CN109288013A - The preparation method of Tibet smooth pit peach Ultramicro-powder - Google Patents

The preparation method of Tibet smooth pit peach Ultramicro-powder Download PDF

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Publication number
CN109288013A
CN109288013A CN201811216530.4A CN201811216530A CN109288013A CN 109288013 A CN109288013 A CN 109288013A CN 201811216530 A CN201811216530 A CN 201811216530A CN 109288013 A CN109288013 A CN 109288013A
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China
Prior art keywords
peach
powder
smooth pit
ultramicro
freeze
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CN201811216530.4A
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Inventor
毕金峰
吕健
陈芹芹
左立旭
刘璇
周沫
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Institute of Food Science and Technology of CAAS
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Institute of Food Science and Technology of CAAS
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Priority to CN201811216530.4A priority Critical patent/CN109288013A/en
Publication of CN109288013A publication Critical patent/CN109288013A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L25/00Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
    • A23L25/30Mashed or comminuted products, e.g. pulp, pastes, meal, powders; Products made therefrom, e.g. blocks, flakes, snacks; Liquid or semi-liquid products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/01Instant products; Powders; Flakes; Granules
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/03Organic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/36Freezing; Subsequent thawing; Cooling
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/20Removal of unwanted matter, e.g. deodorisation or detoxification
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a kind of preparation methods of Tibet smooth pit peach Ultramicro-powder, comprising the following steps: Step 1: raw material pre-freeze to be processed to material center temperature is -2~-3 DEG C, obtains pre-freeze material;Step 2: pre-freeze material is 3%~6% through vacuum refrigeration to material moisture, dried material is obtained;Step 3: dried material grinding and sieving, obtains coarse powder broken material;Step 4: comminuting matter is placed in vibromill, regulation power is 1.0~1.4kW, and amplitude is 3~5mm, and temperature is 5~10 DEG C, crushes 10~30min, obtains ultramicro grinding material, pulverizes material and packs after sterilizing.The present invention has the beneficial effect for obtaining the Tibet smooth pit peach Ultramicro-powder that diameter of particle is small, particle size distribution span is narrow, the uniformity is high, dissolubility is good.

Description

The preparation method of Tibet smooth pit peach Ultramicro-powder
Technical field
The present invention relates to fruit powder preparation fields.It is more particularly related to a kind of system of Tibet smooth pit peach Ultramicro-powder Preparation Method.
Background technique
Tibet smooth pit peach category rosaceae peach category deciduous tree, is Tibet region one of wild fruit tree distributed more widely.Light core Peach pericarp surface covers villus, and fruit stone surface is smooth, and fruit is subsphaeroidal, fresh food slightly bitter taste, rich in minerals, vitamin, The nutriments such as dietary fiber, reduced sugar.At present about Tibet smooth pit peach utilization be concentrated mainly on fruit jelly, fruit wine, preserved fruit and Fruit juice etc., but limited by factors such as traffic, information, environment and regions, cause Tibet smooth pit peach industrialization level non- Often low, product cannot be introduced into mainland market.Fruit vegetable powder is low to ingredient requirement, and the scope of application is extremely wide, especially to the skin of edibility, core It is available, and fruit vegetable powder is convenient, adjustability is strong, full of nutrition, can utmostly keep the original battalion of fruit and vegetable It supports, flavor, is often used as ingredient and processes other food, become a kind of good nutrition deep processed product, further, fruit vegetable powder water Point content is low, can suppress growth of microorganism and enzymatic activity, substantially reduces the expense of storage, transport, packaging etc., is conducive to Promote the industrialization of Tibet smooth pit peach;
Ultramicro grinding is a kind of materiel machining technology for being the development of adaptation modern high technology and formation the 1970s. It mainly overcomes solid interior cohesiveness to be allowed to broken using mechanical or hydrokinetic method, thus by the object of 3mm or more Material particle is crushed to 10~25um subparticle below, and then product is made to have interfacial activity, shows specific function.Fruits and vegetables Powder after pulverizing, rehydration, retention ability, hold the characteristics such as oily power and significantly improve by dissolubility, nutriment dissolution rate and The amount of dissolution obviously increases.
Therefore, Tibet smooth pit peach is processed by compound fruit powder using superfine communication technique, is not only convenient for storage, transport and pin It sells, the utilization rate of Tibet smooth pit peach can also be improved, promote the industrialization of Tibet smooth pit peach
Summary of the invention
It is an object of the invention to solve at least the above problems, and provide the advantages of at least will be described later.
It is a still further object of the present invention to provide a kind of preparation method of Tibet smooth pit peach Ultramicro-powder,.
