CN109275729A - A kind of preparation method for compounding grease and infant formula goat milk powder and the milk powder containing the compounding grease of simulation breast milk fatty acids - Google Patents

A kind of preparation method for compounding grease and infant formula goat milk powder and the milk powder containing the compounding grease of simulation breast milk fatty acids Download PDF

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CN109275729A
CN109275729A CN201811340961.1A CN201811340961A CN109275729A CN 109275729 A CN109275729 A CN 109275729A CN 201811340961 A CN201811340961 A CN 201811340961A CN 109275729 A CN109275729 A CN 109275729A
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milk powder
powder
compounding
fatty acids
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CN109275729B (en
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李晓东
张宏达
刘璐
冷友斌
赵铭琪
张宇
王立娜
蒋士龙
巩燕妮
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Northeast Agricultural University
Heilongjiang Feihe Dairy Co Ltd
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Northeast Agricultural University
Heilongjiang Feihe Dairy Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1522Inorganic additives, e.g. minerals, trace elements; Chlorination or fluoridation of milk; Organic salts or complexes of metals other than natrium or kalium; Calcium enrichment of milk
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1528Fatty acids; Mono- or diglycerides; Petroleum jelly; Paraffine; Phospholipids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/158Milk preparations; Milk powder or milk powder preparations containing additives containing vitamins or antibiotics
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/16Agglomerating or granulating milk powder; Making instant milk powder; Products obtained thereby
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Biophysics (AREA)
  • Inorganic Chemistry (AREA)
  • Dairy Products (AREA)

Abstract

In order to obtain more close to breast milk, the infant formula goat milk powder of trophic structure equilibrium, this invention describes the preparation methods of a kind of compounding grease of simulation breast milk fatty acids and infant formula goat milk powder and the milk powder containing the compounding grease, a kind of infant formula goat milk powder of the compounding grease containing simulation breast milk fatty acids, including following components: by weight, 150-490 parts of degreasing goat milk powder, 240-520 parts of desalination sheep whey powder, grease 200-270 parts of compounding, 1.8-2.2 parts of docosahexaenoic acid, 2.8-3.2 parts of arachidonic acid, 31-33 parts of oligofructose, 2-3.2 parts of vitamin premix, 1.3-1.6 parts of mineral substance premix, 2.5-3.5 parts of calcium carbonate, 0-1 parts of tricalcium phosphate, L-carnitine 0.2-0.5 Part, 0.4-0.5 parts of nucleotide, 0.04-0.08 parts of lutein.The present invention relates to baby formula milk powder fields, formula goat milk powder documented by the application has not only carried out breast milkization allotment to linolenic and linoleic, breast milkization allotment also has been carried out to several main fat the most abundant of content in breast milk, has guaranteed the full nutrition of infant.

Description

A kind of compounding grease for simulating breast milk fatty acids and the infant containing the compounding grease The preparation method of formula goat milk powder and the milk powder
Technical field
The present invention relates to baby formula milk powder fields, in particular to a kind of compounding oil for simulating breast milk fatty acids The preparation method of rouge and infant formula goat milk powder and the milk powder containing the compounding grease.
Background technique
Breast milk is the important even whole nutriment sources of infant, and substitute of the formula milk as breast milk And complementary goods, it is also necessary to be able to satisfy various nutriments required for infant growth.With dairy science research Deeply and Dairy Production technology development, the baby formula milk powder in China have evolved to emphasis milk powder surround and watch it is nutrition-balanced 4th from generation to generation, pursues nutrition fining proportion, makes every effort to be more nearly female composition of milk and function, make milk powder fed infant more The growth of health.
The ratio between sheep cream, cow's milk, the casein of human milk three and lactalbumin be substantially --- sheep cream (65:35), cow's milk (80:20), human milk (60:40).Compared to current most widely used cow's milk and milk powder, albumen composition is more nearly people in sheep cream Cream, and α s2- casein is very low, is easier to be absorbed and be not easy to cause the allergic reaction of infant, can effectively reduce infant The generation of diarrhea;Meanwhile the total amount of 10 kinds of main vitamin contained by every 100 grams of sheep cream is 780 micrograms.The dimension of itself is raw Plain A, vitamin B1, vitamin B2, vitamin C, pantothenic acid and niacin content can meet the growth needs of baby.
In addition, the fatty acid particularly important for infant growth, although the fatty acid ratio of components cow's milk of sheep cream is more The fatty acid of adjunction person of modern times's cream forms, and Short-Chain Fatty Acids content is up to 20%, and contains sufficient linoleic acid, arachidonic Acid, but there are still certain differences with human milk fat acid composition, it is still necessary to it is adjusted using compounding grease.There are also research tables Bright, n-3 system and n-6 system polyunsaturated fatty acid proportional imbalance in infants, are to lead to infant's obesity, hypoimmunity, intelligence The main reason for many chronic diseases such as power and the low, anaphylactia of Snazzi sensitivity are high-incidence.In addition, breast milk fatty acids carbochain Length is to influence an important factor for baby digests and assimilates, and medium chain fatty acid (MCFA) has important in newborn and infant nursing Nutrition and immunization, and be easier to be digested absorption.
