CN101117614A - Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process - Google Patents
Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process Download PDFInfo
- Publication number
- CN101117614A CN101117614A CNA2007101137228A CN200710113722A CN101117614A CN 101117614 A CN101117614 A CN 101117614A CN A2007101137228 A CNA2007101137228 A CN A2007101137228A CN 200710113722 A CN200710113722 A CN 200710113722A CN 101117614 A CN101117614 A CN 101117614A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- pipeline
- aromatics plant
- chamber
- plant extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Landscapes
- Fats And Perfumes (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The present invention discloses a dry method for refining balsam and essential oil from aromatic plants, aromatic plants are refined and put in a device, a heating chamber (4) is connected with an evaporating chamber (1) through a pipeline, the evaporating chamber (1) is connected with an extraction chamber (2) through a pipeline, the extraction chamber (2) is connected with a blower (3) through a pipeline, the blower (3) is connected with the heating chamber (4) through a pipeline, and a sealed circulation loop device is formed. The hot blast temperature is controlled between 60 DEG C and 90 DEG C, the wind speed is controlled at 1 meter to 15 meters per minutes, the inlet temperature of a condensing reed pipe (23) is 3 DEG C to 25 DEG C, and balsam and essential oil can be collected in a discharge pipe(24). In the present invention, no water, special gas and organic solvent are added into raw material, balsam and essential oil which are refined are uncorrupt in smell, small in equipment volume, simply in art, high in efficiency, low in energy consumption, simply in operation and high in production efficiency; no pollution material is discharged, no cooking water and steam are consumed, balsam after being refined can be used as additive of food, drink and condiment, and used for hairdressing, face-painting, bath, and health care, in addition, the aromatic plants after being refined balsam and essential oil is in the dry shape and reserved in a whole, then can be used sequentially, thereby saving resources.
Description
Affiliated technical field
The present invention relates to a kind of method from aromatics plant extract aromatics extract, is the method for a kind of dry type from aromatics plant extract fragrance liquid and essential oil specifically.
Background technology
At present, current in the world aromatics plant extract essential oil, for example from Rose, extract the method for Flos Rosae Rugosae quintessence oil, have three kinds substantially: first kind is " water-boiling method ", with the fresh Rose still kettle of packing into, add a certain proportion of water, feed the water boiling that is steam heated in the still at the bottom of the still, the aromatoising substance in spending evaporates with water vapour, by cooling off in the conduit importing condenser, cooling fluid flows in the water-and-oil separator, according to profit proportion difference, isolates Flos Rosae Rugosae quintessence oil and rose wate.The subject matter that water-boiling method exists is that long-time high temperature steaming makes the fragrant alcohol ester of Rose morph, the essential oil that is extracted does not have the natural fragrance of fresh flower, but giving off a strong fragrance is pungent, smell is impure, in the production process, equipment is many, and energy consumption is big, operator are many, efficient is low, and raffinate residue discharge amount of pollution is big, needs to consume a large amount of steam and water coolant; Second kind is " solvent extration ", adopts organic solvent, as alcohol, ether or liquefied butane etc., with organic solvent repeatedly sprinkle on new fresh-rose, aromatoising substance in spending is dissolved in the said solvent, adopt the method for low-temperature distillation then, extract the aromatoising substance in the Rose.The subject matter that solvent extration exists is, equipment, complex process also need consume steam and water coolant, because with an organic solvent, have high input, and yield poorly, and easily essential oil are polluted, and oil yield is low, and isolated essential oil is impure; The third is " carbon dioxide supercritical extraction method ", and extraction process is to utilize CO
2In the low temperature critical environment, the aromatoising substance in the Rose is extracted, this technology adapts to the low temperature aromatic character of Rose, the essential oil of extraction, fragrance is pure, and is closely similar with fresh flower.The subject matter of carbon dioxide supercritical extraction method is, equipment, technology are very complicated, and working ability is low, and also there is the waste sludge discharge contaminate environment in the facility investment costliness, and this method only is in laboratory stage at present, does not still have the precedent that enterprise adopts this method to produce in batches.
Before the present invention finishes, not seeing fragrant liquid and the essential oil that the dry type identical with the present invention extract from the method for aromatics plant extract fragrance liquid and essential oil as yet uses daily life, not seeing fragrant liquid and the essential oil that the dry type identical with the present invention extract from the method for aromatics plant extract fragrance liquid and essential oil has sale in market, and it is on the books in the literature from the fragrant liquid and the essential oil of the method for aromatics plant extract fragrance liquid and essential oil and extraction thereof also not see the dry type identical with the present invention.