In order to realize these purposes and other advantages according to the present invention, a kind of smooth pit peach Ultramicro-powder in Tibet living is provided Preparation method, comprising the following steps:
Step 1: pre-freeze is handled: raw material pre-freeze to be processed to material center temperature is -2~-3 DEG C, obtains pre-freeze material;
Step 2: vacuum refrigeration is handled: pre-freeze material is 3%~6% through vacuum refrigeration to material moisture, obtains dried object Material;
Step 3: coarse crushing is handled: dried material grinding and sieving obtains coarse powder broken material;
Step 4: crushing packing is handled: comminuting matter is placed in vibromill, and regulation power is 1.0~1.4kW, amplitude 3 ~5mm, temperature are 5~10 DEG C, crush 10~30min, obtain ultramicro grinding material, pulverize material and pack after sterilizing.
Preferably, raw material to be processed is ripe smooth pit peach or very likely in ripe smooth pit peach mixture very likely in step 1 It is a kind of, wherein ripe smooth pit peach mixture component meter by weight includes: 30~50 parts of ripe smooth pit peaches very likely very likely, and 20~40 Part strawberry, 10~20 portions of apples, 10~20 portions of raspberries, 5~10 parts of auxiliary materials, auxiliary material are mainly pasted by the malt that mass ratio is 5:5:3 Essence, xylitol, calcium lactate composition;
Ripe smooth pit peach carries out stoning processing before carrying out pre-freeze processing very likely.
Preferably, when raw material to be processed is ripe smooth pit peach mixture very likely, ripe smooth pit peach, strawberry, apple very likely Fruit, raspberry carry out pre-freeze processing and vacuum refrigeration processing respectively, carry out coarse crushing after vacuum refrigeration treated each raw material mixing It is mixed after processing or respectively progress coarse crushing processing.
Preferably, the temperature of pre-freeze is -20~-50 DEG C in step 1.
Preferably, in step 2 vacuum freeze drying vacuum degree be 0.10~0.14Mpa, drying time be 40~ 60h。
Preferably, dried material breaking method is one of low-temperature grinding or interval crushing in step 3, wherein low Temperature crushes specifically: controlled at 5~10 DEG C, is crushed 3~5min;Interval crushes specifically: carries out 25~35s of pulverization process 25~35s of radiating treatment is carried out afterwards, repeats to interval to crush the cumulative time as 3~5min;
It is 80 mesh that grit number is crossed in step 3.
Preferably, step 4 is arranged using the vibrating head quantity in vibromill are as follows: every 100g coarse powder broken material correspondence is set Set 3~5 thin sticks, 3~5 medium rods, 2~4 root thickness sticks.
Preferably, the method for disinfection in step 4 is the infrared sterilization of intermediate waves, specifically: wavelength is 1~4 μm, infrared The power of lamp is 450~2025W, and sterilization temperature is 100~120 DEG C, and sterilizing time is 1~5min.
Preferably, raw material to be processed is ripe smooth pit peach very likely in step 1, and ripe smooth pit peach carries out at pre-freeze very likely Pre-processed, pre-processed before reason specifically: after being enucleated after ripe smooth pit peach is cleaned very likely pulp and fruit stone, at fruit stone Manage to obtain peach kernel, peach kernel crush after peach kernel powder, peach kernel powder, which is added after the tealeaves mixing that 2-3 times of its gross mass is measured, to be entered pot and is fried with slow fire 60~70 DEG C of 10~15min of holding reject tealeaves and obtain frying peach kernel powder and frying tealeaves, frying peach kernel powder is placed in Decocting pot The water that 20-25 times of its gross mass is measured is added, support frame is set up in Decocting pot, cage cloth is laid on support frame, frying tealeaves is equal It is even to be layed on cage cloth, after decocting 1h, support frame and frying tealeaves are removed, continues decoction 20min and obtains decoction material, mix decoction material And pulp obtains mixture, mixture carries out pre-freeze processing.
The present invention is include at least the following beneficial effects:
The first, traditional using caused by vacuum drying in conjunction with can effectively be avoided by the way of vacuum refrigeration after first pre-freeze Drying time longer problem, can within the relatively short time abundant dried material, while vacuum refrigeration may advantageously facilitate The nutriment dissolution of material to be dried at a lower temperature, cooperates subsequent crushing process, improves Tibet smooth pit peach nutrients Matter dissolution rate, as shown in Table 1, even coarse powder broken material, titratable acid, polyphenol, flavones and minerals have higher molten Out;Further, first carry out precomminution in such a way that low-temperature grinding or interval crush, precomminution process effectively prevent due to Processing temperature is excessively high and destroys the ingredient and flavor of product, and precomminution cooperation pulverizes, and obtains that diameter of particle is small, particle diameter distribution The Tibet smooth pit peach Ultramicro-powder that span is narrow, the uniformity is high, dissolubility is good, as shown in Table 1 relative to coarse powder broken material Tibet light core Peach Ultramicro-powder moisture content is low, and Color Quality is preferable, and average grain diameter is small, and powder granule is evenly distributed, and dissolubility is preferable, effective component Dissolution rate is high, that is, further increases Ultramicro-powder performance.