Through calculating, MCFA content is 5.4% in mature breast milk, wherein myristic acid (C14:0) content highest.Mature breast milk Middle long chain fatty acids (LCFA) content is about 33.7%, and in fact LCFA content does not have the difference of conspicuousness in entire lactation period, It is palmitinic acid (C16:0) that wherein content is the most abundant, is 22.08%, followed by stearic acid (C18:0), reaches in mature cream Up to 5.38%.In addition, according to we detect as a result, it has been found that, in breast milk the highest five kinds of fatty acid of content be respectively oil Acid, linoleic acid, palmitinic acid, stearic acid and myristic acid, content is respectively 31.17%, 22.57%, 22.08%, 5.38%, 4.58%, and this five kinds of content of fatty acid are 20.79%, 4.43%, 19.08%, 8.45%, 9.03% in sheep cream, with breast milk There is some difference, and the content of alpha-linolenic acid is also much higher than sheep cream (human milk 1.66%, sheep cream 0.63%) in breast milk.
And formula milk majority on the market is all adjusted just for linoleic acid and alpha-linolenic acid at present, to other rouge The content concern of fat acid is seldom.But in fact, the content of other fatty acid to the healthy growth of infant be also have it is important Meaning.Oleic acid is the most abundant fatty acid of content in most representational and breast milk in ω -9 class unsaturated fatty acid, The diseases such as its and apoplexy cardiovascular to prevention play an important role, and can promote the development of infant immunisation system, can be with It cooperates with ω -3 class unsaturated fatty acid to improve human body lipid metabolism, reduces the deposition of cholesterol;Linoleic acid as essential fatty acid, The synthesis that phosphatide is participated in human body, is histiocytic constituent, especially important to cytoplasma membrane and structure of mitochondria, tool There is reduction cholesterol, the effect of atherosclerosis is arachidonic precursor substance;Although palmitinic acid is infant One of important fatty acid needed for growth and development, but containing for palmitinic acid is seldom paid close attention to when current formula milk allotment on the market Amount, palmitic acid content is generally higher, easily leads to the generation of baby's constipation;And myristic acid and serum cholesterol levels are in significant Positive correlation, be to lead to fat and cardiovascular and cerebrovascular disease one of the major reasons, formula milk suitably reduces wherein meat when deploying The content of myristic acid is close to breast milk, has positive effect to the development of infant's cardiovascular and cerebrovascular.
Inventor is in " the allotment research of fatty breast milk in babies ' formula milk powder " (Li Xiaodong, Chinese dairy products work before Industry, the 20th phase of volume 38 in 2010) research in show coconut oil, palm oil, sunflower seed oil, soybean oil, Purple Perilla Seed Oil in baby Proportion in formula milk is respectively 13.6%, and 50%, 14%, 21%, 1.4% when obtains preferable simulation effect, but does not have Attempt the effect with sheep milk fat cooperation.Jiang Dongmei etc. is in " research of Novel baby prescription emulsifiable powder fatty acid breast milkization " (Chinese dairy products Industry, the 1st phase of volume 45 in 2017) the result shows that addition soybean oil 6.0%, corn oil 7.0%, the compounding of palm oil 1.20% Oil also can get preferable breast milk degree.
Other people also have corresponding research before, such as CN103053694A discloses a kind of infant's milk for simulating breast milk composition Powder, Structure grease OPO selection palm oil, sunflower oil, rapeseed oil and soybean oil are made according to the ratio, but its technology solved is asked Topic is only so that milk powder overall ratio is close to breast milk, it is easier to be digested absorption, but be not concerned with the fatty acid in final products It is not selection or the source for focusing on fatty acid therein whether close to breast milk yet.CN105746728A discloses one kind Baby formula milk powder and its preparation of breast milk are simulated, the source of the fatty acid in milk powder is also 5 vegetable oils, and is added OPO structured lipid, but fat mimetic situation in milk powder is had not focused on, it is providing nor sheep milk powder.CN108157533A is public What is opened is a kind of people's milk fat analogue and baby formula lotion and preparation method thereof, and people's milk fat analogue uses lard, oil tea Seed oil, soybean oil and coconut oil are constituted, although also close to human milk fat, lard is not actually to be suitable for infant Best oil source.
In view of the above cause, the infant formula milk of simulation breast milk fatty acids proportion is invented using sheep milk fat combination vegetable oil Powder is of great significance.
Summary of the invention
An object of the present invention is to provide a kind of compounding grease of compositional modeling breast milk fatty acids composition, is added to and matches After in square goat milk powder the fatty acid of formula goat milk powder can form and be more nearly breast milk, make oily in infant formula goat milk powder This six kinds of fatty acid groups of acid, linoleic acid, alpha-linolenic acid, palmitinic acid, stearic acid and myristic acid are realized related to breast milk simultaneously Coefficient is up to 0.997.
The second object of the present invention is to provide a kind of fatty acid composition more close to breast milk, trophic structure is balanced, mouthfeel is good Good infant formula goat milk powder.
It is more good close to breast milk, trophic structure equilibrium, mouthfeel that the third object of the present invention is to provide a kind of fatty acid composition The preparation method of good infant formula goat milk powder, this method preparation is simple, is suitable for industrialized production.
