CN109221258A - Chinese traditional medicine composition insecticide and preparation method thereof containing Digenea simplex and elegant jessamine extract - Google Patents
Chinese traditional medicine composition insecticide and preparation method thereof containing Digenea simplex and elegant jessamine extract Download PDFInfo
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- CN109221258A CN109221258A CN201811160980.6A CN201811160980A CN109221258A CN 109221258 A CN109221258 A CN 109221258A CN 201811160980 A CN201811160980 A CN 201811160980A CN 109221258 A CN109221258 A CN 109221258A
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- 239000000284 extract Substances 0.000 title claims abstract description 54
- 241000649992 Digenea simplex Species 0.000 title claims abstract description 30
- 239000002917 insecticide Substances 0.000 title claims abstract description 28
- 240000006859 Jasminum officinale Species 0.000 title claims abstract description 27
- 235000010254 Jasminum officinale Nutrition 0.000 title claims abstract description 27
- 239000000203 mixture Substances 0.000 title claims abstract description 26
- 239000003814 drug Substances 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 235000007516 Chrysanthemum Nutrition 0.000 claims abstract description 14
- 210000000582 semen Anatomy 0.000 claims abstract description 10
- 235000007871 Chrysanthemum coronarium Nutrition 0.000 claims abstract description 7
- 244000067456 Chrysanthemum coronarium Species 0.000 claims abstract description 7
- 229940048383 pyrethrum extract Drugs 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 239000002904 solvent Substances 0.000 claims description 36
- 238000003756 stirring Methods 0.000 claims description 24
- 239000007788 liquid Substances 0.000 claims description 19
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 18
- 239000000843 powder Substances 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 239000000706 filtrate Substances 0.000 claims description 14
- 241000723353 Chrysanthemum Species 0.000 claims description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 239000006184 cosolvent Substances 0.000 claims description 11
- 230000000740 bleeding effect Effects 0.000 claims description 9
- 239000003995 emulsifying agent Substances 0.000 claims description 9
- 239000003755 preservative agent Substances 0.000 claims description 9
- 230000002335 preservative effect Effects 0.000 claims description 9
- 235000019441 ethanol Nutrition 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000012141 concentrate Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 238000013019 agitation Methods 0.000 claims description 4
- 238000011049 filling Methods 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 3
- 240000006891 Artemisia vulgaris Species 0.000 claims description 3
- 240000006927 Foeniculum vulgare Species 0.000 claims description 3
- 235000004204 Foeniculum vulgare Nutrition 0.000 claims description 3
- 239000000908 ammonium hydroxide Substances 0.000 claims description 3
- 239000000920 calcium hydroxide Substances 0.000 claims description 3
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 3
- 238000009792 diffusion process Methods 0.000 claims description 3
- 230000029087 digestion Effects 0.000 claims description 3
- 238000004090 dissolution Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000007654 immersion Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 3
- 238000011084 recovery Methods 0.000 claims description 3
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical group [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 2
- 241000580923 Acer buergerianum Species 0.000 claims description 2
- 239000001293 FEMA 3089 Substances 0.000 claims description 2
- 210000000481 breast Anatomy 0.000 claims description 2
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 230000000694 effects Effects 0.000 claims description 2
- 239000004302 potassium sorbate Substances 0.000 claims description 2
- 229940069338 potassium sorbate Drugs 0.000 claims description 2
- 235000010241 potassium sorbate Nutrition 0.000 claims description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 2
- VBIIFPGSPJYLRR-UHFFFAOYSA-M Stearyltrimethylammonium chloride Chemical group [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)C VBIIFPGSPJYLRR-UHFFFAOYSA-M 0.000 claims 1
- 229920006266 Vinyl film Polymers 0.000 claims 1
- 239000004615 ingredient Substances 0.000 claims 1