The second, raw material to be processed prepares smooth pit peach Ultramicro-powder when being smooth pit peach need not add any auxiliary material, and pulverize Time is shorter, minimum 10min, and water soluble pectin and organic acid the amount of dissolution improve after ultramicro grinding, can be used as after reconstituting The regulating acid agent and stabilizer of fruit drink;Raw material to be processed be very likely ripe smooth pit peach mixture when, cooperation auxiliary material addition preparation Smooth pit peach composite superfine powder also have moisture content low, Color Quality is preferable, and average grain diameter is small, and powder granule is evenly distributed, molten Solution property is preferable, and effective component dissolution rate is high, the higher characteristic of product integrated quality, promotees in enhancing smooth pit peach composite superfine powder mouthfeel It is comprehensive meanwhile, it is capable to improve apple powder hygroscopicity problems into nutritional ingredient.
Third, will its peach kernel of smooth pit peach processing after with smooth pit peach pulp be jointly processed by obtain the full fruit Ultramicro-powder of smooth pit peach, light Walnut peach kernel and smooth pit peach pulp itself all have slight bitter taste, and smooth pit peach slightly has astringent taste, by by smooth pit peach peach kernel with The common frying of tealeaves, frying processing cooperation tealeaves faint scent is effectively improved peach kernel itself bitter taste, and promotes benefit materials in peach kernel Later period dissolution, further Catechin in Tea is partially soluble in decoction liquor by steaming, the unsaturated lipid with smooth pit peach peach kernel The synergistic function of the anti-oxidation function for the polyphenol being rich in fat acid and corresponding pulp, while being decocted after frying, in cooperation fruit Water-soluble difference caused by a series of processing such as meat progress pre-freeze, vacuum refrigeration can effectively avoid smooth pit peach peach kernel from adding Problem improves the full fruit Ultramicro-powder solubility of smooth pit peach.
Further advantage, target and feature of the invention will be partially reflected by the following instructions, and part will also be by this The research and practice of invention and be understood by the person skilled in the art.
Specific embodiment
The present invention will be further described in detail below with reference to the embodiments, to enable those skilled in the art referring to specification Text can be implemented accordingly.
<embodiment 1>
The preparation method of Tibet smooth pit peach Ultramicro-powder, comprising the following steps:
Step 1: pre-freeze is handled: very likely after ripe smooth pit peach picking, circulating water is cleaned up, and mass fraction is 3% salt water After soak at room temperature 5h, clear water flushing, cutting, stoning obtain pretreatment smooth pit peach, and pretreatment smooth pit peach is -20 DEG C of environment in temperature Lower pre-freeze to material center temperature is -2.6 DEG C, obtains pre-freeze material;
Step 2: vacuum refrigeration is handled: pre-freeze material is placed in vacuum freezing drying oven, regulation vacuum degree is 0.10~ Within the scope of 0.14Mpa, it to material moisture is 5.7% that drying time, which is 40h, obtains dried material;
Step 3: coarse crushing is handled: dried material is placed in pulverizer, controlled within the scope of 5~10 DEG C, is crushed After 3min, 80 meshes are crossed, part enters next round and is mechanically pulverized on sieve, obtains coarse powder broken material;
Step 4: crushing packing handle: comminuting matter is placed in vibromill, regulation power be 1.0~1.4kW within the scope of, Amplitude is within the scope of 3~5mm, and temperature is to crush 20min within the scope of 5~10 DEG C, obtains ultramicro grinding material, pulverizes material The aseptic packaging after sterilizing, wherein be arranged using the vibrating head quantity in vibromill are as follows: every 100g coarse powder broken material is corresponding 3 thin sticks, 3 medium rods are set, and 2 root thickness sticks select whole radical with specific reference to material requirement, and method for disinfection is that intermediate waves is infrared Sterilization, specifically: wavelength is 4 μm, and the power of infrared lamp is 450W, and sterilization temperature is 120 DEG C, sterilizing time 5min.