To achieve the above object, the technical solution adopted by the present invention is as follows:
A kind of compounding grease for simulating breast milk fatty acids, the compounding grease be following components it is mixed by weight percentage and At: sheep milk fat 15-17.5%, linseed oil 3.5-4.5%, soybean oil 1-1.5%, sunflower oil 30-35%, palm oil 25- 30%, coconut oil 16-18%.
A kind of infant formula goat milk powder of the compounding grease containing simulation breast milk fatty acids, including following components: by weight Measure part meter, 150-490 parts of degreasing goat milk powder, 240-520 parts of desalination sheep whey powder, compounding grease 200-270 parts, 22 carbon six 1.8-2.2 parts of olefin(e) acid, 2.8-3.2 parts of arachidonic acid, 31-33 parts of oligofructose, 2-3.2 parts of vitamin premix, minerals 1.3-1.6 parts of premix, 2.5-3.5 parts of calcium carbonate, 0-1 parts of tricalcium phosphate, 0.2-0.5 parts of L-carnitine, nucleotide 0.4-0.5 Part, 0.04-0.08 parts of lutein.
Preferably, the vitamin premix is formed by following components and weight percent mixture: ascorbic acid 51%- 57%, dl- α-D-α-tocopherol acetate 5%-7%, cigarette phthalein amine 4%-5%, D-VB5 calcium 1%-2%, thiamine hydrochloride 1%- 2.5%, puridoxine hydrochloride 0.5%-1.5%, axerophtholum aceticum 0.6%-1%, folic acid 0.1%-0.2%, phytondione 0.03%-0.07%, biotin 0.005%-0.01%, Vitamin D3 0.0008%-0.0012%, Dobetin 0.0008%- 0.0012%, inositol 28%-32%.
Preferably, the mineral substance premix is formed by following components and weight percent mixture: calcium carbonate 33-36%, Calcium chloride 17-20%, sodium citrate 17%-20%, potassium citrate 15-17%, magnesium chloride 7-11%, ferrous sulfate 1-2%, sulphur Sour zinc 0.3%-0.6%, copper sulphate 0.05%-0.15%, manganese sulfate 0.02%-0.03%, sodium selenite 0.001%- 0.003%, potassium iodide 0.01%-0.03%.
A kind of preparation method of the infant formula goat milk powder of the compounding grease containing simulation breast milk fatty acids, including it is following Step:
Step 1: premix adds the degreasing goat milk powder of proportional quantity, desalination sheep whey powder, the compounding pre- hot mixing of grease water-soluble Solution mixes, and obtains mixed liquor;
Step 2: mixed liquor made from step 1 is carried out in homogenizer homogeneous, obtains mixed liquor by homogeneous;
Step 3: sterilization sterilizes the mixed liquor after step 2 homogeneous in chip sterilizer;
Step 4: concentration, the mixed liquor after step 3 is sterilized are concentrated in evaporator, obtain concentration mixed liquor;
Step 5: re-pasteurization, the concentration mixed liquor that step 4 is obtained carry out re-pasteurization in tubular type sterilizer;
Step 6: the concentration mixed liquor after re-pasteurization is carried out second homogenate by second homogenate;
Step 7: it is dry, the concentration mixed liquor after second homogenate is sent into spray drying tower and is spray-dried, obtains the One mixed powder;
Step 8: the first mixing powder by fluidized bed after spray drying is carried out two-stage drying, obtains second by two-stage drying Mixed powder;
Step 9: it is dry-mixed, by the oligofructose of proportional quantity, vitamin premix, mineral substance premix, calcium carbonate, phosphoric acid After tricalcium, L-carnitine, nucleotide, lutein, docosahexaenoic acid, arachidonic acid raw material premix, with the second mixed powder It is mixed in dry-mixed machine, obtained third mixed powder is the infant formula goat milk powder.
Preferably, in step 1, the temperature of the pre- hot mixing is 45-55 DEG C.
Preferably, in step 2 and step 6, the homogenizing temperature is 45-55 DEG C, and homogenization pressure is 15- 20Mpa。
Preferably, in step 3, the sterilization temperature is 110-115 DEG C, sterilizing time 4-8s.
Preferably, in step 4, the thickening temperature are as follows: 50-60 DEG C.
Preferably, in step 5, the sterilization temperature is 70-75 DEG C, sterilizing time 30-90s.
The beneficial effect of the present invention compared with the existing technology is: the present invention creatively adopts on the basis of early-stage study The inventive concept mutually assembled with sheep milk fat with particular types vegetable oil provides one kind in conjunction with the difference of sheep milk fat and human milk rouge It is good simulation breast milk fatty acids composition specific compounding grease, i.e. sheep milk fat 15-17.5%, linseed oil 3.5-4.5%, Soybean oil 1-1.5%%, sunflower oil 30-35%, palm oil 25-30%, coconut oil 16-18%, compounding grease each component are tight Close fit forms organic whole.
