CN109280458A - A kind of conch meal biological environmental production interior wall coating and preparation method thereof - Google Patents
A kind of conch meal biological environmental production interior wall coating and preparation method thereof Download PDFInfo
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- CN109280458A CN109280458A CN201810904994.8A CN201810904994A CN109280458A CN 109280458 A CN109280458 A CN 109280458A CN 201810904994 A CN201810904994 A CN 201810904994A CN 109280458 A CN109280458 A CN 109280458A
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- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
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- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
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- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
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- C08K2003/323—Ammonium polyphosphate
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Abstract
The invention discloses a kind of conch meal biological environmental production interior wall coating, the raw material including following parts by weight: aqueous epoxy resins, conch meal, rutile, superfine silicon dioxide, talcum powder, acrylic emulsion, xanthan gum, glycerol, neopelex, ichthyodin, ethoxy, ammonium polyphosphate, ethyl alcohol, dispersing agent, wetting agent, suspending agent, preservative, water；Preparation method includes the following steps: S1: the aqueous epoxy resins of the above parts by weight and rutile being added sequentially in micronizer, obtain admixed finepowder A after sufficiently crushing；S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 60~70 DEG C, and after 70%~80% admixed finepowder A fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, is continued stirring and is dissolved in ethyl alcohol to admixed finepowder A.Preparation process of the present invention is simple, and each raw material is uniformly mixed, and preparation process is pollution-free, high production efficiency, environmental-friendly, is worthy to be popularized.
Description
Technical field
The present invention relates to building material technical field more particularly to a kind of conch meal biological environmental production interior wall coating and its preparations
Method.
Background technique
Coating is to form one layer of firm continuous film in conjunction with coated article surface, plays decoration and protects coated article
Effect, is widely used in building field.House build complete when, inner wall surface usually has a cement mortar, when finishing in order to
Beauty can smear powder of lacquer putty for use on cement mortar surface, then in powder of lacquer putty for use on external coating coating, and the color of coating can also root
Change according to the difference of decoration style.Water paint, solvent reducible coatings, powdery paints and Gao Gu can be divided into according to the form of coating
Body divides coating, and water-based coating is although safe and environment-friendly, but in work progress and material surface cleannes require it is high, because of water
Surface tension it is big, dirt easily make film generate shrinkage cavity, and generate film stability and poor water resistance, film to substrate
Spreadability it is poor；Pure solvent coating improves the problem of the spreadability difference of water paint, while levelability also increases, but
Pure solvent coating would generally use toluene or dimethylbenzene as solvent, and this coating will be slow in use distributes toluene
Or dimethylbenzene, and toluene and dimethylbenzene can all cause certain injury to the health of people；Powdery paints and high solid apply
The production process of material is more complex, and storing process is more demanding, more difficult for the upper powder in corner area, and paint film defect is difficult after solidification
To cover, and execution conditions are harsh.
With the continuous improvement of people's living standards, demand of the people to everyday environments is also higher and higher.Family's conduct
The most important recreating facility of people, comfort and health after fitting up receive people and widely pay close attention to.Usually interior dress
After repairing, room air can become unusual muddiness.Because house decoration is improper affect human health report it is innumerable.By
The ornament materials of various continuous release harmful chemicals is excessively used when fitting up to interior in people, in addition indoor
Ventilation condition is bad, and people lives in this environment for a long time, and body will gradually appear various abnormal symptoms, and serious person is even
Threat to life.In addition, water paint slow drying speed, solvent reducible coatings taste weight when dry during coating application, with
Occur turning yellow using the extension wall of time, fade, coating can cause second-time burning to aggravate the intensity of a fire and rescue in the case of fire
The problems such as difficulty.Therefore, it is above-mentioned for solving that we have proposed a kind of conch meal biological environmental production interior wall coatings and preparation method thereof
Problem.
Summary of the invention
Harmful chemical is discharged based on coating existing for background technique, endangers serious and slow drying speed, solvent borne
The technical problem of coating taste weight when dry, the invention proposes a kind of conch meal biological environmental production interior wall coating and its preparation sides
Method.
