CN109257928A - Organic material refining device - Google Patents
Organic material refining device Download PDFInfo
- Publication number
- CN109257928A CN109257928A CN201880000927.1A CN201880000927A CN109257928A CN 109257928 A CN109257928 A CN 109257928A CN 201880000927 A CN201880000927 A CN 201880000927A CN 109257928 A CN109257928 A CN 109257928A
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- Prior art keywords
- organic material
- board member
- cylinder
- sectional shape
- cross sectional
- Prior art date
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- 239000011368 organic material Substances 0.000 title claims abstract description 99
- 238000007670 refining Methods 0.000 title claims description 53
- 238000005452 bending Methods 0.000 claims description 67
- 238000000746 purification Methods 0.000 abstract description 12
- 230000002093 peripheral effect Effects 0.000 abstract description 8
- 239000000463 material Substances 0.000 description 23
- 238000002309 gasification Methods 0.000 description 22
- 238000000034 method Methods 0.000 description 16
- 239000012535 impurity Substances 0.000 description 11
- 238000010276 construction Methods 0.000 description 10
- 239000007789 gas Substances 0.000 description 9
- 239000010935 stainless steel Substances 0.000 description 9
- 229910001220 stainless steel Inorganic materials 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 8
- 238000004064 recycling Methods 0.000 description 8
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 2
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- 229910052581 Si3N4 Inorganic materials 0.000 description 2
- 239000004809 Teflon Substances 0.000 description 2
- 229920006362 Teflon® Polymers 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000012776 electronic material Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000006698 induction Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 2
- 230000003252 repetitive effect Effects 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 239000010937 tungsten Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910001928 zirconium oxide Inorganic materials 0.000 description 2
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- 229910001362 Ta alloys Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 239000007767 bonding agent Substances 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000010891 electric arc Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005401 electroluminescence Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000005297 pyrex Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000011218 segmentation Effects 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D7/00—Sublimation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D7/00—Sublimation
- B01D7/02—Crystallisation directly from the vapour phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
Abstract
An organic material purification device (1) is provided with: a cylinder (2) in which the vaporized organic material flows inside the cylinder (2), and the cylinder (2) includes a collection space (22) for collecting the organic material; and a first plate member (61) which is disposed inside the tubular body (2) in the collection section (22) and extends in the longitudinal direction of the tubular body (2). The first plate member (61) is integrally formed into a cross-sectional shape including a bent portion, and at least one end (611) of the cross-sectional shape of the first plate member (61) is in contact with the inner peripheral surface of the cylindrical body (2).
Description
Technical field
The present invention relates to the refining plants of organic material.
Background technique
In the past, as the refining methd of organic material, it is known to column chromatography, recrystallization, distillation, distillation etc..Here, especially
It is in the organic material for being used as electronic material, optical material, the impurity in material can cause big influence to performance.For example,
For the material of organic EL (Electroluminescence) element, impurity becomes carrier (electronics, hole)
Trap leads to delustring, so that the luminous intensity of organic EL element, luminous efficiency or durability be made to reduce.Therefore, it is proposed to
The improvement of the refining methd of various organic materials.
For example, describing following technology in patent document 1: in the trap of the organic material of captured gas shape,
The inside configuration of cylinder has the component in the axially extending face along cylinder, thus reduces exhaust resistance, and increase has simultaneously
The trapping area of machine material.According to such technology, organic material can be refined as high-purity, and also improve organic material simultaneously
The purification efficiency of material.
Citation
Patent document
Patent document 1: International Publication No. 2013/145833
Summary of the invention
Subject to be solved by the invention
Fig. 8, embodiment party shown in Fig. 9 in the technology documented by above-mentioned patent document 1, such as in patent document 1
Describe following content in formula: cylinder be formed to divide, additionally be able to using Screw to be installed on the rib of cylinder into
Luggage is torn open.Cylinder and rib are decomposed after refining step as a result, can easily recycle the organic material trapped on surface
Material.However, it is necessary to the process of decomposing cylinder and rib before the recycling of organic material and after recycling by cylinder and rib again
The process of assembling, technology documented by patent document 1 still has room for improvement in this regard.
In view of above content, it is an object of the present invention to provide in the trapping area that will be used to increase organic material
Component be configured at the inside of cylinder in the case where, the purification dress of the organic material of process relevant to the component can be simplified
It sets.
Solution for solving the problem
A viewpoint according to the present invention, provide a kind of refining plant of organic material, have: cylinder has gasified
Organic material the cylinder internal flow, and the cylinder include trap organic material trapping section；And first board member,
It is configured at the inside of cylinder in trapping section, and extends along the length direction of cylinder, the refining plant of the organic material
It is characterized in that, the first board member is formed integrally as the cross sectional shape comprising bending part, the cross sectional shape of the first board member
The inner circumferential face contact of at least one end and cylinder.
According to above-mentioned structure, in the refining plant of organic material, in the trapping area that will be used to increase organic material
Component be configured at the inside of cylinder in the case where, process relevant to the component can be simplified.
Detailed description of the invention
Fig. 1 is the brief horizontal cross of the refining plant of the organic material of first embodiment of the invention.
Fig. 2 is the I-I line cross-sectional view of refining plant shown in FIG. 1.
