CN109172627A - The preparation method of cactus fine powder - Google Patents
The preparation method of cactus fine powder Download PDFInfo
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- CN109172627A CN109172627A CN201811045987.3A CN201811045987A CN109172627A CN 109172627 A CN109172627 A CN 109172627A CN 201811045987 A CN201811045987 A CN 201811045987A CN 109172627 A CN109172627 A CN 109172627A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/33—Cactaceae (Cactus family), e.g. pricklypear or Cereus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/141—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
- A61K9/143—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with inorganic compounds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a kind of preparation methods of cactus fine powder, including the following steps: 1) cactus deburring, cleaning, drying and slice, it is stand-by as raw material；2) raw material is freeze-dried；3) powder after drying is subjected to pulverization process；4) smashed powder is subjected to broken wall treatment；5) broken wall slurries are stood, is centrifugated；6) powder after being centrifugated is freeze-dried, and is packed, is obtained cactus fine powder.The present invention provides a kind of preparation method of cactus fine powder using poly- methylgalactose as promotor is ground, and improves defibrination rate；Using glusulase and glutamine collaboration as broken wall promotor, shell-broken effect is improved, soluble component in raw material is made sufficiently to discharge and be dissolved out, improves extract yield；This preparation method reduces destruction of the temperature to bioactive substance and nutritional ingredient without high temperature drying；Cactus fine powder prepared by the present invention can treat constipation in the short time, effect is lasting, no dependence.
Description
Technical field
The present invention relates to the manufacture fields of bioactive natural products, more particularly to a kind of preparation side of cactus fine powder
Method.
Background technique
Cactus contains 8 kinds of amino acid, organic acid, fiber, multivitamin and microelement etc. needed by human；Simultaneously
Containing various bioactive components, such as: triterpene, flavones, polysaccharide, polyphenol, pigment.Supplementary Amplifications of the Compendium of Materia Medica, " wide in China
Western Chinese herbal medicine ", describe the related data that cactus is used as medicine in the medical books such as " the civil recipe collection in Guizhou ".In Mexico,
Cactus is the plant that often eats of locals, the products such as cactus biscuit, dessert, vegetable tablets, can, tea, fruit wine, beverage with
Locate visible.Cactus not only has nutritive value also with health role, often edible to treat constipation, but cactus contains
Water up to 90%~96%wt, will relatively destroy it after temperature is more than 100 DEG C including protein, this
Outer such as vitamin C, flavones, pigment heat-sensitive ingredients, with temperature gradually rising by room temperature, changes will occur, temperature
Higher loss is more, so not easy to be processed.And it is longer the time required to being dried, thermal sensitivity biology in cactus can be destroyed
Ingredient, temperature is excessively high in the drying process still can destroy part biological ingredient.
Summary of the invention
In view of the above shortcomings, the purpose of the present invention is to provide a kind of preparation methods of cactus fine powder.
Technical solution of the present invention is summarized as follows:
A kind of preparation method of cactus fine powder, wherein include the following steps:
1) cactus deburring, cleaning, drying and slice, it is stand-by as raw material；
2) raw material is placed in freeze drier, carries out 8~12h of freeze-drying, make moisture content 3%~5%；
3) powder after drying is put into pulverizer, is added and crushes promotor progress pulverization process, smashing fineness 200~
300 mesh；
4) smashed powder is put into wall-breaking machine, water and broken wall promotor is added, carried out broken wall treatment, obtain broken wall
Slurries, 1000~1200 mesh of broken wall fineness；
5) broken wall slurries are stood, is centrifugated；
6) powder after being centrifugated is placed in freeze drier, is carried out 6~8h of freeze-drying, is made moisture content <
0.5%, flowable is added, is packed, obtains cactus fine powder.
Preferably, the preparation method of the cactus fine powder, wherein the crushing promotor is poly- methyl gala
Sugar, ratio by mass part meter of poly- methylgalactose is added, raw material: poly- methylgalactose is 100:1~5.