A kind of conch meal biological environmental production interior wall coating proposed by the present invention, the raw material including following parts by weight: water-base epoxy
45~60 parts of resin, 45~60 parts of conch meal, 30~45 parts of rutile, 30~40 parts of superfine silicon dioxide, talcum powder 25~35
Part, 25~35 parts of acrylic emulsion, 15~20 parts of xanthan gum, 12~18 parts of glycerol, 10~16 parts of neopelex, sulphur
10~13 parts of sour ammonium, 10~13 parts of ethoxy, 6~9 parts of ammonium polyphosphate, 5~8 parts of ethyl alcohol, 5~8 parts of dispersing agent, wetting agent 5~8
Part, 4~8 parts of suspending agent, 3~6 parts of preservative, 220~250 parts of water.
Preferably, the raw material including following parts by weight: 50~55 parts of aqueous epoxy resins, 50~55 parts of conch meal, golden red
35~40 parts of stone, 32~38 parts of superfine silicon dioxide, 28~33 parts of talcum powder, 28~33 parts of acrylic emulsion, xanthan gum 16~
18 parts, 14~16 parts of glycerol, 12~14 parts of neopelex, 11~12 parts of ichthyodin, 11~12 parts of ethoxy, poly- phosphorus
7~8 parts of sour ammonium, 6~7 parts of ethyl alcohol, 6~7 parts of dispersing agent, 6~7 parts of wetting agent, 5~7 parts of suspending agent, 4~5 parts of preservative, water
230~240 parts.
Preferably, the raw material including following parts by weight: 53 parts of aqueous epoxy resins, 53 parts of conch meal, 38 parts of rutile, surpass
35 parts of fine silica, 30 parts of talcum powder, 30 parts of acrylic emulsion, 17 parts of xanthan gum, 15 parts of glycerol, neopelex
13 parts, 11.5 parts of ichthyodin, 11.5 parts of ethoxy, 7.5 parts of ammonium polyphosphate, 6.5 parts of ethyl alcohol, 6.5 parts of dispersing agent, wetting agent 6.5
Part, 6 parts of suspending agent, 4.5 parts of preservative, 235 parts of water.
Preferably, the granularity of the superfine silicon dioxide is 400~1200 mesh.
Preferably, the weight part ratio of the aqueous epoxy resins and conch meal is 1:1.
Preferably, the degree of polymerization in the ammonium polyphosphate is 20~30.
The invention also provides a kind of preparation method of conch meal biological environmental production interior wall coating, preparation method includes following
Step:
S1: the aqueous epoxy resins of the above parts by weight and rutile are added sequentially in micronizer, are sufficiently crushed
Admixed finepowder A is obtained afterwards；
S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 60~70 DEG C, to 70%~80%
Admixed finepowder A fusing after, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring to admixed finepowder A and is dissolved in second
In alcohol, mixed liquid B is obtained；
S3: keeping the temperature-resistant of kneading machine, and conch meal, the talcum powder, third of corresponding parts by weight are added into mixed liquid B
Olefin(e) acid lotion, neopelex and ethoxy are kneaded 8~11min to get mixed liquor C；
S4: taking the ichthyodin of corresponding parts by weight and ammonium polyphosphate to be placed in reactor, and adds water while stirring, to ichthyodin
It is all dissolved with ammonium polyphosphate, is further continued for 10~20min of stirring to get mixed liquor D, takes the xanthan gum and glycerol of corresponding parts by weight
It is mixed with the water of surplus, until be uniformly mixed to get mixed liquor E, it is spare；
S5: into mixed liquor C be added mixed liquor D, stir 20~30min after add dispersing agent, wetting agent, suspending agent,
Preservative, continues redisperse superfine silicon dioxide after 10~20min of stirring, adds after mixing to superfine silicon dioxide mixed
Liquid E is closed, 20~35min is stirred with the speed of 90~120r/min, is uniformly mixed and is applied up to conch meal biological environmental production interior wall
Material.
Preferably, in the S1, aqueous epoxy resins and rutile smash it through 260~320 meshes.
Preferably, in the S2, admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 62~68 DEG C,
After 72%~78% admixed finepowder A fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, it is micro- to mixing to continue stirring
Powder A is dissolved in ethyl alcohol, obtains mixed liquid B.
Preferably, in the S4, the accounting of the water and the water for preparing mixed liquor E that prepare mixed liquor D is 40%:60%.