Fig. 3 is the work for indicating to take out board member from the inside for the cylinder that can divide in the first embodiment of the present invention
The exemplary figure of sequence.
Fig. 4 is the cross-sectional view of the refining plant of second embodiment of the present invention.
Fig. 5 is the cross-sectional view of the refining plant of third embodiment of the present invention.
Fig. 6 A is the inner cylinder of the refining plant of other embodiments of the invention and the cross-sectional view of board member.
Fig. 6 B is the inner cylinder of the refining plant of other embodiments of the invention and the cross-sectional view of board member.
Fig. 6 C is the inner cylinder of the refining plant of other embodiments of the invention and the cross-sectional view of board member.
Fig. 6 D is the inner cylinder of the refining plant of other embodiments of the invention and the cross-sectional view of board member.
Fig. 6 E is the inner cylinder of the refining plant of other embodiments of the invention and the cross-sectional view of board member.
Fig. 6 F is the inner cylinder of the refining plant of other embodiments of the invention and the cross-sectional view of board member.
Specific embodiment
<first embodiment>
(1) structure of refining plant
Fig. 1 is the brief horizontal cross of the refining plant 1 of the organic material of first embodiment of the invention.Purification
Device 1 includes inner cylinder 2, outer barrel 3, temperature-regulating system 4, vacuum pump 5 and twisted plate 6.Hereinafter, further illustrating purification dress
Set the structure of 1 each section.
Inner cylinder 2 be for gasification organic material M internal flow cylinder example.In the present embodiment, inner cylinder
Body 2 includes the gasification section 21 for making organic material M gasify and the trapping section 22 for trapping the organic material to have gasified.In gasification zone
Between 21 configured be contained in plate-like container 211 powdered organic material M.Trapping section 22 includes the first trapping section
22A, the second trapping section 22B and third trap section 22C.In the example shown in the series of figures, inner cylinder 2 is divided in the longitudinal direction
Section is trapped to trap section 22A, the second trapping section 22B and third with four above-mentioned sections, i.e. gasification section 21, first
Corresponding four parts 22C, these parts are connected to each other.
Inner cylinder 2 as described above is by being that inactive substance is formed relative to organic material M.Material as inner cylinder 2
Matter, such as the alloy that the category of glass such as quartz glass, pyrex, stainless steel, tantalum, tungsten, molybdenum, titanium can be enumerated etc. etc..In addition,
Can be used the ceramics such as zirconium oxide, aluminium oxide, boron nitride, silicon nitride, copper, zinc or alloy comprising iron, copper, zinc, tin etc., carbon,
Teflon (registered trademark) etc..It should be noted that the material of inner cylinder 2 can be identical in whole range, in addition may be used
With different according to the section being partitioned into as described above.Specifically, constituting the gasification section 21 and trapping section of inner cylinder 2
22 material can also be different, such as can enumerate the material in gasification section 21 is the category of glass such as quartz glass, trapping section 22
Material is the example of the alloys such as stainless steel.
Outer barrel 3 extends to direction identical with inner cylinder 2, and is configured at the outside of inner cylinder 2.In present embodiment
In, outer barrel 3 is integrally formed.Lid 31,32 is installed at the both ends of outer barrel 3.Lid 31 closes being located at for outer barrel 3
The end of gasification 21 side of section of inner cylinder 2, similarly lid 32 closes the end for being located at trapping 22 side of section of outer barrel 3,
Thus outer barrel 3 constitutes the sealing container of receiving inner cylinder 2.It should be noted that, although not illustrating, it is arranged on lid 31
There is feeder, the feeder is when the inside of outer barrel 3 has been depressurized by micro gas (such as nitrogen) to outer barrel 3
Inside supply.
Outer barrel 3 and lid 31,32 as described above is also by being non-live relative to organic material M in the same manner as inner cylinder 2
The substance of property is formed.For example, outer barrel 3 is formed by quartz glass, lid 31,32 is formed by stainless steel.
Temperature-regulating system 4 include be configured at cylinder outside as temperature adjusting mechanism exemplary heater 41,
42.In the present embodiment, heater 41 is annularly configured at outer cylinder in the corresponding section in gasification section 21 with inner cylinder 2
The outside of body 3.In addition, heater 42 includes in the corresponding section trapping section 22A, 22B, 22C with inner cylinder 2 in ring
Shape it is configured at heater 42A, 42B, the 42C in the outside of outer barrel 3.Heater 41,42A, 42B, 42C are by 44 base of control device
In temperature sensor 43 measurement result and independently control.As illustrated, temperature sensor 43 includes that temperature measurement fraction is not matched
Be placed in inner cylinder 2 gasification section 21 and trap section 22A, 22B, 22C temperature sensor 431 and temperature sensor 432A,
432B、432C。
Heater 41 that temperature-regulating system 4 as described above is included, 42, temperature sensor 43 and control device 44 by
The various devices that can be utilized are constituted.Heater 41,42 is, for example, infrared heater.In addition, temperature sensor 43
E.g. thermocouple.Control device 44 is, for example, to have to send control signal to heater 41,42 and from temperature sensor 43
The communication unit of measurement result, measurement result based on temperature are received to determine operational part and the storage of the controlling value of heater
The controller or computer of the storage unit of the program and data of operational part.