Preferably, the preparation method of the cactus fine powder, wherein in the step 4), powder: water=1:1~
2。
Preferably, the preparation method of the cactus fine powder, wherein in the step 4), broken wall promotor includes
Glusulase, the additional amount of the glusulase are 3~5U/g.
Preferably, the preparation method of the cactus fine powder, wherein in the step 4), broken wall promotor is also wrapped
Glutamine is included, the additional amount of the glutamine is 6~8U/g.
Preferably, the preparation method of the cactus fine powder, wherein in the step 4), the broken wall treatment time is
5h, broken wall temperature are 30~50 DEG C.
Preferably, the preparation method of the cactus fine powder, wherein when the step 5) is centrifugated, centrifugation speed
Degree is 6000rpm/min, centrifugation time 30min.
Preferably, the preparation method of the cactus fine powder, wherein in the step 2) and step 6), freezing is dry
Dry temperature is -30 DEG C~-50 DEG C.
Preferably, the preparation method of the cactus fine powder, wherein the flowable is food grade silicon dioxide,
Ratio by mass part meter of silica is added, powder: silica is 100:0.5~2.
Preferably, the preparation method of the cactus fine powder, wherein the partial size of the cactus fine powder be 500~
800 mesh.
The beneficial effects of the present invention are:
The present invention provides a kind of preparation method of cactus fine powder, passes through in wall-breaking machine handled respectively, improves celestial
People slaps pulp and fiber utilization rate；Using poly- methylgalactose as promotor is ground, defibrination rate is improved；With glusulase and paddy ammonia
Amide collaboration is used as broken wall promotor, improves shell-broken effect, soluble component in raw material is made sufficiently to discharge and be dissolved out, and improves
Extract yield；This preparation method reduces destruction of the temperature to bioactive substance and nutritional ingredient without high temperature drying；This hair
The cactus fine powder of bright preparation can treat constipation in the short time, effect is lasting, no dependence.
Specific embodiment
The present invention will be further described in detail below with reference to the embodiments, to enable those skilled in the art referring to specification
Text can be implemented accordingly.
Embodiment 1:
A kind of preparation method of cactus fine powder, including the following steps:
1) cactus deburring, cleaning, drying and slice, it is stand-by as raw material；
2) raw material is placed in freeze drier, carries out freeze-drying 12h at being -30 DEG C in freeze-drying temperature, it is dry
To moisture 3%~5%；
3) powder after drying is put into pulverizer, poly- methylgalactose is added, the ratio of poly- methylgalactose is added
By weight, raw material: poly- methylgalactose is 100:1, carries out pulverization process, smashing fineness 200-300 mesh；
4) smashed powder is put into wall-breaking machine, water and broken wall promotor is added, carry out broken wall treatment, broken wall treatment
Time is 5h, and broken wall temperature is 30 DEG C, obtains broken wall slurries, broken wall fineness 1000-1200 mesh；Water: powder weight=1:1 is broken
Wall promotor is glusulase and glutamine, and the additional amount of glusulase is 3U/g, and the additional amount of glutamine is 6U/g；
5) broken wall slurries are stood, is centrifugated, centrifugal speed 6000rpm/min, centrifugation time 30min；
6) powder after being centrifugated is placed in freeze drier, and it is dry to carry out freezing at being -30 DEG C in freeze-drying temperature
Dry 8h, it is dry to moisture < 0.5%, food grade silicon dioxide is added, ratio by mass part meter of silica is added, powder:
Silica is 100:0.5, is packed, and the cactus fine powder that partial size is 500~800 mesh is obtained.
