powder of partial size
Mixed-powder (i.e. organopolysiloxane elastomers globular powder and the hydrophobized silica being composed with specific weight ratio
The mixed-powder of powder), the oil comprising the above organic silicone oil of 30% weight, the organo-clay mine as emulsion adjuvant
Object.In addition, proposing following scheme in patent document 2: by using specific hydrophobized silica as emulsion stabilizer
And use silicone based surfactants as the specific of emulsifier, thus improve the ageing stability of emulsified state, sense of touch, make
The property used.But opaque emulsus is presented in usually system, in order to stablize properties of product, general lubricant component is more (to make up
Content in product accounts for 50% or so), it moistens but more thick and heavy.
Based on above-mentioned analysis, a kind of appearance transparent, moisturizing moisten and non-greasy, stability, sense of touch, usability it is more preferably saturating
Bright Water-In-Oil dosage form is badly in need of in current industry.
Summary of the invention
In view of above-mentioned deficiency, the purpose of the present invention is to provide a kind of clean oil packet water aqua type preparation method and applications,
The oil components of 10%-15% are only added in the preparation method, although product is the emulsifying structure of Water-In-Oil, in product
It is oily mutually consistent with the refractive index of water phase, make product that the transparent appearance of novel and unique be presented, it is impermeable to have overturned traditional oils packet water aqua type
Bright appearance, moisturizing salubrious non-greasy while moistening.
The present invention specifically uses following technical scheme to achieve the goals above:
A kind of clean oil packet water aqua type, is made of the raw material of following weight percent: Aqueous Phase Raw Material 25%-45%, oily phase raw material
10%-15%, additive 5%-10%, water-in-oil emulsifier 1%-3%, preservative 0.1%-0.5%, essence 0.02%-0.1%, surplus
For deionized water.
Further, which is made of the raw material of following weight percent: Aqueous Phase Raw Material 35%, and oily phase raw material 13% adds
Add agent 7%, water-in-oil emulsifier 2%, preservative 0.3%, essence 0.06%, surplus is deionized water.
A kind of preparation method of clean oil packet water aqua type, comprising the following steps:
(1) Aqueous Phase Raw Material is uniformly mixed, is heated to 80-100 DEG C, sterilize 10-30min, is completely dissolved all the components, obtains mixed
It is spare to close raw material a；
(2) raw material a to be mixed is cooled to room temperature, and additive is slowly added to be uniformly mixed, and it is spare to obtain mixed raw material b；
(3) water-in-oil emulsifier is added in oily phase raw material, is uniformly mixed, it is spare to obtain mixed raw material c；
(4) in the case where moderate-speed mixer, mixed raw material b is slowly added to emulsify in mixed raw material c, obtains mixed raw material d
It is spare；
Mixed raw material d is subjected to high speed homogenization under the conditions of (5) -0.04 ~ -0.08MPa, adds preservative and essence, is continued
It is stirred at low speed under vacuum, after mixing evenly discharging packing.
Further, two or more of the Aqueous Phase Raw Material in sodium chloride, glycerol, propylene glycol, other polyalcohols.
Further, the additive is lucidum extracting liquid, Radix Ophiopogonis fermentation liquid, Cortex Magnoliae Officinalis extracting solution, Cortex Eucommiae extracting solution, Cortex Phellodendri
One of extracting solution, heartsease extracting solution and other plant extracting solution are a variety of.
Further, the water-in-oil emulsifier is cetyl PEG/PPG-10/1 dimethyl silicone polymer.
Further, the oily phase raw material is selected from ring five dimethyl silicone polymer, dimethyl silicone polymer/vinyl poly- two
Methylsiloxane cross-linked polymer, dimethyl silicone polymer, two or more in tocopherol acetate, and oily phase raw material contains
Amount accounts for the 10%-15% of entire dosage form.
Further, the preservative be Bis(hydroxymethyl)imidazolidinyl urea, iodopropynyl butyl carbamate,
One of DMDM hydantoin is a variety of, and the odorant is essence.