- 241000238631 Hexapoda Species 0.000 abstract description 7
- 101710088194 Dehydrogenase Proteins 0.000 abstract description 5
- 241000607479 Yersinia pestis Species 0.000 abstract description 5
- 230000029058 respiratory gaseous exchange Effects 0.000 abstract description 5
- 230000004936 stimulating effect Effects 0.000 abstract description 5
- 230000015572 biosynthetic process Effects 0.000 abstract description 4
- 238000009395 breeding Methods 0.000 abstract description 4
- 230000001488 breeding effect Effects 0.000 abstract description 4
- 210000003169 central nervous system Anatomy 0.000 abstract description 4
- 230000012447 hatching Effects 0.000 abstract description 4
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 abstract 1
- 241000239290 Araneae Species 0.000 description 5
- 241001046947 Ectropis obliqua Species 0.000 description 5
- 241001124076 Aphididae Species 0.000 description 4
- 241000255967 Helicoverpa zea Species 0.000 description 4
- 241000258937 Hemiptera Species 0.000 description 4
- 241000985245 Spodoptera litura Species 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 210000004894 snout Anatomy 0.000 description 4
- 241000488583 Panonychus ulmi Species 0.000 description 3
- 241000018137 Trialeurodes vaporariorum Species 0.000 description 3
- VLSMHEGGTFMBBZ-UHFFFAOYSA-N alpha-Kainic acid Natural products CC(=C)C1CNC(C(O)=O)C1CC(O)=O VLSMHEGGTFMBBZ-UHFFFAOYSA-N 0.000 description 3
- VLSMHEGGTFMBBZ-OOZYFLPDSA-N kainic acid Chemical compound CC(=C)[C@H]1CN[C@H](C(O)=O)[C@H]1CC(O)=O VLSMHEGGTFMBBZ-OOZYFLPDSA-N 0.000 description 3
- 229950006874 kainic acid Drugs 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 239000000575 pesticide Substances 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 1
- DDXCFDOPXBPUJC-UHFFFAOYSA-N Digeneaside Natural products OCC(C(O)=O)OC1OC(CO)C(O)C(O)C1O DDXCFDOPXBPUJC-UHFFFAOYSA-N 0.000 description 1
- 240000003553 Leptospermum scoparium Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 229930195725 Mannitol Natural products 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 240000004460 Tanacetum coccineum Species 0.000 description 1
- ROVGZAWFACYCSP-MQBLHHJJSA-N [2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-MQBLHHJJSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- AJXBTRZGLDTSST-UHFFFAOYSA-N amino 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)ON AJXBTRZGLDTSST-UHFFFAOYSA-N 0.000 description 1
- 229960003237 betaine Drugs 0.000 description 1
- 230000023852 carbohydrate metabolic process Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 210000000981 epithelium Anatomy 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000003137 locomotive effect Effects 0.000 description 1
- 235000010355 mannitol Nutrition 0.000 description 1
- 239000000594 mannitol Substances 0.000 description 1
- 125000000311 mannosyl group Chemical group C1([C@@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000011321 prophylaxis Methods 0.000 description 1
- 229940015367 pyrethrum Drugs 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/03—Algae
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Biotechnology (AREA)
- Agronomy & Crop Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides a kind of Chinese traditional medicine composition insecticide containing Digenea simplex and elegant jessamine extract, the Chinese traditional medicine composition insecticide active ingredient is calculated by mass percentage by 8%~15% Digenea simplex extract, 5%~10% elegant jessamine extract, 2%~10% pyrethrum extract, 10%~20% crowndaisy chrysanthemum extract, 8%~15% Folium seu Semen Daphniphylli macropodi leaf extract composition, a kind of Chinese traditional medicine composition insecticide preparation method containing Digenea simplex and elegant jessamine extract is provided simultaneously, it is prepared including raw material, the preparation of Chinese traditional medicine composition insecticide and etc., the Chinese traditional medicine composition insecticide is by tagging, benumb insect motion flesh, stimulating central nervous system, it draws up breathing and the formation of dehydrogenase, kill its larva, adult, it draws up harmful egg hatching, control its Population breeding speed, reach pest control purpose.
Description
Technical field
The invention belongs to agriculturals to apply field of pesticides, and in particular to a kind of Chinese medicine group containing Digenea simplex and elegant jessamine extract
Close insecticide and preparation method thereof.