Summary of the invention
The object of the present invention is to provide the method for a kind of dry type from aromatics plant extract fragrance liquid and essential oil, the product fragrance liquid and the essential oil that adopt the inventive method to extract, raw material does not add water in the preparation process, do not add special gas, do not add any chemical organic solvent and auxiliary agent, with the blower fan is power, the airtight warm air of cold cycle is a media, adopt the method for evaporative condenser, can extract fragrant liquid and essential oil in the aromatics plant, the fragrant liquid and the essential oil that are extracted keep its natural fragrance, and smell are pure, strong not pungent, the processing units volume is little, technology is simple, the efficient height, and energy consumption is low, the level of automation height, operator are few, and are simple to operate, rate of output height, without any disposal of pollutants, do not need to build boiler, do not consume water coolant, only use low amounts of power, fragrant liquid behind the extraction essential oil, still contain part aromatoising substance and nutritive ingredient, can make food, beverage, the additive of seasonings also can be done beauty treatment and make up, the health care of taking a shower is used, and, extract the complete reservation of aromatics plant Cheng Ganzhuan behind fragrant liquid and the essential oil, can continue development and use, save fragrant resource.
For achieving the above object, the present invention adopts following technical proposals:
A kind of dry type is from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that it mainly adopts following method:
With the aromatics plant, place in the aromatic substance extraction element, extract fragrant liquid and essential oil,
Said aromatic substance extraction element, comprise casing, the casing internal fixing has heating chamber, evaporator room, extraction chamber and blower fan, heating chamber by pipeline and evaporator room, evaporator room by pipeline and extraction chamber, the extraction chamber is by pipeline and blower fan, blower fan is connected with heating chamber by pipeline, forms airtight circulation line device
Be provided with electric heating tube in the said heating chamber, electric heating tube is connected with power supply,
Said evaporator room is airtight container, and container inner wall is provided with some upper and lower stratified carriages, can put the pallet with holes that can pass through air-flow on the said carriage,
Said extraction chamber is airtight container, in establish condensation comb and fragrant liquid and essential oil vent pipe, refrigerator connects the condensation comb by the refrigerant pipeline,
The aromatics plant is placed in the pallet of evaporator room, open heating chamber and fan power, hot blast temperature is controlled between 60 ℃-90 ℃, and the evaporation of low temperature hot blast is promptly started working, the blower fan wind speed be controlled at 1-15 rice/minute, open refrigerator, condensation comb inlet temperature is 3 ℃-25 ℃, and a large amount of aromatic substances of evaporation are at condensation comb condensation and dewfall in the evaporation tank, collect the aromatic substance that is extracted from the aromatic substance vent pipe, then, by water-and-oil separator, isolate fragrant liquid and essential oil.
In technique scheme, said heating chamber is provided with the heating agent dispatch tube, and said heating agent dispatch tube links by pipeline and water vapour source of the gas, flue hot gas source of the gas or cycling hot oil pump.
In technique scheme, said refrigerator also can adopt cooling circulating water system, can also adopt refrigerant ice water circulation system and underground water to gather the recycle system.
In technique scheme, said aromatics plant can for Rose, sweet osmanthus, Flower of Arabian Jasmine, lavender, peppermint, Thymus vulgaris, cape jasmine, Milan, flores anthemidis, Hyssopus officinalis, Rosmarinus officinalis, wild marjoram, Salvia japonica Thunb., sweet basil, peppermint, lemon, beeweed or fennel.
In technique scheme, said aromatics plant can be bud, petal, leaf, stem, root, seed or the fruit of said plant.
In technique scheme, said aromatics plant can also be various leaf classes, root class, stem class, fruit type vegetables, fruit, wild fruit, berry, grain, oil crops, dry fruit, nut or herbal medicine medicinal material.
