CN109316433A - A kind of facial treatment mask reducing heavy metal pollution - Google Patents
A kind of facial treatment mask reducing heavy metal pollution Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention relates to cosmetic technical fields, and a kind of facial treatment mask for reducing heavy metal pollution is disclosed, the raw material including following weight: purifying konjaku powder 4-6 parts, 1-4 parts of carragheen powder, 0.25-0.75 parts of polyethylene glycol, 0.01-0.03 parts of hyaluronic acid, 0.007-0.013 parts of D-sorbite, 0.01-0.03 parts of lactic acid, 0.5-1.5 parts of zeroth order iron powder, 0.3-0.7 parts of biomass carbon dust, 0.08-0.12 parts of graphene oxide, 4-8 parts of deionized water.The facial treatment mask of the reduction heavy metal pollution, by forming heavy metal ion adsorbed iron carbon microcell, oxidation and removal, it can fundamentally solve the problems, such as facial heavy metal element accumulation, simultaneous reactions heat has insulation effect to facial mask, facilitate the skin effect for efficiently playing facial mask, is provided safeguard for human health.
Description
Technical field
The present invention relates to cosmetic technical field, specially a kind of facial treatment mask for reducing heavy metal pollution.
Background technique
Cosmetics are to be used to promote the substance of human body beauty degree other than simple cleaning supplies, cosmetics
It is quite early and universal using origin, it can be especially commonly used in the women for having certain economic base, cosmetics refer to amendment people
Body smell, chemical industrial product or fine chemical product for the purpose of maintaining a good state, either with smearing, sprinkling or other classes
Like method, any position of human body surface is interspersed among, such as skin, hair, refer to toenail, lips and teeth, to reach cleaning, maintenance, beauty
Hold, the effect of modification and change appearance.
Lead has very strong attachment and concealing ability, so being often added in whitening as a Heavy Metallic Elements
In cosmetic, the whitening effect of cosmetics is improved.But since lead is not element needed by human, the lead contained in cosmetics easily by
Absorption of human body, to human body generate greatly harm, after excess intake lead in human body, can to blood circulation, nerve, digest and secrete
Urinary system generates poisonous effect, influences human body development, can be tight especially after intelligence and skeleton development, especially child's lead poisoning
Ghost image rings intellectual development.Therefore national regulation lead is strictly limited the quantity as harmful element, must not be higher than 40 mg/kgs, but
It is to have certain dependence to lead due to skin-lightening cosmetic, especially some illegal manufacturers are to improve cosmetics to use effect
Fruit often makes content of heavy metal lead be higher than several times tens times of standard.And user is without knowing it, is used for a long time exceeded
Cosmetics will cause the accumulation of heavy metal element lead.User only wipes the mode of epicuticle remaining cosmetic with makeup remover,
It is poor to the removal effect of metallic element, especially heavy metal element lead.
Facial mask be apply or spread on human facial skin surface, taken off after a period of time from, clean or retain, play concentration shield
The product of reason or cleaning action.In order to achieve the effect that skin care, many people can select facial mask to nurse face, to keep good
Good face skin state.Facial mask on the market, the mainly function such as skin of face moisturizing moisturizing, whitening spot-removing, anti-aging now
Can, almost without the similar product for heavy metal element removal, it cannot fundamentally solve facial heavy metal element lead accumulation
The problem of, for a long time, biggish harm is generated to the health of human body.
Summary of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of facial treatment mask for reducing heavy metal pollution, pass through to be formed
Iron carbon microcell is heavy metal ion adsorbed, aoxidizes and removes, and can fundamentally solve the problems, such as facial heavy metal element accumulation,
Simultaneous reactions heat has insulation effect to facial mask, facilitates the skin effect for efficiently playing facial mask, provides safeguard for human health.