Vacuum pump 5 carries out closed lid 32 with 22 side of trapping section to outer barrel 3 via piping 51 and valve 52 and connect.
In the state that outer barrel 3 constitutes sealing container together with lid 31,32, opens valve 52 and act vacuum pump 5, thus
The inside of outer barrel 3 comprising inner cylinder 2 can be depressurized.It should be noted that, although it is not shown, it is removed in piping 51
It is provided with other than valve 52 and is also provided with trap devices.
Twisted plate 6 is arranged in the example of the inside of cylinder and the board member along the extension of the length direction of cylinder.At this
In embodiment, twisted plate 6 is configured at the inside of inner cylinder 2 in trapping section 22A, 22B, 22C.Twisted plate 6 on the whole along
The length direction of inner cylinder 2 extends, but is respectively correspondingly divided into three in the longitudinal direction with trapping section 22A, 22B, 22C
Part 6A, 6B, 6C, and further two parts are divided into the longitudinal direction respectively in trapping section 22A, 22B, 22C.Tool
For body, the part 6A for being configured at the twisted plate of trapping section 22A includes part 6AA, 6AB, is configured at the curved of trapping section 22B
The part 6B of bent plate includes part 6BA, 6BB, and the part 6C for being configured at the twisted plate of trapping section 22C includes part 6CA, 6CB.
It can configure to contiguity each other in the longitudinal direction these parts as illustrated, or these parts can also be made in length side
It is separated from each other compartment of terrain configuration upwards.It should be noted that the cross sectional shape about twisted plate 6, is described below referring to Fig. 2.
(2) movement of refining plant
Then, illustrate the movement of the refining plant 1 of present embodiment referring to Fig.1.In the refining step of organic material M
In, inner cylinder 2 is enclosed to the inside of outer barrel 3 first.Specifically, removing the shape of either one in lid 31,32
Under state, inner cylinder 2 is inserted into inside from the end of the opening of outer barrel 3.Later, install lid 31,32 and outer barrel 3 is close
Envelope.Organic material M is configured at the gasification section 21 of inner cylinder 2 until at this time.In addition, twisted plate 6 also configures until at this time
In the trapping section 22 of inner cylinder 2.
Then, act vacuum pump 5 in the state of opening valve 52, to the inside of the outer barrel 3 comprising inner cylinder 2
It is depressurized.At this point, supplying micro gas from the feeder for being set to lid 31, thus generated in the inside of outer barrel 3
The air-flow of the direction of lid 32 is gone to from lid 31.The organic material M to have gasified is carried by the air-flow and in the inside of inner cylinder 2
Flowing.Moreover, temperature-regulating system 4 so that the inside of outer barrel 3, specifically inner cylinder 2 gasification section 21 and trapping area
Between 22A, 22B, 22C remain respectively as defined in the mode of temperature execute control of the control device 44 to heater 41,42.
In the present embodiment, during the refining step of organic material M, the gasification section 21 of inner cylinder 2 is remained
Make temperature of the organic material M from solid variation for gas.It is configured at the powdered organic material M gas in gasification section 21 as a result,
Change, trapping section 22 is transported to by the air-flow of the inside of outer barrel 3 as described above.In trapping section 22, closest to gasification
The first trapping section 22A in section 21 remains the first temperature, is located in the middle the second trapping section 22B and remains the second temperature
Degree, the third trapping section 22C farthest away from gasification section 21 remain third temperature.The organic material M that has gasified as a result, and
The impurity component to have gasified together with organic material M is in trapping section 22 by the surface of the inner peripheral surface of inner cylinder 2 and twisted plate 6
Trapping.
In the examples described above, the first temperature is more slightly higher from the temperature that gas variation is solid than making pure organic material M.Second
Temperature is more slightly lower than the temperature.Third temperature is lower than second temperature.It is remained respectively in this way by trapping section 22A, 22B, 22C
Temperature, thus first trapping section 22A in than pure organic material M high at a temperature of from gas variation be solid it is miscellaneous
Matter ingredient is captured, and traps in the 22C of section in third and changes at a temperature of lower than pure organic material M from gas as solid
Impurity component is captured.Result can be improved the purity of the organic material M trapped in the second trapping section 22B as a result,.
Organic material M in the gasification section 21 for being configured at inner cylinder 2 all gasifies or have passed through the defined time
In the case of, the refining step of organic material M terminates.In this case, it closes valve 52 or vacuum pump 5 is made to stop and release outer barrel
The decompression state of 3 inside, and either one in lid 31,32 is removed on this basis, from the end of the opening of outer barrel 3
Take out inner cylinder 2 in portion.
Later, the organic material M and impurity component trapped in the trapping section 22 of inner cylinder 2 is recovered.At this point, by curved
Bent plate 6 takes out from inner cylinder 2, and organic material M and impurity is separately recovered from the surface of the inner peripheral surface of inner cylinder 2 and twisted plate 6
Ingredient.After the recycling of organic material M and impurity component, twisted plate 6 is configured to the inside of inner cylinder 2 again, and further
Inner cylinder 2 is inserted into the inside of outer barrel 3, to start the refining step of next organic material M.It is being consecutively carried out organic material
In the case where the refining step for expecting M, can also make temperature-regulating system 4 to the control of heater 41,42 by inner cylinder 2 from outer
Also continue during taking out the inside of cylinder 3.