The aromatic substance extraction element that a kind of dry type is used from the method for aromatics plant extract fragrance liquid and essential oil, comprise casing, the casing internal fixing has heating chamber, evaporator room, extraction chamber and blower fan, heating chamber by pipeline and evaporator room, evaporator room by pipeline and extraction chamber, the extraction chamber is by pipeline and blower fan, blower fan is connected with heating chamber by pipeline, forms airtight circulation line device
Be provided with electric heating tube in the said heating chamber, electric heating tube is connected with power supply,
Said evaporator room is airtight container, and container inner wall is provided with some upper and lower stratified carriages, can put the pallet with holes that can pass through air-flow on the said carriage,
Said extraction chamber is airtight container, in be provided with refrigerator by the joining condensation comb of refrigerant pipeline and fragrant liquid and essential oil vent pipe,
In technique scheme, the heating agent dispatch tube is set in the said heating chamber, said heating agent dispatch tube links by pipeline and water vapour source of the gas, flue hot gas source of the gas or cycling hot oil pump.
In technique scheme, said refrigerator also can adopt cooling circulating water system, can also adopt refrigerant ice water circulation system and underground water to gather the recycle system.
In technique scheme, said aromatics plant can for Rose, sweet osmanthus, Flower of Arabian Jasmine, lavender, peppermint, Thymus vulgaris, cape jasmine, Milan, flores anthemidis, Hyssopus officinalis, Rosmarinus officinalis, wild marjoram, Salvia japonica Thunb., sweet basil, peppermint, lemon, beeweed or fennel.
In technique scheme, said aromatics plant can be bud, petal, leaf, stem, root, seed or the fruit of said plant.
In technique scheme, said aromatics plant can also be various leaf classes, root class, fruit class, stem class vegetables, fruit, wild fruit, berry, grain, oil crops, dry fruit, nut or herbal medicine medicinal material.
Aromatics plant fragrance class material, fragrant liquid and the essential oil produced from the method for aromatics plant extract fragrance liquid and essential oil according to the said a kind of dry type of technique scheme.
The present invention has more following effects and positively effect:
The invention provides the method for a kind of dry type from aromatics plant extract fragrance liquid and essential oil, the product fragrance liquid and the essential oil that adopt the inventive method to extract, raw material does not add water in the preparation process, do not add special gas, do not add any chemical organic solvent and auxiliary agent, with the blower fan is power, the cold cycle warm air is a media, method through evaporative condenser, can extract fragrant liquid and essential oil in the aromatics plant, the fragrant liquid and the essential oil that extract keep its natural fragrance, and smell are pure, strong not pungent, the processing units volume is little, technology is simple, the efficient height, and energy consumption is low, the level of automation height, operator are few, and are simple to operate, rate of output height, without any disposal of pollutants, do not need to build boiler, do not consume water coolant and steam, only use low amounts of power, fragrant liquid behind the extraction essential oil, still contain part aromatoising substance and nutritive ingredient, can make food, beverage, the additive of seasonings also can be done beauty treatment and make up, the health care of taking a shower is used, and, extract the complete reservation of aromatics plant Cheng Ganzhuan behind fragrant liquid and the essential oil, can continue development and use, save fragrant resource.
Embodiment
Below in conjunction with drawings and Examples, the present invention is described in further detail:
Fig. 1 is embodiment 1 said aromatic substance extraction element and the extraction process schema of a kind of dry type of the present invention from aromatics plant extract fragrance liquid and essential oil method;
Fig. 2 is the embodiment 1 employed aromatic substance extraction element synoptic diagram of a kind of dry type of the present invention from aromatics plant extract fragrance liquid and essential oil method.
In Fig. 1, long closed circuit arrow is represented connecting pipeline and the flow direction of circulating air in the sealing pipeline that is connected,
The 1st, evaporator room, the 2nd, the extraction chamber, the 3rd, blower fan, the 4th, heating chamber, the 42nd, electric heating tube, the 5th, fragrant liquid and essential oil, the 6th, the aromatics plant, the 7th, aromatics plant dry product,
The 11st, carriage, the 12nd, pallet, the 21st, pipeline, the 23rd, the condensation comb, the 24th, fragrant liquid and essential oil vent pipe, the 32nd, pipeline, the 34th, pipeline, the 41st, pipeline,
The 8th, container, the 9th, refrigerator, the 91st, the refrigerant pipeline, the 92nd, the refrigerant pipeline, the 10th, casing,
Embodiment 1:
See Fig. 1 and Fig. 2,
The aromatic substance extraction element that a kind of dry type is used from the method for aromatics plant extract fragrance liquid and essential oil, comprise casing 10, be provided with heating chamber 4, evaporator room 1, extraction chamber 2 and blower fan 3 in the casing 10, heating chamber 4 is connected with evaporator room 1 by pipeline 41, evaporator room 1 is connected with extraction chamber 2 by pipeline 21, and extraction chamber 2 is connected with blower fan 3 by pipeline 32, and blower fan 3 is connected with heating chamber 4 by pipeline 34, form airtight circulation line device
Be provided with electric heating tube 42 in the said heating chamber 4, electric heating tube 42 is connected with power supply,
Said evaporator room 1 is airtight container, and container inner wall is provided with some upper and lower stratified carriages 11, and said getting can be put the pallet with holes 12 that can pass through air-flow on the carriage 11,
Said extraction chamber 2 is airtight container, in be provided with refrigerator 9 by refrigerant pipeline 91 and refrigerant pipeline 92 joining condensation combs 23 and fragrant liquid and essential oil vent pipe 24.
