CN109161443A - A kind of fresh rosemary processing method - Google Patents
A kind of fresh rosemary processing method Download PDFInfo
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- CN109161443A CN109161443A CN201711115457.7A CN201711115457A CN109161443A CN 109161443 A CN109161443 A CN 109161443A CN 201711115457 A CN201711115457 A CN 201711115457A CN 109161443 A CN109161443 A CN 109161443A
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- rosemary
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- fresh rosemary
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- 241001529742 Rosmarinus Species 0.000 title claims abstract description 53
- 238000003672 processing method Methods 0.000 title claims abstract description 18
- 238000001035 drying Methods 0.000 claims abstract description 21
- 239000000341 volatile oil Substances 0.000 claims abstract description 12
- 238000010009 beating Methods 0.000 claims abstract description 9
- 238000000926 separation method Methods 0.000 claims abstract description 7
- 239000010668 rosemary oil Substances 0.000 claims abstract description 6
- 229940058206 rosemary oil Drugs 0.000 claims abstract description 6
- 206010013786 Dry skin Diseases 0.000 claims abstract description 5
- 238000002224 dissection Methods 0.000 claims abstract description 3
- 230000007423 decrease Effects 0.000 abstract description 4
- 230000000857 drug effect Effects 0.000 abstract description 4
- DOUMFZQKYFQNTF-WUTVXBCWSA-N (R)-rosmarinic acid Chemical compound C([C@H](C(=O)O)OC(=O)\C=C\C=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 DOUMFZQKYFQNTF-WUTVXBCWSA-N 0.000 description 26
- ZZAFFYPNLYCDEP-HNNXBMFYSA-N Rosmarinsaeure Natural products OC(=O)[C@H](Cc1cccc(O)c1O)OC(=O)C=Cc2ccc(O)c(O)c2 ZZAFFYPNLYCDEP-HNNXBMFYSA-N 0.000 description 13
- DOUMFZQKYFQNTF-MRXNPFEDSA-N rosemarinic acid Natural products C([C@H](C(=O)O)OC(=O)C=CC=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 DOUMFZQKYFQNTF-MRXNPFEDSA-N 0.000 description 13
- TVHVQJFBWRLYOD-UHFFFAOYSA-N rosmarinic acid Natural products OC(=O)C(Cc1ccc(O)c(O)c1)OC(=Cc2ccc(O)c(O)c2)C=O TVHVQJFBWRLYOD-UHFFFAOYSA-N 0.000 description 13
- 239000002994 raw material Substances 0.000 description 8
- 239000007791 liquid phase Substances 0.000 description 5
- 102000004190 Enzymes Human genes 0.000 description 4
- 108090000790 Enzymes Proteins 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 238000009423 ventilation Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 230000007071 enzymatic hydrolysis Effects 0.000 description 1
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
- A23L5/21—Removal of unwanted matter, e.g. deodorisation or detoxification by heating without chemical treatment, e.g. steam treatment, cooking
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/34—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using microwaves
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Medical Informatics (AREA)
- Epidemiology (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Alternative & Traditional Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicines Containing Plant Substances (AREA)
- Fats And Perfumes (AREA)
Abstract
A kind of fresh rosemary processing method, it is: first spreads the fresh rosemary under picking under the conditions of temperature is lower than 32 DEG C, then dissection or crushing are carried out under the conditions of temperature is no more than 35 DEG C, steam beating is used at 95~120 DEG C, or at 55~80 DEG C with microwave de-enzyming, again with 45~60 DEG C of hot wind continuous dryings, the air-flow with steam and Some essential oils being discharged in water-removing or drying course is by condenser, Rosemary Oil is isolated in collection, then stem, leaf separation are carried out with stem-leaf separating machine, rosemary leave is packed.It can solve the problem of to cause after rosemary directly dries effective component decline, drug effect reduction to encounter rainy day using the present invention not to be capable of processing.