Background technique
The pesticide plant Digenea simplex being currently known is the frond of Rhodomelaceae plant Digenea simplex, and effective component is a kind of nitrogenous
Kainic acid, in addition contain volume mucilaginous substance and sodium glycerinate, mannitol etc.；Work of the kainic acid to Enterozoa
It can be dissolved and be separated its gut epithelium with being, while made to move myoparalysis and paralyse, contain α-kainic acid, allokainic acid,
Digeneaside, that is, mannose group sodium glycerinate, glycine betaine.Insecticidal mechanism is to make pest that pathosis locomotor stimulatory occur, to consume it
Energy benumbs its movement, upsets its glycometabolism, active principle substance is by inhibiting the effect of dehydrogenase in muscle to tissue respiration
There is extremely strong inhibiting effect.
Elegant jessamine, to nocuousness such as scale insect, red spider, white spider, aphid, trialeurodes vaporariorum, snout moth's larva, bollworm, tea geometrid, prodenia lituras
Insect, can be effectively by tagging, benumbing insect motion flesh, stimulating central nervous system, and draw up breathing and the formation of dehydrogenase kill it
Larva, adult, harmful egg hatching of drawing up control its Population breeding speed, reach pest control purpose；
Digenea simplex and elegant jessamine extract combination are prepared into insecticide in prevention and treatment scale insect, red spider, white spider, aphid, white at present
Research still belongs to blank in terms of the harmful insects such as aleyrodid, snout moth's larva, bollworm, tea geometrid, prodenia litura, researches and develops the combined plant source
Insecticide is imperative.
Summary of the invention
The purpose of the present invention is to provide a kind of Chinese traditional medicine composition insecticide containing Digenea simplex and elegant jessamine extract and its preparations
Method has for preventing and treating scale insect, red spider, white spider, aphid, trialeurodes vaporariorum, snout moth's larva, bollworm, tea geometrid, prodenia litura etc.
Evil insect.
Based on object above, the present invention provides a kind of Chinese traditional medicine composition insecticide containing Digenea simplex and elegant jessamine extract, in this
Medicine combination insecticide active ingredient is calculated by mass percentage by 8%~15% Digenea simplex extract, 5%~10% elegant jessamine extract,
2%~10% pyrethrum extract, 10%~20% crowndaisy chrysanthemum extract, 8%~15% Folium seu Semen Daphniphylli macropodi leaf extract composition, remaining component press matter
Measuring percentage calculating includes: solvent A: 10%~30%；Solvent B:20%~40%, cosolvent: 5%~5%, synergist: 0.1%~
3%, emulsifier: 2%~4%, bleeding agent: 2%~4%, diffusant: 1%~3%, preservative: 0.1%~0.2%.
In the above Chinese traditional medicine composition insecticide, the solvent A is 95% ethyl alcohol, and solvent B is turpentine oil, and cosolvent is 99% different
Propyl alcohol, synergist are 99% camphorated oil, and emulsifier is agriculture breast 600#, and bleeding agent is dimethyl trident maple, and diffusant is octadecyl three
Ammonio methacrylate, preservative are potassium sorbate.
And a kind of Chinese traditional medicine composition method for producing insecticide containing Digenea simplex Yu elegant jessamine extract is provided, it includes following step
It is rapid:
(1) prepared by raw material:
A. the preparation of Digenea simplex extract: a certain amount of Digenea simplex cauline leaf dried is taken to crush the coarse powder for 1~1.5mm, by feed liquid
Ionized water is added than 1:4,3h is decocted at 90~95 DEG C, repeatedly once, the concentrate of 1:3 is made as 1 in merging filtrate, concentration
Component is spare；