<embodiment 2>
The preparation method of Tibet smooth pit peach Ultramicro-powder, comprising the following steps:
Step 1: circulating water cleans up, and mass fraction is 5% salt water soak at room temperature very likely after ripe smooth pit peach picking After 3h, clear water flushing, cutting, stoning obtain pretreatment smooth pit peach, and pre-freeze is extremely in the case where temperature is -40 DEG C of environment for pretreatment smooth pit peach Material center temperature is -3 DEG C, obtains pre-freeze material;
Step 2: pre-freeze material is placed in vacuum freezing drying oven, regulation vacuum degree is to do within the scope of 0.10~0.14Mpa It to material moisture is 3.3% that the dry time, which is 60h, obtains dried material;
Step 3: dried material is placed in pulverizer, carry out radiating treatment 30s after carrying out pulverization process 30s, repeat to It has a rest and crushes the cumulative time as 5min, cross 80 meshes, part enters next round and is mechanically pulverized on sieve, obtains coarse powder broken material;
Step 4: comminuting matter is placed in vibromill, regulation power is within the scope of 1.0~1.4kW, and amplitude is 3~5mm model In enclosing, temperature is to crush 10min within the scope of 5~10 DEG C, obtains ultramicro grinding material, pulverizes material after sterilizing without bacterium bag Dress, wherein vibrating head quantity in vibromill is used to be arranged are as follows: every 100g coarse powder broken material is correspondingly arranged 5 thin sticks, and 5 Root medium rod, 4 root thickness sticks select whole radical with specific reference to material requirement, and method for disinfection is the infrared sterilization of intermediate waves, specifically: wave A length of 3 μm, the power of infrared lamp is 1056W, and sterilization temperature is 120 DEG C, sterilizing time 5min.
<embodiment 3>
The preparation method of Tibet smooth pit peach Ultramicro-powder, comprising the following steps:
Step 1: raw material to be processed is ripe smooth pit peach mixture very likely, ripe smooth pit peach mixture group by weight very likely Dividing meter includes: 30 parts of ripe smooth pit peaches very likely, and 20 portions of strawberries, 10 portions of apples, 10 portions of raspberries, 5 parts of auxiliary materials, auxiliary material is mainly by quality Than maltodextrin, xylitol, the calcium lactate composition for 5:5:3;
Very likely after ripe smooth pit peach picking, circulating water is cleaned up, after mass fraction is 4% salt water soak at room temperature 4h, clearly Water flushing, cutting, stoning, obtain pretreatment smooth pit peach;
It after strawberry stalk, apple remove handle, cleans up, is cut into 0.5cm thin slice, apple and pretreatment grass must be pre-processed The certain kind of berries;
It drenches and does after raspberry cleaning, raspberry must be pre-processed;
Pre-processing smooth pit peach, pretreatment apple, pretreatment strawberry and pretreatment raspberry is respectively -30 DEG C of environment in temperature Lower pre-freeze to material center temperature is to obtain pre-freeze smooth pit peach, pre-freeze apple, pre-freeze strawberry and pre-freeze tree within the scope of -2~-3 DEG C The certain kind of berries;
Step 2: pre-freeze smooth pit peach, pre-freeze apple, pre-freeze strawberry and pre-freeze raspberry are respectively placed in vacuum freezing drying oven, Regulating and controlling vacuum degree is within the scope of 0.10~0.14Mpa, and it to material moisture is to obtain in 3%~6% range that drying time, which is 50h, Dry smooth pit peach, dry apple, dry strawberry and dry raspberry;
Step 3: dry smooth pit peach, dry apple, dry strawberry and dry raspberry are respectively placed in pulverizer, control temperature Degree is after being crushed 4min, to cross 80 meshes, part enters next round mechanical crushing on sieve, obtains coarse crushing light core within the scope of 5~10 DEG C Peach, coarse crushing apple, coarse crushing strawberry and coarse crushing raspberry, coarse crushing smooth pit peach, coarse crushing apple, coarse crushing strawberry and thick It crushes raspberry and mixes to obtain coarse powder broken material;
Step 4: comminuting matter is placed in vibromill, regulation power is within the scope of 1.0~1.4kW, and amplitude is 3~5mm model In enclosing, temperature is to crush 20min within the scope of 5~10 DEG C, obtains ultramicro grinding material, pulverizes material after sterilizing without bacterium bag Dress, wherein vibrating head quantity in vibromill is used to be arranged are as follows: every 100g coarse powder broken material is correspondingly arranged 4 thin sticks, and 4 Root medium rod, 3 root thickness sticks select whole radical with specific reference to material requirement, and method for disinfection is the infrared sterilization of intermediate waves, specifically: wave A length of 1 μm, the power of infrared lamp is 450W, and sterilization temperature is 100 DEG C, sterilizing time 5min.
