CN109232194A - A kind of extracting method of fresh fruit medicinal material content - Google Patents
A kind of extracting method of fresh fruit medicinal material content Download PDFInfo
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- CN109232194A CN109232194A CN201811232839.2A CN201811232839A CN109232194A CN 109232194 A CN109232194 A CN 109232194A CN 201811232839 A CN201811232839 A CN 201811232839A CN 109232194 A CN109232194 A CN 109232194A
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
- C07D311/60—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2
- C07D311/62—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2 with oxygen atoms directly attached in position 3, e.g. anthocyanidins
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/004—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from plant material or from animal material
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of extracting methods of fresh fruit medicinal material content, comprising the following steps: rinses fresh fruit, once rubs juice, first separation is primary to filter, and once fills juice, secondary to rub juice, secondary filter, secondary filling juice, the extraction of content.The present invention uses a kind of above-mentioned extracting method of fresh fruit medicinal material content, and extracting method is simple and practical, without heating, saves the energy, and raw material will not be destroyed, and be reduced costs.
Description
Technical field
The present invention relates to anthocyanidin and resveratrol extractive technique field, more particularly, to a kind of fresh fruit medicinal material content
Extracting method.
Background technique
Since the nineties, domestic and international scientific researcher discovery, and announce on publication, procyanidine and white black false hellebore
Alcohol is widely present in fruit.Resveratrol exists in the form of free state and two kinds of glucosides under field conditions (factors), white black false hellebore
The chemical structure of alcohol and its glucosides is also respectively present two kinds of isomers of cis and trans, i.e. cis-resveratrol, trans- white black false hellebore
Alcohol and cis-resveratrol glucosides, trans-resveratrol glucosides.Latter two form releases under glucosides enzyme effect in enteron aisle
Resveratrol, resveratrol mainly exists with trans forms in plant, research shows that the physiological activity of transisomer be better than it is suitable
Formula isomers.But from the point of view of document report situation, most study at present, only grape, the peanut etc. being most concerned a few
The Chinese medicines such as edible plant and polygonum cuspidate.Some resveratrols are extracted from the natural plant resources such as Grape Skin, seed
It arrives.But the plantation of natural plants occupies a large amount of arable lands, be easy to cause soil erosion and the deterioration of the ecological environment；It is used in planting process
Pesticide, chemical fertilizer can be remained in extract, directly affect the safety of product；While the Resveratrol content in plant is very
It is low, lead to extraction purification high expensive；Because plant growth is affected by environment larger, the content of resveratrol is unstable, causes to mention
Take the unstable product quality of acquisition.
The white Chenopodiaceae that natural resveratrol is mostly extracted to obtain, but extracted from polygonum cuspidate with Chinese medicine polygonum cuspidate (root) for raw material at present
There is rheum emodin toxicity in reed alcohol, simultaneously because the market prospects that resveratrol is tempting, all over the world all in contention polygonum cuspidate
Resource, it is anticipated that in the near future, polygonum cuspidate resource will face atrophy, cause the serious situation that source is striven with medicine.Therefore, resource is asked
Topic will be the huge obstacle for restricting resveratrol industry development.Traditional heating and refluxing extraction method is mostly used both at home and abroad at present,
Such circumfluence method extracting solution heated time in evaporation boiler is longer, therefore is not suitable for the leaching of heated easily destroyed material composition
Out, return time is long, and technique is relative complex.
Summary of the invention
The object of the present invention is to provide a kind of extracting methods of fresh fruit medicinal material content, and extracting method is simple and practical, is not necessarily to
Heating, saves the energy, and raw material will not be destroyed, and be reduced costs.