Compared with prior art, the beneficial effects of the present invention are:
1, the characteristic dissolved each other by second alcohol and water makes each component in composition be uniformly mixed in coating and easily wave when in use
Hair, accelerates the rate of drying of coating, and using cheap and easy to get and superior performance aqueous epoxy resins and rutile as base-material, pass through
The workability that neopelex improves coating is added, ichthyodin, being used in compounding for ammonium polyphosphate significantly improve coating
The superfine silicon dioxide that flame retardant property large specific surface area at addition, is easily dispersed, when coating uses, superfine silicon dioxide is evenly dispersed
Film is protected in film coated surface, significantly improves the shock resistance of film；
2, safe and non-toxic and environmental-friendly by using conch meal as raw material, while xanthan gum and glycerol being added in coating
Protective film can be formed in film coated surface while guaranteeing coating viscosity, by ichthyodin, polyphosphoric acid with flame retardant property
Fixed ammonium is not easy to be lost in coating surface, increases the utilization rate of fire retardant, effectively improves the use quality of interior wall coating.
The present invention has rational design, and preparation process is simple, and each raw material is uniformly mixed, and preparation process is pollution-free, production efficiency
Height, it is environmental-friendly, it is worthy to be popularized.
Specific embodiment
Combined with specific embodiments below the present invention is made further to explain.
Embodiment one
The present embodiment proposes a kind of conch meal biological environmental production interior wall coating, the raw material including following parts by weight: aqueous ring
45 parts of oxygen resin, 45 parts of conch meal, 30 parts of rutile, 30 parts of superfine silicon dioxide, 25 parts of talcum powder, 25 parts of acrylic emulsion,
15 parts of xanthan gum, 12 parts of glycerol, 10 parts of neopelex, 10 parts of ichthyodin, 10 parts of ethoxy, 6 parts of ammonium polyphosphate, second
5 parts of alcohol, 5 parts of dispersing agent, 5 parts of wetting agent, 4 parts of suspending agent, 3 parts of preservative, 220 parts of water；
Preparation method includes the following steps:
S1: the aqueous epoxy resins of the above parts by weight and rutile are added sequentially in micronizer, are sufficiently crushed
260 meshes are crossed afterwards, obtain admixed finepowder A；
S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 60 DEG C, to 70% admixed finepowder A
After fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring and is dissolved in ethyl alcohol to admixed finepowder A, must be mixed
Liquid B；
S3: keeping the temperature-resistant of kneading machine, and conch meal, the talcum powder, third of corresponding parts by weight are added into mixed liquid B
Olefin(e) acid lotion, neopelex and ethoxy are kneaded 8min to get mixed liquor C；
S4: taking the ichthyodin of corresponding parts by weight and ammonium polyphosphate to be placed in reactor, and adds water while stirring, to ichthyodin
All dissolved with ammonium polyphosphate, be further continued for stirring 10min to get mixed liquor D, take corresponding parts by weight xanthan gum and glycerol with it is remaining
The water of amount is mixed, until be uniformly mixed to get mixed liquor E, it is spare, wherein preparing the water of mixed liquor D and preparing mixed liquor E
Water accounting be 40%:60%；
S5: mixed liquor D being added into mixed liquor C, adds dispersing agent, wetting agent, suspending agent, anti-corrosion after stirring 20min
Agent continues redisperse superfine silicon dioxide after stirring 10min, adds mixed liquor E after mixing to superfine silicon dioxide, with
The speed of 90r/min stirs 20min, is uniformly mixed up to conch meal biological environmental production interior wall coating.
