CN109275955B - Filter tip additive for increasing filtering capacity of cigarette filter tip and preparation method and application thereof - Google Patents

Filter tip additive for increasing filtering capacity of cigarette filter tip and preparation method and application thereof Download PDF

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Publication number
CN109275955B
CN109275955B CN201810907825.XA CN201810907825A CN109275955B CN 109275955 B CN109275955 B CN 109275955B CN 201810907825 A CN201810907825 A CN 201810907825A CN 109275955 B CN109275955 B CN 109275955B
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filter
additive
cigarette
filter tip
percent
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CN109275955A (en
Inventor
杜佳
许克静
韩路
席高磊
许佩
李明伟
郭华诚
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China Tobacco Henan Industrial Co Ltd
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China Tobacco Henan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/067Use of materials for tobacco smoke filters characterised by functional properties
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/16Use of materials for tobacco smoke filters of inorganic materials

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention relates to a filter tip additive for increasing the filtering capacity of a cigarette filter tip, which consists of the following raw materials in percentage by mass: 5 to 10 percent of carrageenan, 5 to 12 percent of xanthan gum, 10 to 20 percent of guar gum, 10 to 19 percent of sodium alginate, 20 to 30 percent of agar and 18 to 50 percent of active carbon. The invention is found by experiments that: the filter tip additive is added into a two-section filter tip or a three-section filter tip by 0.1-0.3 percent of the quality of the filter tip, so that the filtering effect on smoke can be enhanced, and the total particulate matter and tar content of cigarettes can be better reduced, thereby more effectively reducing tar and harm.