Embodiment 2:
In April, 2007, the applicant of present patent application utilizes the said aromatic substance extraction element of the present invention at Shandong Province's Pingying County, has carried out the industrial experimentation of this method,
24 kilograms in Rose bud is placed in the pallet 12 of evaporator room 1, open heating chamber 4 and blower fan 3 power supplys, hot blast temperature is controlled at 75 ℃, start working, open refrigerator, worked 2 hours, hot blast temperature rises to 85 ℃ then, 6 hours again, blower fan 3 wind speed are controlled at 9 meters/minute, condensation comb 23 inlet temperatures are 8 ℃, and a large amount of aromatic substances of evaporation are collected 16 kilograms of the aromatic substances that extracted at condensation comb 23 condensation and dewfalls from fragrant liquid and essential oil vent pipe 24 in the evaporation tank, then, by water-and-oil separator, isolate fragrant liquid and essential oil, and collect the dried flower flower bud.
Embodiment 3:
In April, 2007, the applicant of present patent application utilizes the said aromatic substance extraction element of the present invention at Shandong Province's Pingying County, has carried out the industrial experimentation of this method,
9 kilograms on Rose petal is placed in the pallet 12 of evaporator room 1, open heating chamber 4 and blower fan 3 power supplys, hot blast temperature is controlled at 70 ℃, start working, open refrigerator, after 1 hour, hot blast temperature rises to 75 ℃, worked again 5 hours, blower fan 3 wind speed are controlled at 9 meters/minute, and condensation comb 23 inlet temperatures are 10 ℃, and a large amount of aromatic substances of evaporation are at condensation comb 23 condensation and dewfalls in the evaporation tank, collect 6.6 kilograms of the aromatic substances that extracted, 2 kilograms on dried Rose petal from fragrant liquid and essential oil vent pipe 24.
The Rose fragrance liquid and the essential oil that adopt aforesaid method to produce adopt the GC-MS(gas chromatography-mass spectrography) analysis through Chinese materia medica research institute of Nanjing University of Traditional Chinese Medicine, and its result is as follows:
No | Retention time (min) | Molecular formula | Molecular weight | The compound title | Content (%) | |
English name | Chinese name | |||||
1 | 10.927 | C 7H 8O | 108 | Benzyl alcohol | Phenylcarbinol | 1.092 |
2 | 12.954 | C 8H 10O | 122 | Phenylethyl alcohol | Phenylethyl alcohol | 70.03 2 |
3 | 13.363 | C 10H 18O | 154 | Isopulegol | Isopulegol | 0.179 |
4 | 14.844 | C 10H 20O | 156 | Citronel lol | Geraniol | 2.738 |
5 | 15.300 | C 10H 18O | 154 | linalool | Phantol | 0.170 |
6 | 15.737 | C 12H 26 | 170 | Decane,3,7- |
3,7-diformazan decane | 0.150 |
7 | 17.124 | C 10H 12O 2 | 164 | Eugenol | Oxymethoxyallylbenzene | 0.170 |
8 | 17.827 | C 11H 14O 2 | 178 | Methyl iso-eugenol | The methyl isoeugenol | 1.706 |
9 | 19.189 | C 8H 10O 2 | 138 | Benzeneethanol,2-hy droxy | The 2- |
|
10 | 19.287 | C 14H 30 | 198 | tethadecene | The tetradecane | 0.155 |
11 | 19.546 | C 14H 22O | 206 | Phenol,2,4-bis(1,1- |
2, the 4-diisobutyl phenol | 0.282 |
12 | 20.833 | C 16H 34 | 226 | Hexandecane | N-Hexadecane | 0.185 |
13 | 21.178 | C 12H 16O | 208 | Asarone | Propenyl-2,4,5-trimethoxy beozene | 0.366 |
14 | 21.714 | C 12H 14O 3 | 206 | Eugenol methyl ether acetate | The methyl eugenol acetic ester | 0.349 |
15 | 21.968 | C 10H 12O 4 | 196 | Ethanoe,1-(2-hydrox y-4,6-dimethoxyphen yl) | 2-hydroxyl-4, the 6-dimethoxy-acetophenone | 0.704 |