The invention is realized in this way facial heavy metal element accumulation can be fundamentally solved the problems, such as realization is above-mentioned,
There is insulation effect by forming heavy metal ion adsorbed iron carbon microcell, oxidation and removal, simultaneous reactions heat to facial mask, help
In the skin effect for efficiently playing facial mask, it is reached for the purpose that human health provides safeguard, the invention provides the following technical scheme:
A kind of facial treatment mask reducing heavy metal pollution, the raw material including following weight: purifying konjaku powder 4-6 parts, OK a karaoke club
1-4 parts of rubber powder end, 0.25-0.75 parts of polyethylene glycol, 0.01-0.03 parts of hyaluronic acid, 0.007-0.013 parts of D-sorbite, cream
0.01-0.03 parts sour, 0.5-1.5 parts of zeroth order iron powder, 0.08-0.12 parts of graphene oxide, is gone 0.3-0.7 parts of biomass carbon dust
4-8 parts of ionized water.
Preferably, the raw material including following weight: purifying 4 parts of konjaku powder, 1 part of carragheen powder, poly- second two
0.25 part of alcohol, 0.01 part of hyaluronic acid, 0.007 part of D-sorbite, 0.01 part of lactic acid, 0.5 part of zeroth order iron powder, biomass carbon dust
0.3 part, 0.08 part of graphene oxide, 4 parts of deionized water.
Preferably, the raw material including following weight: purifying 5 parts of konjaku powder, 2.5 parts of carragheen powder, poly- second
0.5 part of glycol, 0.02 part of hyaluronic acid, 0.01 part of D-sorbite, 0.02 part of lactic acid, 1 part of zeroth order iron powder, biomass carbon dust 0.5
Part, 0.1 part of graphene oxide, 6 parts of deionized water.
Preferably, the raw material including following weight: purifying 6 parts of konjaku powder, 4 parts of carragheen powder, poly- second two
0.75 part of alcohol, 0.03 part of hyaluronic acid, 0.013 part of D-sorbite, 0.03 part of lactic acid, 1.5 parts of zeroth order iron powder, biomass carbon dust
0.7 part, 0.12 part of graphene oxide, 8 parts of deionized water.
A kind of facial treatment mask reducing heavy metal pollution, preparation method includes the following steps:
S1: taking above-mentioned raw materials according to weight, aseptically, purifying konjaku powder is evenly spread to deionized water
In, 30min is stood, uses electric blender to stir 30min in the case where revolving speed is 200-500 rev/min, makes its swelling, it is quiet
It purchases use;
S2: solution obtained in S1 is heated under 70 DEG C of water bath conditions, is stirred using electric mixer, revolving speed 80-
120 revs/min, slowly carragheen powder is added among the above in batches, stirs 30min, after evenly mixing, stand for standby use;
S3: under 70 DEG C of condition of water bath heating, being stirred using electric mixer, and revolving speed is 20-80 revs/min, by poly- second two
Alcohol is even added in the obtained solution of S2, is slowly stirred 10min, after mixing, stand for standby use;
S4: under 50 DEG C of condition of water bath heating, being stirred using electric mixer, and revolving speed is 10-60 revs/min, is obtained to S3
Solution in sequentially add hyaluronic acid, D-sorbite and lactic acid, after mixing, cooling it is spare;
Zeroth order iron powder: being filtered by S5 using the filter screen of 80 mesh, is carried out using the filter screen of 40-60 mesh to biomass carbon dust
Filtering, is filtered graphene oxide using the filter screen of 160 mesh, takes filtered zeroth order iron powder, biomass carbon dust and oxygen
Graphite alkene is added in S4 in solution obtained in sterile vacuum environment, the revolving speed with high emulsification cutter at 8000 revs/min
Lower stirring 2-5 minutes is packed after cooling using molding is carried out after microwave sterilization according to a conventional method.
Compared with prior art, the beneficial effects of the present invention are:
(1) facial heavy metal element accumulation can be fundamentally solved the problems, such as, by forming iron carbon microcell heavy metal ion
Absorption, oxidation and removal, can fundamentally solve the problems, such as facial heavy metal element accumulation, and simultaneous reactions heat has heat preservation to facial mask
Effect facilitates the skin effect for efficiently playing facial mask, provides safeguard for human health.
