CN109233403A - A kind of wear-resisting luminous resin glue, preparation method and application - Google Patents
A kind of wear-resisting luminous resin glue, preparation method and application Download PDFInfo
- Publication number
- CN109233403A CN109233403A CN201710414758.3A CN201710414758A CN109233403A CN 109233403 A CN109233403 A CN 109233403A CN 201710414758 A CN201710414758 A CN 201710414758A CN 109233403 A CN109233403 A CN 109233403A
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- wear
- resisting
- resin glue
- luminous
- luminous resin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/22—Luminous paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/02—Polyureas
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Road Paving Structures (AREA)
- Floor Finish (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to a kind of wear-resisting luminous resin glue, not only there are good luminescent properties, also there is excellent weatherability and wearability, wear-resisting property being capable of long sustaining, it solves resin adhesive layer painting to be covered with when individually doing wearing layer again, glass microballoon or the micro- sand of glass are easy to wear, the problem of falling off.The preparation method of the wear-resisting luminous resin glue of the present invention, simple process, the luminescent powder, glass microballoon or the micro- sand of glass are uniformly dispersed, stablize, is not easy to precipitate.A kind of wear-resisting luminous resin glue of the invention is used to prepare the application of luminous brick, it prepares resulting luminous brick and has both luminous and wear-resisting service performance, compared to directly by wear-resistant material paving spill on luminous glue-line, luminous brick surface is smooth for its, does not influence normal walking, and Acceptable life greatly prolongs.
Description
Technical field
The present invention relates to resinous coat technical fields, and in particular to a kind of wear-resisting luminous resin glue, preparation method and answers
With.
Background technique
Luminous resin glue is made up of special processing process by a certain percentage of resin glue, various fillers and auxiliary agent.Hair
The multi-purpose floor tile indoors of photopolymer resin glue, is made into indoor luminous brick, outdoor luminous brick is seldom, mainly due to outdoor luminous brick pair
The weatherability and anti-pressure and abrasion-proof performance requirement of luminous resin glue are harsh.
In order to improve the wearability of outdoor luminous brick, increase by one layer of inorganic ceramic particle wearing layer on coating sometimes, but
It is since directly the pavings such as ceramic particle being sprinkled upon on coating, the binding force of wearing layer and coating is weaker, and particulate matter is easy to fall off, resistance to
Mill property cannot be kept for a long time, and particle directly spreads the uneven surface spilt and can cause outdoor luminous brick, first is that will affect product
Beauty can even cause people to fall second is that will affect walking experience, generate dangerous.
Summary of the invention
Based on problem above, one purpose of the present invention be to provide it is a kind of can be used for the outer luminous brick of make-up room, it is weatherability, resistance to
Grind the wear-resisting luminous resin glue of function admirable.
Another object of the present invention, which is to provide, a kind of prepares wear-resisting property is uniform, performance is stable wear-resisting luminous resin glue
Method.
Another object of the present invention be to provide it is a kind of by wear-resisting luminous resin glue be used to prepare with Smooth wear-resistant shine apply
The application of the luminous brick of layer.
Wear-resisting luminous resin glue according to the present invention, the wear-resisting luminous resin glue include: in parts by weight
80-120 parts of carbamide resins,
90-110 parts of luminescent powders,
10-50 parts of glass microballoons or the micro- sand of glass,
60-80 parts of curing agent, and
5-15 parts of auxiliary agents；
The auxiliary agent includes defoaming agent, drier, ultraviolet absorbing agent, coupling agent and polyamide wax, the weight of the above auxiliary agent
Amount is than being 0.3-0.5:0.1-0.35:0.3-0.5:1.3-1.8:1.2-1.6.
The auxiliary agent is free of heavy metal compound, avoids the wear-resisting luminous resin glue right in the production and use process
The pollution of environment and the threat of organism life security.
Carbamide resin adhesive force is excellent, and cementability is good；With excellent high temperature resistance, resistance to acid and alkali and boiling resistance
Energy；Reaction speed is fast, and coating duration is short；With high resiliency, durable flexibility, abrasion resistance, low water-swellable and low-permeable
The features such as, and solvent-free release when use, energy conservation and environmental protection.
Wear-resisting luminous resin glue according to the present invention, performance is uniform, stablizes, and not only has good luminescent properties, also has
Have excellent a weatherability and wearability, wear-resisting property can long sustaining, be not in the glass microballoon or glass of wear-resisting matter
Micro- sand is easy to wear, the phenomenon that falling off, and will not generate not because of the glass microballoon or the micro- sand of glass that wear-resisting matter is added to walking safety
Benefit influences.