<embodiment 4>
The preparation method of Tibet smooth pit peach Ultramicro-powder, comprising the following steps:
Step 1: raw material to be processed is ripe smooth pit peach mixture very likely, ripe smooth pit peach mixture group by weight very likely Dividing meter includes: 50 parts of ripe smooth pit peaches very likely, and 40 portions of strawberries, 20 portions of apples, 20 portions of raspberries, 10 parts of auxiliary materials, auxiliary material is mainly by matter Amount is formed than the maltodextrin, xylitol, calcium lactate for being 5:5:3;
Very likely after ripe smooth pit peach picking, circulating water is cleaned up, after mass fraction is 5% salt water soak at room temperature 3h, clearly Water flushing, cutting, stoning, obtain pretreatment smooth pit peach;
It after strawberry stalk, apple remove handle, cleans up, is cut into 0.5cm thin slice, apple and pretreatment grass must be pre-processed The certain kind of berries;
It drenches and does after raspberry cleaning, raspberry must be pre-processed;
Pre-processing smooth pit peach, pretreatment apple, pretreatment strawberry and pretreatment raspberry is respectively -40 DEG C of environment in temperature Lower pre-freeze to material center temperature is to obtain pre-freeze smooth pit peach, pre-freeze apple, pre-freeze strawberry and pre-freeze tree within the scope of -2~-3 DEG C The certain kind of berries;;
Step 2: pre-freeze smooth pit peach, pre-freeze apple, pre-freeze strawberry and pre-freeze raspberry are respectively placed in vacuum freezing drying oven, Regulating and controlling vacuum degree is within the scope of 0.10~0.14Mpa, and it to material moisture is to obtain in 3%~6% range that drying time, which is 60h, Dry smooth pit peach, dry apple, dry strawberry and dry raspberry, dry smooth pit peach, dry apple, dry strawberry and dry tree The certain kind of berries mixes to obtain dried material;
Step 3: dried material is placed in pulverizer, carry out radiating treatment 30s after carrying out pulverization process 30s, repeat to It has a rest and crushes the cumulative time as 5min, cross 80 meshes, part enters next round mechanical crushing (crushing operation of step 3) on sieve, obtains Coarse powder broken material;
Step 4: comminuting matter is placed in vibromill, regulation power is within the scope of 1.0~1.4kW, and amplitude is 3~5mm model In enclosing, temperature is to crush 10min within the scope of 5~10 DEG C, obtains ultramicro grinding material, pulverizes material after sterilizing without bacterium bag Dress, wherein vibrating head quantity in vibromill is used to be arranged are as follows: every 100g coarse powder broken material is correspondingly arranged 5 thin sticks, and 5 Root medium rod, 4 root thickness sticks select whole radical with specific reference to material requirement, and method for disinfection is the infrared sterilization of intermediate waves, specifically: wave A length of 3 μm, the power of infrared lamp is 1056W, and sterilization temperature is 120 DEG C, sterilizing time 5min.
<embodiment 5>
The preparation method of Tibet smooth pit peach Ultramicro-powder, comprising the following steps:
Step 1: circulating water cleans up, and mass fraction is 5% salt water soak at room temperature very likely after ripe smooth pit peach picking After 3h, pulp and fruit stone are obtained after clear water flushing, cutting, stoning, fruit stone carries out handling to obtain peach kernel, and peach kernel obtains peach kernel powder after crushing, Peach kernel powder, which is added after the tealeaves mixing that 2-3 times of its gross mass measures, to be entered pot and is fried with slow fire holding 13min 60~70 DEG C within the scope of, rejecting Tealeaves obtains frying peach kernel powder and frying tealeaves, and frying peach kernel powder is placed in Decocting pot to the water that 23 times of its gross mass amounts are added, Support frame is set up in Decocting pot, is laid with cage cloth on support frame, frying tealeaves is uniformly layed on cage cloth, after decocting 1h, removal Support frame and frying tealeaves continue decoction 20min and obtain decoction material, mixes decoction material and pulp obtains mixture, mixture is in temperature It is -2.5 DEG C for pre-freeze under -40 DEG C of environment to material center temperature, obtains pre-freeze material;
Step 2: pre-freeze material is placed in vacuum freezing drying oven, regulation vacuum degree is to do within the scope of 0.10~0.14Mpa It to material moisture is 3.6% that the dry time, which is 60h, obtains dried material;
Step 3: dried material is placed in pulverizer, carry out radiating treatment 30s after carrying out pulverization process 30s, repeat to It has a rest and crushes the cumulative time as 5min, cross 80 meshes, part enters next round and is mechanically pulverized on sieve, obtains coarse powder broken material;
Step 4: comminuting matter is placed in vibromill, regulation power is within the scope of 1.0~1.4kW, and amplitude is 3~5mm model In enclosing, temperature is to crush 10min within the scope of 5~10 DEG C, obtains ultramicro grinding material, pulverizes material after sterilizing without bacterium bag Dress, wherein vibrating head quantity in vibromill is used to be arranged are as follows: every 100g coarse powder broken material is correspondingly arranged 5 thin sticks, and 5 Root medium rod, 4 root thickness sticks select whole radical with specific reference to material requirement, and method for disinfection is the infrared sterilization of intermediate waves, specifically: wave A length of 3 μm, the power of infrared lamp is 1056W, and sterilization temperature is 120 DEG C, sterilizing time 5min.