Embodiment 2:
A kind of preparation method of cactus fine powder, including the following steps:
1) cactus deburring, cleaning, drying and slice, it is stand-by as raw material；
2) raw material is placed in freeze drier, carries out freeze-drying 9h at being -40 DEG C in freeze-drying temperature, drying is extremely
Moisture 3%~5%；
3) powder after drying is put into pulverizer, poly- methylgalactose is added and carries out pulverization process, smashing fineness 200
~300 mesh, ratio by mass part meter of poly- methylgalactose is added, raw material: poly- methylgalactose is 100:3；
4) smashed powder is put into wall-breaking machine, water and broken wall promotor is added, carried out broken wall treatment, obtain broken wall
Slurries, 1000~1200 mesh of broken wall fineness, powder: water=1:1.5, broken wall promotor include glusulase and glutamine, snail
The additional amount of enzyme is 4U/g, and the additional amount of glutamine is 7U/g；The broken wall treatment time is 5h, and broken wall temperature is 30~50 DEG C；
5) broken wall slurries are stood, is centrifugated, centrifugal speed 6000rpm/min, centrifugation time 30min.
6) powder after being centrifugated is placed in freeze drier, and it is dry to carry out freezing at being -35 DEG C in freeze-drying temperature
Dry 8h, it is dry to moisture < 0.5%, food grade silicon dioxide is added, ratio by mass part meter of silica is added, powder:
Silica is 100:1, is packed, and the cactus fine powder that partial size is 500-800 mesh is obtained.
Embodiment 3:
A kind of preparation method of cactus fine powder, wherein include the following steps:
1) cactus deburring, cleaning, drying and slice, it is stand-by as raw material；
2) raw material is placed in freeze drier, carries out freeze-drying 12h at being -50 DEG C in freeze-drying temperature, it is dry
To moisture 3%~5%；
3) powder after drying is put into pulverizer, poly- methylgalactose is added and carries out pulverization process, smashing fineness 200
~300 mesh, ratio by mass part meter of poly- methylgalactose is added, raw material: poly- methylgalactose is 100:1~5；
4) smashed powder is put into wall-breaking machine, water and broken wall promotor is added, carry out broken wall treatment, broken wall treatment
Time is 5h, and broken wall temperature is 50 DEG C, obtains broken wall slurries, 1000~1200 mesh of broken wall fineness, powder: water=1:2, broken wall promote
It include glusulase and glutamine into agent, the additional amount of glusulase is 5U/g, and the additional amount of glutamine is 8U/g；
5) broken wall slurries are stood, is centrifugated, centrifugal speed 6000rpm/min, centrifugation time 30min；
6) powder after being centrifugated is placed in freeze drier, and it is dry to carry out freezing at being -50 DEG C in freeze-drying temperature
Dry 6h, it is dry to moisture < 0.5%, food grade silicon dioxide is added, ratio by mass part meter of silica is added, powder:
Silica is 100:2, is packed, and the cactus fine powder that partial size is 500~800 mesh is obtained.
1~embodiment of embodiment, 3 testing result is listed below:
Table 1:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Protein (mg/100g) | 880 | 1120 | 1300 |
| Fatty (mg/100g) | 200 | 210 | 225 |
| Total reducing sugar (mg/100g) | 6200 | 6800 | 7100 |
| Threonine (mg/100g) | 17.23 | 17.45 | 17.97 |
| Valine (mg/100g) | 28.22 | 28.78 | 29.06 |
| Methionine (mg/100g) | 8.62 | 9.04 | 9.30 |
| Isoleucine (mg/100g) | 21.45 | 22.02 | 22.19 |
| Leucine (mg/100g) | 32.94 | 34.05 | 36.42 |
| Phenylalanine (mg/100g) | 19.42 | 20.02 | 20.94 |
| Lysine (mg/100g) | 17.07 | 17.29 | 18.28 |
| Histidine (mg/100g) | 20.78 | 21.65 | 23.75 |
| Tryptophan (mg/100g) | 3.65 | 4.09 | 4.98 |
| Vitamin A (mg/100g) | 0.17 | 0.21 | 0.22 |
| Vitamin B1 (mg/100g) | 0.02 | 0.03 | 0.04 |
| Vitamin B2 (mg/100g) | 0.01 | 0.02 | 0.03 |
| Vitamin C (mg/100g) | 15.9 | 19.2 | 20.9 |
| Potassium (mg/100g) | 310.9 | 317.3 | 317.6 |
| Calcium (mg/100g) | 302 | 308 | 310 |
| Magnesium (mg/100g) | 106 | 108 | 110 |
Cactus fine powder of the invention contain leucine, isoleucine, lysine, methionine, phenylalanine, threonine,
Tryptophan, valine, this 8 kinds of amino acid are that human body must be obtained from food and cannot be synthesized in vivo, are called required ammonia
