CN109288117A - A kind of composition and its application in cigarette - Google Patents
A kind of composition and its application in cigarette Download PDFInfo
- Publication number
- CN109288117A CN109288117A CN201811226093.4A CN201811226093A CN109288117A CN 109288117 A CN109288117 A CN 109288117A CN 201811226093 A CN201811226093 A CN 201811226093A CN 109288117 A CN109288117 A CN 109288117A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- composition
- tobacco leaf
- acid
- additive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
A kind of application the present invention relates to composition and its in cigarette.The composition includes following component: malic acid, citric acid, xylitol, glucose, benzoic acid, lauric acid, lactic acid, glycerol and water.The composition can reduce main flume pH value, so that the flue gas of cigarette is coordinated, is submissive, comfort level it is strong.
Description
Technical field
The invention belongs to technical field of tobacco, are related to a kind of composition and its application in cigarette.The composition can
Reduce main flume pH value, so that the flue gas of cigarette is coordinated, is submissive, comfort level it is strong.
Background technique
The pH of cigarette mainstream flue gas is one of the overall target of cigarette total quality reflection, and the influence to aesthetic quality is aobvious
It writes.The pH value of cigarette mainstream flue gas is able to reflect flue gas strength, flue gas irritation and the nicotine soakage that smoker experiences.
Chinese-style cigarette be different from external blended type cigarette one important feature be its main flume pH value it is significantly inclined
It is low.If the pH value of Chinese style flue-cured tobacco type cigarette mainstream flue gas increases, free nicotine increases relative to tar content in flue gas, irritation
Enhancing, dry sensation are obvious.
The pH value for how reducing cigarette mainstream flue gas, coordinates flue gas, submissive, and comfort level is strong, is formed and strengthens Chinese style volume
The exclusive sense organ style and features of cigarette, become tobacco industrial enterprise focus of attention.
Summary of the invention
The present invention relates to a kind of compositions comprising following component: malic acid, citric acid, xylitol, glucose, benzene first
Acid, lauric acid, lactic acid, glycerol and water.
In certain embodiments, composition of the present invention includes following component in parts by weight:
In certain embodiments, the aforementioned described in any item compositions of the present invention include in parts by weight such as the following group
Point:
In certain embodiments, any one of aforementioned composition of the present invention comprising apple in parts by weight
2,3,4,5,6,7 or 8 parts of acid.
In certain embodiments, any one of aforementioned composition of the present invention comprising lemon in parts by weight
2,3,4,5,6,7 or 8 parts of acid.
In certain embodiments, any one of aforementioned composition of the present invention comprising xylose in parts by weight
1,2,3,4 or 5 part of alcohol.
In certain embodiments, any one of aforementioned composition of the present invention comprising grape in parts by weight
3,4,5,6 or 7 parts of sugar.
In certain embodiments, any one of aforementioned composition of the present invention comprising benzene first in parts by weight
1,1.2,1.5,1.8 or 2 part of acid.
In certain embodiments, any one of aforementioned composition of the present invention comprising laurel in parts by weight
2,2.5,3,3.5 or 4 parts of acid.
In certain embodiments, any one of aforementioned composition of the present invention comprising lactic acid in parts by weight
0.5,0.7,0.8 or 1 part.
In certain embodiments, any one of aforementioned composition of the present invention comprising glycerol in parts by weight
1,1.2,1.5,1.8,2,2.2,2.5,2.8 or 3 parts.
In certain embodiments, any one of aforementioned composition of the present invention comprising water 50 in parts by weight,
55,60,65,70,75,80,85,90,95 or 100 parts.
The invention further relates to the aforementioned described in any item compositions of the present invention to prepare the purposes in cigarette.
Purposes the invention further relates to the aforementioned described in any item compositions of the present invention as tobacco leaf additive.
The invention further relates to the aforementioned described in any item compositions of the present invention for reducing the use of cigarette mainstream flue gas pH value
On the way.
The invention further relates to a kind of tobacco leaf additives, by the preparation of the aforementioned described in any item compositions of the present invention
At.
The invention further relates to the methods for preparing tobacco leaf additive of the present invention, including following operation: by apple
Acid, citric acid, xylitol, glucose, benzoic acid, lauric acid, lactic acid, glycerol and water mixing, obtain mixture.
It in certain embodiments, further include heating back in the method for the present invention for preparing tobacco leaf additive
Obtained mixture is heated to reflux by the operation of stream.
In certain preferred aspects, it is heated to reflux and is carried out at 45~55 DEG C.
In certain preferred aspects, return time is 2~8 hours.
Also a kind of method for reducing cigarette mainstream flue gas pH value of the present invention, including tobacco leaf of the present invention is added
Agent is applied to the step of piece cigarette, and preferred applying mode is sprinkling.