The invention also discloses clean oil packet water aqua types made from a kind of above-mentioned preparation method and the Water-In-Oil dosage form to exist
The purposes in cosmetics is prepared, which includes preparing cream kind product.
Beneficial effects of the present invention are as follows:
The invention particularly discloses a kind of clean oil packet water aqua type preparation methods, and content of the oil components in cosmetics is reduced
10%-15% is arrived, the transparent appearance that novel and unique is presented in product forms one on skin surface while keeping skin moisture
The ventilative film of layer achievees the effect that moisten and non-greasy.
Specific embodiment
The following are embodiment, present invention is further described in detail:
Embodiment 1
A kind of clean oil packet water aqua type preparation method, is specifically applied in cosmetics cream kind product, test procedure is as follows:
(1) 10kg sodium chloride and 15kg mixed with propylene glycol is uniform, 80 DEG C are heated to, sterilize 30min, keeps all the components completely molten
Solution, it is spare to obtain mixed raw material a；
(2) raw material a to be mixed is cooled to room temperature, and 2.5kg lucidum extracting liquid and 2.5kg heartsease extracting solution are slowly added to mix
Uniformly, it is spare to obtain mixed raw material b；
(3) by 1kg cetyl PEG/PPG-10/1 dimethyl silicone polymer is added to 2kg ring five dimethyl silicone polymer, 2kg gathers
Dimethyl siloxane/vinyl dimethicone cross polymer, 2kg dimethyl silicone polymer, 4kg tocopherol acetate
In, and be uniformly mixed with 200 revs/min of revolving speed, it is spare to obtain mixed raw material c；
(4) under 1000 revs/min of revolving speed stirring, mixed raw material b is slowly added to emulsify in mixed raw material c, must be mixed
Raw material d is spare；
(5) under the conditions of -0.04MPa by mixed raw material d to carry out homogeneous under conditions of 3000 revs/min, add preservative
0.02kg Bis(hydroxymethyl)imidazolidinyl urea, 0.04kg iodopropynyl butyl carbamate, 0.04kgDMDM hydantoins
With 0.02kg essence, continuation is stirred with 80 revs/min under vacuum, discharges and dispense after mixing evenly.
Embodiment 2
(1) 15kg glycerol and 15kg mixed with propylene glycol is uniform, 90 DEG C are heated to, sterilize 20min, keeps all the components completely molten
Solution, it is spare to obtain mixed raw material a；
(2) wait be cooled to room temperature, 3kg Radix Ophiopogonis fermentation liquid, 2kg Cortex Magnoliae Officinalis extracting solution and 2kg heartsease extracting solution is slow after sterilizing
It is added and is uniformly mixed, it is spare to obtain mixed raw material b；
(3) 2kg cetyl PEG/PPG-10/1 dimethyl silicone polymer 6kg dimethyl silicone polymer/vinyl is added to gather
It in dimethicone crosspolymers, 7kg tocopherol acetate, and is uniformly mixed, is obtained mixed with 200 revs/min of revolving speed
It is spare to close raw material c；
(4) in the case where the revolving speed stirring with 1000 revs/min, mixed raw material b is slowly added to carry out cream in mixed raw material c
Change, it is spare to obtain mixed raw material d；
(5) mixed raw material d is subjected to homogeneous under conditions of 3000 revs/min under the conditions of -0.06MPa, adds the bis- (hydroxyls of 0.15kg
Methyl) imidazolidinyl urea, 0.15kgDMDM hydantoins and 0.06kg essence, continue to be stirred under vacuum with 80 revs/min,
It discharges and dispenses after mixing evenly.