<comparative example 1>
The preparation method of Tibet smooth pit peach powder, comprising the following steps:
Step 1: Step 2: the concrete operations of step 3 obtain coarse powder broken material with embodiment 2;
Step 4: the aseptic packaging after sterilizing of coarse powder broken material, wherein method for disinfection is the same as embodiment 2.
<comparative example 2>
The preparation method of Tibet smooth pit peach composite superfine powder, comprising the following steps:
Pretreatment smooth pit peach, pretreatment apple, pretreatment strawberry and pre- place are obtained according to the method for 4 step 1 of embodiment Raspberry is managed, pretreatment smooth pit peach, pretreatment apple, pretreatment strawberry and pretreatment raspberry are respectively in the case where temperature is -40 DEG C of environment Pre-freeze to material center temperature is to obtain pre-freeze smooth pit peach, pre-freeze apple, pre-freeze strawberry and pre-freeze raspberry within the scope of -2~-3 DEG C, Pre-freeze smooth pit peach, pre-freeze apple, pre-freeze strawberry and pre-freeze raspberry are as pre-freeze material respectively according to embodiment 4 Step 2: step Three, the mode of step 4 obtains corresponding ultra micro powder material, i.e. smooth pit peach Ultramicro-powder, apple Ultramicro-powder, strawberry Ultramicro-powder and tree Certain kind of berries Ultramicro-powder;
Step 5: component meter by weight, 50 parts of smooth pit peach Ultramicro-powders are taken, 40 parts of apple Ultramicro-powders, 20 parts of strawberry Ultramicro-powders, 20 parts of raspberry Ultramicro-powders, 10 parts of auxiliary materials mix to obtain composite superfine powder, and composite superfine powder is stirred to fruit powder color stability, compound ultra micro Powder aseptic packaging after sterilizing, auxiliary material are mainly made of maltodextrin, xylitol, calcium lactate that mass ratio is 5:5:3, In, the mode of sterilization is the same as embodiment 4.
<comparative example 3>
The preparation method of Tibet smooth pit peach Ultramicro-powder, comprising the following steps:
Step 1: circulating water cleans up, and mass fraction is 5% salt water soak at room temperature very likely after ripe smooth pit peach picking After 3h, pulp and fruit stone are obtained after clear water flushing, cutting, stoning, fruit stone carries out handling to obtain peach kernel, and mixing peach kernel and pulp must mix Material, mixture pre-freeze to material center temperature in the case where temperature is -40 DEG C of environment is -2.6 DEG C, obtains pre-freeze material;
Step 2: pre-freeze material is placed in vacuum freezing drying oven, regulation vacuum degree is to do within the scope of 0.10~0.14Mpa It to material moisture is 3.8% that the dry time, which is 60h, obtains dried material;
Step 3: dried material is placed in pulverizer, carry out radiating treatment 30s after carrying out pulverization process 30s, repeat to It has a rest and crushes the cumulative time as 5min, cross 80 meshes, part enters next round mechanical crushing (crushing operation of step 3) on sieve, obtains Coarse powder broken material;
Step 4: comminuting matter is placed in vibromill, regulation power is within the scope of 1.0~1.4kW, and amplitude is 3~5mm model In enclosing, temperature is to crush 10min within the scope of 5~10 DEG C, obtains ultramicro grinding material, pulverizes material after sterilizing without bacterium bag Dress, wherein vibrating head quantity in vibromill is used to be arranged are as follows: every 100g coarse powder broken material is correspondingly arranged 5 thin sticks, and 5 Root medium rod, 4 root thickness sticks, method for disinfection are the infrared sterilization of intermediate waves, specifically: wavelength is 3 μm, and the power of infrared lamp is 1056W, Sterilization temperature is 120 DEG C, sterilizing time 5min.