Wear-resisting luminous resin glue according to the present invention, in order to further enhance the weatherability of the wear-resisting luminous resin glue,
The curing agent is aliphatic polymeric isocyanate curing agent.
Wear-resisting luminous resin glue according to the present invention, in order to guarantee the luminous efficacy of luminescent powder and in the wear-resisting Luminous tree
Dispersion homogeneity in rouge glue, the partial size of the luminescent powder are 80-300 mesh；
Wear-resisting luminous resin glue according to the present invention, in order to guarantee the wearability of the wear-resisting luminous resin glue, and with institute
The viscosity cooperation for stating carbamide resin, is easily uniformly dispersed in the carbamide resin, the partial size of the glass microballoon or the micro- sand of glass
For 50-200 mesh.
The preparation method of wear-resisting luminous resin glue according to the present invention, comprising the following steps:
(1) polyamide wax is added into carbamide resin while stirring, is stirred evenly, obtain mixed raw material；
(2) glass microballoon or the micro- sand of glass, luminescent powder are added in the mixed raw material obtained to step (1), stirs evenly, obtains
To mixed raw material；
(3) defoaming agent, ultraviolet absorbing agent, coupling agent, drier are added into the obtained mixed raw material of step (2),
It stirs evenly, obtains mixed raw material；
(4) curing agent is added in the mixed raw material obtained to step (3) to stir evenly, luminous resin glue can be obtained.
The preparation method of wear-resisting luminous resin glue according to the present invention, can prepare luminescent powder, glass microballoon or glass
The evenly dispersed wear-resisting luminous resin glue of micro- sand.
The preparation method of wear-resisting luminous resin glue according to the present invention makes described shine to guarantee biggish shearing force
Powder, glass microballoon or the micro- sand full and uniform dispersion of glass stir 20- in the step (2) with the revolving speed of >=2000r/min
30 minutes.
The preparation method of wear-resisting luminous resin glue according to the present invention, in order to guarantee that preferable mobility, appropriate reduce are glued
Property, so that each raw material can be fully dispersed, the temperature when stirring is not less than 30 DEG C, is not higher than 60 DEG C.
Wear-resisting luminous resin glue according to the present invention is used to prepare the application of luminous brick, and the wear-resisting luminous resin glue is applied
It overlays on floor tile, forms wear-resisting luminescent coating, then toasted, the luminous brick is made.
The floor tile especially includes acidproof brick, marble tile and bread brick.
Wear-resisting luminous resin glue according to the present invention prepares the application of luminous brick, prepare resulting luminous brick have both shine and
Wear-resisting service performance, and Acceptable life greatly prolongs.Wear-resisting luminous resin glue according to the present invention is used to prepare luminous
The application of brick, in order to guarantee coating uniformly, the wear-resisting luminescent coating levelling, thickness were uniform, with 35-43g/ seconds dispensing rates
The wear-resisting luminous resin glue point glue is coated on floor tile.The wear-resisting luminous resin glue is coated on ground using gluing process
It on brick, can guarantee wear-resisting luminous resin glue uniform levelling on floor tile, high uniformity, and then guarantee luminous brick obtained
Luminescent properties and wear-resisting property embody uniformly, reduce the wear-resisting luminescent coating internal stress, prolong the service life.
Wear-resisting luminous resin glue according to the present invention is used to prepare the application of luminous brick, in order to make the wear-resisting luminescent coating
Show after drying it is smooth, guarantee floor tile aesthetics and good service performance, while guarantee the wear-resisting luminescent coating and ground
Brick good combination, 30-40 DEG C baking 20-40 minutes.
Wear-resisting luminous resin glue according to the present invention is used to prepare the application of luminous brick, in order to guarantee the hair of the luminous brick
Light and wear-resisting efficiency, and guarantee the good combination of the wear-resisting luminescent coating and the floor tile, it is not described wear-resisting luminous
Coating generates the phenomenon that easy delamination, and the coated weight of the wear-resisting luminous resin glue is 0.2-0.3g/cm2Floor tile.
The invention has the benefit that
Wear-resisting luminous resin glue according to the present invention not only has good luminescent properties, also with excellent resistance to
Time property and wearability, wear-resisting property can long sustaining, solve glass microballoon on resin gel coating or the micro- sand of glass be easy
The problem of wearing, falling off.