Embodiment two
The present embodiment proposes a kind of conch meal biological environmental production interior wall coating, the raw material including following parts by weight: aqueous ring
50 parts of oxygen resin, 50 parts of conch meal, 35 parts of rutile, 33 parts of superfine silicon dioxide, 28 parts of talcum powder, 28 parts of acrylic emulsion,
17 parts of xanthan gum, 14 parts of glycerol, 12 parts of neopelex, 11 parts of ichthyodin, 11 parts of ethoxy, 7 parts of ammonium polyphosphate, second
6 parts of alcohol, 6 parts of dispersing agent, 6 parts of wetting agent, 5 parts of suspending agent, 4 parts of preservative, 230 parts of water；
Preparation method includes the following steps:
S1: the aqueous epoxy resins of the above parts by weight and rutile are added sequentially in micronizer, are sufficiently crushed
280 meshes are crossed afterwards, obtain admixed finepowder A；
S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 63 DEG C, to 73% admixed finepowder A
After fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring and is dissolved in ethyl alcohol to admixed finepowder A, must be mixed
Liquid B；
S3: keeping the temperature-resistant of kneading machine, and conch meal, the talcum powder, third of corresponding parts by weight are added into mixed liquid B
Olefin(e) acid lotion, neopelex and ethoxy are kneaded 9min to get mixed liquor C；
S4: taking the ichthyodin of corresponding parts by weight and ammonium polyphosphate to be placed in reactor, and adds water while stirring, to ichthyodin
All dissolved with ammonium polyphosphate, be further continued for stirring 13min to get mixed liquor D, take corresponding parts by weight xanthan gum and glycerol with it is remaining
The water of amount is mixed, until be uniformly mixed to get mixed liquor E, it is spare, wherein preparing the water of mixed liquor D and preparing mixed liquor E
Water accounting be 40%:60%；
S5: mixed liquor D being added into mixed liquor C, adds dispersing agent, wetting agent, suspending agent, anti-corrosion after stirring 23min
Agent continues redisperse superfine silicon dioxide after stirring 13min, adds mixed liquor E after mixing to superfine silicon dioxide, with
The speed of 100r/min stirs 25min, is uniformly mixed up to conch meal biological environmental production interior wall coating.
Embodiment three
The present embodiment proposes a kind of conch meal biological environmental production interior wall coating, the raw material including following parts by weight: aqueous ring
55 parts of oxygen resin, 55 parts of conch meal, 40 parts of rutile, 37 parts of superfine silicon dioxide, 32 parts of talcum powder, 32 parts of acrylic emulsion,
19 parts of xanthan gum, 16 parts of glycerol, 14 parts of neopelex, 12 parts of ichthyodin, 12 parts of ethoxy, 8 parts of ammonium polyphosphate, second
7 parts of alcohol, 7 parts of dispersing agent, 7 parts of wetting agent, 7 parts of suspending agent, 5 parts of preservative, 240 parts of water；
Preparation method includes the following steps:
S1: the aqueous epoxy resins of the above parts by weight and rutile are added sequentially in micronizer, are sufficiently crushed
300 meshes are crossed afterwards, obtain admixed finepowder A；
S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 67 DEG C, to 77% admixed finepowder A
After fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring and is dissolved in ethyl alcohol to admixed finepowder A, must be mixed
Liquid B；
S3: keeping the temperature-resistant of kneading machine, and conch meal, the talcum powder, third of corresponding parts by weight are added into mixed liquid B
Olefin(e) acid lotion, neopelex and ethoxy are kneaded 10min to get mixed liquor C；
S4: taking the ichthyodin of corresponding parts by weight and ammonium polyphosphate to be placed in reactor, and adds water while stirring, to ichthyodin
All dissolved with ammonium polyphosphate, be further continued for stirring 17min to get mixed liquor D, take corresponding parts by weight xanthan gum and glycerol with it is remaining
The water of amount is mixed, until be uniformly mixed to get mixed liquor E, it is spare, wherein preparing the water of mixed liquor D and preparing mixed liquor E
Water accounting be 40%:60%；
S5: mixed liquor D being added into mixed liquor C, adds dispersing agent, wetting agent, suspending agent, anti-corrosion after stirring 27min
Agent continues redisperse superfine silicon dioxide after stirring 17min, adds mixed liquor E after mixing to superfine silicon dioxide, with
The speed of 110r/min stirs 30min, is uniformly mixed up to conch meal biological environmental production interior wall coating.