Sheep milk fat is different from butter fat and lard, is rich in Short-Chain Fatty Acids abundant, this makes the group of its fatty acid At the digestion and absorption for being more conducive to infant with structure, on the other hand, Short-Chain Fatty Acids also have anti-cholesterol deposition, prevention The functions such as bowel dysfunction are also easier to play a role jointly with sheep milk powder.The formula goat milk powder is not only to linolenic acid and Asia Oleic acid carried out breast milkization allotment, also to several fatty acid, that is, oleic acid the most abundant of content in breast milk, palmitinic acid, stearic acid and Myristic acid has carried out breast milkization allotment;In addition to sufficient, balanced nutrition is provided for the infants growth and development phase, it can also improve Infant's lipid metabolism function reduces fat, constipation generation;Appropriateness reduces containing for palmitinic acid and myristic acid in milk powder Amount reduces baby's body fat deposits, ensures the healthy development of infant's cardiovascular and cerebrovascular and prevents baby fat;It has adjusted in milk powder The content of oleic acid, compared to the formula milk for only adjusting polyunsaturated fatty acid, the adjusting of ω -9 class unsaturated fatty acid not only may be used To promote the healthy development of infant immunisation system, performance its physiological function that linoleic acid, linolenic acid can also be promoted better, Promote digestion and absorption of the infant to lipid.It can make to be formulated after being added in formula goat milk powder using the grease that sheep cream compounds The fatty acid composition of goat milk powder is more nearly breast milk, is oleic acid, linoleic acid, alpha-linolenic acid, palmitinic acid, stearic acid and nutmeg This sour six kinds of fatty acid groups realize the infant formula goat milk powder with the related coefficient of breast milk up to 0.997 simultaneously.
Specific embodiment
Specific embodiment one
A kind of compounding grease for simulating breast milk fatty acids, the compounding grease be following components it is mixed by weight percentage and At: sheep milk fat 15-17.5%, linseed oil 3.5-4.5%, soybean oil 1-1.5%, sunflower oil 30-35%, palm oil 25- 30%, coconut oil 16-18%.
A kind of infant formula goat milk powder of the compounding grease containing simulation breast milk fatty acids, including following components: by weight Measure part meter, 150-490 parts of degreasing goat milk powder, 240-520 parts of desalination sheep whey powder, compounding grease 200-270 parts, 22 carbon six 1.8-2.2 parts of olefin(e) acid, 2.8-3.2 parts of arachidonic acid, 31-33 parts of oligofructose, 2-3.2 parts of vitamin premix, minerals 1.3-1.6 parts of premix, 2.5-3.5 parts of calcium carbonate, 0-1 parts of tricalcium phosphate, 0.2-0.5 parts of L-carnitine, nucleotide 0.4-0.5 Part, 0.04-0.08 parts of lutein.
Preferably, the vitamin premix is formed by following components and weight percent mixture: ascorbic acid 51%- 57%, dl- α-D-α-tocopherol acetate 5%-7%, cigarette phthalein amine 4%-5%, D-VB5 calcium 1%-2%, thiamine hydrochloride 1%- 2.5%, puridoxine hydrochloride 0.5%-1.5%, axerophtholum aceticum 0.6%-1%, folic acid 0.1%-0.2%, phytondione 0.03%-0.07%, biotin 0.005%-0.01%, Vitamin D3 0.0008%-0.0012%, Dobetin 0.0008%- 0.0012%, inositol 28%-32%.
Preferably, the mineral substance premix is formed by following components and weight percent mixture: calcium carbonate 33-36%, Calcium chloride 17-20%, sodium citrate 17%-20%, potassium citrate 15-17%, magnesium chloride 7-11%, ferrous sulfate 1-2%, sulphur Sour zinc 0.3%-0.6%, copper sulphate 0.05%-0.15%, manganese sulfate 0.02%-0.03%, sodium selenite 0.001%- 0.003%, potassium iodide 0.01%-0.03%.
A kind of preparation method of the infant formula goat milk powder of the compounding grease containing simulation breast milk fatty acids, including it is following Step:
Step 1: the degreasing goat milk powder of predetermined specific gravity, desalination sheep whey powder, the compounding pre- hot mixing of grease are added water by premix Dissolution mixes, and obtains mixed liquor, and the temperature of the pre- hot mixing is 45-55 DEG C;
Step 2: mixed liquor made from step 1 is carried out homogeneous by homogeneous in homogenizer, obtains mixed liquor, homogeneous temperature Degree is 45-55 DEG C, and homogenization pressure is 15-20Mpa;
Step 3: sterilization sterilizes the mixed liquor after step 2 homogeneous, sterilization temperature is in chip sterilizer 110-115 DEG C, sterilizing time 4-8s;
Step 4: concentration, the mixed liquor after step 3 is sterilized are concentrated in evaporator, obtain concentration mixed liquor, Thickening temperature is 50-60 DEG C;
Step 5: re-pasteurization, the concentration mixed liquor that step 4 is obtained carry out re-pasteurization in tubular type sterilizer, kill Bacterium temperature is 70-75 DEG C, sterilizing time 30-90s;
Step 6: the concentration mixed liquor after re-pasteurization is carried out second homogenate by second homogenate, and homogenizing temperature is 45- 55 DEG C, homogenization pressure is 15-20Mpa;
Step 7: it is dry, the concentration mixed liquor after second homogenate is sent into spray drying tower and is spray-dried, obtains the One mixed powder;
Step 8: the first mixing powder by fluidized bed after spray drying is carried out two-stage drying, obtains second by two-stage drying Mixed powder;
Step 9: it is dry-mixed, by oligofructose, vitamin premix, mineral substance premix, calcium carbonate, tricalcium phosphate, left-handed After carnitine, nucleotide, lutein, docosahexaenoic acid, arachidonic acid raw material premix, with the second mixed powder in dry-mixed machine It mixes, obtained third mixed powder is the infant formula goat milk powder.