(2) by increasing the substances such as zero-valent iron particle, biomass carbon particle, graphene oxide, composition iron, biomass carbon are micro-
Battery, the addition of graphene oxide increase the electric conductivity of micro cell system, reduce ohm pole in micro cell reaction process
Change, improves reaction rate.Using the reduction of Zero-valent Iron, face, the oxidation on reducing heavy metal oxide and surface are acted on
Group, rear heavy metal are reduced to small solid particles, are adsorbed by biomass carbon, achieve the purpose that remove heavy metal.
(3) in the micro cell course of work, Zero-valent Iron is reduced, and has certain reaction heat to release, and keeps facial mask in higher temperatures
Degree is lower to be used, and while this temperature promotes pore to open, can also be promoted blood circulation, and the effect of various maintenance ingredients is played
To utmostly, to seek the effect of beautifying skin effect bigizationner, at the same time, biomass carbon provides high specific surface
Product has strong adsorptivity, and lactic acid provides acidic environment, and the unlimited system in use process provides the oxygen in air, improves zero
Valence iron reduction effect, to achieve the purpose that heavy metal ion adsorbed, oxidation and removal.
(4) it uses konjac glucomannan, carragheen and polyethylene glycol for hydrogel made of matrix, can be swollen in water and keeps big
It measures moisture and does not dissolve, there is good biocompatibility.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1
A kind of facial treatment mask reducing heavy metal pollution, the raw material including following weight: 4 parts of konjaku powder of purifying, card
Draw rubber powder last 1 part, 0.25 part of polyethylene glycol, 0.01 part of hyaluronic acid, 0.007 part of D-sorbite, 0.01 part of lactic acid, zeroth order iron powder
0.5 part, 0.3 part of biomass carbon dust, 0.08 part of graphene oxide, 4 parts of deionized water.
Embodiment 2
A kind of facial treatment mask reducing heavy metal pollution, the raw material including following weight: 5 parts of konjaku powder of purifying, card
Draw rubber powder last 2.5 parts, 0.5 part of polyethylene glycol, 0.02 part of hyaluronic acid, 0.01 part of D-sorbite, 0.02 part of lactic acid, zeroth order iron powder
1 part, 0.5 part of biomass carbon dust, 0.1 part of graphene oxide, 6 parts of deionized water.
Embodiment 3
A kind of facial treatment mask reducing heavy metal pollution, the raw material including following weight: 6 parts of konjaku powder of purifying, card
Draw rubber powder last 4 parts, 0.75 part of polyethylene glycol, 0.03 part of hyaluronic acid, 0.013 part of D-sorbite, 0.03 part of lactic acid, zeroth order iron powder
1.5 parts, 0.7 part of biomass carbon dust, 0.12 part of graphene oxide, 8 parts of deionized water.
Any one in embodiment 1-3 reduces the facial treatment mask of heavy metal pollution, and preparation method includes the following steps:
S1: taking above-mentioned raw materials according to weight, aseptically, will evenly spread to deionization in purifying konjaku powder
Water stands 30min, uses electric blender to stir 30min in the case where revolving speed is 200-500 rev/min, makes its swelling, quiet
It purchases use;
S2: solution obtained in S1 is heated under 70 DEG C of water bath conditions, is stirred using electric mixer, revolving speed 80-
120 revs/min, slowly carragheen powder is added among the above in batches, stirs 30min, after evenly mixing, stand for standby use;
S3: under 70 DEG C of condition of water bath heating, being stirred using electric mixer, and revolving speed is 20-80 revs/min, by poly- second two
Alcohol is even added in the obtained solution of S2, is slowly stirred 10min, after mixing, stand for standby use;
S4: under 50 DEG C of condition of water bath heating, being stirred using electric mixer, and revolving speed is 10-60 revs/min, is obtained to S3
Solution in sequentially add hyaluronic acid, D-sorbite and lactic acid, after mixing, cooling it is spare;
Zeroth order iron powder: being filtered by S5 using the filter screen of 80 mesh, is carried out using the filter screen of 40-60 mesh to biomass carbon dust
Filtering, is filtered graphene oxide using the filter screen of 160 mesh, takes filtered zeroth order iron powder, biomass carbon dust and oxygen
Graphite alkene is added in S4 in solution obtained in sterile vacuum environment, the revolving speed with high emulsification cutter at 8000 revs/min
Lower stirring 2-5 minutes is packed after cooling using molding is carried out after microwave sterilization according to a conventional method.