Description
Technical field
The present invention relates to a kind of fresh rosemary processing methods.
Background technique
Because containing in fresh rosemary raw material, there are many enzymes, if temperature reaches 35 DEG C, the activity of enzyme can become by force, can make to be confused
Repeatedly fragrant acid, which occurs to digest, causes content to decline, and overlong time can make the content zero of Rosmarinic acid.Traditional processing method is straight
It connects and manually separates cauline leaf after drying, in process if there is a Absent measures are bad, Rosmarinic acid can be made
Content decline can be had an effect with the long enzyme of the rosemary storage of traditional processing, and content can also decline；From fresh raw material to adding
Work is controlled at dry raw material, each link needs.It is not capable of processing in addition, traditional processing method once encounters rainy day.
Therefore, it needs that the destruction of rosemary effective component, drug effect is caused to reduce after one kind avoids rosemary from directly drying at present,
Encounter the fresh rosemary processing method that rainy day is not capable of processing.
Summary of the invention
Cause effective component broken after avoiding rosemary from directly drying the technical problem to be solved by the invention is to provide one kind
Bad, drug effect reduces, and encounters the fresh rosemary processing method that rainy day is not capable of processing.
The technical solution adopted by the present invention to solve the technical problems is: a kind of fresh rosemary processing method is: will first adopt
The fresh rosemary taken is spread under the conditions of temperature is lower than 32 DEG C, then carries out dissection under the conditions of temperature is no more than 35 DEG C
Or crush, steam beating is used at 95~120 DEG C, or at 55~80 DEG C with microwave de-enzyming, then continuously dried with 45~60 DEG C of hot winds
Dry, the air-flow with steam and Some essential oils being discharged in water-removing or drying course isolates rosemary by condenser, collection
Essential oil, then carries out stem, leaf separation with stem-leaf separating machine, and rosemary leave is packed.
Further, time≤12 hour, preferably 2~6 hours are spread.
Further, the temperature of steam beating is 100~110 DEG C.
Further, the time of steam beating is 0.5~5 minute.
Further, the temperature of microwave de-enzyming is 60~70 DEG C.
Further, with 50~55 DEG C of hot wind continuous dryings.
The effect of steam beating or microwave de-enzyming of the present invention is to kill enzyme, to prevent enzymatic hydrolysis Rosmarinic acid.
It can solve that effective component destruction, drug effect is caused to reduce after rosemary directly dries using the present invention, encounter rainy day
The problem of not being capable of processing.
Detailed description of the invention
Fig. 1 is Rosmarinic acid liquid phase test map after comparative example rosemary Raw material processing；
Fig. 2 is Rosmarinic acid liquid phase test map after 1 rosemary Raw material processing of the embodiment of the present invention；
Fig. 3 is Rosmarinic acid liquid phase test map after 2 rosemary Raw material processing of the embodiment of the present invention；
Fig. 4 is Rosmarinic acid liquid phase test map after 3 rosemary Raw material processing of the embodiment of the present invention；
Fig. 5 is Rosmarinic acid liquid phase test map after 4 rosemary Raw material processing of the embodiment of the present invention.
Specific embodiment
The invention will be further described with reference to the accompanying drawings and embodiments.
Comparative example
It is beneath directly under the sun spread drying by the fresh rosemary branches and leaves 120 kg under picking, it is small to spread the time 28
When, stem, leaf separation are manually carried out, rosemary leave is packed, and obtains 29.5 kilograms of rosemary leave, rosmarinic acid contents are
0.68%(is shown in Fig. 1).