In the present embodiment, twisted plate 6 (part 6B), the thus trapping of organic material M are configured in trapping section 22B
Area increases.Therefore, more organic material M can be trapped in the trapping section 22B of identical length.For example pass through as a result,
Increase the amount for being configured at the powdered organic material M in gasification section 21 of inner cylinder 2 or makes to produce in the inside of outer barrel 3
The speed of raw air-flow rises, so as to improve the purification efficiency of the organic material M in refining plant 1.
In addition, by being configured with twisted plate 6 (part 6A, 6C) in trapping section 22A, 22C, the thus trapping of impurity component
Area increases.Impurity component is also possible to together with air-flow release and be attached to outer from inner cylinder 2 in the case where collection at large
The piping 51 that the inner peripheral surface of cylinder 3 or inflow are connect with vacuum pump 5, therefore by increasing catching in trapping section 22A, 22C
Collect area, can be beneficial to fully trap impurity component in the inside of inner cylinder 2.
Even if it should be noted that for example be unworthy of setting twisted plate 6 also can fully be trapped in the inside of inner cylinder 2 it is miscellaneous
The case where matter ingredient, will not because the impurity component that is not captured is released from inner cylinder 2 lead to the problem of in the case where, can also be with
Not in trapping section 22A, 22C configuration twisted plate 6 (part 6A, 6C).
(3) cross sectional shape of cylinder and twisted plate
Fig. 2 is the I-I line cross-sectional view of refining plant 1 shown in FIG. 1.It should be noted that though I-I line illustrates in Fig. 1
In the trapping section 22B of inner cylinder 2, but in the present embodiment, the shape of inner cylinder 2 and twisted plate 6 trapping section 22A,
It is all likewise, therefore in the following description, using inner cylinder 2 (trapping section 22) and the attached drawing of twisted plate 6 in 22B, 22C
Label.In addition, omitting the diagram of heater 41,42 and temperature sensor 43 in the cross-sectional view after Fig. 2.
In the example shown in the series of figures, twisted plate 6 includes the first twisted plate 61 and the second twisted plate 62.First twisted plate 61 and
Two twisted plates 62 all have the cross sectional shape of the convex (semi-cylindrical shaped) formed by the bending in section, by relative to organic material
Material M is inactive substance, such as stainless steel is integrally formed.Two ends 611 of the cross sectional shape of the first twisted plate 61,
612 with the inner circumferential face contact of inner cylinder 2.In the present embodiment, in the cross sectional shape of the convex of the first twisted plate 61, in place
In with two ends 611,612 be base portion when top part on the outside of be formed with the first contact portion 613.On the other hand,
Two twisted plates 62 are in such a way that the cross sectional shape of convex is overturn in the up-down direction relative to the cross sectional shape of the first twisted plate 61
Configuration.The second contact portion 623 is formed on the outside of the cross sectional shape of the convex of the second twisted plate 62.In the present embodiment,
First twisted plate 61 and the second twisted plate 62 configure in such a way that contact portion 613,623 is in contact with each other.Here, can also contact
Portion 613,623 forms the flat surface extended along the length direction of inner cylinder 2.In this case, the first twisted plate 61 can be more
Steadily support the second twisted plate 62.
As described above, in the present embodiment, by being configured with twisted plate 6 in the trapping section 22 of inner cylinder 2, thus
The trapping area of organic material M increases, and the purification efficiency of the organic material M in refining plant 1 improves.Even if here, only matching
In the case where setting the first above-mentioned twisted plate 61, trapping area also increases, and the purification efficiency of organic material M also improves, but passes through
The second twisted plate 62 is configured, trapping area can be further increased, further increases the purification efficiency of organic material M.
In addition to this, in the present embodiment, the construction of the twisted plate 6 including the first twisted plate 61 and the second twisted plate 62
Body is by the end 611,612 of the first twisted plate 61 and the contact of the inner peripheral surface of inner cylinder 2 and is formed in the first twisted plate 61
First contact portion 613 in outside supported with the contact of second contact portion 623 in the outside for being formed in the second twisted plate 62.
Therefore, in the present embodiment, between inner cylinder 2 and twisted plate 6 and the first twisted plate 61 and the second twisted plate 62 it
Between, the not set joint construction such as cut-in portion, Screw hole.
For example twisted plate 6 is being taken out from inner cylinder 2 and is further dividing the first twisted plate 61 with the second twisted plate 62 as a result,
From come process when recycling the organic material M trapped on surface, without carrying out releasing joint construction.In addition, organic material M's
Without the process for carrying out engaging joint construction when assembling twisted plate 6 after recycling.Therefore, in the present embodiment, will be used for
The component (twisted plate 6) of the trapping area of increase organic material M is configured at the process of the inside of inner cylinder 2 and in order to recycle
The organic material M that traps and the component is taken out from inner cylinder 2 and the process further decomposed is simplified.
In addition, in the present embodiment, the first twisted plate 61 and the second twisted plate 62 all have the bending by section
The cross sectional shape of the convex (semi-cylindrical shaped) of formation.Moreover, as described above, on the first twisted plate 61 and the second twisted plate 62
Not set joint construction.Therefore, the organic material M trapped on the first twisted plate 61 and the respective surface of the second twisted plate 62
It will not be stranded in bumps, cut-in portion, the hole etc. of component surface, can easily be recycled.