Description

Filter tip additive for increasing filtering capacity of cigarette filter tip and preparation method and application thereof
Technical Field
The invention belongs to the technical field of tobacco, and particularly relates to a filter tip additive for increasing the filtering capacity of a cigarette filter tip, and a preparation method and application thereof.
Background
In recent years, with the progress of tar and harm reduction of tobacco, research on tobacco filters has been continuously conducted. The filter tip is used as a direct and effective physical tar and harm reducing means, and part of particulate matters and tar generated by burning tobacco are filtered on the filter tip through filtration. In order to seek better filtering effect, the effects of further reducing tar and harm are achieved by increasing the length of the filter tip, adding an adsorbent into the filter tip and the like.
At present, the domestic cigarette industry mainly adopts single substances such as activated carbon and the like as cigarette filter tip additives, and the effect is common. For example, patent CN2015104215702 discloses a preparation method and application of an embedded activated carbon filter adsorption additive, which is obtained by pretreating activated carbon, colloidal solution and sodium stearate, and can effectively and selectively reduce the content of various components in cigarette smoke without bringing about the negative effect of active component migration, but the effect is general. In addition, the adsorption capacity of the conventional additive to the filter tip can not be changed along with the smoking of the cigarette, and the adsorption capacity can be reduced in some cases, but the filtering effect of the tobacco shreds is reduced along with the burning of the cigarette, and meanwhile, the enrichment of harmful substances can cause the relative increase of the harmful substances.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the filter tip additive for increasing the filtering capacity of the cigarette filter tip, and the filter tip additive can better reduce the contents of total particulate matters and tar in cigarettes, thereby more effectively reducing tar and harm.
The invention also provides a preparation method and application of the filter tip additive for increasing the filtering capacity of the cigarette filter tip.
In order to achieve the purpose, the invention adopts the following technical scheme:
a filter tip additive for increasing the filtering capacity of a cigarette filter tip is composed of the following raw materials in percentage by mass: 5 to 10 percent of carrageenan, 5 to 12 percent of xanthan gum, 10 to 20 percent of guar gum, 10 to 19 percent of sodium alginate, 20 to 30 percent of agar and 18 to 50 percent of active carbon.
A preparation method of the filter tip additive for increasing the filtering capacity of the cigarette filter tip specifically comprises the following steps: weighing the raw materials according to the proportion, fully and uniformly mixing to obtain the product, sealing, drying and storing in dark place.
The invention also provides application of the filter tip additive for increasing the filtering capacity of the cigarette filter tip in cigarettes.
Specifically, the filter additive for increasing the filtering capacity of the cigarette filter can be added into a two-section filter or a three-section filter by 0.1-0.3% of the mass of the filter in the section.
Specifically, above-mentioned increase cigarette filter tip filter ability's application in the cigarette can add this filter tip additive at the interlude that is close to tobacco shred section or syllogic filter of two segmentation filters.
In the invention, the carrageenan has strong stability, and the dry powder is not easy to degrade after being placed for a long time. It is also stable in neutral and alkaline solutions and does not hydrolyze even when heated, and is commonly used in the food industry as a thickener, gelling agent, suspending agent, emulsifier, stabilizer, and the like. Xanthan gum is white or light yellow powder, has excellent thickening property, suspension property, emulsifying property and water solubility, and has good heat and acid-base stability, so that the xanthan gum is widely applied to various foods. Guar gum and its derivatives have better water solubility and exhibit very high viscosity at low mass fractions. Sodium alginate belongs to natural polysaccharide, and has the stability, solubility, viscosity and safety required by pharmaceutical preparation auxiliary materials. Sodium alginate is also used in some liquid drugs to increase viscosity and improve suspension of solids. Agar is a hydrophilic colloid extracted from red seaweed, and belongs to food additive. The activated carbon has the characteristics of large surface area, strong adsorption force, high purity, high filtration speed, stable quality, flocculation effect, filtration assisting effect and the like.
Compared with the prior art, the invention has the following beneficial effects:
1) the cigarette filter additive can better reduce the contents of total particulate matters and tar in cigarettes;
2) the additive of the cigarette filter tip of the invention shortens with the burning of the cigarette, the humidity in the filter tip becomes large, wherein the additive gradually increases the adsorption capacity to substances such as tar and the like after absorbing water, and more effectively plays a role in reducing tar and harm;
3) the filter additive can be directly added on the basis of a two-section filter or a three-section filter, and the adopted filter additive raw materials are nontoxic and pollution-free;
4) the filter tip additive has the advantages of simple preparation method, strong practicability and good application prospect.
Detailed Description
The technical solution of the present invention is further described in detail with reference to the following examples, but the scope of the present invention is not limited thereto.
The concrete implementation is carried out according to the conventional technology in the field by people who are not specially noted, and the raw materials are all common products which can be purchased.
Example 1
A filter tip additive for increasing the filtering capacity of a cigarette filter tip is composed of the following raw materials in percentage by mass: 10% of carrageenan, 12% of xanthan gum, 20% of guar gum, 10% of sodium alginate, 30% of agar and 18% of activated carbon.
The preparation method of the filter tip additive for increasing the filtering capacity of the cigarette filter tip specifically comprises the following steps: weighing the raw materials according to the proportion, fully and uniformly mixing to obtain the product, sealing, drying and storing in dark place.
Example 2
A filter tip additive for increasing the filtering capacity of a cigarette filter tip is composed of the following raw materials in percentage by mass: 7% of carrageenan, 9% of xanthan gum, 15% of guar gum, 19% of sodium alginate, 20% of agar and 30% of activated carbon.
A preparation method of the filter tip additive for increasing the filtering capacity of the cigarette filter tip specifically comprises the following steps: weighing the raw materials according to the proportion, fully and uniformly mixing to obtain the product, sealing, drying and storing in dark place.
Example 3
A filter tip additive for increasing the filtering capacity of a cigarette filter tip is composed of the following raw materials in percentage by mass: 5% of carrageenan, 5% of xanthan gum, 10% of guar gum, 10% of sodium alginate, 20% of agar and 50% of activated carbon.
A preparation method of the filter tip additive for increasing the filtering capacity of the cigarette filter tip specifically comprises the following steps: weighing the raw materials according to the proportion, fully and uniformly mixing to obtain the product, sealing, drying and storing in dark place.
Application test
The filter additive prepared in the embodiments 1 to 3 is added into a double-section filter according to the addition amount of 0.1 percent of the mass of the filter, cigarettes are made by adopting the conventional technology in the field, and the filter additive which is not added is used as a blank control group. The contents of the total particulate matters and the tar oil and the aroma concentration of the cigarette after the cigarette is burnt are detailed in the following table.
Figure DEST_PATH_IMAGE001
As can be seen from the above table: the filter tip additives with different proportions reduce the total particulate matters and tar of the cigarettes in different degrees after the cigarettes are combusted. Wherein, the total particulate matter of example 1 is reduced by 18 percent, the tar content is reduced by 8 percent, the total particulate matter of example 2 is reduced by 15 percent, the tar content is reduced by 8 percent, the total particulate matter of example 3 is reduced by 14 percent, and the tar content is reduced by 6 percent.