Embodiment 1-3 is prepared into gained facial mask and gives 50 women people with wrinkle of skin and dry skin state at random
Group uses, daily using primary, service life be counted after 15 days, 15 days whether improvement.Following table is human body experiment effect:
Group | Test number | Efficiently individual quantity | Invalid number | Allergy number | It is efficient |
Embodiment 1 | 50 | 43 | 7 | 0 | 86% |
Embodiment 2 | 50 | 45 | 5 | 0 | 90% |
Embodiment 3 | 50 | 42 | 8 | 0 | 84% |
As can be seen from the above table: for the effective percentage of embodiment 1-3 preparation gained facial mask 84% or more, allergy rate is 0, is had good
The good effect for reducing wrinkle of skin and increasing moisture of skin, it is highly-safe.
The chemical activity of Zero-valent Iron is higher, electrode potential E0(Fe2+/Fe0)=- 0.44V has stronger reducing power, can be with
Partial oxidative ion or compound are restored, then constituted much when iron simple substance enters in aqueous solution with graphite or biomass carbon
Small primary battery, Zero-valent Iron become anode, graphite and biomass carbon as cathode, electrode reaction occur, fundamental reaction is as follows:
Anode reaction: Fe → Fe2++2e- E0(Fe2+/Fe0)=- 0.44V
Cathode reaction: 2H-+2e-→2 [H ]→H2 E0(H+/H2)=- 0.00V
When there is O2When: O2+4H++4e-→2H2O E0(O2/H2O)=- 1.23V(acid solution)
O2+2H2O+4e-→4OH- E0(O2/H2O)=- 1.23V(neutrality or alkaline solution)
Under the acidic environment and aerobic condition that lactic acid provides following electrochemical reaction occurs for iron-carbon micro-electrolysis system:
Anode reaction: Fe-2e → Fe2+, φθ(Fe2+/ Fe)=- 0.44V
Cathode reaction: 2H++2e→2[H ]→H2, φθ(H+/H2)=0V
When there are metal ion, cathode also occurs that following reaction:
Pb2++ 2e → Pb, φθ(Pb2+/ Pb)=- 0.126V
Detailed process is exactly: biomass carbon provides high-specific surface area, has strong adsorptivity, and lactic acid provides acid environment, used
The unlimited system of journey provides the oxygen in air, and the addition of graphene oxide increases the electric conductivity of micro cell system, reduces micro-
Ohmic polarization during cell reaction improves reaction rate, and iron provides reproducibility, and whole light electrolysis system is to heavy metal ion
Adsorbed, aoxidized and removed, meanwhile, generate certain reaction heat in reaction process, the temperature of reaction heat can improve skin care because
The activity of son, provides guarantee for the absorption of skin-protecting factor.
The sensory evaluation and heavy metal lead absorption detecting of the facial mask of embodiment 1 ~ 3
1) detection organoleptic indicator is provided according to " People's Republic of China's light industry standard " facial mask standard QB/T2872-2007:
Appearance and fragrance, physical and chemical index;PH value, heat-resisting and cold-resistant, sanitary index;Lead, mercury, arsenic etc., as a result as shown in table 1 below:
[table 1]
2) 10 sensory evaluation personnel are chosen, age 20-26, wherein women 6, form evaluation group, subjective appreciation is carried out,
Total score 100 is divided, and evaluation result see the table below 2:
[table 2]
3) absorption detecting of heavy metal lead:
1. the preparation of rat skin in vitro
Healthy female SD rat is taken, 4% Nembutal sodium solution is anaesthetized by 40mg/kg intraperitoneal injection, avoids pinprick, 8% sulphur
Change sodium solution depilation and remove same position skin of abdomen, clears up remaining subcutaneous tissue and fat, and rushed repeatedly with physiological saline
Wash, until no muddiness, skin be dipped in spare in physiological saline, be stored in one 4 DEG C of refrigerators, for 24 hours in tested.