Fig. 3 is to indicate to take out twisted plate 6 from the inside for the inner cylinder 2 that can divide in the first embodiment of the present invention
Process exemplary figure.In the example shown in the series of figures, the inner cylinder 2 of refining plant 1 is able to be divided on semicylindrical
Side member 2A and lower side member 2B.Upper member 2A and lower side member 2B is linked by hinge 25.
(a) of Fig. 3 indicates the hinge-opening 25 after taking out inner cylinder 2 from outer barrel 3 and inner cylinder 2 is divided into upside
The state of component 2A and lower side member 2B.It should be noted that in the case where not set hinge 25 as described later, upside structure
Part 2A is separated at the moment from lower side member 2B.For example, in the case where contact portion 613,623 is formed with flat surface, even if
In the state of (a) that removes upper member 2A, the second twisted plate 62 also maintains the state for being placed in the first twisted plate 61.
(b) of Fig. 3 indicates the state for taking out the second twisted plate 62 from inner cylinder 2 after the state of above-mentioned (a).Institute as above
It states, in the present embodiment, contact portion 613,623 not set connector structures between the first twisted plate 61 and the second twisted plate 62
It makes, therefore is easy to take out the second twisted plate 62.
What (c) expression of Fig. 3 further also took out the first twisted plate 61 from inner cylinder 2 after the state of above-mentioned (b)
State.As described above, in the present embodiment, two ends 611,612 and (the downside structure of inner cylinder 2 in the first twisted plate 61
Part 2B) inner peripheral surface between not set joint construction, therefore also be easy take out the first twisted plate 61.
The first twisted plate 61 and the second twisted plate 62 that are taken out by above such process and the inner cylinder 2 left
Upper member 2A and lower side member 2B be transferred to from surface recycling organic material M process.In the recycling of organic material M
Afterwards, according to the sequence opposite with (a) to (c) of above-mentioned Fig. 3 by the configuration of the first twisted plate 61 on lower side member 2B, and
Further by the configuration of the second twisted plate 62 on the first twisted plate 61, and then closes hinge 25 and form inner cylinder 2.These works
Sequence is also same as the process of taking-up, by between inner cylinder 2 and twisted plate 6 and the first twisted plate 61 and the second twisted plate 62
Between not set joint construction and be simplified.
It should be noted that in the present embodiment, inner cylinder 2 can also may not example as shown in Figure 3 like that can
Segmentation, such as can also be integrally formed in the circumferential.In this case, using fixture etc. that the first twisted plate 61 and second is curved
Bent plate 62 is inserted into from the end of the opening of inner cylinder 2, passes through not set joint construction between components like that also described above at this time
And simplify process.In addition, upper member 2A and lower side member 2B can also may not be as shown in Figure 3 example like that by hinge 25
Connection.For example, it is also possible to upper member 2A is enable to separate with lower side member 2B, and the structure on the upside of mounting on the lower side member 2B
Part 2A.In this case, the end of the semicircular cross sectional shape of upper member 2A and lower side member 2B abuts each other.Alternatively,
Concaveconvex shape corresponding with the end of semicircular cross sectional shape of upper member 2A and lower side member 2B can also be formed,
And it is fitted into these concaveconvex shapes each other.
<second embodiment>
Fig. 4 is the cross-sectional view of the refining plant 1E of the organic material of second embodiment of the present invention.As shown, at this
In embodiment, the configuration of the twisted plate 6E of the inside of inner cylinder 2 is different from above-mentioned first embodiment.In addition to this
On point, the structure of present embodiment is same as above-mentioned first embodiment, therefore the repetitive description thereof will be omitted.
As shown, in the present embodiment, twisted plate 6E includes same as above-mentioned first embodiment first curved
Bent plate 61 and the second twisted plate 62.But, it is different from the first embodiment, in the present embodiment, the first twisted plate 61 and
The cross sectional shape of two twisted plates 62 is overturn in the lateral direction relative to each other.In this case, the section of the first twisted plate 61
The inner circumferential face contact of the end 621 of the end 611 of the downside of shape and the downside of the second twisted plate 62 and inner cylinder 2, and formed
In the second contact portion 623 of first contact portion 613 and the outside for being formed in the second twisted plate 62 in the outside of the first twisted plate 61
Be in contact with each other, thus constitute the first twisted plate 61 and the second twisted plate 62 by inner cylinder 2 inner circumferential surface bearing tectosome.
In the present embodiment, also same as above-mentioned first embodiment, between inner cylinder 2 and twisted plate 6E, with
And twisted plate 6E included the first twisted plate 61 and the second twisted plate 62 between not set joint construction, thus twisted plate 6E
Configuration, the process taken out and decomposed are simplified.
<third embodiment>
Fig. 5 is the cross-sectional view of the refining plant 1F of the organic material of third embodiment of the present invention.As shown, at this
In embodiment, in the inside of inner cylinder 2, bending plate 6F is configured with instead of the twisted plate 6 of first embodiment.Except this with
On outer point, the structure of present embodiment is same as above-mentioned first embodiment, therefore the repetitive description thereof will be omitted.