Embodiment 1
By 540 kilograms of fresh rosemary branches and leaves under picking, is spread under the conditions of 25~32 DEG C of temperature, spreads the time 3 hours,
Then it is cut into the segment of 1~3cm with medicine cutter, is used steam beating 2 minutes at 110 DEG C, then continuously dried with 50~60 DEG C of hot winds
Dry, the air-flow with steam and Some essential oils being discharged in drying course enters in condenser by ventilation duct, and collection is isolated
Rosemary Oil, then the rosemary after drying carries out stem with stem-leaf separating machine, leaf separates, and rosemary leave is packed, must be confused
Repeatedly 135.5 kilograms of spiceleaf, essential oil obtain 2.5 kilograms.Rosmarinic acid contents are that 2.51%(is shown in Fig. 2).
Embodiment 2
By 1202 kilograms of fresh rosemary branches and leaves under picking, is spread under the conditions of 18~25 DEG C of temperature, it is small to spread the time 2
When, it is then cut into the segment of 1~3cm with medicine cutter, is used steam beating 2 minutes at 105 DEG C, then continuous with 50~60 DEG C of hot winds
It dries, the air-flow with steam and Some essential oils being discharged in drying course enters in condenser by ventilation duct, collects separation
Rosemary Oil out, then the rosemary after drying carries out stem with stem-leaf separating machine, leaf separates, and rosemary leave is packed, obtained
300.5 kilograms of rosemary leave, essential oil obtains 5.4 kilograms.Rosmarinic acid contents are that 2.11%(is shown in Fig. 3).
Embodiment 3
By 1620 kilograms of fresh rosemary branches and leaves under picking, is spread under the conditions of 18~25 DEG C of temperature, it is small to spread the time 3
When, the segment of 1~3cm, microwave de-enzyming are then cut into medicine cutter, temperature is 60~70 DEG C, then continuous with 50~60 DEG C of hot winds
It dries, the air-flow with steam and Some essential oils being discharged in drying course enters in condenser by ventilation duct, collects separation
Rosemary Oil out, then the rosemary after drying carries out stem with stem-leaf separating machine, leaf separates, and rosemary leave is packed, obtained
405 kilograms of rosemary leave, essential oil obtains 7.29 kilograms.Rosmarinic acid contents are that 2.32%(is shown in Fig. 4).
Embodiment 4
By 2020 kilograms of fresh rosemary branches and leaves under picking, is spread under the conditions of 18~25 DEG C of temperature, it is small to spread the time 2.5
When, the segment of 1~3cm, microwave de-enzyming are then cut into medicine cutter, temperature is 60~70 DEG C, then continuous with 50~60 DEG C of hot winds
It dries, the air-flow with steam and Some essential oils being discharged in drying course enters in condenser by ventilation duct, collects separation
Rosemary Oil out, then the rosemary after drying carries out stem with stem-leaf separating machine, leaf separates, and rosemary leave is packed, obtained
505.9 kilograms of rosemary leave, essential oil obtains 9.1 kilograms.Rosmarinic acid contents are that 2.24%(is shown in Fig. 5).
Claims (9)
1. a kind of fresh rosemary processing method, which is characterized in that be: the fresh rosemary under picking being first lower than 32 DEG C of items in temperature
It is spread under part, dissection or crushing is then carried out under the conditions of temperature is no more than 35 DEG C, is killed at 95~120 DEG C with steam
Blueness, or at 55~80 DEG C with microwave de-enzyming, then with 45~60 DEG C of hot wind continuous dryings, what is be discharged in water-removing or drying course is had
The air-flow of steam and Some essential oils passes through condenser, and collection isolates Rosemary Oil, then carries out stem, leaf with stem-leaf separating machine
Separation, rosemary leave are packed.
2. fresh rosemary processing method according to claim 1, which is characterized in that spread time≤12 hour.
3. fresh rosemary processing method according to claim 2, which is characterized in that spreading the time is 2~6 hours.
4. fresh rosemary processing method according to claim 1 or 2 or 3, which is characterized in that the temperature of steam beating is
100~110 DEG C.
5. fresh rosemary processing method according to claim 4, which is characterized in that the time of steam beating is 0.5~5 point
Clock.