Embodiment three
The present embodiment proposes a kind of conch meal biological environmental production interior wall coating, the raw material including following parts by weight: aqueous ring
60 parts of oxygen resin, 60 parts of conch meal, 45 parts of rutile, 40 parts of superfine silicon dioxide, 35 parts of talcum powder, 35 parts of acrylic emulsion,
20 parts of xanthan gum, 18 parts of glycerol, 16 parts of neopelex, 13 parts of ichthyodin, 13 parts of ethoxy, 9 parts of ammonium polyphosphate, second
8 parts of alcohol, 8 parts of dispersing agent, 8 parts of wetting agent, 8 parts of suspending agent, 6 parts of preservative, 250 parts of water；
Preparation method includes the following steps:
S1: the aqueous epoxy resins of the above parts by weight and rutile are added sequentially in micronizer, are sufficiently crushed
320 meshes are crossed afterwards, obtain admixed finepowder A；
S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 70 DEG C, to 80% admixed finepowder A
After fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring and is dissolved in ethyl alcohol to admixed finepowder A, must be mixed
Liquid B；
S3: keeping the temperature-resistant of kneading machine, and conch meal, the talcum powder, third of corresponding parts by weight are added into mixed liquid B
Olefin(e) acid lotion, neopelex and ethoxy are kneaded 11min to get mixed liquor C；
S4: taking the ichthyodin of corresponding parts by weight and ammonium polyphosphate to be placed in reactor, and adds water while stirring, to ichthyodin
All dissolved with ammonium polyphosphate, be further continued for stirring 20min to get mixed liquor D, take corresponding parts by weight xanthan gum and glycerol with it is remaining
The water of amount is mixed, until be uniformly mixed to get mixed liquor E, it is spare, wherein preparing the water of mixed liquor D and preparing mixed liquor E
Water accounting be 40%:60%；
S5: mixed liquor D being added into mixed liquor C, adds dispersing agent, wetting agent, suspending agent, anti-corrosion after stirring 30min
Agent continues redisperse superfine silicon dioxide after stirring 20min, adds mixed liquor E after mixing to superfine silicon dioxide, with
The speed of 120r/min stirs 35min, is uniformly mixed up to conch meal biological environmental production interior wall coating.
Performance detection is carried out to conch meal biological environmental production interior wall coating prepared by embodiment one~tetra-, testing result is as follows:
Testing result shows that the flame retardant rating of coating prepared by embodiment one~tetra- can reach A grades, shows its fire-retardant effect
Fruit is good, and surface drying and does solid work that speed is fast, further demonstrates that organic solvent ethyl alcohol can accelerate the rate of drying of coating in coating, into
And the construction efficiency of coating is improved, shorten construction period.
After carrying out coating surface and doing solid work test, the corresponding coating of Example one~tetra- carries out dissolvent residual inspection respectively
It surveys, finds in every 100g sample, ethyl alcohol obtains residual quantity in 0.05mg hereinafter, showing that organic solvent ethyl alcohol is after use in coating
It is volatile, and do not cause harm to the human body.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of conch meal biological environmental production interior wall coating, which is characterized in that the raw material including following parts by weight: aqueous epoxy resins
45~60 parts, 45~60 parts of conch meal, 30~45 parts of rutile, 30~40 parts of superfine silicon dioxide, 25~35 parts of talcum powder, third
25~35 parts of olefin(e) acid lotion, 15~20 parts of xanthan gum, 12~18 parts of glycerol, 10~16 parts of neopelex, ichthyodin
10~13 parts, 10~13 parts of ethoxy, 6~9 parts of ammonium polyphosphate, 5~8 parts of ethyl alcohol, 5~8 parts of dispersing agent, 5~8 parts of wetting agent,
4~8 parts of suspending agent, 3~6 parts of preservative, 220~250 parts of water.
2. a kind of conch meal biological environmental production interior wall coating according to claim 1, which is characterized in that including following parts by weight
Raw material: 50~55 parts of aqueous epoxy resins, 50~55 parts of conch meal, 35~40 parts of rutile, superfine silicon dioxide 32~38
Part, 28~33 parts of talcum powder, 28~33 parts of acrylic emulsion, 16~18 parts of xanthan gum, 14~16 parts of glycerol, detergent alkylate sulphur
12~14 parts of sour sodium, 11~12 parts of ichthyodin, 11~12 parts of ethoxy, 7~8 parts of ammonium polyphosphate, 6~7 parts of ethyl alcohol, dispersing agent 6
~7 parts, 6~7 parts of wetting agent, 5~7 parts of suspending agent, 4~5 parts of preservative, 230~240 parts of water.
3. a kind of conch meal biological environmental production interior wall coating according to claim 1, which is characterized in that including following parts by weight
Raw material: 53 parts of aqueous epoxy resins, 53 parts of conch meal, 38 parts of rutile, 35 parts of superfine silicon dioxide, 30 parts of talcum powder, third
30 parts of olefin(e) acid lotion, 17 parts of xanthan gum, 15 parts of glycerol, 13 parts of neopelex, 11.5 parts of ichthyodin, ethoxy 11.5
Part, 7.5 parts of ammonium polyphosphate, 6.5 parts of ethyl alcohol, 6.5 parts of dispersing agent, 6.5 parts of wetting agent, 6 parts of suspending agent, 4.5 parts of preservative, water
235 parts.