Claims (5)

1. A filter tip additive for increasing the filtering capacity of a cigarette filter tip is characterized by comprising the following raw materials in percentage by mass: 5 to 10 percent of carrageenan, 5 to 12 percent of xanthan gum, 10 to 20 percent of guar gum, 10 to 19 percent of sodium alginate, 20 to 30 percent of agar and 18 to 50 percent of active carbon;
this filter additive is applied to in the cigarette, and filter additive shortens along with a cigarette burning, the humidity grow in the filter tip, and wherein the additive absorbs water the back and to tar substance adsorption capacity grow gradually, and more effective tar reducing harm effect that plays.
2. The method for preparing the filter additive for increasing the filtering capacity of the cigarette filter according to claim 1, wherein the raw materials are weighed according to the proportion and uniformly mixed to obtain the filter additive.
3. The use of the filter additive for increasing the filtering ability of a cigarette filter according to claim 1 in a cigarette.
4. The use of a filter additive for increasing the filtration capacity of a cigarette filter according to claim 3 in a cigarette, wherein the filter additive is added to a two-segment filter or a three-segment filter at 0.1% to 0.3% of the mass of the filter.
5. Use of a filter additive for increasing the filtration capacity of a cigarette filter according to claim 3 in a cigarette, wherein the filter additive is added to the middle section of a two-section filter which is adjacent to the tobacco rod section or a three-section filter.
CN201810907825.XA 2018-08-10 2018-08-10 Filter tip additive for increasing filtering capacity of cigarette filter tip and preparation method and application thereof Active CN109275955B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810907825.XA CN109275955B (en) 2018-08-10 2018-08-10 Filter tip additive for increasing filtering capacity of cigarette filter tip and preparation method and application thereof

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Application Number Priority Date Filing Date Title
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CN109275955B true CN109275955B (en) 2021-07-20

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Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1682614A (en) * 2004-04-16 2005-10-19 中国科学院化学研究所 Sea weed polysaccharide and its derivatives used for cigarette filter tip additives
US20060090769A1 (en) * 2004-11-02 2006-05-04 Philip Morris Usa Inc. Temperature sensitive powder for enhanced flavor delivery in smoking articles
JP4959342B2 (en) * 2004-12-27 2012-06-20 株式会社ダイセル Tobacco filter material and tobacco filter
WO2006082748A1 (en) * 2005-02-02 2006-08-10 Daicel Chemical Industries, Ltd. Cigarette filter material and cigarette filter
CN101385574B (en) * 2008-10-22 2010-11-03 武汉理工大学 Composite environment protection cigarettes tar absorbent
CN102423132B (en) * 2011-08-15 2013-11-27 武汉力诚生物科技有限公司 Plant polysaccharide cigarette filter tip and preparation method thereof
GB2503644A (en) * 2012-05-03 2014-01-08 British American Tobacco Co Filter
CN103584281B (en) * 2013-11-25 2015-10-28 湖北中烟工业有限责任公司 A kind of cigarette filter and preparation method thereof
CN104095288A (en) * 2014-07-04 2014-10-15 中国烟草总公司郑州烟草研究院 Additive for preparing cigarette paper for paper filter tip
CN105266196B (en) * 2015-10-13 2019-06-14 江苏长泰药业有限公司 Acetone acid compounds are preparing the application in cigarette filter as the additive for reducing harmful substances from flue gases soakage
CN105996124A (en) * 2016-05-27 2016-10-12 阜阳卷烟材料厂 Cigarette filter stick with tar reduction and aroma enhancement performance

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