In certain embodiments, in the method for the present invention for reducing cigarette mainstream flue gas pH value, the cigarette cigarette
The additive amount of leaf additive be piece cigarette weight 0.1~3%, such as 0.5%, 0.8%, 1%, 1.2%, 1.5%, 1.8%,
2%, 2.2%, 2.5% or 2.8%.
The invention further relates to a kind of cigarette, and it includes composition of the present invention or the tobacco leaf additives.
In certain embodiments, cigarette of the present invention is Virginian-type cigarette.
In certain embodiments, tobacco leaf of the present invention is cured tobacco leaf.
Composition cleavable provided by the invention generates acid ingredient, can be used as tobacco leaf additive.It will be of the invention
The composition of offer is added in piece cigarette, can reduce cigarette mainstream flue gas pH value so that the main flume of cigarette have it is following i)
~iv) described in any item advantages:
I) coordinate;
Ii) submissive;
Iii) comfort level is strong;
Iv) weaker dry sensation;
V) miscellaneous gas reduces.
Specific embodiment
Essentiality content of the invention is further illustrated below with reference to specific embodiments of the present invention, it should be appreciated that following
Embodiment is merely to illustrate the present invention, but is not limited the scope of protection of the present invention with this.Tool is not specified in following example
Concrete conditions in the establishment of a specific crime person, according to normal conditions or manufacturer suggest progress.Production firm person is not specified in drug or reagent used, and being can
With conventional products that are commercially available.
Although many materials used in following embodiment and operating method be it is known in the art that still the present invention still
So it is described in detail as far as possible herein.It will be apparent to those skilled in the art that if not specified, material used in following example
Material and operating method are well known in the art.
The piece cigarette used in following embodiment is flue-cured tobacco matrix cigarette.
The detection method of the pH value of main flume in following example is as follows:
Cigarette sample is placed in temperature (20 ± 1) DEG C, is balanced 48 hours in the environment of relative humidity (60 ± 2) %.It is surveyed
Test agent is selected with draw ambient condition by national standard (definition of GB/T16450-2004 conventional analysis smoking machine and standard
Condition and GB/T19609-2004 cigarette measure total granules and tar with conventional analysis with smoking machine) regulation carries out.
4 cigarette are aspirated on smoking machine according to standard conditions, and collect granule phase substance with cambridge filter, collection is had into flue gas
The filter disc of granule phase substance is transferred in the stuffed conical flask that clean capacity is 50mL, is wiped trap 2 times with mineral wool, is placed in cone
In shape bottle, distilled water 20mL is accurately added in conical flask, plug is covered and oscillation 30min extracts on percussion table
It takes, measures its pH value using pH potentiometric titrimeter.
Sensory evaluating smoking's experiment in following example is pressed by the sensory evaluating smoking committee of Fujian China Tobacco Industrial Co., Ltd.
GB5606.4-2005 carries out comparison of smokeing panel test to cigarette sample.Sensory Quality of Cigarette judgment criteria is as in Table A.
Table A Sensory Quality of Cigarette judgment criteria
Sensory evaluating smoking's inspection rule:
1, participating in number of smokeing panel test is 13 people.
2, aesthetic quality scores using hundred-mark system, and highest score is 100 points.
3, projects are unit of scoring with 0.5 point.
4, it smokes panel test when scoring to six gloss, fragrance, harmony, miscellaneous gas, irritation, pleasant impression projects, each project quality
The requirement for reaching respective item, then accordingly score.
Embodiment 1
A kind of tobacco leaf additive, in parts by weight, composed of the following components:
After said components are mixed evenly, it is heated to reflux at 55 DEG C 8 hours, obtains tobacco leaf additive.
The tobacco leaf additive added into piece cigarette, addition manner are sprinkling, and additive amount is the 1% of piece cigarette weight.
Cigarette is made as sample 1 in the piece cigarette for being added to tobacco leaf additive, the pH value of its main flume is detected, as a result sees
Table 1.
Cigarette made of the piece cigarette of tobacco leaf additive is not used as control sample.
Sensory evaluating smoking's experiment is carried out to sample by GB5606.4-2005, smokeing panel test compares scoring event and be shown in Table 2.
Through sensory evaluating smoking, the excitement of sample 1 is reduced, and comfort level improves, and miscellaneous gas reduces.
Embodiment 2
A kind of tobacco leaf additive, in parts by weight, composed of the following components:
After said components are mixed evenly, after 6 hours are heated to reflux at 45 DEG C, tobacco leaf additive is obtained.
The tobacco leaf additive added in piece cigarette, addition manner are sprinkling, and additive amount is the 0.8% of piece cigarette weight.