Base acid, as long as there is this 8 kinds of essential amino acids, body can produce various other amino acid, so that it may sustain life and into
In addition to this row growth and development also contains histidine, lysine promotes brain development, is the constituent of liver and gallbladder, can promote
Fat metabolism adjusts pineal body, mammary gland, corpus luteum and ovary, prevents cell degradation；Tryptophan promotes the generation of gastric juice and pancreatic juice；
Phenylalanine participates in eliminating the loss of kidney and bladder function；Methionine participates in composition hemoglobin, tissue and serum, there is promotion spleen
The function of dirty, pancreas and lymph；Threonine certain amino acid that change reach the function of balance；Isoleucine participates in thymus gland, spleen
Dirty and infracerebral gland adjusting and metabolism；Infracerebral gland belongs to general headquarter and acts on Thyreoidine, sexual gland；Leucine effect balance is different bright
Propylhomoserin；Valine acts on corpus luteum, mammary gland and ovary；Protein has the function of synthesized human cell；Fat is intracellular good
Good ergastic substances mainly provide thermal energy, protect internal organ, maintain body temperature, assist the absorption of liposoluble vitamin, and it is each to participate in body
The metabolic activity of aspect；Total reducing sugar has the function of adjusting immune system；Vitamin A maintains normal vision function, safeguards epithelium group
It knits the health of cell and promotes immunoglobulin, facilitate cell Proliferation and growth；Vitamin B1 helps digest, especially carbon
The digestion of hydrate, improve mental status, maintain nerve fiber, muscle, cardiomotility it is normal, when the energy of human body is main
When from carbohydrate, the requirement of vitamin B1 is maximum, and still maintains heart, and nerve and digestive system normal function must
It needs；Vitamin B2 can prevent canker sore；Vitamin C has the function of anti-trip base and reduces cholesterol；Potassium improves heart and brain blood
Pipe；Calcium promotes bone growth；Magnesium promotes cell metabolism.
The application of cactus fine powder obtained by 1 Examples 1 to 3 of test example: according to hospital outpatient case history, caused by screening stomach fire is contained
Constipation patient 600, wherein women 260, male 340, oldest 65 years old, 20 years old the smallest, right before test
The crowd is observed continuously, and records symptom and variation.
Diagnostic criteria: 1. stomach fires are vigorous, there is swelling and aching of gum, halitosis, the easily symptoms such as famine, insomnia, agitation；2. constipation,
There are the symptoms such as defecation is difficult, be hard and dry, bowel frequency reduction, abdominal pain.
Test method: being randomly divided into 4 groups, 450 people of experimental group, 150 people of control group.Experimental group uses Examples 1 to 3 institute
, it takes daily twice, a 5g, warm boiled water；Control group uses other conventional method (Huanglianshangqing Tablets, hemp intestine-moistening
Ball, Bezoar pill for clearing away the stomach-heat etc.).
Curative effect determinate standard: cure: after taking cactus fine powder ten days, clinical symptoms all disappear, and stool is normal, have no
Recurrence；Effective: after taking cactus fine powder ten days, main clinic symptoms disappear, no relapse；It is effective: to take cactus fine powder
After ten days, main clinic symptoms are alleviated, and occasionally have recurrence；It is invalid: without change before clinical symptoms and treatment.Total effective rate=cure rate
+ obvious effective rate+effective percentage.
The treatment results of four groups of patients are as shown in table 1:
Cactus fine powder of the invention can targetedly treat constipation caused by stomach fire is contained, and therapeutic effect is significant, clinical
Experiments have shown that its total effective rate can reach 99.3%, the physical condition of edible Patients Before And After is also obviously improved.
Although the embodiments of the present invention have been disclosed as above, but its is not only in the description and the implementation listed
With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can be easily
Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is simultaneously unlimited
In specific details.