B. the preparation of elegant jessamine extract: taking the root, stem, leaf of a certain amount of elegant jessamine dried to crush is 30~40 mesh coarse powder, with 3%
NaOH ionized water is impregnated 10h at 50~55 DEG C, is repeated once by solid-liquid ratio 1:3, merging filtrate, with 30% hydrochloric acid tune PH=
6.5, the immersion liquid that 1:3 is made in concentration is spare as 2 components；
C. it the preparation of pyrethrum extract: takes the flower dried and crushed of a certain amount of Dalmatian chrysanthemum for the coarse powder of 40 mesh, is packed into after sieve
It is put into vacuum tank in polythene film bag, normal hexane-ethyl alcohol, pressurization 50MPa pressure leaching 5min, release is added by solid-liquid ratio 1:5
Afterwards, it is filtered to remove filter residue, 1.82% dry powder is made to normal hexane is free of in extract drying by concentration and recovery, then is diluted with T-80
Be made 25% or 50% Dalmatian chrysanthemum paste it is spare as 3 components；
D. the preparation of crowndaisy chrysanthemum extract: taking a certain amount of fennel wormwood artemisia cauline leaf to dry in the shade to crush and be uniformly mixed for the powder of 1mm with bud 1:1,
Press solid-liquid ratio 1:5 digestion 2h at 75 DEG C~90 DEG C of temperature with the milk of lime 5% of PH=11, by leachate with 30% hydrochloric acid tune PH=
6.5, it is spare as 4 components that the medicinal extract for being 1:3 is concentrated under reduced pressure at 40 DEG C；
E. the preparation of Folium seu Semen Daphniphylli macropodi leaf extract: taking a certain amount of Folium seu Semen Daphniphylli macropodi leaf to dry in the shade to crush is 30 mesh coarse powder, is impregnated with 3% ammonium hydroxide
After 5h, with 75% ethyl alcohol solid-liquid ratio 1:6 refluxing extraction 2h, filtrate is recovered by filtration, then mixed with filter residue with 75% ethyl alcohol solid-liquid ratio 1:3
Refluxing extraction 1h, is repeated 2 times, and filtrate merging is recovered by filtration with 30% hydrochloric acid tune PH=6.5 and is concentrated in vacuo my 1:5 at 55 DEG C
Concentrate it is spare as 5 components；
(2) preparation of the Chinese traditional medicine composition insecticide:
Solvent B is uniformly mixed with cosolvent, is added in agitator tank and stirs, 1 component is uniformly mixed with 2 components and uses solvent A dilute
It releases to be added in solvent B and the agitator tank of cosolvent mixed solution and stir, 3 components are uniformly mixed with solvent A, stirring for agitation is added
It mixes in tank, 4 components is uniformly mixed with 5 components to be added in agitator tank after being diluted with solvent A and continue to stir evenly, synergist is used
It is added in agitator tank and stirs after solvent A dissolution, open addition agitator tank with solvent A is molten after emulsifier, bleeding agent, diffusant are mixed
In, it is added, finally stirs evenly molten open in addition agitator tank of preservative solvent A while stirring, it is filling after standing 2h.
In above-mentioned technical proposal, in the step (2), the mixing ratio of solvent B and cosolvent is 3:1,3 components and solvent A
Mixing ratio be 1:3, the mixing ratio of synergist and solvent A is 1:3, emulsifier, bleeding agent, diffusion and solvent A mixing ratio be
The mixing ratio of 1:1, preservative and solvent A is 1:1.
Digenea simplex of the present invention and elegant jessamine extract are by tagging, benumbing insect motion flesh, stimulating central nervous system, breathing of drawing up
And dehydrogenase formation, kill its larva, adult, harmful egg hatching of drawing up controls its Population breeding speed, reaches pest control mesh
's.
Specific embodiment
Below with reference to embodiment, the present invention will be further described, and protection scope of the present invention is not limited to following institute
It states.