Bending plate 6F and the twisted plate of first embodiment 6 are equally arranged in the inside of cylinder and the length along cylinder
The example for the board member that direction extends.In the example shown in the series of figures, bending plate 6F includes the first bending plate 61F and the second bending plate
62F.First bending plate 61F and the second bending plate 62F all has the section of the convex formed by the bending of the part in section
Shape, by being that inactive substance, such as stainless steel are integrally formed relative to organic material M.The section of first bending plate 61F
Two ends 611,612 of shape and the inner circumferential face contact of inner cylinder 2.In the cross sectional shape of the convex of the first bending plate 61F,
The first contact portion 613F is formed on the outside of the part at the top when being located at is base portion with two ends 611,612.Another party
Face, cross sectional shape of the second bending plate 62F with the cross sectional shape of convex relative to the first bending plate 61F are overturn in the up-down direction
Mode configure.The second contact portion 623F is formed on the outside of the cross sectional shape of the convex of the second bending plate 62F.In this implementation
In mode, the first bending plate 61F and the second bending plate 62F are configured in such a way that contact portion 613F, 623F are in contact with each other.As schemed
Show, is each formed with the flat part of the length direction extension along inner cylinder 2, therefore the first bending plate in contact portion 613F, 623F
61F can steadily support the second bending plate 62F.
Here, convex in the cross sectional shape of the first bending plate 61F as described above by two obtuse angles bending part 614,
615 form.Equally, the convex in the cross sectional shape of the second bending plate 62F is formed by the bending part 624,625 at two obtuse angles.?
In the example of diagram, bending part 614,615,624,625 is locally bent to be formed with defined curvature by section.Bending part
614,615,624,625 by bending formed, thus be easy recycling the first bending plate 61F and the second bending plate 62F respectively
The organic material M that traps of surface.
<other embodiments>
Fig. 6 A to Fig. 6 F is the inner cylinder 2 and board member of the refining plant of the organic material of other embodiments of the invention
Cross-sectional view.Bending plate 61G, 62G and twisted plate 61H, 62H for showing in these figures are also arranged in inside and the edge of cylinder
Cylinder length direction extend board member example.It should be noted that outer barrel 3 is omitted in Fig. 6 A to Fig. 6 F
And it is configured at the diagram of the component in the outside of outer barrel 3.
Fig. 6 A and Fig. 6 B show it is above-mentioned referring to Fig. 2 and Fig. 4 illustrate it is exemplary on the basis of by the second twisted plate 62
Replace with the example of bending plate 62G.Convex in the cross sectional shape of bending plate 62G is formed by the bending part 624G of approximate right angle.
In the example of Fig. 6 A and Fig. 6 B, it is formed in the second contact portion 623G in the outside of bending part 624G and is formed in the first twisted plate
First contact portion 613 in 61 outside contacts.In addition, in the example of 6 b it, the end 621G of the downside of bending plate 62G with it is interior
The inner circumferential face contact of cylinder 2.
Fig. 6 C show it is above-mentioned referring to Fig. 2 illustrate it is exemplary on the basis of the first twisted plate 61 replaced with into bending plate
The example of 61G.It is same as above-mentioned bending plate 62G, convex in the cross sectional shape of bending plate 61G by approximate right angle bending part
614G is formed.In the example of Fig. 6 C, the inner circumferential of two end 611G, 612G and inner cylinder 2 of the cross sectional shape of bending plate 61G
Face contact.In addition, being formed in the first contact portion 613G in the outside of bending part 614G and being formed in the outside of the second twisted plate 62
The second contact portion 623 be in contact with each other.It should be noted that, although it is not shown, it can also be curved by the first twisted plate 61 and second
This two side of bent plate 62 replaces with bending plate 61G, 62G respectively.
Fig. 6 D show it is above-mentioned referring to Fig. 5 illustrate it is exemplary on the basis of the second bending plate 62F replaced with and schemed
The example of the same bending plate 62G of the example of 6A and Fig. 6 B.Be formed in the outside of the bending part 624G of bending plate 62G second connects
Contact portion 623G is contacted with the contact portion 613F in the outside for being formed in the first bending plate 61F.It should be noted that, although it is not shown,
First bending plate 61F can also be replaced with to bending plate 61G same as example shown in Fig. 6 C.
Fig. 6 E is shown in the inside of inner cylinder 2 configured with the shape different from the example illustrated referring to Fig. 2 and Fig. 4
The example of first twisted plate 61H and the second twisted plate 62H.First twisted plate 61H and the second twisted plate 62H are respective to be formed in
The mode that contact portion 613H, the 623H in the outside of the cross sectional shape of convex are in contact with each other configures.Here, contact portion 613H, 623H
It is formed at the top of the cross sectional shape with convex and is staggered or eccentric position.In addition, in the example shown in the series of figures, the first twisted plate
The end 621H of the downside of two ends 611H, 612H and the second twisted plate 62H of the cross sectional shape of 61H and inner cylinder 2
Inner circumferential face contact.Constitute as a result, the first twisted plate 61H and the second twisted plate 62H by inner cylinder 2 inner circumferential surface bearing construction
Body.