Index of quality measurement
Moisture content: it is measured referring to the direct drying method of GB 5009.3-2010.
Water activity: it is measured using admeasuring apparatus for measuring moisture content of substance.
Color: it is measured using hand-held color difference meter.
Average grain diameter and particle size distribution span: it is measured using laser particle size analyzer.
Dissolubility: according to dissolubility (WS) formula calculated, WS=(W/W0) × 100, W is the fruit powder for being dissolved in water in formula Quality, g;W0For initial weighed fruit powder quality, g.
Titratable acid: referring to the method for measuring of GB12293-1990 titrable acidity, as a result with titratable acid content (g apple Tartaric acid/100g) it indicates.
Attributional analysis is carried out to the product of embodiment 2 and comparative example 1 in the manner described above, is specifically shown in Table 1:
The attributional analysis data of table 1 embodiment 2 and 1 product of comparative example
The index of quality Embodiment 1 Comparative example 1
Moisture content (%) 5.43±0.12 5.08±0.23
Water activity 0.12±0.01 0.13±0.00
Color L* 86.47±0.06 84.85±0.61
Color a* -1.75±0.07 -0.23±0.01
Color b* 14.20±0.35 14.97±0.45
Average grain diameter (μm) 15.71±1.21 85.93±5.36
Particle size distribution span 2.08±0.08 3.62±0.04
Dissolubility (%) 41.21±1.23 33.96±1.06
Titratable acid (g malic acid/100g) 0.30±0.05 0.25±0.04
Polyphenol (mg galla turcica/g) 35.17±0.18 34.52±0.16
Flavones (mg rutin/g) 81.37±3.20 76.53±1.84
Minerals (ppm) 5846.27±123.21 5446.23±103.26
As shown in Table 1, Tibet smooth pit peach powder of the Tibet smooth pit peach Ultramicro-powder that prepared by embodiment 2 relative to comparative example 1, contains Water rate is low, and Color Quality is preferable, and average grain diameter is small, and powder granule is evenly distributed, and dissolubility is preferable, and effective component dissolution rate is high, The integrated quality of Tibet smooth pit peach Ultramicro-powder product prepared by embodiment 2 obtains very relative to the Tibet smooth pit peach powder of comparative example 1 It is big to be promoted.
Attributional analysis is carried out to the product of embodiment 4 and comparative example 2 in the manner described above, is specifically shown in Table 2:
The attributional analysis data of table 2 embodiment 4 and 2 product of comparative example
The index of quality Embodiment 2 Embodiment 3
Moisture content (%) 6.43±0.11 7.08±0.21
Water activity 0.22±0.01 0.33±0.01
Color L* 89.47±1.05 85.85±6.69
Color a* -2.75±0.05 -2.23±0.54
Color b* 13.20±0.31 13.97±1.42
Average grain diameter (μm) 16.71±1.25 18.93±5.06
Particle size distribution span 2.68±0.05 3.92±0.08
Dissolubility (%) 40.21±1.23 39.23±1.16
Titratable acid (g malic acid/100g) 0.43±0.06 0.35±0.05
Polyphenol (mg galla turcica/g) 30.17±0.12 29.52±0.11
Flavones (mg rutin/g) 71.47±3.10 66.53±1.04
Minerals (ppm) 5046.27±123.21 4946.23±103.26
As shown in Table 2, in example 4, coarse crushing and ultramicro grinding are carried out again after the completion of raw material proportioning, relative to comparison Raw material is individually carried out coarse crushing and ultramicro grinding by example 2, is compounded after obtaining Ultramicro-powder according to different formulas, embodiment 4 Being sufficiently mixed for raw material and ingredient is effectively facilitated, guarantees ultra micro composite powder uniform color, further embodiment 4 is made as shown in Table 2 Standby smooth pit peach composite superfine powder has moisture content low, and Color Quality is preferable, and average grain diameter is small, and powder granule is evenly distributed, molten Solution property is preferable, and effective component dissolution rate is high, the higher characteristic of product integrated quality.
Solubility analysis is carried out to the product of embodiment 2, embodiment 5, comparative example 3 in the manner described above, is specifically shown in Table 3:
The solubility of table 3 embodiment 2 and 5 product of embodiment
Index Implement 2 Embodiment 5 Comparative example 3
Dissolubility (%) 41.21±1.23 41.06±1.07 37.06±1.27
As shown in Table 3, in embodiment 5, the light of dissolubility and embodiment 2 preparation of the full fruit Ultramicro-powder of the smooth pit peach of preparation The dissolubility of walnut Ultramicro-powder is suitable, i.e., there is no the additions because of peach kernel, and its solubility to be caused significant change occur, and compares The solubility of example 3 is then significantly lower than embodiment 5.