(1) raw material is prepared:
The preparation of Digenea simplex extract: it weighs the Digenea simplex cauline leaf dried to crush the coarse powder 100kg for being 1-1.5mm, adds 400kg
Ionized water decocts 3h at 95 DEG C, releases filtrate, adds 200kg ionized water and decocts 3h, merging filtrate, concentration at 90 DEG C
The concentrate that 300kg is made is spare as 1 component；
The preparation of elegant jessamine extract: weighing RADIX GELSEMII, the cauline leaf that 100kg is dried and being sliced crushing is 30-40 mesh coarse powder, uses 3%NaOH
+ ionized water 300kg impregnates 10h at 50 DEG C, releases filtrate, impregnates again at 50 DEG C in addition 3%NaOH+ ionized water 200kg
10h, merging filtrate, with 30% hydrochloric acid tune PH=6.5, the immersion liquid that 300kg is made in concentration is spare as 2 components；
The preparation of pyrethrum extract: it takes the flower dried and crushed of a certain amount of Dalmatian chrysanthemum for the coarse powder of 40 mesh, is packed into poly- second after sieve
It is put into vacuum tank in alkene bag film, normal hexane-ethyl alcohol is added by solid-liquid ratio 1:5, pressurization 50MPa pressure soaks 5min, after release, mistake
Filter residue is filtered out, 1.82% dry powder is made to normal hexane is free of in extract drying by concentration and recovery, then is made of T-80 dilution
25% or 50% Dalmatian chrysanthemum paste is spare as 3 components；
The preparation of crowndaisy chrysanthemum extract: it takes a certain amount of fennel wormwood artemisia cauline leaf to dry in the shade to crush and is uniformly mixed for the powder of 1mm with bud 1:1, used
The milk of lime 5% of PH=11 presses solid-liquid ratio 1:5 digestion 2h at 75 DEG C~90 DEG C of temperature, by 30% hydrochloric acid tune PH=6.5 of leachate,
It is spare as 4 components that the medicinal extract for being 1:3 is concentrated under reduced pressure at 40 DEG C；
The preparation of Folium seu Semen Daphniphylli macropodi leaf extract: taking a certain amount of Folium seu Semen Daphniphylli macropodi leaf to dry in the shade to crush is 30 mesh coarse powder, impregnates 5h with 3% ammonium hydroxide
Afterwards, with 75% ethyl alcohol solid-liquid ratio 1:6 refluxing extraction 2h, filtrate is recovered by filtration, then is mixed back with 75% ethyl alcohol solid-liquid ratio 1:3 with filter residue
Stream extracts 1h, is repeated 2 times, and filtrate merging is recovered by filtration, with 30% hydrochloric acid tune PH=6.5, being concentrated in vacuo my 1:5's at 55 DEG C
Concentrate is spare as 5 components；
Chinese traditional medicine composition insecticide is by 1 component Digenea simplex extract, 2 component elegant jessamine extracts；3 component pyrethrum extracts, 4 groups
Point crowndaisy chrysanthemum extract, 5 component Folium seu Semen Daphniphylli macropodi leaf extracts, 6 component solvent A, 7 component solvent B, 8 component cosolvents, 9 component synergy
Agent, 10 component emulsifiers, 11 component bleeding agents, 12 diffusion of components agent, 13 components of component preservative 13 are formulated.
Embodiment 1
Prepare Chinese traditional medicine composition insecticide, by every 100 parts preparations: by 22.54 parts of 7 component with 8 component 11.26 parts be uniformly mixed, add
Enter in agitator tank and stirs；10 parts of 1 component are uniformly mixed with 8 parts of 2 component the agitator tank that 7 components and 8 component mixed solutions are added
Middle stirring；3 parts of 3 component are uniformly mixed in the agitator tank that agitation is added with 9 parts of 6 component；By 10 parts of 10 parts of 4 component and 5 component
It is added in agitator tank after mixing and continues to stir evenly；1 part of 9 component is stirred in addition agitator tank after 3 parts of 6 component dissolutions
It mixes；Will 2 parts of 10 component, 2 parts of 11 component, 2 parts of 12 component mixing after with 6 parts of 6 component it is molten open addition agitator tank in, while stirring plus
Enter；Finally by 0.1 part of 13 component with 0.1 part of 6 component it is molten open to be added in agitator tank stir evenly, be made 100 parts containing Digenea simplex with
The Chinese traditional medicine composition insecticide of elegant jessamine extract is put into standing tank filling after standing 2h.
Embodiment 2
Chinese traditional medicine composition insecticide is prepared, is prepared by every 100kg: 7 component 20.40kg being uniformly mixed with 8 component 10.2kg, are added
Enter in agitator tank and stirs；1 component 8kg is uniformly mixed with 2 component 5kg in the agitator tank that 7 components and 8 component mixed solutions are added
Stirring；3 component 5kg are uniformly mixed with 6 component 15kg in the agitator tank that agitation is added；4 component 10kg and 5 component 8kg are mixed
It is added in agitator tank after closing uniformly and continues to stir；It is added in agitator tank and stirs after 9 component 0.5kg are dissolved with 6 component 1.5kg；
It is added in agitator tank after 10 component 3kg, 11 component 3kg, 12 component 2kg are mixed with molten open of 6 component 8kg, is added while stirring；
13 component 0.2kg are stirred evenly with molten open in addition agitator tank of 6 component 0.2kg finally, 100kg is made containing Digenea simplex and elegant jessamine
The Chinese traditional medicine composition insecticide of extract is put into standing tank filling after standing 2h.