2. absorption experiment method
Test temperature is maintained at 37 DEG C or so, fixes mouse skin sample 1,2,3,4 and 5 respectively;It is 5% lead oxide emulsifiable paste by content
Mouse skin sample 1,2,3 and 4 surfaces are pasted on, cuticula and drug delivery layer are in close contact, and skin corium is contacted with acceptable solution;Respectively 2,
6,12 and for 24 hours when cut off sample 1,2,3 and 4 areas and be the skin of 2cm*2cm, and wiped with makeup remover, sample 1 measures after drying
Content of heavy metal lead in mouse skin, 2 trial target embodiment of sample, 1 facial mask, 3 trial target embodiment of sample, 2 facial mask, 4 trial target of sample
3 facial mask of embodiment after rear wiped clean drying, measured the content of heavy metal lead of sample 2,3 and 4, sample 5 is made using 15 minutes
Content of heavy metal lead is measured after directly drying for blank control.
3. mouse skin sample measures content of heavy metal lead
I, it after the quality of accurate weighing sample 1,2,3,4 and 5, is separately added into tetrafluoroethene inner canister, 5ml nitric acid is added, gently
It shakes up, stands 20-30min, (150 DEG C of temperature, pressure 15 atm, power 2000W, keep by established procedure by microwave dissolver
10min;180 DEG C of temperature, pressure 25 atm, power 2000W, keep 10min) resolution;It is cooled to room temperature, takes out after the completion of resolution
Inner canister sets and is slowly concentrated into 2-3ml in 150 DEG C on electric hot plate, removes and be cooled to room temperature;Digestion solution is transferred to accurate
1ml is added and contains 2.5% magnesium nitrate and 12.5% biphosphate by mixed liquor in 25ml measuring bottle, then is repeatedly washed on a small quantity with nitric acid
Counteracting tank, cleaning solution are incorporated in measuring bottle, and are diluted to scale, shake up to get.
II, using graphite furnace atomic absorption spectrometry;To the solution of the sample 1,2,3,4 and 5 after micro-wave digestion, according to
The measurement of the following conditions progress lead content: wavelength 283.3nm;Dry: 1,60-90 DEG C of initial temperature, heat up 10s on slope, keeps
20s;2,90-140 DEG C of initial temperature, heat up 10s on slope, keeps 20s;3,90-140 DEG C of initial temperature, heat up 10s on slope, protects
Hold 20s;4,90-140 DEG C of initial temperature, heat up 10s on slope, keeps 20s;5, initial temperature: 140-500 DEG C, slope heating
10s keeps 40s;Atomization temperature: 2000 DEG C, continue 5s;Background correction is Zeemen effect;Precision measures lead single element standard
Solution (concentration 1000ug/ml), which is diluted to, is equivalent to (Pb) 0.0 leaded respectively in every lml solution, and 8.0,16.0,24.0,
32.0 40.0ng;Precision draws standard solution 20ul, injects in graphite furnace atomizer, absorbance is measured, with absorbance
It (A) is ordinate, standard substance Pb concentration (X) is abscissa, obtains regression equation A=0.0049X+0.017, r=0.9995.
4. measurement result: the content (ng/mg) of heavy metal lead in mouse skin
Sample/time | 2h | 6h | 12h | 24h |
1 | 54.9 | 83.2 | 135.3 | 255.8 |
2 | 35.4 | 54.1 | 78.3 | 110.8 |
3 | 32.1 | 46.7 | 76.5 | 102.5 |
4 | 39.6 | 62.4 | 82.7 | 125.3 |
5 | 2.3 | 2.5 | 1.8 | 2.6 |
There is result it is found that the facial mask in EXPERIMENTAL EXAMPLE 1-3 preparation there is apparent absorb to remove the heavy metal lead in skin
Effect.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that
There is also other identical elements in process, method, article or equipment including the element.