Embodiment 3
(1) 15kg sodium chloride, 15kg glycerol, 15kg mixed with propylene glycol is uniform, 100 DEG C are heated to, sterilize 10min, makes to own
Ingredient is completely dissolved, and it is spare to obtain mixed raw material a；
(2) after sterilizing, wait be cooled to room temperature, by 2kg Radix Ophiopogonis fermentation liquid, 2kg Cortex Eucommiae extracting solution, 2kg cortex phellodendri extract, 2kg spirit
Sesame extracting solution and 2kg heartsease extracting solution are slowly added to be uniformly mixed, and it is spare to obtain mixed raw material b；
(3) 3kg cetyl PEG/PPG-10/1 dimethyl silicone polymer is added to 7kg dimethyl silicone polymer, 8kg tocopherol
In acetic acid esters, and it is uniformly mixed with 200 revs/min of revolving speed, it is spare to obtain mixed raw material c；
(4) in the case where the revolving speed stirring with 1000 revs/min, mixed raw material b is slowly added to carry out cream in mixed raw material c
Change, it is spare to obtain mixed raw material d；
(5) mixed raw material d is subjected to homogeneous under conditions of 3000 revs/min under the conditions of -0.08MPa, adds 0.5kgDMDM second
Interior uride and 0.1kg essence, continuation are stirred with 80 revs/min under vacuum, discharge and dispense after mixing evenly.
Comparative example 1
A kind of cream shape cosmetics
Ingredient: water, Nipasol, vaseline, dimethyl silicone polymer, -3 myristinate of myristyl alcohol polyethers, spermaceti are hard
Lipidol, ceteareth -20, glycerol, triethanolamine, methyl hydroxybenzoate, CI 47005, (daily) essence, acyl in DMDM second
Urea, retinyl palmitate, sunflower seed oil, Butylated Hydroxytoluene, EDTA disodium.
Comparative example 2
A kind of cream shape cosmetics
Ingredient: water, saualane, 1,3- propylene glycol, C13-16 isoparaffin, glycerol, Butyrospermum parkii fruit rouge, Jojoba seed
Oil, cetostearyl alcohol, Flos Chrysanthemi water, tea extract, phytosterol, Sodium Hyaluronate, butanediol, decoyl hydroximic acid, third
Alkene acyl dimethyltaurine ammonium/VP copolymer, Tujue's rose caul-fat.
Test example
1. experimental method
The evaluation of 1.1 appearance characters
Take appropriate cream shape cosmetics by visual observations, the method that upper feel is received carries out the indexs such as appearance, the smell of matrix
Evaluation.
The experiment of 1.2 centrifugal stabilities
It takes 10g cream kind cosmetics loaded in centrifuge tube, after being centrifuged 30min under conditions of 3000r/min revolving speed, takes out observation
Whether there is or not layerings.
1.3 heat-resistant experiment
It takes 10g cream kind cosmetics to be placed in a beaker, is sealed with preservative film, is put in 45 DEG C of baking oven 24 hours, take out cooling
To room temperature, observation cream has unchanged.
1.4 cold-resistant experiments
It takes 10g cream kind cosmetics to be placed in plastic cup, is sealed with preservative film, is put in -20 DEG C of refrigerator 24 hours, take out and see
Examine cream have it is unchanged.
1.5 moisture retention
It takes 5g cream kind cosmetics to be placed on glass slide, is placed in 8h in 37 DEG C of baking oven, quality is weighed after taking-up, and press formula
(1) average value of each cream kind cosmetics moisturizing rate is found out.
Moisturizing rate=residue cream kind cosmetics quality/5g
2. experimental result
Each embodiment of table 1 is compared with the cream quality of comparative example
。
As can be known from Table 1, the cream performance prepared by the present invention compared with comparative example 1,2 of embodiment 1 ~ 3 is stable, and lotion is saturating
Bright uniformity, clearly not sticky screening characteristics is good.The present invention still can get under the oiliness raw material for only adding 10%-15%
Preferable performance of keeping humidity, lotion is transparent, does not stick clearly greasy.Although the performance of keeping humidity of comparative example 2 is also close to 80%, compared to implementation
Example 1 ~ 3, stability is not good enough, especially after high temperature or freezing, lotion water outlet.
The above description is only a preferred embodiment of the present invention, is not intended to restrict the invention, patent protection model of the invention
It encloses and is subject to claims, it is all to change with equivalent structure made by description of the invention, similarly should all include
Within the scope of the present invention.