The preparation method of wear-resisting luminous resin glue according to the present invention, preparation method is simple, and can be sent out
Light powder, glass microballoon or the micro- sand of glass are uniformly dispersed, stablize, and are not easy the wear-resisting luminous resin glue precipitated.
Wear-resisting luminous resin glue according to the present invention is used to prepare the application of luminous brick, prepares resulting luminous brick and has both hair
Light and wear-resisting service performance, compared to directly spilling wear-resistant material paving and on luminous glue-line, luminous brick surface is smooth, not shadow
Normal walking is rung, and Acceptable life greatly prolongs.The wear-resisting luminous resin glue is coated on floor tile using gluing process
On, it can guarantee wear-resisting luminous resin glue uniform levelling on floor tile, high uniformity, and then guarantee luminous brick obtained
Luminescent properties are consistent with each position of wear-resisting property, reduce the wear-resisting luminescent coating internal stress, prolong the service life.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Embodiment 1
Wear-resisting luminous resin glue includes: in parts by weight
100 parts of carbamide resins,
100 parts of luminescent powders, partial size are 200 mesh,
30 parts of glass microballoons or the micro- sand of glass, partial size are 180 mesh,
66 parts of aliphatic polymeric isocyanate curing agent, and
10 parts of auxiliary agents；
The auxiliary agent includes defoaming agent, drier, ultraviolet absorbing agent, coupling agent and polyamide wax, the weight of the above auxiliary agent
Amount is than being 0.4:0.25:0.4:1.6:1.4.
The preparation method of the wear-resisting luminous resin glue, comprising the following steps:
(1) polyamide wax is added into carbamide resin while stirring with the revolving speed of 700r/min, is extremely stirred within stirring 6 minutes
Uniformly, mixed raw material is obtained；
(2) glass microballoon or the micro- sand of glass, luminescent powder are added in the mixed raw material obtained to step (1), with 3000r/min
Revolving speed stir 25 minutes to stirring evenly, obtain mixed raw material；
(3) defoaming agent, ultraviolet absorbing agent, coupling agent, drier are added into the obtained mixed raw material of step (2),
8 minutes are stirred to stirring evenly with the revolving speed of 800r/min, obtain mixed raw material；
(4) curing agent is added in the mixed raw material obtained to step (3) and stirs 4 minutes extremely with the revolving speed of 400r/min
It stirs evenly, luminous resin glue can be obtained.
The wear-resisting luminous resin glue is used to prepare the application of luminous brick, and the wear-resisting luminous resin glue passes through dispensing work
Skill is coated on floor tile, forms wear-resisting luminescent coating, and the rate for dispensing glue is 40g/ seconds, controls the wear-resisting luminous resin glue
Coated weight be 0.24g/cm2Floor tile；
Then it is toasted 28 minutes at 35 DEG C, the luminous brick is made.
Embodiment 2
Wear-resisting luminous resin glue includes: in parts by weight
80 parts of carbamide resins,
110 parts of luminescent powders, partial size 80, mesh,
10 parts of glass microballoons or the micro- sand of glass, partial size are 200 mesh
80 parts of aliphatic polymeric isocyanate curing agent, and
5 parts of auxiliary agents；
The auxiliary agent includes defoaming agent, drier, ultraviolet absorbing agent, coupling agent and polyamide wax, the weight of the above auxiliary agent
Amount is than being 0.5:0.1:0.5:1.3:1.6.
The preparation method of the wear-resisting luminous resin glue, comprising the following steps:
(1) polyamide wax is added into carbamide resin while stirring with the revolving speed of 500r/min, is extremely stirred within stirring 8 minutes
Uniformly, mixed raw material is obtained；
(2) glass microballoon or the micro- sand of glass, luminescent powder are added in the mixed raw material obtained to step (1), with 2000r/min
Revolving speed stir 30 minutes to stirring evenly, obtain mixed raw material；
(3) defoaming agent, ultraviolet absorbing agent, coupling agent, drier are added into the obtained mixed raw material of step (2),
10 minutes are stirred to stirring evenly with the revolving speed of 500r/min, obtain mixed raw material；
(4) curing agent is added in the mixed raw material obtained to step (3) and stirs 5 minutes extremely with the revolving speed of 300r/min
It stirs evenly, luminous resin glue can be obtained.