The above is merely preferred embodiments of the present invention, be not intended to limit the invention, it is all in spirit of the invention and
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within principle.
Claims (5)
1. a kind of facial treatment mask for reducing heavy metal pollution, which is characterized in that the raw material including following weight: purifying evil spirit
4-6 parts of taro fine powder, 1-4 parts of carragheen powder, 0.25-0.75 parts of polyethylene glycol, 0.01-0.03 parts of hyaluronic acid, D-sorbite
0.007-0.013 parts, 0.01-0.03 parts of lactic acid, 0.5-1.5 parts of zeroth order iron powder, 0.3-0.7 parts of biomass carbon dust, graphite oxide
0.08-0.12 parts of alkene, 4-8 parts of deionized water.
2. a kind of facial treatment mask for reducing heavy metal pollution according to claim 1, which is characterized in that including following weight
The raw material of part proportion: purifying 4 parts of konjaku powder, 1 part of carragheen powder, 0.25 part of polyethylene glycol, 0.01 part of hyaluronic acid, sorb
0.007 part of sugar alcohol, 0.01 part of lactic acid, 0.5 part of zeroth order iron powder, 0.3 part of biomass carbon dust, 0.08 part of graphene oxide, deionization
4 parts of water.
3. a kind of facial treatment mask for reducing heavy metal pollution according to claim 1, which is characterized in that including following weight
The raw material of part proportion: purifying 5 parts of konjaku powder, 2.5 parts of carragheen powder, 0.5 part of polyethylene glycol, 0.02 part of hyaluronic acid, mountain
0.01 part of pears sugar alcohol, 0.02 part of lactic acid, 1 part of zeroth order iron powder, 0.5 part of biomass carbon dust, 0.1 part of graphene oxide, deionized water 6
Part.
4. a kind of facial treatment mask for reducing heavy metal pollution according to claim 1, which is characterized in that including following weight
The raw material of part proportion: purifying 6 parts of konjaku powder, 4 parts of carragheen powder, 0.75 part of polyethylene glycol, 0.03 part of hyaluronic acid, sorb
0.013 part of sugar alcohol, 0.03 part of lactic acid, 1.5 parts of zeroth order iron powder, 0.7 part of biomass carbon dust, 0.12 part of graphene oxide, deionization
8 parts of water.
5. a kind of facial treatment mask for reducing heavy metal pollution according to claim 1, which is characterized in that preparation method packet
Include following steps:
S1: taking above-mentioned raw materials according to weight, aseptically, purifying konjaku powder is evenly spread to deionized water
In, 30min is stood, uses electric blender to stir 30min in the case where revolving speed is 200-500 rev/min, makes its swelling, it is quiet
It purchases use;
S2: solution obtained in S1 is heated under 70 DEG C of water bath conditions, is stirred using electric mixer, revolving speed 80-
120 revs/min, slowly carragheen powder is added among the above in batches, stirs 30min, after evenly mixing, stand for standby use;
S3: under 70 DEG C of condition of water bath heating, being stirred using electric mixer, and revolving speed is 20-80 revs/min, by poly- second two
Alcohol is even added in the obtained solution of S2, is slowly stirred 10min, after mixing, stand for standby use;
S4: under 50 DEG C of condition of water bath heating, being stirred using electric mixer, and revolving speed is 10-60 revs/min, is obtained to S3
Solution in sequentially add hyaluronic acid, D-sorbite and lactic acid, after mixing, cooling it is spare;
Zeroth order iron powder: being filtered by S5 using the filter screen of 80 mesh, is carried out using the filter screen of 40-60 mesh to biomass carbon dust
Filtering, is filtered graphene oxide using the filter screen of 160 mesh, takes filtered zeroth order iron powder, biomass carbon dust and oxygen
Graphite alkene is added in S4 in solution obtained in sterile vacuum environment, the revolving speed with high emulsification cutter at 8000 revs/min