To achieve the above object, the present invention provides a kind of extracting methods of fresh fruit medicinal material content, comprising the following steps:
A, rinse fresh fruit: fresh fruit is poured into the first container, manually selects impurity removal leaf and sundries by the fresh fruit in selection medicinal material,
Then water is outwelled after being rinsed twice with clear water；
B, it once rubs juice: wearing Rubber gloves, the fresh fruit in the first container is rubbed into juice with hand, to the fresh fruit in the first container
Until equal juice, there are fresh juice, seed and carpopodium in the first container at this time；
C, first separation: selecting out the carpopodium and part fruit seed in the first container, put it into big basin, and first holds at this time
It is left fresh juice and fruit seed in device；
D, primary filtering: above-mentioned fresh juice and fruit seed are slowly poured into the magma cylinder for being placed with filter screen, and filter screen is by fruit seed
It filters out and stays on strainer, fresh juice flows into magma cylinder and obtains magma fruit juice, then removes the strainer with fruit seed and is poured on fruit seed
It is dried on ground, it is spare, then gaze scrubbing is completely put on the filter screen of magma cylinder；
E, it once fills juice: the magma fruit juice in magma cylinder is poured into the first glue bucket got ready；
F, secondary to rub juice: clear water will be added in second container, then carpopodium and part fruit seed are put into second container,
Rub carpopodium and part fruit seed with hand, to the pulp on clear clean carpopodium until, select out carpopodium, remaining fruit in second container at this time
Slurry and fruit seed are stand-by；
G, secondary filter: by above-mentioned second container pulp and fruit seed slowly pour into and be placed with the secondary slurry cylinder of filter screen
In, filter screen stays in fruit seed on strainer, and pulp is flowed into secondary slurry cylinder and obtains secondary berry juice, then will have fruit seed
Strainer is removed dries fruit seed on the ground, spare, is then put into filter mesh sieve wash clean on the filter screen of secondary slurry cylinder；
H, secondary filling juice: the secondary berry juice in secondary slurry cylinder is poured into the second glue bucket got ready；
I, the extraction of content: out of in the secondary berry juice in the magma fruit juice and the second glue bucket in the first glue bucket extract
Inclusion, the content include anthocyanidin, resveratrol, ribosome inactivating protein, plant polypeptide, plant polyose, esculentoside,
16 kinds of amino acid and multivitamin.
Preferably, the first container in the step A is tub or glue basin.
Preferably, prepare filter screen in the step D, the strainer got ready is placed on sieve, as filter screen, then will
Filter screen is placed on magma cylinder for use.
Preferably, the capacity of the first glue bucket is 50L in the step E.
Preferably, in the step F second container clear water additional amount be the second container one third.
Preferably, prepare filter screen in the step G, the strainer got ready is placed on sieve, as filter screen, then will
Filter screen is placed on secondary slurry cylinder for use.
Preferably, the capacity of the second glue bucket is 50L in the step H.
Resveratrol is a kind of natural antioxidant, can reduce blood viscosity, and coagulating platelets and blood vessel is inhibited to relax
, keep unobstructed blood, can pre- anti-cancer generation and development, have antiatherosclerosis and coronary heart disease, ischemic heart
Disease, the preventive and therapeutic effect of hyperlipidemia.Inhibiting the effect of tumour also has estrogen-like action, can be used for treating the diseases such as breast cancer.
Therapeutic efficiency is played by a variety of different approach, there is certain antipyretic and analgesic activity.Trans-resveratrol and cis- white
Veratryl alcohol all has anticancer activity, the reason is that they can inhibit the activity of proteintyrosine kinase.Resveratrol is expected
As the inhibitor of tyrosine protein kinase PTK, many medical researches discovery resveratrols are to breast cancer, gastric cancer, colon cancer, preceding
The Several Kinds of Malignancy such as column gland cancer, leukaemia, oophoroma, cutaneum carcinoma cell has apparent inhibiting effect.
Resveratrol is mainly from the following aspects plays antiatherosclerosis, prevention and treatment of coronary heart disease to angiocarpy
To protective effect: adjusting blood lipid；Inhibit platelet aggregation, promotes fibrinolysis, anti-thrombosis function；It protects intravascular
Skin, inhibition of endothelial cell proliferation；Vascular smooth machine cell is protected, its proliferation is inhibited；Anti- leucocyte effect；Antagonism endothelin -1 is made
With；The function of anti-LDL oxidation.Resveratrol and its derivative are the more a kind of phytoalexin of research, the heart
Vascular protection effect gradually becomes research hotspot, it is expected to be made in terms of the drug development for preventing and treating cardiovascular disease
For, but its mechanism of action is clear far away, needs further to be furtherd investigate.