The wear-resisting luminous resin glue is used to prepare the application of luminous brick, and the wear-resisting luminous resin glue passes through dispensing work
Skill is coated on floor tile, forms wear-resisting luminescent coating, and the rate for dispensing glue is 35g/ seconds, controls the wear-resisting luminous resin glue
Coated weight be 0.3g/cm2Floor tile；
Then it is toasted 40 minutes at 30 DEG C, the luminous brick is made.
Embodiment 3
Wear-resisting luminous resin glue includes: in parts by weight
120 parts of carbamide resins,
90 parts of luminescent powders, partial size are 300 mesh,
50 parts of glass microballoons or the micro- sand of glass, partial size are 50 mesh,
60 parts of aliphatic polymeric isocyanate curing agent, and
15 parts of auxiliary agents；
The auxiliary agent includes defoaming agent, drier, ultraviolet absorbing agent, coupling agent and polyamide wax, the weight of the above auxiliary agent
Amount is than being 0.3:0.35:0.3:1.8:1.2.
The preparation method of the wear-resisting luminous resin glue the following steps are included:
(1) polyamide wax is added into carbamide resin while stirring with the revolving speed of 1000r/min, stirring 5 minutes to stirring
It mixes uniformly, obtains mixed raw material；
(2) glass microballoon or the micro- sand of glass, luminescent powder are added in the mixed raw material obtained to step (1), with 5000r/min
Revolving speed stir 20 minutes to stirring evenly, obtain mixed raw material；
(3) defoaming agent, ultraviolet absorbing agent, coupling agent, drier are added into the obtained mixed raw material of step (2),
5 minutes are stirred to stirring evenly with the revolving speed of 1000r/min, obtain mixed raw material；
(4) curing agent is added in the mixed raw material obtained to step (3) and stirs 3 minutes extremely with the revolving speed of 500r/min
It stirs evenly, luminous resin glue can be obtained.
The wear-resisting luminous resin glue is used to prepare the application of luminous brick, and the wear-resisting luminous resin glue passes through dispensing work
Skill is coated on floor tile, forms wear-resisting luminescent coating, and the rate for dispensing glue is 43g/ seconds, controls the wear-resisting luminous resin glue
Coated weight be 0.2g/cm2Floor tile；
Then it is toasted 20 minutes at 40 DEG C, the luminous brick is made.
Experimental example
Carry out wearability, luminescent properties test and other pavement brick correlations of luminous brick made from above embodiments 1-3
It can test, the mean values parameter of performance test is as shown in table 1.Comparative example does not change the wear-resisting Luminous tree in embodiment 1-3
Other weight of rouge glue form, for directly by abrasion resistant particles component glass microballoon therein or the micro- sand of glass respectively directly paving spill in
The performance test mean values parameter of the luminous brick obtained in the brick layer of luminous resin glue-line has been set.Partial properties examination criteria
With method according to GB28635-2012 " concrete road pavement brick " and GB6566-2010 " radioactive material radionuclides limitation ".
Table 1
As can be seen from Table 1, under other technological parameters and the identical situation of raw material components, the embodiment of the present application 1-3 system
The various performance parameters especially wear-resisting property of the luminous brick obtained, which is significantly better than that directly to spread wear resistant components, to be spilt in luminous glue-line
The luminous brick on upper system ground, optical property is also more stable, and has to mechanical properties such as the compression strength of the luminous brick and obviously change
It is kind, the compound Cc50 standard of luminous brick compression strength obtained.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of wear-resisting luminous resin glue, which is characterized in that the wear-resisting luminous resin glue includes: in parts by weight
80-120 parts of carbamide resins,
90-110 parts of luminescent powders,
10-50 parts of glass microballoons or the micro- sand of glass,
60-80 parts of curing agent, and
5-15 parts of auxiliary agents；
The auxiliary agent includes defoaming agent, drier, ultraviolet absorbing agent, coupling agent and polyamide wax, the weight ratio of the above auxiliary agent
For 0.3-0.5:0.1-0.35:0.3-0.5:1.3-1.8:1.2-1.6.
2. wear-resisting luminous resin glue according to claim 1, which is characterized in that the curing agent is aliphatic poly isocyanic acid
Ester curing agent.
3. wear-resisting luminous resin glue according to claim 1, which is characterized in that the partial size of the luminescent powder is 80-300
Mesh.
4. wear-resisting luminous resin glue according to claim 1, which is characterized in that the grain of the glass microballoon or the micro- sand of glass
Diameter is 50-200 mesh.