Embodiment 1
A kind of compounding grease for simulating breast milk fatty acids, the compounding grease be following components it is mixed by weight percentage and At: sheep milk fat 16.7%, linseed oil 4.1%, soybean oil 1.2%, sunflower oil 32.8%, palm oil 27.9%, coconut oil 17.3%.
A kind of infant formula goat milk powder of the compounding grease containing above-mentioned simulation breast milk fatty acids, including following components: By weight, 180 parts of degreasing goat milk powder, 520 parts of desalination sheep whey powder, compounding 262 parts of grease, 2 parts of docosahexaenoic acid, 3 parts of arachidonic acid, 32 parts of oligofructose, 3.2 parts of vitamin premix, 1.6 parts of mineral substance premix, 2.5 parts of calcium carbonate, phosphorus 1 part of sour tricalcium, 0.2 part of L-carnitine, 0.42 part of nucleotide, 0.08 part of lutein.
Preferably, the vitamin premix is formed by following components and weight percent mixture: ascorbic acid 54%, Dl- α-D-α-tocopherol acetate 6%, cigarette phthalein amine 4.5%, D-VB5 calcium 1.5%, thiamine hydrochloride 2%, puridoxine hydrochloride 1%, acetic acid Vitamin A 0.8%, folic acid 0.14%, phytondione 0.05%, biotin 0.008%, Vitamin D3 0.001%, Dobetin 0.001%, inositol 30%.
Preferably, the mineral substance premix is formed by following components and weight percent mixture: calcium carbonate 34.9%, chlorine Change calcium 18.6%, sodium citrate 18.6%, potassium citrate 16.3%, magnesium chloride 9.3%, ferrous sulfate 1.6%, zinc sulfate 0.56%, copper sulphate 0.093%, manganese sulfate 0.025%, sodium selenite 0.002%, potassium iodide 0.02%.
A kind of preparation method of the infant formula goat milk powder of the above-mentioned compounding grease containing simulation breast milk fatty acids, including Following steps:
Step 1: premix adds the degreasing goat milk powder of said ratio amount, desalination sheep whey powder, the compounding pre- hot mixing of grease Water dissolution mixes, and obtains mixed liquor;Wherein the temperature of pre- hot mixing is 50 DEG C;
Step 2: mixed liquor made from step 1 is carried out in homogenizer homogeneous, obtains mixed liquor by homogeneous;Homogeneous temperature Degree is 50 DEG C, homogenization pressure 15Mpa;
Step 3: sterilization sterilizes the mixed liquor after step 2 homogeneous, sterilization temperature 115 in chip sterilizer DEG C, sterilizing time 6s;If you need to temporary, 0-1 DEG C of temperature of control be must not exceed 12 hours;
Step 4: concentration, the mixed liquor after step 3 is sterilized are concentrated in evaporator, obtain concentration mixed liquor; Wherein, thickening temperature control is at 55 DEG C;
Step 5: re-pasteurization, the concentration mixed liquor that step 4 is obtained carry out re-pasteurization in tubular type sterilizer, kill Bacterium temperature is 70 DEG C, sterilizing time 60s;
Step 6: the concentration mixed liquor after re-pasteurization was both carried out second homogenate, homogenizing temperature 50 by second homogenate DEG C, homogenization pressure 15Mpa;
Step 7: it is dry, the concentration mixed liquor after second homogenate is sent into spray drying tower and is spray-dried, obtains the One mixed powder;
Step 8: the first mixing powder by fluidized bed after spray drying is carried out two-stage drying, prevents milk powder by two-stage drying Agglomeration, obtains the second mixed powder;
Step 9: it is dry-mixed, by the oligofructose of proportional quantity, vitamin premix, mineral substance premix, calcium carbonate, phosphoric acid After tricalcium, L-carnitine, nucleotide, lutein, docosahexaenoic acid, arachidonic acid raw material premix, with the second mixed powder It is mixed in dry-mixed machine, obtained third mixed powder is the infant formula goat milk powder;Wherein vitamin premix, minerals Said ratio configuration is pressed in premix.
Embodiment 2
A kind of compounding grease for simulating breast milk fatty acids, the compounding grease be following components it is mixed by weight percentage and At: sheep milk fat 16.7%, linseed oil 4.1%, soybean oil 1.2%, sunflower oil 32.8%, palm oil 27.9%, coconut oil 17.3%.