Claims (10)
1. a kind of preparation method of cactus fine powder, characterized in that it comprises the following steps:
1) fresh cactus deburring, cleaning, drying and the slice of plantation in 10 years are taken, it is stand-by as raw material；
2) raw material is placed in freeze drier, is freeze-dried 8~12h, makes moisture content 3%~5%；
3) powder after drying is put into pulverizer, is added and crushes promotor progress pulverization process, smashing fineness 200~300
Mesh；
4) smashed powder is put into wall-breaking machine, water and broken wall promotor is added, carry out broken wall treatment, obtain broken wall slurry
Liquid, 1000~1200 mesh of broken wall fineness；
5) broken wall slurries are stood, is centrifugated；
6) powder after being centrifugated is placed in freeze drier, is carried out 6~8h of freeze-drying, is made moisture content < 0.5%, add
Enter flowable, packed, obtains cactus fine powder.
2. the preparation method of cactus fine powder according to claim 1, which is characterized in that the crushing promotor is poly- first
Base galactolipin, ratio by mass part meter of poly- methylgalactose is added, raw material: poly- methylgalactose is 100:1~5.
3. the preparation method of cactus fine powder according to claim 1, which is characterized in that in the step 4), powder: water
=1:1~2.
4. the preparation method of cactus fine powder according to claim 1, which is characterized in that in the step 4), broken wall promotees
It include glusulase into agent, the additional amount of the glusulase is 3~5U/g.
5. the preparation method of cactus fine powder according to claim 4, which is characterized in that in the step 4), broken wall promotees
It further include glutamine into agent, the additional amount of the glutamine is 6~8U/g.
6. the preparation method of cactus fine powder according to claim 1, which is characterized in that in the step 4), at broken wall
The reason time is 5h, and broken wall temperature is 30~50 DEG C.
7. the preparation method of cactus fine powder according to claim 1, which is characterized in that the step 5) centrifuge separation
When, centrifugal speed 6000rpm/min, centrifugation time 30min.
8. the preparation method of cactus fine powder according to claim 1, which is characterized in that the step 2) and step 6)
In, freeze-drying temperature is -30 DEG C~-50 DEG C.
9. the preparation method of cactus fine powder according to claim 1, which is characterized in that the flowable is food-grade two
Silica, ratio by mass part meter of silica is added, powder: silica is 100:0.5~2.
10. the preparation method of cactus fine powder according to claim 1, which is characterized in that the grain of the cactus fine powder
Diameter is 500~800 mesh.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1069632A (en) * | 1991-08-26 | 1993-03-10 | 麻金庭 | pollen wall breaking technology |
| CN101467688A (en) * | 2007-12-30 | 2009-07-01 | 陈奎生 | Method for preparing health product made of edible cactus |
| CN102952815A (en) * | 2012-02-10 | 2013-03-06 | 华南理工大学 | Method for producing microbial transglutaminase by use of pro-transglutaminase |
| CN106343581A (en) * | 2016-08-31 | 2017-01-25 | 郭迎庆 | Preparation method of snailase auxiliary degradation soluble dietary fiber |
-
2018
- 2018-09-07 CN CN201811045987.3A patent/CN109172627A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1069632A (en) * | 1991-08-26 | 1993-03-10 | 麻金庭 | pollen wall breaking technology |
| CN101467688A (en) * | 2007-12-30 | 2009-07-01 | 陈奎生 | Method for preparing health product made of edible cactus |
| CN102952815A (en) * | 2012-02-10 | 2013-03-06 | 华南理工大学 | Method for producing microbial transglutaminase by use of pro-transglutaminase |
| CN106343581A (en) * | 2016-08-31 | 2017-01-25 | 郭迎庆 | Preparation method of snailase auxiliary degradation soluble dietary fiber |
Non-Patent Citations (1)
| Title |
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| 王佳等: "不同破壁方法提取无乳链球菌质粒DNA的比较", 《食品科技》 * |
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Application publication date: 20190111 |
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