4 Digenea simplex feeding method of table, drop method are to the control efficiency of tea tree tea geometrid
As can be seen from the above table, insecticide of the present invention containing Digenea simplex Yu elegant jessamine extract combination, for preventing and treating scale insect, red
The harmful insects such as spider, white spider, aphid, trialeurodes vaporariorum, snout moth's larva, bollworm, tea geometrid, prodenia litura, can effectively pass through stomach toxicity,
Tag, benumb insect motion flesh, stimulating central nervous system, its larva, adult are killed in draw up breathing and the formation of dehydrogenase, draw up
Evil egg hatching, controls its Population breeding speed, reaches prophylactic treatment pest purpose.
Claims (4)
1. a kind of Chinese traditional medicine composition insecticide containing Digenea simplex and elegant jessamine extract, which is characterized in that the Chinese traditional medicine composition insecticide has
Effect ingredient is calculated by mass percentage by 8%~15% Digenea simplex extract, 5%~10% elegant jessamine extract, 2%~10% Dalmatian chrysanthemum
Extract, 10%~20% crowndaisy chrysanthemum extract, 8%~15% Folium seu Semen Daphniphylli macropodi leaf extract composition, remaining component are calculated by mass percentage
It include: solvent A: 10%~30%；Solvent B:20%~40%, cosolvent: 5%~5%, synergist: 0.1%~3%, emulsifier: 2%
~4%, bleeding agent: 2%~4%, diffusant: 1%~3%, preservative: 0.1%~0.2%.
2. a kind of Chinese traditional medicine composition insecticide containing Digenea simplex Yu elegant jessamine extract according to claim 1, which is characterized in that
The solvent A is 95% ethyl alcohol, and solvent B is turpentine oil, and cosolvent is 99% isopropanol, and synergist is 99% camphorated oil, emulsifier
For agriculture breast 600#, bleeding agent is dimethyl trident maple, and diffusant is octadecyltrimethylammonium chloride, and preservative is potassium sorbate.
3. a kind of Chinese traditional medicine composition method for producing insecticide containing Digenea simplex Yu elegant jessamine extract according to claim 1,
It is characterized in that, it the following steps are included:
(1) prepared by raw material:
A. the preparation of Digenea simplex extract: a certain amount of Digenea simplex cauline leaf dried is taken to crush the coarse powder for 1~1.5mm, by feed liquid
Ionized water is added than 1:4,3h is decocted at 90~95 DEG C, repeatedly once, the concentrate of 1:3 is made as 1 in merging filtrate, concentration
Component is spare；
B. the preparation of elegant jessamine extract: taking the root, stem, leaf of a certain amount of elegant jessamine dried to crush is 30~40 mesh coarse powder, with 3%
NaOH ionized water is impregnated 10h at 50~55 DEG C, is repeated once by solid-liquid ratio 1:3, merging filtrate, with 30% hydrochloric acid tune PH=
6.5, the immersion liquid that 1:3 is made in concentration is spare as 2 components；
C. the preparation of pyrethrum extract: taking the flower dried and crushed of a certain amount of Dalmatian chrysanthemum for the coarse powder of 40 mesh, is packed into after sieve poly-
It being put into vacuum tank in vinyl film bag, normal hexane-ethyl alcohol is added by solid-liquid ratio 1:5, pressurization 50MPa pressure soaks 5min, after release,
It is filtered to remove filter residue, 1.82% dry powder is made to normal hexane is free of in extract drying by concentration and recovery, then is diluted and made with T-80
It is spare as 3 components at 25% or 50% Dalmatian chrysanthemum paste；
D. the preparation of crowndaisy chrysanthemum extract: taking a certain amount of fennel wormwood artemisia cauline leaf to dry in the shade to crush and be uniformly mixed for the powder of 1mm with bud 1:1,
Press solid-liquid ratio 1:5 digestion 2h at 75 DEG C~90 DEG C of temperature with the milk of lime 5% of PH=11, by leachate with 30% hydrochloric acid tune PH=