A kind of infant formula goat milk powder of the compounding grease containing above-mentioned simulation breast milk fatty acids, including following components: By weight, 425 parts of degreasing goat milk powder, 325 parts of desalination sheep whey powder, compounding 205 parts of grease, 2 parts of docosahexaenoic acid, 3 parts of arachidonic acid, 32 parts of oligofructose, 3 parts of vitamin premix, 1.3 parts of mineral substance premix, 3 parts of calcium carbonate, left-handed meat 0.2 part of alkali, 0.46 part of nucleotide, 0.04 part of lutein.
Preferably, the vitamin premix is formed by following components and weight percent mixture: ascorbic acid 54%, Dl- α-D-α-tocopherol acetate 6%, cigarette phthalein amine 4.5%, D-VB5 calcium 1.5%, thiamine hydrochloride 2%, puridoxine hydrochloride 1%, acetic acid Vitamin A 0.8%, folic acid 0.14%, phytondione 0.05%, biotin 0.008%, Vitamin D3 0.001%, Dobetin 0.001%, inositol 30%.
Preferably, the mineral substance premix is formed by following components and weight percent mixture: calcium carbonate 34.9%, chlorine Change calcium 18.6%, sodium citrate 18.6%, potassium citrate 16.3%, magnesium chloride 9.3%, ferrous sulfate 1.6%, zinc sulfate 0.56%, copper sulphate 0.093%, manganese sulfate 0.025%, sodium selenite 0.002%, potassium iodide 0.02%.
A kind of preparation method of the infant formula goat milk powder of the above-mentioned compounding grease containing simulation breast milk fatty acids, including Following steps:
Step 1: premix adds the degreasing goat milk powder of said ratio amount, desalination sheep whey powder, the compounding pre- hot mixing of grease Water dissolution mixes, and obtains mixed liquor;Wherein the temperature of pre- hot mixing is 53 DEG C;
Step 2: mixed liquor made from step 1 is carried out in homogenizer homogeneous, obtains mixed liquor by homogeneous;Homogeneous temperature Degree is 53 DEG C, homogenization pressure 18Mpa;
Step 3: sterilization sterilizes the mixed liquor after step 2 homogeneous, sterilization temperature 113 in chip sterilizer DEG C, sterilizing time 5s;If you need to temporary, 0-1 DEG C of temperature of control be must not exceed 12 hours;
Step 4: concentration, the mixed liquor after step 3 is sterilized are concentrated in evaporator, obtain concentration mixed liquor; Wherein, thickening temperature control is at 58 DEG C;
Step 5: re-pasteurization, the concentration mixed liquor that step 4 is obtained carry out re-pasteurization in tubular type sterilizer, kill Bacterium temperature is 73 DEG C, sterilizing time 50s;
Step 6: the concentration mixed liquor after re-pasteurization was both carried out second homogenate, homogenizing temperature 53 by second homogenate DEG C, homogenization pressure 18Mpa;
Step 7: it is dry, the concentration mixed liquor after second homogenate is sent into spray drying tower and is spray-dried, obtains the One mixed powder;
Step 8: the first mixing powder by fluidized bed after spray drying is carried out two-stage drying, prevents milk powder by two-stage drying Agglomeration, obtains the second mixed powder;
Step 9: it is dry-mixed, by the oligofructose of proportional quantity, vitamin premix, mineral substance premix, calcium carbonate, left-handed After carnitine, nucleotide, lutein, docosahexaenoic acid, arachidonic acid raw material premix, with the second mixed powder in dry-mixed machine It mixes, obtained third mixed powder is the infant formula goat milk powder;Wherein vitamin premix, mineral substance premix are pressed Said ratio configuration.
Embodiment 3
A kind of compounding grease for simulating breast milk fatty acids, the compounding grease be following components it is mixed by weight percentage and At: sheep milk fat 16.7%, linseed oil 4.1%, soybean oil 1.2%, sunflower oil 32.8%, palm oil 27.9%, coconut oil 17.3%.
A kind of infant formula goat milk powder of the compounding grease containing above-mentioned simulation breast milk fatty acids, including following components: By weight, 485 parts of degreasing goat milk powder, 240 parts of desalination sheep whey powder, compounding 230 parts of grease, 2 parts of docosahexaenoic acid, 3 parts of arachidonic acid, 32 parts of oligofructose, 3 parts of vitamin premix, 1.3 parts of mineral substance premix, 3 parts of calcium carbonate, left-handed meat 0.2 part of alkali, 0.46 part of nucleotide, 0.04 part of lutein.
Preferably, the vitamin premix is formed by following components and weight percent mixture: ascorbic acid 54%, Dl- α-D-α-tocopherol acetate 6%, cigarette phthalein amine 4.5%, D-VB5 calcium 1.5%, thiamine hydrochloride 2%, puridoxine hydrochloride 1%, acetic acid Vitamin A 0.8%, folic acid 0.14%, phytondione 0.05%, biotin 0.008%, Vitamin D3 0.001%, Dobetin 0.001%, inositol 30%.
Preferably, the mineral substance premix is formed by following components and weight percent mixture: calcium carbonate 34.9%, chlorine Change calcium 18.6%, sodium citrate 18.6%, potassium citrate 16.3%, magnesium chloride 9.3%, ferrous sulfate 1.6%, zinc sulfate 0.56%, copper sulphate 0.093%, manganese sulfate 0.025%, sodium selenite 0.002%, potassium iodide 0.02%.