Claims (10)
1. a kind of clean oil packet water aqua type, which is characterized in that the dosage form is made of the raw material of following weight percent: Aqueous Phase Raw Material
25%-45%, oily phase raw material 10%-15%, additive 5%-10%, water-in-oil emulsifier 1%-3%, preservative 0.1%-0.5%, essence
0.02%-0.1%, surplus are deionized water.
2. clean oil packet water aqua type according to claim 1, which is characterized in that the dosage form by following weight percent original
Material is made: Aqueous Phase Raw Material 35%, oily phase raw material 13%, additive 7%, water-in-oil emulsifier 2%, preservative 0.3%, essence
0.06%, surplus is deionized water.
3. a kind of preparation method of clean oil packet water aqua type according to claim 1 or 2, which is characterized in that this method packet
Include following steps:
(1) Aqueous Phase Raw Material is uniformly mixed, is heated to 80-100 DEG C, sterilize 10-30min, is completely dissolved all the components, obtains mixed
It is spare to close raw material a；
(2) raw material a to be mixed is cooled to room temperature, and additive is slowly added to be uniformly mixed, and it is spare to obtain mixed raw material b；
(3) water-in-oil emulsifier is added in oily phase raw material, is uniformly mixed, it is spare to obtain mixed raw material c；
(4) in the case where moderate-speed mixer, mixed raw material b is slowly added to emulsify in mixed raw material c, obtains mixed raw material d
It is spare；
Mixed raw material d is subjected to high speed homogenization under the conditions of (5) -0.04 ~ -0.08MPa, adds preservative and essence, is continued
It is stirred at low speed under vacuum, after mixing evenly discharging packing.
4. preparation method according to claim 3, which is characterized in that the Aqueous Phase Raw Material is selected from sodium chloride, glycerol, the third two
Two or more in alcohol, other polyalcohols.
5. preparation method according to claim 3, which is characterized in that the additive is lucidum extracting liquid, Radix Ophiopogonis fermentation
One of liquid, Cortex Magnoliae Officinalis extracting solution, Cortex Eucommiae extracting solution, cortex phellodendri extract, heartsease extracting solution and other plant extracting solution or
It is a variety of.
6. preparation method according to claim 3, which is characterized in that the water-in-oil emulsifier is cetyl PEG/
PPG-10/1 dimethyl silicone polymer.
7. Preparation Method according to claim 3, which is characterized in that the oil phase raw material is selected from five polydimethylsiloxanes of ring
Alkane, Dimethicone/Vinyl Dimethicone cross-linked polymer, dimethyl silicone polymer, tocopherol acetate
In two or more, and the content of oily phase raw material accounts for the 10%-15% of entire dosage form.
8. preparation method according to claim 3, which is characterized in that the preservative is bis- (methylol) imidazolidinyls
One of urea, iodopropynyl butyl carbamate, DMDM hydantoin are a variety of, and the odorant is essence.
9. clean oil packet water aqua type made from a kind of preparation method according to claim 3 ~ 8 any one.
10. a kind of clean oil packet water aqua type according to claim 9 is preparing the purposes in cosmetics, which is characterized in that
The purposes includes preparing the preparation of cream kind product.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638665A (en) * | 2019-09-27 | 2020-01-03 | 陕西慧康生物科技有限责任公司 | 3D cream with skin feel capable of being controlled automatically and combined by two different matrixes and preparation method thereof |
| CN110721097A (en) * | 2019-11-06 | 2020-01-24 | 广州环亚化妆品科技有限公司 | Water-in-oil frost and preparation method and application thereof |
Citations (3)
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| CN110721097A (en) * | 2019-11-06 | 2020-01-24 | 广州环亚化妆品科技有限公司 | Water-in-oil frost and preparation method and application thereof |
| CN110721097B (en) * | 2019-11-06 | 2022-04-08 | 广州环亚化妆品科技有限公司 | Water-in-oil frost and preparation method and application thereof |
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