Fig. 6 F shows the first twisted plate 61H and the second twisted plate with shape same as example shown in Fig. 6 E
The example that 62H is configured in a manner of being in contact with each other on the outside of end 621H, 622H in the upside of respective cross sectional shape.At this
In the case of, end 621H, 622H are also contact portion.In addition, in the example shown in the series of figures, the end of the downside of the first twisted plate 61H
The end 621H of the downside of 611H and the second twisted plate 62H respectively with the inner circumferential face contact of inner cylinder 2.It is curved that first is constituted as a result,
Bent plate 61H and the second twisted plate 62H are supported on the tectosome on the inner peripheral surface of inner cylinder 2.It should be noted that the first twisted plate
End 621H, 622H of the upside of 61H and the second twisted plate 62H can also may not be with the inner circumferential face contacts of inner cylinder 2.
It this concludes the description of illustrative embodiment of the invention, but technical scope of the invention is not limited to these realities
Mode is applied, it is logical according to having for technical field belonging to the present invention in the scope including the technical idea documented by technical solution
The personnel of normal knowledge it is conceivable that point and carried out change or modified embodiment.
For example, in the above-described embodiment, as formation inner cylinder 2, outer barrel 3, lid 31,32 and twisted plate
6, the board members such as 6E and bending plate 6F is inactive material relative to organic material M, instantiates quartz glass and stainless steel,
But other materials also can be used.It, can be by the alloy of tantalum, tungsten, molybdenum, titanium etc. and above-mentioned for example, as inactive metal
Stainless steel is used in the same manner.In addition, quartz, zirconium oxide, aluminium oxide, boron nitride, silicon nitride etc. can be used as ceramics.Make
For other materials, carbon, Teflon (registered trademark) etc. also can be used.In addition, in the above-described embodiment as by phase
With the component that is formed of material and the component that illustrates can also be formed by material different from each other, conversely, as by each other not
With the component that is formed of material and the component that illustrates can also be formed by identical material.
In addition, in the above-described embodiment, illustrating that inner cylinder 2 is divided into gasification section 21 in the longitudinal direction and catches
Collect section 22 and will further trap section 22 and be divided into three examples for trapping section 22A, 22B, 22C, but other real
It applies in mode, inner cylinder 2 also may include that gasification section 21 and trapping section 22 are integrally formed interiorly.In addition, inner cylinder 2
Gasification section 21 and trapping section 22 can also be divided into and be integrally formed in trapping section 22.Alternatively, inner cylinder 2 can also
To be divided into two or four or more in trapping section 22.In the case where trapping section 22 is divided into more than four situations, make
The temperature in each section is set as more stages, and thus, it is possible to improve the purity of the organic material M trapped.
In addition, in the above-described embodiment, trapping section 22A, 22B, 22C be each configured with board member, it is specific and
Speech is twisted plate 6, but board member can also only be configured at a part of trapping section 22A, 22B, 22C.For example, board member can also
To be only configured at the trapping section 22B of trapping organic material M.In addition, in the above-described embodiment, board member is in trapping section
Be divided into two parts in 22A, 22B, 22C in the longitudinal direction respectively, but board member can also trapping section 22A, 22B,
Be in the longitudinal direction in each (or a part) of 22C it is integrated, three or more parts can also be divided into.Alternatively, plate
Component can also only be configured at a part of length direction in each (or a part) of trapping section 22A, 22B, 22C.
In addition, in the above-described embodiment, showing organic material M is powdered example, but organic material M can also
Be it is powdered, powdered other than solid-like, it is liquid in either.Furthermore in the above-described embodiment, You Jicai
Material M is contained in the container 211 configured in the gasification section 21 of inner cylinder 2, but organic material M can also be without using container and in gas
Change the inner peripheral surface that inner cylinder 2 is directly configured in section 21.
In addition, in the above-described embodiment, as temperature-regulating system 4 heater 41,42 and instantiate infrared ray
Heater, but can also be using other light heating (arc light radiant heating or laser emission heating etc.), resistance heating (metal system
Or nonmetallic system), induction heating, plasma heating, electric arc heated, flame heating heater.For example, in configuration thoughts
Should be in the case where the heater of heating, inner cylinder 2 and outer barrel 3 are by being nonactive relative to organic material M and can pass through electricity
Magnetic induction and generate heat material, specifically stainless steel etc. formation.Equally, temperature sensor 43 is also not limited to thermocouple, can
To use various thermometers.
In addition, in the above-described embodiment, illustrating the board members such as twisted plate 6,6E and bending plate 6F by stainless steel etc.
The example that material is integrally formed, but in other embodiments, board member be functionally it is integrated, can also may not
It is constructively integrated.For example, board member also can have the cross sectional shape for being divided into multiple portions, and multiple part makes
It is engaged with each other with welding or bonding agent etc..
In addition, in the above-described embodiment, illustrating in the inside of inner cylinder 2 configured with twisted plate 6,6E and bending plate
The example of the board members such as 6F, but be configured to increase the trapping area of organic material M the board member of the inside of inner cylinder 2
Cross sectional shape is not limited to these examples.For example, in other embodiments, its of the convex comprising bending part can also be configured
The board member of his cross sectional shape, such as V-shaped, U-shaped or M font.Or it is not convex for can also configuring comprising bending part
The board member of the cross sectional shape of shape.Bending part for example can be as the twisted plate 6 in first embodiment by board member
The whole bending of cross sectional shape is formed, such as can also pass through board member as the bending plate 6F in third embodiment
The bending of part of cross sectional shape formed.