6. fresh rosemary processing method according to claim 1 or 2 or 3, which is characterized in that the temperature of microwave de-enzyming is 60
~70 DEG C.
7. fresh rosemary processing method according to claim 1 or 2 or 3, which is characterized in that continuous with 50~55 DEG C of hot winds
Drying.
8. fresh rosemary processing method according to claim 4, which is characterized in that with 50~55 DEG C of hot wind continuous dryings.
9. fresh rosemary processing method according to claim 5, which is characterized in that with 50~55 DEG C of hot wind continuous dryings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711115457.7A CN109161443A (en) | 2017-11-13 | 2017-11-13 | A kind of fresh rosemary processing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711115457.7A CN109161443A (en) | 2017-11-13 | 2017-11-13 | A kind of fresh rosemary processing method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109161443A true CN109161443A (en) | 2019-01-08 |
Family
ID=64897063
Family Applications (1)
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|---|---|---|---|
| CN201711115457.7A Pending CN109161443A (en) | 2017-11-13 | 2017-11-13 | A kind of fresh rosemary processing method |
Country Status (1)
| Country | Link |
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| CN (1) | CN109161443A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101117614A (en) * | 2007-08-30 | 2008-02-06 | 宋永快 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
| CN101157880A (en) * | 2007-10-11 | 2008-04-09 | 上海交通大学 | Aromatic plant essential oil ecological processing method |
| CN103031210A (en) * | 2012-08-02 | 2013-04-10 | 福建紫红苑本草科技有限公司 | Rosemary dehydration method capable of preparing rosemary essential oil incidentally |
| CN104490994A (en) * | 2014-12-18 | 2015-04-08 | 民权鼎昕生物科技有限公司 | Method for extracting lipid-soluble and water-soluble antioxidant from rosemary |
| CN106281719A (en) * | 2016-10-30 | 2017-01-04 | 庞群 | The method extracting rosemary ethereal oil from Herba Rosmarini Officinalis grass |
| CN106318642A (en) * | 2016-10-20 | 2017-01-11 | 北京玫瑰谷香露有限公司 | Preparation method of high-purity essential oil by low-temperature distillation extraction |
| CN107502451A (en) * | 2017-09-13 | 2017-12-22 | 河南森源本草天然产物股份有限公司 | The preparation method of Rosmarinus officinalis extract |
-
2017
- 2017-11-13 CN CN201711115457.7A patent/CN109161443A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101117614A (en) * | 2007-08-30 | 2008-02-06 | 宋永快 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
| CN101157880A (en) * | 2007-10-11 | 2008-04-09 | 上海交通大学 | Aromatic plant essential oil ecological processing method |
| CN103031210A (en) * | 2012-08-02 | 2013-04-10 | 福建紫红苑本草科技有限公司 | Rosemary dehydration method capable of preparing rosemary essential oil incidentally |
| CN104490994A (en) * | 2014-12-18 | 2015-04-08 | 民权鼎昕生物科技有限公司 | Method for extracting lipid-soluble and water-soluble antioxidant from rosemary |
| CN106318642A (en) * | 2016-10-20 | 2017-01-11 | 北京玫瑰谷香露有限公司 | Preparation method of high-purity essential oil by low-temperature distillation extraction |
| CN106281719A (en) * | 2016-10-30 | 2017-01-04 | 庞群 | The method extracting rosemary ethereal oil from Herba Rosmarini Officinalis grass |
| CN107502451A (en) * | 2017-09-13 | 2017-12-22 | 河南森源本草天然产物股份有限公司 | The preparation method of Rosmarinus officinalis extract |
Non-Patent Citations (2)
| Title |
|---|
| 廖俊杰，等: "粤产迷迭香的精油提取及其主要成分分析", 《中成药》 * |
| 张俊清，等: "迷迭香精油水蒸气蒸馏最佳提取工艺筛选研究", 《海南医学院学报》 * |
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