CN203724803U - Organic material subliming and purifying device capable of supplying and extracting air and quickly cooling - Google Patents
Organic material subliming and purifying device capable of supplying and extracting air and quickly cooling Download PDFInfo
- Publication number
- CN203724803U CN203724803U CN201420042441.3U CN201420042441U CN203724803U CN 203724803 U CN203724803 U CN 203724803U CN 201420042441 U CN201420042441 U CN 201420042441U CN 203724803 U CN203724803 U CN 203724803U
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- CN
- China
- Prior art keywords
- air
- vacuum chamber
- heater
- furnace body
- organic material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 239000011368 organic material Substances 0.000 title claims abstract description 27
- 238000001816 cooling Methods 0.000 title claims abstract description 13
- 238000000746 purification Methods 0.000 claims abstract description 22
- 238000000859 sublimation Methods 0.000 claims abstract description 7
- 230000008022 sublimation Effects 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000004821 distillation Methods 0.000 description 12
- 238000010586 diagram Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
The utility model discloses an organic material subliming and purifying device capable of supplying and extracting air and quickly cooling. The device comprises a furnace body and a vacuum chamber (11), wherein the vacuum chamber (11) is formed in the middle of the furnace body; the furnace body comprises a left furnace body (10) and a right furnace body (13) which are capable of oppositely moving; the left furnace body (10) and the right furnace body (13) can oppositely move to be separated and are combined into a whole; the furnace body is movably supported on a base (6); different temperature areas are arranged in the length direction of the furnace body; an air supply device is arranged in the axial direction of the vacuum chamber and comprises air nozzles (18) and an air supply pipe (17); the air nozzles (18) are arranged at intervals and are used for cooling the vacuum chamber in the different temperature areas; the air supply pipe (17) is connected to the air nozzles; an air extracting device is arranged at the position opposite to the air supply device, and comprises an air extracting hood (12) and an air extracting pipe (3); the air extracting hood is capable of collecting hot air; the air extracting pipe is connected to the air extracting hood. The device is capable of uniformly and quickly cooling all the temperature areas of the vacuum chamber, improving the efficiency of subliming and purifying the organic materials, reducing the working temperature, improving the working environment, saving the energy and reducing the costs of sublimation, purification and production.
Description
Technical field
The utility model relates to a kind of organic material purifying plant, especially relates to one and send exhausting speed cold sublimation purification device of organic material.
Background technology
In the preparation process of organic material, obtain highly purified organic material product, must be through chemical method or physical method purifying, wherein preparation is mostly to adopt physical purification in batches.The pure China of physics is after organic material is heated to uniform temperature, makes organic material distillation, utilizes the different warm areas of purifier apparatus, and the impurity in organic material is separated, and the purification devices of this organic material is exactly organic material distillation purifying machine.At present, though organic material is purified, the purifying machine structure using is had nothing in common with each other, refining effect is more or less the same, but in use all there is following problems in them: in the vacuum chamber in the middle of organic material being placed in to heating furnace, complete after distillation purification, want cooling 4-5 hour, could will be cooled to organic material product-collecting in the vacuum chamber of normal temperature, the cooling cycle is long, thereby reduce distillation purification efficiency, improved distillation cost for purification.For the problem of above-mentioned existence, the applicant had once applied for a utility model patent that the patent No. is ZL201320092109.3, make the distillation purification of organic material product shorten to 1 hour cool time, but find in patent working process, because vacuum chamber has certain length, and air exhauster is arranged on one end of vacuum chamber, thereby can cause organic material difference cool time of each warm area in vacuum chamber, away from warm area cool time of air exhauster sometimes more than 1 hour, cooling uniformity is not very good, thereby the purification efficiency that makes to distil is high not enough; And the hot blast that air exhauster is extracted out is unprocessed, make sometimes workplace temperature raise, also can other equipment be produced and be damaged.
Utility model content
For existing problem in above-mentioned prior art, the utility model provides one can make each warm area Quick uniform of vacuum chamber cooling, and that further improves distillation purification efficiency send exhausting speed cold sublimation purification device of organic material.
The technical problems to be solved in the utility model take technical scheme be: described in send the cold sublimation purification device of organic material of exhausting speed to comprise body of heater and be positioned at the vacuum chamber in the middle of body of heater, described body of heater comprises left body of heater and the right body of heater that can relatively move and separate and be combined into one, body of heater movable supporting is on base, on body of heater length direction, be provided with different warm areas, axially be provided with air-supply arrangement along vacuum chamber, described air-supply arrangement comprises that interval arranges and can carry out cooling tuyere and the ajutage being connected with tuyere to the vacuum chamber in different warm areas, on air-supply arrangement relative position, be provided with extractor fan, described extractor fan comprises can collect the draught hood of hot blast and the exhaust column being connected with draught hood.
The course of work of the present utility model is: after purifying machine distillation is purified, close heating power supply, shake (Electrified Transmission) handwheel makes screw mandrel rotation, two nuts that drive and have right-and-left threaded screw mandrel to match move left and right, thereby the left body of heater that drive is connected with two nuts and right body of heater relatively move and separate, now start air-supply arrangement and the extractor fan of different warm areas simultaneously and regulate and send, air draft speed, air-supply arrangement absorbs heat by tuyere transporting cold wind through the outer wall of vacuum chamber, extractor fan is pumped into the hot blast with vacuum chamber heat rapidly draught hood and takes away from exhaust column simultaneously, make the temperature of the different warm areas of vacuum chamber evenly drop to fast at short notice normal temperature, thereby can quick collection the organic material product of distillation after purifying.