5. the preparation method of wear-resisting luminous resin glue described in claim 1, which comprises the following steps:
(1) polyamide wax is added into carbamide resin while stirring, is stirred evenly, obtain mixed raw material；
(2) glass microballoon or the micro- sand of glass, luminescent powder are added in the mixed raw material obtained to step (1), stirs evenly；
(3) defoaming agent, ultraviolet absorbing agent, coupling agent, drier are added in the mixed raw material obtained to step (2), stirring is equal
It is even；
(4) curing agent is added in the mixed raw material obtained to step (3) to stir evenly, the wear-resisting luminous resin glue is made.
6. the preparation method of wear-resisting luminous resin glue according to claim 5, which is characterized in that in the step (2),
It is stirred 20-30 minutes with the revolving speed of >=2000r/min.
7. the application that wear-resisting luminous resin glue described in claim 1 is used to prepare luminous brick, which is characterized in that will be described wear-resisting
Luminous resin glue is coated on floor tile, is formed wear-resisting luminescent coating, is then toasted, the luminous brick is made.
8. the application that wear-resisting luminous resin glue according to claim 7 is used to prepare luminous brick, which is characterized in that with 35-
The wear-resisting luminous resin glue point glue is coated on floor tile by 43g/ seconds dispensing rates.
9. the application that wear-resisting luminous resin glue according to claim 7 is used to prepare luminous brick, which is characterized in that in 30-
40 DEG C baking 20-40 minutes.
10. the application that wear-resisting luminous resin glue according to claim 7 is used to prepare luminous brick, which is characterized in that described
The coated weight of wear-resisting luminous resin glue is 0.2-0.3g/cm2Floor tile.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710414758.3A CN109233403B (en) | 2017-06-05 | 2017-06-05 | Wear-resistant luminescent resin adhesive, and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710414758.3A CN109233403B (en) | 2017-06-05 | 2017-06-05 | Wear-resistant luminescent resin adhesive, and preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109233403A true CN109233403A (en) | 2019-01-18 |
| CN109233403B CN109233403B (en) | 2021-08-03 |
Family
ID=65082557
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710414758.3A Active CN109233403B (en) | 2017-06-05 | 2017-06-05 | Wear-resistant luminescent resin adhesive, and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113604129A (en) * | 2021-07-27 | 2021-11-05 | 苏州地枢新材料科技有限公司 | High-strength and convenient-to-maintain light-emitting floor tile |
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| CN101298537A (en) * | 2008-07-01 | 2008-11-05 | 中山市三和气雾有限公司 | UV intimating super-antiwear floor paint |
| CN101638547A (en) * | 2009-08-29 | 2010-02-03 | 山东斯泰普力高新建材有限公司 | Water-based energy storage luminescence floor coating and preparation method thereof |
| CN104497824A (en) * | 2014-12-30 | 2015-04-08 | 深圳市嘉达高科产业发展有限公司 | Polyurea floor coating and preparation and application methods thereof as well as carbamide resin |
| CN106758686A (en) * | 2017-03-02 | 2017-05-31 | 周抒函 | A kind of outdoor energy-accumulating luminous crystal floor tile |
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2017
- 2017-06-05 CN CN201710414758.3A patent/CN109233403B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101298537A (en) * | 2008-07-01 | 2008-11-05 | 中山市三和气雾有限公司 | UV intimating super-antiwear floor paint |
| CN101638547A (en) * | 2009-08-29 | 2010-02-03 | 山东斯泰普力高新建材有限公司 | Water-based energy storage luminescence floor coating and preparation method thereof |
| CN104497824A (en) * | 2014-12-30 | 2015-04-08 | 深圳市嘉达高科产业发展有限公司 | Polyurea floor coating and preparation and application methods thereof as well as carbamide resin |
| CN106758686A (en) * | 2017-03-02 | 2017-05-31 | 周抒函 | A kind of outdoor energy-accumulating luminous crystal floor tile |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113604129A (en) * | 2021-07-27 | 2021-11-05 | 苏州地枢新材料科技有限公司 | High-strength and convenient-to-maintain light-emitting floor tile |
| CN113604129B (en) * | 2021-07-27 | 2022-08-26 | 苏州地枢新材料科技有限公司 | High-strength and convenient-to-maintain light-emitting floor tile |
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| Publication number | Publication date |
|---|---|
| CN109233403B (en) | 2021-08-03 |
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