Resveratrol is the natural being present in plant, main by removing or free radical being inhibited to generate, suppression
Lipid peroxidation processed adjusts the mechanisms plays antioxidations such as anti-oxidant related enzyme activity.Resveratrol substance mostly has
Anti-oxidant, anti-radical action.When resveratrol is in 1.3 μ g/mL, can obviously inhibit red blood cell autoxidation haemolysis and by
H2O2Caused oxidative hemolysis, the anti-oxidant of resveratrol lure the pharmacological function except free radical and influence arachidonic acid metabolic to draw
The broad interest of people is played, because these physiological metabolisms are related to many physiological maladies closely related with human health, example
Such as atherosclerosis, senile dementia, virus hepatitis, gastric ulcer, inflammation and allergic reaction.
Anthocyanidin is a kind of water colo(u)r, can change color with the soda acid of cell liquid.Cell liquid is in acid then inclined
Red, cell liquid is then partially blue in alkalinity.Anthocyanidin is to constitute one of petal and the primary pigments of fruit color.Anthocyanidin is plant two
Grade metabolite, is physiologically playing the part of important role.The color of petal and fruit can attract animal to carry out pollination and seed biography
It broadcasts.Be common in flower, fruit tissue in and cauline leaf epidermal cell and underlying epidermis layer.Part fruit determines fruit with shade
The market price.Also have in purple vegetables.Anthocyanidin is also known as anthocyanidin, and it is water-soluble in plant to be that nature one kind is widely present in
Property natural pigment, belong to flavonoids.It is also the main color-generation substance in plant petals, the five colours such as water fruits and vegetables, flowers are in riotous profusion
Confused color is largely associated therewith.Anthocyanidin is present in the vacuole of plant cell, can be transformed by chlorophyll.In plant
Under the different pH value condition of Cell vacuoles, make petal that multicoloured color be presented.Autumn soluble sugar increases, and cell is acidity,
It takes on a red color in acid condition or purple, so petal is anthocyanidin effect in red, purple, the depth of color and anthocyanidin
Being positively correlated property of content can quickly be measured with spectrophotometer, blue under alkaline condition.
Pigment used in food industry is mostly synthetic dyestuff at present, nearly all there is different degrees of toxicity, is used for a long time
The health of people can be endangered, therefore natural pigment just increasingly causes the concern of scientific research field, due on domestic market so far also
There is no anthocyanidin sterling, so the anthocyanidin of extraction high-purity provides indispensability with exploitation to the further investigation of anthocyanin class pigment
Characterization condition and theoretical foundation, and facilitate its industrial utilization.Due to there is no market to occur anthocyanidin sterling not yet, because
This needs to take in anthocyanidin, then can only for example eat blueberry, strawberry, grape, Qarnet rice etc. by way of tonic at present
It obtains.
Anthocyanidin helps to prevent a variety of diseases related with free radical, including cancer, heart disease, excessively presenility and joint
It is scorching；The generation of heart disease and stroke is reduced by preventing platelet aggregation caused by stress reaction and smoking；Enhance siberian crabapple
System ability resists carcinogen；It reduces the number of flu and shortens the duration；Has the function of anti-mutation to reduce cause
The formation of the cancer factor；With anti-inflammatory efficacy, thus the inflammation including arthritis and swelling can be prevented；Alleviate pollinosis and
Other allergy；Enhance artery, vein and capillary elasticity；Protect arteries inner wall；Keep the flexible of orthocytosis
Property to help erythrocyte by tiny capillary, therefore enhance the blood circulation of whole body, for body various pieces
Organ and system bring direct benefit, and enhance cell viability；Anthocyanidin can promote the visual purple in retina cell
Regeneration, pre- myopia prevention promote eyesight.
Therefore, a kind of extracting method of the fresh fruit medicinal material content of the present invention using the above structure, extracting method are simply real
With, without heating, save the energy, and raw material will not be destroyed, and be reduced costs.
Below by embodiment, technical scheme of the present invention will be described in further detail.