Lower stirring 2-5 minutes is packed after cooling using molding is carried out after microwave sterilization according to a conventional method.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811476921.XA CN109316433B (en) | 2018-12-05 | 2018-12-05 | Skin care mask capable of reducing heavy metal pollution |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811476921.XA CN109316433B (en) | 2018-12-05 | 2018-12-05 | Skin care mask capable of reducing heavy metal pollution |
Publications (2)
Publication Number | Publication Date |
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CN109316433A true CN109316433A (en) | 2019-02-12 |
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Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111239240A (en) * | 2020-02-21 | 2020-06-05 | 通标标准技术服务(天津)有限公司 | Method for determining harmful elements in iron ore |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2042216A1 (en) * | 2007-09-28 | 2009-04-01 | ACO Hud Nordic AB | Body and hair cleansing formulations |
CN101973620A (en) * | 2010-09-21 | 2011-02-16 | 上海大学 | Method for removing heavy metal ions in water by using graphene oxide sheet |
CN102228410A (en) * | 2011-05-28 | 2011-11-02 | 福建农林大学 | Skin-care composite facial mask fluid and preparation method thereof |
CN104525159A (en) * | 2015-01-13 | 2015-04-22 | 张一梅 | Preparation method of heavy metal ion adsorbent |
CN104587956A (en) * | 2015-01-11 | 2015-05-06 | 温州泓呈祥科技有限公司 | Preparation method of coated nano zero-valent iron taking multilayer activated-carbon-coated graphene oxide composite powder as carrier |
CN106362697A (en) * | 2016-11-10 | 2017-02-01 | 过冬 | Heavy metal iron adsorption material modified by aminated graphene oxide |
CN107929111A (en) * | 2017-12-18 | 2018-04-20 | 广州市汇吉科技企业孵化器有限公司 | A kind of cleaning mud film for adsorbing heavy metal |
CN108056933A (en) * | 2017-12-14 | 2018-05-22 | 广州丽彦妆生物科技有限公司 | A kind of biomass graphene facial mask and preparation method thereof |
CN108078869A (en) * | 2018-02-02 | 2018-05-29 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of adsorbing composition |
CN108294977A (en) * | 2018-01-26 | 2018-07-20 | 湖南御茯堂健康管理咨询有限公司 | A kind of graphene black jade facial mask |
-
2018
- 2018-12-05 CN CN201811476921.XA patent/CN109316433B/en active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2042216A1 (en) * | 2007-09-28 | 2009-04-01 | ACO Hud Nordic AB | Body and hair cleansing formulations |
CN101973620A (en) * | 2010-09-21 | 2011-02-16 | 上海大学 | Method for removing heavy metal ions in water by using graphene oxide sheet |
CN102228410A (en) * | 2011-05-28 | 2011-11-02 | 福建农林大学 | Skin-care composite facial mask fluid and preparation method thereof |
CN104587956A (en) * | 2015-01-11 | 2015-05-06 | 温州泓呈祥科技有限公司 | Preparation method of coated nano zero-valent iron taking multilayer activated-carbon-coated graphene oxide composite powder as carrier |
CN104525159A (en) * | 2015-01-13 | 2015-04-22 | 张一梅 | Preparation method of heavy metal ion adsorbent |
CN106362697A (en) * | 2016-11-10 | 2017-02-01 | 过冬 | Heavy metal iron adsorption material modified by aminated graphene oxide |
CN108056933A (en) * | 2017-12-14 | 2018-05-22 | 广州丽彦妆生物科技有限公司 | A kind of biomass graphene facial mask and preparation method thereof |
CN107929111A (en) * | 2017-12-18 | 2018-04-20 | 广州市汇吉科技企业孵化器有限公司 | A kind of cleaning mud film for adsorbing heavy metal |
CN108294977A (en) * | 2018-01-26 | 2018-07-20 | 湖南御茯堂健康管理咨询有限公司 | A kind of graphene black jade facial mask |
CN108078869A (en) * | 2018-02-02 | 2018-05-29 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of adsorbing composition |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111239240A (en) * | 2020-02-21 | 2020-06-05 | 通标标准技术服务(天津)有限公司 | Method for determining harmful elements in iron ore |
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