Cigarette is made in the piece cigarette for being added to tobacco leaf additive, as sample 2, detects the pH value of its main flume, as a result
It is shown in Table 1.
Sensory evaluating smoking's experiment is carried out to sample by GB5606.4-2005, smokeing panel test compares scoring event and be shown in Table 2.
Through sensory evaluating smoking, the excitement of sample 2 is reduced, and comfort level improves, and flue gas is coordinated.
Embodiment 3
A kind of tobacco leaf additive, in parts by weight, composed of the following components:
After said components are mixed evenly, after 8 hours are heated to reflux at 55 DEG C, tobacco leaf additive is obtained.
The tobacco leaf additive added in piece cigarette, addition manner are sprinkling, and additive amount is the 2% of piece cigarette weight.
Cigarette is made as sample 3 in the piece cigarette for being added to tobacco leaf additive, the pH value of its main flume is detected, as a result sees
Table 1.
Sensory evaluating smoking's experiment is carried out to sample by GB5606.4-2005, smokeing panel test compares scoring event and be shown in Table 2.
Through sensory evaluating smoking, the excitement of sample 3 is reduced, and dry sensation weakens, and flue gas is coordinated, submissive.
The pH value testing result of 1 cigarette mainstream flue gas of table
2 Sensory Quality of Cigarette smoking result of table
Finally it should be noted that: the above embodiments are merely illustrative of the technical scheme of the present invention and are not intended to be limiting thereof;To the greatest extent
The present invention is described in detail with reference to preferred embodiments for pipe, it should be understood by those ordinary skilled in the art that: still
It can modify to a specific embodiment of the invention or some technical features can be equivalently replaced;Without departing from this hair
The spirit of bright technical solution should all cover within the scope of the technical scheme claimed by the invention.
Claims (10)
1. a kind of composition comprising following component: malic acid, citric acid, xylitol, glucose, benzoic acid, lauric acid, cream
Acid, glycerol and water.
2. the composition of claim 1 comprising following component in parts by weight:
3. the composition of claim 2 comprising following component in parts by weight:
4. the composition of any one of claims 1 to 3 is preparing the purposes in cigarette,
Preferably, the cigarette is Virginian-type cigarette.
5. purposes of the composition of any one of claims 1 to 3 as tobacco leaf additive, it is preferable that the tobacco leaf is roasting
Cigarette tobacco leaf.
6. the composition of any one of claims 1 to 3 is for reducing the purposes of cigarette mainstream flue gas pH value,
Preferably, the cigarette is Virginian-type cigarette.
7. a kind of tobacco leaf additive, it is prepared by the composition of any one of claims 1 to 3.
8. the method for preparing the tobacco leaf additive of claim 7, including following operation:
Malic acid, citric acid, xylitol, glucose, benzoic acid, lauric acid, lactic acid, glycerol and water are mixed, mixture is obtained,
Preferably, further include the operation being heated to reflux, obtained mixture be heated to reflux,
Preferably, it is heated to reflux and is carried out at 45~55 DEG C,
Preferably, return time is 2~8 hours.
9. a kind of method for reducing cigarette mainstream flue gas pH value, including the tobacco leaf additive of claim 7 is applied to piece
The step of cigarette, preferred applying mode are sprinkling.
Preferably, wherein the additive amount of the tobacco leaf additive is the 0.1~3% of piece cigarette weight,
Preferably, the cigarette is Virginian-type cigarette.
10. a kind of cigarette, it includes the composition of any one of claims 1 to 3 or the tobacco leaf additive of claim 7,
Preferably, the cigarette is Virginian-type cigarette.
Priority Applications (1)
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CN201811226093.4A CN109288117B (en) | 2018-10-22 | 2018-10-22 | Composition and application thereof in cigarettes |
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CN201811226093.4A CN109288117B (en) | 2018-10-22 | 2018-10-22 | Composition and application thereof in cigarettes |
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CN109288117A true CN109288117A (en) | 2019-02-01 |
CN109288117B CN109288117B (en) | 2022-06-17 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109619663A (en) * | 2019-02-22 | 2019-04-16 | 上海烟草集团有限责任公司 | Tobacco additive agent and its preparation method and application |
CN114886154A (en) * | 2022-05-27 | 2022-08-12 | 河南中烟工业有限责任公司 | Additive for improving filter tip ventilated cigarette dry feeling and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109619663A (en) * | 2019-02-22 | 2019-04-16 | 上海烟草集团有限责任公司 | Tobacco additive agent and its preparation method and application |
CN114886154A (en) * | 2022-05-27 | 2022-08-12 | 河南中烟工业有限责任公司 | Additive for improving filter tip ventilated cigarette dry feeling and preparation method thereof |
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