Specific embodiment
Embodiment
The present invention provides a kind of extracting methods of fresh fruit medicinal material content, comprising the following steps:
A, rinse fresh fruit: the fresh fruit in selection medicinal material pours into fresh fruit in the first container, and the first container is tub or glue
Basin manually selects impurity removal leaf and sundries, outwells water after then being rinsed twice with clear water；
B, it once rubs juice: wearing Rubber gloves, the fresh fruit in the first container is rubbed into juice with hand, to the fresh fruit in the first container
Until equal juice, there are fresh juice, seed and carpopodium in the first container at this time；
C, first separation: selecting out the carpopodium and part fruit seed in the first container, put it into big basin, and first holds at this time
It is left fresh juice and fruit seed in device；
D, primary filtering: prepare filter screen, the strainer got ready is placed on sieve, as filter screen, then by filter screen
It is placed on magma cylinder for use, above-mentioned fresh juice and fruit seed is slowly poured into the magma cylinder for being placed with filter screen, filter screen filters fruit seed
It stays on strainer out, fresh juice flows into magma cylinder and obtains magma fruit juice, then removes the strainer with fruit seed and is poured on ground for fruit seed
It is dried on face, it is spare, then gaze scrubbing is completely put on the filter screen of magma cylinder；
E, it once fills juice: the magma fruit juice in magma cylinder is poured into the first glue bucket got ready, the capacity of the first glue bucket is
50L；
F, secondary to rub juice: clear water will to be added in second container, the clear water additional amount of second container is the second container
Then carpopodium and part fruit seed are put into second container by one third, rub carpopodium and part fruit seed with hand, to clear clean
Until pulp on carpopodium, carpopodium is selected out at this time, is left pulp in second container and fruit seed is stand-by；
G, secondary filter: prepare filter screen, the strainer got ready is placed on sieve, as filter screen, then by filter screen
Be placed on secondary slurry cylinder it is stand-by, by above-mentioned second container pulp and fruit seed slowly pour into and be placed with the secondary slurry cylinder of filter screen
In, filter screen stays in fruit seed on strainer, and pulp is flowed into secondary slurry cylinder and obtains secondary berry juice, then will have fruit seed
Strainer is removed dries fruit seed on the ground, spare, is then put into filter mesh sieve wash clean on the filter screen of secondary slurry cylinder；
H, secondary filling juice: the secondary berry juice in secondary slurry cylinder is poured into the second glue bucket got ready, the appearance of the second glue bucket
Amount is 50L；
I, the extraction of content: out of in the secondary berry juice in the magma fruit juice and the second glue bucket in the first glue bucket extract
Inclusion, the content include anthocyanidin, resveratrol, ribosome inactivating protein, plant polypeptide, plant polyose, esculentoside,
16 kinds of amino acid and multivitamin.
Therefore, the present invention uses a kind of above-mentioned extracting method of fresh fruit medicinal material content, and extracting method is simple and practical, is not necessarily to
Heating, saves the energy, and raw material will not be destroyed, and be reduced costs.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than is limited,
Although the present invention is described in detail with reference to preferred embodiments, those skilled in the art should understand that: its according to
So can be with modification or equivalent replacement of the technical solution of the present invention are made, and these modifications or equivalent replacement cannot also make to repair
Technical solution after changing is detached from the spirit and scope of technical solution of the present invention.