The utility model has carried out cooling simultaneously and rapidly by the cooperation of air-supply arrangement and extractor fan to the organic material of different warm areas in vacuum chamber, guarantee that each warm area of vacuum chamber is cooled to normal temperature within an hour can be evenly fast short-term training, thereby the purification of organic material product is further shortened cool time, not only improve organic material product distillation purification efficiency, and can reduce work indoor temperature, improve working environment, save the energy, reduce distillation purification production cost.
Brief description of the drawings
Fig. 1 is main TV structure schematic diagram of the present utility model,
Fig. 2 is the A-A sectional structure schematic diagram of Fig. 1,
Fig. 3 is the B-B sectional structure schematic diagram of Fig. 1.
Header pipe 2, support 3, exhaust column 4, supporting seat I 5, gripper shoe 6, base 7, handwheel 8, screw mandrel 9, nut 10, left body of heater 11, vacuum chamber 12, draught hood 13, right body of heater 14, thermometer 15, supporting seat II 16, slide bar 17, ajutage 18, tuyere in the drawings, 1.
Detailed description of the invention
In order to make those skilled in the art understand better the technical solution of the utility model, below in conjunction with the drawings and specific embodiments, the utility model is described in further detail.
At Fig. 1, in Fig. 2 and Fig. 3, the described cold sublimation purification device of organic material of exhausting speed that send comprises body of heater and is positioned at the middle vacuum chamber 11 in a tubular form of body of heater, described vacuum chamber is connected with vavuum pump, vacuum chamber two ends are supported on respectively on support 2, in vacuum chamber, place organic material, described body of heater two ends are connected with gripper shoe 5, gripper shoe is movably arranged on base 6 by supporting seat I 4 and slide bar 16, described body of heater comprises and can relatively move separately and be combined into one and left body of heater 10 and the right body of heater 13 of be rectangle (also can be other shapes), be fixedly installed respectively nut 9 at left body of heater and right body of heater middle lower portion, nut matches with screw mandrel 8, on described screw mandrel, be provided with positive/negative thread, screw mandrel is arranged on base by supporting base II 15, screw mandrel one end is connected with handwheel 7, when screw mandrel work, two nuts produce and relatively move, described left body of heater and right body of heater are at nut and have under right-and-left threaded screw mandrel mating reaction and can be separated from each other and be combined into one.On body of heater length direction, be provided with four different warm areas and (be followed successively by from left to right distillation district, high temperature purification district, inferior high temperature purification district, middle temperature purification section and low temperature purification section), on each warm area, be provided with thermometer 14, lower end at vacuum chamber is provided with air-supply arrangement, described air-supply arrangement comprises the tuyere 18 that is positioned at vacuum chamber below and is arranged on left body of heater and right body of heater binding site along vacuum chamber axially spaced-apart, tuyere upper port is parallel to the lower end of left body of heater and right body of heater, described tuyere upper port also can be embedded in the junction between left body of heater and right body of heater, can make like this Distance Shortened of tuyere and vacuum chamber, thereby more can improve cooling effect, described tuyere is connected with ajutage 17, ajutage is two, ajutage is also overall, ajutage is connected with header pipe 1, also can on tuyere, be provided with control valve to regulate cooling wind speed, header pipe is connected with pressure fan (not shown in FIG.), in vacuum chamber upper end and along vacuum chamber axially between the left body of heater of (relative with air-supply arrangement position) and right body of heater position be provided with extractor fan, described extractor fan comprises draught hood 12 that can centralized collection hot blast, described draught hood is rectangle also and exhaust column 3 one end are axially connected, the exhaust column other end is connected with air exhauster (not shown in FIG.).
Except above-mentioned specific embodiment, the utility model can also have other embodiments, as air-supply arrangement being arranged on to the upper end of vacuum chamber, the upper end that extractor fan is arranged on vacuum chamber).All employings are equal to replacement and those skilled in the art easily expect by the enlightenment of above-described embodiment the technical scheme forming, and all drop on the protection domain of the utility model requirement.
Claims (1)
1. one kind is sent exhausting speed cold sublimation purification device of organic material, it comprises body of heater and is positioned at the middle vacuum chamber (11) of body of heater, described body of heater comprises left body of heater (10) and the right body of heater (13) that can relatively move and separate and be combined into one, body of heater movable supporting is on base (6), on body of heater length direction, be provided with different warm areas, it is characterized in that: be axially provided with air-supply arrangement along vacuum chamber, described air-supply arrangement comprises that interval arranges and can carry out cooling tuyere (18) and the ajutage (17) being connected with tuyere to the vacuum chamber in different warm areas, on air-supply arrangement relative position, be provided with extractor fan, described extractor fan comprises can collect the draught hood (12) of hot blast and the exhaust column (3) being connected with draught hood.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420042441.3U CN203724803U (en) | 2014-01-23 | 2014-01-23 | Organic material subliming and purifying device capable of supplying and extracting air and quickly cooling |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420042441.3U CN203724803U (en) | 2014-01-23 | 2014-01-23 | Organic material subliming and purifying device capable of supplying and extracting air and quickly cooling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203724803U true CN203724803U (en) | 2014-07-23 |
Family
ID=51194905
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420042441.3U Expired - Lifetime CN203724803U (en) | 2014-01-23 | 2014-01-23 | Organic material subliming and purifying device capable of supplying and extracting air and quickly cooling |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203724803U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109257928A (en) * | 2017-05-12 | 2019-01-22 | 出光兴产株式会社 | Organic material refining device |
-
2014
- 2014-01-23 CN CN201420042441.3U patent/CN203724803U/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109257928A (en) * | 2017-05-12 | 2019-01-22 | 出光兴产株式会社 | Organic material refining device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20140723 |