A kind of preparation method of the infant formula goat milk powder of the above-mentioned compounding grease containing simulation breast milk fatty acids, including Following steps:
Step 1: premix adds the degreasing goat milk powder of said ratio amount, desalination sheep whey powder, the compounding pre- hot mixing of grease Water dissolution mixes, and obtains mixed liquor;Wherein the temperature of pre- hot mixing is 45 DEG C;
Step 2: mixed liquor made from step 1 is carried out in homogenizer homogeneous, obtains mixed liquor by homogeneous;Homogeneous temperature Degree is 45 DEG C, homogenization pressure 20Mpa;
Step 3: sterilization sterilizes the mixed liquor after step 2 homogeneous, sterilization temperature 110 in chip sterilizer DEG C, sterilizing time 4s;If you need to temporary, 0-1 DEG C of temperature of control be must not exceed 12 hours;
Step 4: concentration, the mixed liquor after step 3 is sterilized are concentrated in evaporator, obtain concentration mixed liquor; Wherein, thickening temperature control is at 60 DEG C;
Step 5: re-pasteurization, the concentration mixed liquor that step 4 is obtained carry out re-pasteurization in tubular type sterilizer, kill Bacterium temperature is 75 DEG C, sterilizing time 90s;
Step 6: the concentration mixed liquor after re-pasteurization was both carried out second homogenate, homogenizing temperature 55 by second homogenate DEG C, homogenization pressure 20Mpa;
Step 7: it is dry, the concentration mixed liquor after second homogenate is sent into spray drying tower and is spray-dried, obtains the One mixed powder;
Step 8: the first mixing powder by fluidized bed after spray drying is carried out two-stage drying, prevents milk powder by two-stage drying Agglomeration, obtains the second mixed powder;
Step 9: it is dry-mixed, by the oligofructose of proportional quantity, vitamin premix, mineral substance premix, calcium carbonate, phosphoric acid After tricalcium, L-carnitine, nucleotide, lutein, docosahexaenoic acid, arachidonic acid raw material premix, with the second mixed powder It is mixed in dry-mixed machine, obtained third mixed powder is the infant formula goat milk powder;Wherein vitamin premix, minerals Said ratio configuration is pressed in premix.
Baby formula milk powder is divided into 3 stages mostly.It is formulated for baby's somatogenic need of different age group Scientific matching, to adapt to the needs of baby's growth and development.
0-6 months are a stage, are called babies ' formula milk powder.
6-12 months are the two-stage, are called larger babies ' formula milk powder.
12-36 months were three stages, were called baby formulas milk powder.
Goat milk powder made from the embodiment of the present invention 1 is mainly suitable for consumption by infants, goat milk powder made from embodiment 2,3 be suitble to compared with Big infants and young is edible.
It is compared experiment using gas chromatography-mass spectrography (GC-MS), the results are shown in Table 1, wherein lard group is embodiment 1 In sheep grease substituted using the lard of isodose, other conditions are constant.
The relative amount (% total fatty acids) of each fatty acid of table 1
Note: (1) there is significant difference between the different letters of a, b
Correlation analysis is carried out by SPSS software, it is found that fatty acid profile is distributed in breast milk fatty acids in embodiment 1 Relative coefficient is 0.989;This six kinds of fatty acid of oleic acid, linoleic acid, alpha-linolenic acid, palmitinic acid, stearic acid and myristic acid Relative coefficient is even more to have reached 0.997.
2 embodiment 1 of table and breast milk fatty acids Pearson (Pearson) related coefficient
Total fatty acids Selected six kinds of fatty acid
0.989 0.997
The result shows that the composition and ratio of 1 fatty acid of embodiment are more nearly breast milk.Sheep grease, meeting are substituted using lard Reduce the short-chain fat acid content in product, and cholesterol level increases, less effective, in research process, it was also found that no matter The dosage for how adjusting lard and other vegetable oil is also difficult to reach ideal effect, sheep milk fat in the formula milk with it is other Vegetable oil and other components have formed harmonious organic whole.
Embodiment product of the present invention is this six kinds of rouge of oleic acid, linoleic acid, alpha-linolenic acid, palmitinic acid, stearic acid and myristic acid Fat acid group realizes the infant formula goat milk powder with the related coefficient of breast milk up to 0.997 simultaneously.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with Modification, all should belong to covering scope of the invention.

Claims (10)

1. a kind of compounding grease for simulating breast milk fatty acids, it is characterised in that: the compounding grease is following components by weight hundred Point formed than mixture: sheep milk fat 15-17.5%, linseed oil 3.5-4.5%, soybean oil 1-1.5%, sunflower oil 30-35%, Palm oil 25-30%, coconut oil 16-18%.
2. a kind of infant formula goat milk powder of the compounding grease containing simulation breast milk fatty acids described in claim 1, special Sign is, including following components: by weight, 150-490 parts of degreasing goat milk powder, 240-520 parts of desalination sheep whey powder, compounding 200-270 parts of grease, 1.8-2.2 parts of docosahexaenoic acid, 2.8-3.2 parts of arachidonic acid, 31-33 parts of oligofructose, dimension Raw element 2-3.2 parts of premix, 1.3-1.6 parts of mineral substance premix, 2.5-3.5 parts of calcium carbonate, 0-1 parts of tricalcium phosphate, left-handed meat 0.2-0.5 parts of alkali, 0.4-0.5 parts of nucleotide, 0.04-0.08 parts of lutein.
3. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 2, It is characterized by: the vitamin premix is formed by following components and weight percent mixture: ascorbic acid 51-57%, dl- α-D-α-tocopherol acetate 5-7%, cigarette phthalein amine 4-5%, D-VB5 calcium 1-2%, thiamine hydrochloride 1-2.5%, puridoxine hydrochloride 0.5- 1.5%, axerophtholum aceticum 0.6-1%, folic acid 0.1-0.2%, phytondione 0.03-0.07%, biotin 0.005- 0.01%, Vitamin D3 0.0008-0.0012%, Dobetin 0.0008-0.0012%, inositol 28-32%.
4. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 2, It is characterized by: the mineral substance premix is formed by following components and weight percent mixture: calcium carbonate 33-36%, chlorination Calcium 17-20%, sodium citrate 17-20%, potassium citrate 15-17%, magnesium chloride 7-11%, ferrous sulfate 1-2%, zinc sulfate 0.3-0.6%, copper sulphate 0.05-0.15%, manganese sulfate 0.02-0.03%, sodium selenite 0.001-0.003%, potassium iodide 0.01-0.03%.
5. a kind of infant of the compounding grease containing simulation breast milk fatty acids described in claim 2-4 any claim matches The preparation method of square goat milk powder, which comprises the following steps:
Step 1: premix, by the degreasing goat milk powder of proportional quantity, desalination sheep whey powder, the compounding pre- hot mixing of grease, be dissolved in water, It mixes, obtains mixed liquor;
Step 2: mixed liquor made from step 1 is carried out in homogenizer homogeneous, obtains mixed liquor by homogeneous;
Step 3: sterilization sterilizes the mixed liquor after step 2 homogeneous in chip sterilizer;
Step 4: concentration, the mixed liquor after step 3 is sterilized are concentrated in evaporator, obtain concentration mixed liquor;
Step 5: re-pasteurization, the concentration mixed liquor that step 4 is obtained carry out re-pasteurization in tubular type sterilizer,;
Step 6: the concentration mixed liquor after re-pasteurization is carried out second homogenate by second homogenate;
Step 7: it is dry, the concentration mixed liquor after second homogenate is sent into spray drying tower and is spray-dried, it is mixed to obtain first Close powder;
Step 8: the first mixing powder by fluidized bed after spray drying is carried out two-stage drying, obtains the second mixing by two-stage drying Powder;
Step 9: it is dry-mixed, by the oligofructose of proportional quantity, vitamin premix, mineral substance premix, calcium carbonate, tricalcium phosphate, After L-carnitine, nucleotide, lutein, docosahexaenoic acid, arachidonic acid raw material premix, with the second mixed powder dry-mixed It is mixed in machine, obtained third mixed powder is the infant formula goat milk powder.
6. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 5 Preparation method, it is characterised in that: in step 1, the temperature of the pre- hot mixing is 45-55 DEG C.
7. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 5 Preparation method, it is characterised in that: in step 2 and step 6, the homogenizing temperature is 45-55 DEG C, and homogenization pressure is 15-20Mpa。
8. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 5 Preparation method, it is characterised in that: in step 3, the sterilization temperature is 110-115 DEG C, sterilizing time 4-8s.
9. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 5 Preparation method, it is characterised in that: in step 4, the thickening temperature are as follows: 50-60 DEG C.
10. a kind of infant formula goat milk powder of compounding grease containing simulation breast milk fatty acids according to claim 5 Preparation method, it is characterised in that: in step 5, the sterilization temperature be 70-75 DEG C, sterilizing time 30-90s.
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CN111758774A (en) * 2020-08-07 2020-10-13 西安百跃羊乳集团有限公司 Perilla frutescens formula goat milk powder and preparation method thereof
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CN112931628A (en) * 2021-03-26 2021-06-11 东北农业大学 Liposome simulating breast milk lipid structure, formula powder for premature infant and preparation method
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CN110742130A (en) * 2019-11-14 2020-02-04 东北农业大学 Infant formula goat milk powder added with liposome simulating breast milk fat structure and preparation method thereof
CN113115841A (en) * 2019-12-30 2021-07-16 丰益(上海)生物技术研发中心有限公司 Phospholipid-containing infant formula
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CN111838327B (en) * 2020-07-23 2022-09-06 海普诺凯营养品有限公司 Grease for milk powder base powder and preparation method thereof
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CN112931628B (en) * 2021-03-26 2022-02-15 东北农业大学 Liposome simulating breast milk lipid structure, formula powder for premature infant and preparation method
CN114208895A (en) * 2021-12-24 2022-03-22 光明乳业股份有限公司 Novel infant formula milk powder with optimized fat composition and preparation method thereof
CN116076578A (en) * 2023-03-22 2023-05-09 北大荒完达山乳业股份有限公司 Infant formula milk powder containing alpine ecological cow milk compound fat and preparation method thereof

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