Although the embodiments of the present invention have been disclosed as above, but its is not only in the description and the implementation listed With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can be easily Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is simultaneously unlimited In specific details and embodiment shown and described herein.

Claims (9)

1. the preparation method of Tibet smooth pit peach Ultramicro-powder, which comprises the following steps:
Step 1: pre-freeze is handled: raw material pre-freeze to be processed to material center temperature is -2~-3 DEG C, obtains pre-freeze material;
Step 2: vacuum refrigeration is handled: pre-freeze material is 3%~6% through vacuum refrigeration to material moisture, obtains dried material;
Step 3: coarse crushing is handled: dried material grinding and sieving obtains coarse powder broken material;
Step 4: crushing packing handle: comminuting matter is placed in vibromill, regulation power be 1.0~1.4kW, amplitude be 3~ 5mm, temperature are 5~10 DEG C, crush 10~30min, obtain ultramicro grinding material, pulverize material and pack after sterilizing.
2. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that original to be processed in step 1 Material is ripe smooth pit peach or very likely one of ripe smooth pit peach mixture very likely, wherein ripe smooth pit peach mixture is pressed very likely Components by weight percent meter includes: 30~50 parts of ripe smooth pit peaches very likely, 20~40 portions of strawberries, 10~20 portions of apples, 10~20 portions of raspberries, 5~10 parts of auxiliary materials, auxiliary material are mainly made of maltodextrin, xylitol, calcium lactate that mass ratio is 5:5:3;
Ripe smooth pit peach carries out stoning processing before carrying out pre-freeze processing very likely.
3. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that when raw material to be processed is seven When medium well smooth pit peach mixture, ripe smooth pit peach, strawberry, apple, raspberry carry out pre-freeze processing and vacuum refrigeration respectively very likely Processing carries out coarse crushing processing after vacuum refrigeration treated each raw material mixing or mixes after carrying out coarse crushing processing respectively.
4. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that the temperature of pre-freeze in step 1 Degree is -20~-50 DEG C.
5. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that vacuum refrigeration in step 2 Dry vacuum degree is 0.10~0.14Mpa, and drying time is 40~60h.
6. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that dried material in step 3 Breaking method is one of low-temperature grinding or interval crushing, wherein low-temperature grinding specifically: controlled at 5~10 DEG C, is broken Broken 3~5min;Interval crushes specifically: carries out 25~35s of radiating treatment after carrying out 25~35s of pulverization process, repeats to interval The crushing cumulative time is 3~5min;
It is 80 mesh that grit number is crossed in step 3.
7. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that step 4 uses vibromill In vibrating head quantity setting are as follows: every 100g coarse powder broken material is correspondingly arranged 3~5 thin sticks, 3~5 medium rods, 2~4 root thickness Stick.
8. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that the sterilization side in step 4 Method is the infrared sterilization of intermediate waves, specifically: wavelength is 1~4 μm, and the power of infrared lamp is 450~2025W, sterilization temperature 100 ~120 DEG C, sterilizing time is 1~5min.
9. the preparation method of smooth pit peach Ultramicro-powder in Tibet as described in claim 1, which is characterized in that when to be processed in step 1 Raw material is ripe smooth pit peach very likely, and ripe smooth pit peach is pre-processed before carrying out pre-freeze processing very likely, is pre-processed specifically: seven or eight Mature smooth pit peach obtains pulp and fruit stone after being enucleated after cleaning, fruit stone carries out handling to obtain peach kernel, and peach kernel obtains peach kernel powder, peach kernel after crushing Powder, which is added after the tealeaves mixing that 2-3 times of its gross mass measures, to be entered pot and is fried with slow fire 60~70 DEG C of 10~15min of holdings, and rejecting tealeaves obtains Frying peach kernel powder is placed in Decocting pot the water that 20-25 times of its gross mass is added and measures, decocted by frying peach kernel powder and frying tealeaves Support frame is set up in tank, is laid with cage cloth on support frame, frying tealeaves is uniformly layed on cage cloth, after decocting 1h, removal support Frame and frying tealeaves continue decoction 20min and obtain decoction material, mix decoction material and pulp obtains mixture, mixture carries out at pre-freeze Reason.
CN201811216530.4A 2018-10-18 2018-10-18 The preparation method of Tibet smooth pit peach Ultramicro-powder Pending CN109288013A (en)

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Application publication date: 20190201