Claims (7)
1. a kind of extracting method of fresh fruit medicinal material content, which comprises the following steps:
A, rinse fresh fruit: fresh fruit is poured into the first container, manually selects impurity removal leaf and sundries, then by the fresh fruit in selection medicinal material
Water is outwelled after being rinsed twice with clear water；
B, it once rubs juice: wearing Rubber gloves, the fresh fruit in the first container is rubbed into juice with hand, is gone out to the fresh fruit in the first container
Until juice, there are fresh juice, seed and carpopodium in the first container at this time；
C, first separation: the carpopodium and part fruit seed in the first container are selected out, is put it into big basin, at this time in the first container
It is left fresh juice and fruit seed；
D, primary filtering: above-mentioned fresh juice and fruit seed are slowly poured into the magma cylinder for being placed with filter screen, filter screen filters out fruit seed
It stays on strainer, fresh juice flows into magma cylinder and obtains magma fruit juice, then removes the strainer with fruit seed fruit seed being poured on ground
Upper sunning, it is spare, then gaze scrubbing is completely put on the filter screen of magma cylinder；
E, it once fills juice: the magma fruit juice in magma cylinder is poured into the first glue bucket got ready；
F, secondary to rub juice: clear water will be added in second container, then carpopodium and part fruit seed are put into second container, use hand
Rub carpopodium and part fruit seed, to the pulp on clear clean carpopodium until, select out carpopodium at this time, be left in second container pulp with
Fruit seed is stand-by；
G, secondary filter: by above-mentioned second container pulp and fruit seed slowly pour into the secondary slurry cylinder for being placed with filter screen, mistake
Screen stays in fruit seed on strainer, and pulp is flowed into secondary slurry cylinder and obtains secondary berry juice, then will have the strainer of fruit seed
It removes and dries fruit seed on the ground, it is spare, then filter mesh sieve wash clean is put on the filter screen of secondary slurry cylinder；
H, secondary filling juice: the secondary berry juice in secondary slurry cylinder is poured into the second glue bucket got ready；
I, it the extraction of content: extracts and includes from the secondary berry juice in the magma fruit juice and the second glue bucket in the first glue bucket
Object, the content include anthocyanidin, resveratrol, ribosome inactivating protein, plant polypeptide, plant polyose, esculentoside, 16
Kind amino acid and multivitamin.
2. a kind of extracting method of fresh fruit medicinal material content according to claim 1, it is characterised in that: in the step A
The first container be tub or glue basin.
3. a kind of extracting method of fresh fruit medicinal material content according to claim 1, it is characterised in that: in the step D
Prepare filter screen, the strainer got ready is placed on sieve, as filter screen, is then placed on filter screen on magma cylinder for use.
4. a kind of extracting method of fresh fruit medicinal material content according to claim 1, it is characterised in that: in the step E
The capacity of first glue bucket is 50L.
5. a kind of extracting method of fresh fruit medicinal material content according to claim 1, it is characterised in that: in the step F
The clear water additional amount of second container is the one third of the second container.
6. a kind of extracting method of fresh fruit medicinal material content according to claim 1, it is characterised in that: in the step G
Prepare filter screen, the strainer got ready is placed on sieve, as filter screen, is then placed on filter screen on secondary slurry cylinder for use.
7. a kind of extracting method of fresh fruit medicinal material content according to claim 1, it is characterised in that: in the step H
The capacity of second glue bucket is 50L.
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| CN201811232839.2A CN109232194A (en) | 2018-10-23 | 2018-10-23 | A kind of extracting method of fresh fruit medicinal material content |
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| CN201811232839.2A CN109232194A (en) | 2018-10-23 | 2018-10-23 | A kind of extracting method of fresh fruit medicinal material content |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104738749A (en) * | 2015-04-10 | 2015-07-01 | 唐海明 | Preparation method of pure natural nutritional immune health fruit juice |
| CN107683989A (en) * | 2017-10-24 | 2018-02-13 | 田东县八闽农业综合开发有限公司 | mango dragon fruit composite beverage |
| CN107691935A (en) * | 2017-09-29 | 2018-02-16 | 芜湖绿而优农业科技有限公司 | A kind of fruit drink and preparation method thereof |
-
2018
- 2018-10-23 CN CN201811232839.2A patent/CN109232194A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104738749A (en) * | 2015-04-10 | 2015-07-01 | 唐海明 | Preparation method of pure natural nutritional immune health fruit juice |
| CN107691935A (en) * | 2017-09-29 | 2018-02-16 | 芜湖绿而优农业科技有限公司 | A kind of fruit drink and preparation method thereof |
| CN107683989A (en) * | 2017-10-24 | 2018-02-13 | 田东县八闽农业综合开发有限公司 | mango dragon fruit composite beverage |
Non-Patent Citations (1)
| Title |
|---|
| 石相红等: "樱桃汁的制备", 《农产品加工》 * |
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