6.5, it is spare as 4 components that the medicinal extract for being 1:3 is concentrated under reduced pressure at 40 DEG C；
E. the preparation of Folium seu Semen Daphniphylli macropodi leaf extract: taking a certain amount of Folium seu Semen Daphniphylli macropodi leaf to dry in the shade to crush is 30 mesh coarse powder, is impregnated with 3% ammonium hydroxide
After 5h, with 75% ethyl alcohol solid-liquid ratio 1:6 refluxing extraction 2h, filtrate is recovered by filtration, then mixed with filter residue with 75% ethyl alcohol solid-liquid ratio 1:3
Refluxing extraction 1h, is repeated 2 times, and filtrate merging is recovered by filtration with 30% hydrochloric acid tune PH=6.5 and is concentrated in vacuo my 1:5 at 55 DEG C
Concentrate it is spare as 5 components；
(2) preparation of the Chinese traditional medicine composition insecticide:
Solvent B is uniformly mixed with cosolvent, is added in agitator tank and stirs, 1 component is uniformly mixed with 2 components and uses solvent A dilute
It releases to be added in solvent B and the agitator tank of cosolvent mixed solution and stir, 3 components are uniformly mixed with solvent A, stirring for agitation is added
It mixes in tank, 4 components is uniformly mixed with 5 components to be added in agitator tank after being diluted with solvent A and continue to stir evenly, synergist is used
It is added in agitator tank and stirs after solvent A dissolution, open addition agitator tank with solvent A is molten after emulsifier, bleeding agent, diffusant are mixed
In, it is added, finally stirs evenly molten open in addition agitator tank of preservative solvent A while stirring, it is filling after standing 2h.
4. a kind of Chinese traditional medicine composition method for producing insecticide containing Digenea simplex Yu elegant jessamine extract according to claim 3,
It is characterized in that, in the step (2), the mixing ratio of solvent B and cosolvent is 3:1, and the mixing ratio of 3 components and solvent A is 1:
3, the mixing ratio of synergist and solvent A is 1:3, emulsifier, bleeding agent, diffusion and solvent A mixing ratio be 1:1, preservative with
The mixing ratio of solvent A is 1:1.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2352397A (en) * | 1999-07-27 | 2001-01-31 | Anthony Pisacane | Extraction of materials from plants |
| CN1290484A (en) * | 2000-11-21 | 2001-04-11 | 高林 | High-efficiency non-toxic and residue free plant chemical |
| CN101317586A (en) * | 2007-06-04 | 2008-12-10 | 孙克来 | Environment friendly pesticide for vegetables and preparation thereof |
| CN106719956A (en) * | 2016-12-29 | 2017-05-31 | 山西师范大学 | A kind of environment-friendly type biological insecticide formula and preparation method |
-
2018
- 2018-09-30 CN CN201811160980.6A patent/CN109221258A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2352397A (en) * | 1999-07-27 | 2001-01-31 | Anthony Pisacane | Extraction of materials from plants |
| CN1290484A (en) * | 2000-11-21 | 2001-04-11 | 高林 | High-efficiency non-toxic and residue free plant chemical |
| CN101317586A (en) * | 2007-06-04 | 2008-12-10 | 孙克来 | Environment friendly pesticide for vegetables and preparation thereof |
| CN106719956A (en) * | 2016-12-29 | 2017-05-31 | 山西师范大学 | A kind of environment-friendly type biological insecticide formula and preparation method |
Non-Patent Citations (5)
| Title |
|---|
| TSUNEMATSU TAKEMOTO ET AL.: "Studies on the effective principles of digenea simplex Ag.XII:Stereochemical structures of kainic acid and α-allohainic acid", 《YAKUGAKU ZASSHI JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN》 * |
| 上海市农业技术推广服务中心: "《农药安全使用手册》", 30 September 2009, 上海科学技术出版社 * |
| 中国土农药志编辑委员会: "《中国土农药志》", 31 May 1959, 科学出版社 * |
| 曹挥: "《生物农药及其应用》", 30 September 2006, 中国社会出版社 * |
| 邓家刚: "《广西海洋药物》", 30 September 2008, 广西科学技术出版社 * |
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