4. a kind of conch meal biological environmental production interior wall coating according to claim 1, which is characterized in that the ultra-fine titanium dioxide
The granularity of silicon is 400~1200 mesh.
5. a kind of conch meal biological environmental production interior wall coating according to claim 1, which is characterized in that the water-base epoxy tree
The weight part ratio of rouge and conch meal is 1:1.
6. a kind of conch meal biological environmental production interior wall coating according to claim 1, which is characterized in that in the ammonium polyphosphate
The degree of polymerization be 20~30.
7. a kind of preparation method of conch meal biological environmental production interior wall coating according to claim 1-6, feature
It is, preparation method includes the following steps:
S1: the aqueous epoxy resins of the above parts by weight and rutile are added sequentially in micronizer, after sufficiently crushing
Admixed finepowder A；
S2: admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 60~70 DEG C, to 70%~80% it is mixed
After closing micro mist A fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring and is dissolved in ethyl alcohol to admixed finepowder A,
Obtain mixed liquid B；
S3: keeping the temperature-resistant of kneading machine, and the conch meal, talcum powder, acrylic acid of corresponding parts by weight are added into mixed liquid B
Lotion, neopelex and ethoxy are kneaded 8~11min to get mixed liquor C；
S4: taking the ichthyodin of corresponding parts by weight and ammonium polyphosphate to be placed in reactor, and adds water while stirring, to ichthyodin and gathers
Ammonium phosphate all dissolves, and is further continued for 10~20min of stirring to get mixed liquor D, take corresponding parts by weight xanthan gum and glycerol with it is remaining
The water of amount is mixed, until be uniformly mixed to get mixed liquor E, it is spare；
S5: mixed liquor D being added into mixed liquor C, adds dispersing agent, wetting agent, suspending agent, anti-corrosion after stirring 20~30min
Agent continues redisperse superfine silicon dioxide after 10~20min of stirring, adds mixed liquor after mixing to superfine silicon dioxide
E stirs 20~35min with the speed of 90~120r/min, is uniformly mixed up to conch meal biological environmental production interior wall coating.
8. a kind of preparation method of conch meal biological environmental production interior wall coating according to claim 7, which is characterized in that described
In S1, aqueous epoxy resins and rutile smash it through 260~320 meshes.
9. a kind of preparation method of conch meal biological environmental production interior wall coating according to claim 7, which is characterized in that described
In S2, admixed finepowder A is placed in kneading machine, raises simultaneously kneading machine temperature to 62~68 DEG C, to 72%~78% mixing
After micro mist A fusing, the ethyl alcohol of corresponding parts by weight is added into kneading machine, continues stirring and is dissolved in ethyl alcohol to admixed finepowder A, obtained
Mixed liquid B.
10. a kind of preparation method of conch meal biological environmental production interior wall coating according to claim 7, which is characterized in that institute
It states in S4, the accounting of the water and the water for preparing mixed liquor E that prepare mixed liquor D is 40%:60%.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6211262B1 (en) * | 1998-04-20 | 2001-04-03 | Spectra Group Limited, Inc. | Corrosion resistant, radiation curable coating |
| CN107201143A (en) * | 2017-06-27 | 2017-09-26 | 六安三创建筑材料有限公司 | A kind of interior wall environmental protection flame retardant coating and preparation method thereof |
-
2018
- 2018-08-09 CN CN201810904994.8A patent/CN109280458A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6211262B1 (en) * | 1998-04-20 | 2001-04-03 | Spectra Group Limited, Inc. | Corrosion resistant, radiation curable coating |
| CN107201143A (en) * | 2017-06-27 | 2017-09-26 | 六安三创建筑材料有限公司 | A kind of interior wall environmental protection flame retardant coating and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 惠民地区地方史志编纂委员会: "《惠民地区风物综览》", 31 October 1989, 山东友谊书社 * |
| 李子东等: "《实用胶粘剂原材料手册》", 31 July 1999, 国防工业出版社 * |
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