The refining plant of the organic material of embodiments of the present invention as described above for example can be used in organic EL
The purification of the organic material M of element, however, not limited to this, be for example used as electronic material, optical material and use
Various organic materials purification.Alternatively, it is also possible to by having carried out essence to the refining plant for using embodiments of the present invention
The organic material of system is again carried out (to be carried out using the refining plant of embodiments of the present invention or using method in addition to this
) purification, to further increase the purity of organic material.
Description of symbols:
1 ... refining plant；2 ... inner cylinders；21 ... gasification sections；22 ... trapping sections；3 ... outer barreies；The adjustment of 4 ... temperature
System；5 ... vacuum pumps；6,6E ... twisted plate；61 ... first twisted plates；62 ... second twisted plates；6F ... bending plate；61F ...
One bending plate；The second bending plate of 62F ....
Claims (11)
1. a kind of refining plant of organic material, has:
Cylinder, the organic material to have gasified is in the internal flow of the cylinder, and the cylinder includes trapping catching for the organic material
Collect section；And
First board member is configured at the inside of the cylinder in the trapping section, and along the length direction of the cylinder
Extend,
The refining plant of the organic material is characterized in that,
First board member is formed integrally as the cross sectional shape comprising bending part, the cross sectional shape of first board member
The inner circumferential face contact of at least one end and the cylinder.
2. the refining plant of organic material according to claim 1, wherein
First board member is formed integrally as the cross sectional shape of convex,
Two ends of the cross sectional shape of first board member and the inner circumferential face contact of the cylinder.
3. the refining plant of organic material according to claim 1, wherein
The refining plant of the organic material is also equipped with the second board member, and second board member is configured in the trapping section
The inside of the cylinder, and extend along the length direction,
First board member and second board member are formed integrally as the cross sectional shape of the convex comprising bending part, and
And first board member and second board member are to be formed in the outside of the cross sectional shape of the convex of first board member
The first contact portion and second contact portion in the outside of the cross sectional shape for the convex for being formed in second board member be in contact with each other
Mode configure.
4. the refining plant of organic material according to claim 3, wherein
Two ends of the cross sectional shape of first board member and the inner circumferential face contact of the cylinder,
When first contact portion is formed in the cross sectional shape of first board member using described two ends as base portion
Top.
5. the refining plant of organic material according to claim 4, wherein
The flat surface extended along the length direction is formed in first contact portion and second contact portion.
6. the refining plant of organic material according to any one of claim 3 to 5, wherein
First board member and second board member are with the cross sectional shape of the convex of first board member and described second
The mode that the cross sectional shape of the convex of board member is overturn each other configures.
7. the refining plant of organic material according to any one of claim 1 to 6, wherein
The bending part is formed by the whole bending of the cross sectional shape of first board member.
8. the refining plant of organic material according to any one of claim 1 to 6, wherein
The bending part is formed by the bending of the part of the cross sectional shape of first board member.
9. the refining plant of organic material according to any one of claim 1 to 8, wherein
First board member is divided into multiple portions in the length direction.
10. the refining plant of organic material according to any one of claim 1 to 9, wherein
The cylinder is divided into multiple portions in the length direction,
First board member is configured at the inside of at least one of the multiple portions of cylinder part.
11. the refining plant of organic material according to any one of claim 1 to 10, wherein
The refining plant of the organic material is also equipped with temperature adjusting mechanism, and the temperature adjusting mechanism is configured at the cylinder
Outside.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2017-095731 | 2017-05-12 | ||
| JP2017095731 | 2017-05-12 | ||
| PCT/JP2018/017734 WO2018207764A1 (en) | 2017-05-12 | 2018-05-08 | Organic material refining device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109257928A true CN109257928A (en) | 2019-01-22 |
Family
ID=64105530
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201880000927.1A Pending CN109257928A (en) | 2017-05-12 | 2018-05-08 | Organic material refining device |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JPWO2018207764A1 (en) |
| KR (1) | KR20200005985A (en) |
| CN (1) | CN109257928A (en) |
| WO (1) | WO2018207764A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111054090A (en) * | 2019-12-28 | 2020-04-24 | 云南农业大学 | Device for purifying by utilizing component volatility difference |
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- 2018-05-08 KR KR1020187022429A patent/KR20200005985A/en not_active Application Discontinuation
- 2018-05-08 WO PCT/JP2018/017734 patent/WO2018207764A1/en active Application Filing
- 2018-05-08 CN CN201880000927.1A patent/CN109257928A/en active Pending
- 2018-05-08 JP JP2019517630A patent/JPWO2018207764A1/en active Pending
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| CN1714061A (en) * | 2001-12-15 | 2005-12-28 | Skc株式会社 | Apparatus and method for purifying an organic electroluminescent material |
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| CN111054090B (en) * | 2019-12-28 | 2021-01-15 | 云南农业大学 | Device for purifying by utilizing component volatility difference |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2018207764A1 (en) | 2018-11-15 |
| KR20200005985A (en) | 2020-01-17 |
| JPWO2018207764A1 (en) | 2020-03-12 |
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Application publication date: 20190122 |