16 | 22.240 | C 17H 36 | 240 | Heptadecane | Heptadecane | 0.251 |
17 | 22.565 | C 10H 12O 4 | 196 | Benzaldehyde,2,4,5- trimethoxy | Asarylaldehyde | 0.604 |
18 | 22.955 | C 12H 16O 4 | 224 | Aspidinol | Aspidinol | 0.339 |
19 | 23.585 | C 18H 38 | 254 | Octadecane | Octadecane | 0.268 |
20 | 24.192 | C 19H 40 | 268 | Nonadecane | Nonadecane | 0.493 |
21 | 25.640 | C 16H 32O 2 | 256 | n-Hexadecanoic acide | Palmitinic acid | 0.466 |
22 | 26.101 | C 20H 42 | 282 | Eicosane | Eicosane | 0.569 |
23 | 27.272 | C 21H 44 | 296 | Heneicosane | Heneicosane | 0.787 |
24 | 27.657 | C 14H 22O | 206 | Beta.iso-methyl ionone | β-different methyl ionone | 0.235 |
25 | 28.396 | C 22H 46 | 310 | Docosane | Docosane | 0.725 |
26 | 29.468 | C 23H 48 | 324 | Tricosane | Tricosane | 0.510 |
27 | 30.498 | C 24H 50 | 338 | Tetracosane | Tetracosane | 0.708 |
28 | 31.490 | C 25H 52 | 352 | Pentacosane | Pentacosane | 0.679 |
29 | 32.444 | C 26H 54 | 366 | Hexacosane | Hexacosane | 0.715 |
30 | 33.361 | C 27H 56 | 380 | Hetacosane | Heptacosane | 0.449 |
31 | 34.034 | C 26H 52 | 364 | 1-Hexacosene | The 1-hexadecylene | 0.163 |
32 | 34.250 | C 28H 58 | 394 | Octacosane | Octacosane | 0.379 |
33 | 35.106 | C 29H 60 | 408 | Nonacosane | Nonacosane | 0.405 |
34 | 35.938 | C 30H 62 | 422 | Triacontane | Triacontane | 0.267 |
35 | 38.327 | C 30H 60 | 420 | 13-methyl-z-14-nona cosene | 13-methyl 14-is along two octadecylenes | 0.328 |
Claims (13)
1. a dry type is from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that it adopts following method:
With the aromatics plant, place in the aromatic substance extraction element, extract fragrant liquid and essential oil,
Said aromatic substance extraction element, comprise casing (10), casing (10) internal fixing has heating chamber (4), evaporator room (1), extraction chamber (2) and blower fan (3), heating chamber (4) by pipeline and evaporator room (1), evaporator room (1) by pipeline and extraction chamber (2), extraction chamber (2) is by pipeline and blower fan (3), blower fan (3) is connected with heating chamber (4) by pipeline, forms airtight circulation line device
Be provided with electric heating tube (42) in the said heating chamber (4), electric heating tube (42) is connected with power supply,
Said evaporator room (1) is airtight container, and container inner wall is provided with some upper and lower stratified carriages (11), can put the pallet with holes (12) that can pass through air-flow on the said carriage (11),
Said extraction chamber (2) is airtight container, in be provided with refrigerator (9) by refrigerant pipeline (91,92) joining condensation combs (23) and fragrant liquid and essential oil vent pipe (24),
The aromatics plant is placed in the pallet (12) of evaporator room (1), open heating chamber (4), blower fan (3) power supply, hot blast temperature is controlled between 60 ℃-90 ℃, the evaporation of low temperature hot blast is promptly started working, blower fan (3) wind speed be controlled at 1-15 rice/minute, open refrigerator, condensation comb (23) inlet temperature is 3 ℃-25 ℃, a large amount of aromatic substances of evaporation are collected fragrant liquid and the essential oil that is extracted at condensation comb (23) condensation and dewfall from fragrant liquid and essential oil vent pipe (24) in the evaporator room (1).
2. a kind of dry type according to claim 1 is from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that said heating chamber (4) is provided with the heating agent dispatch tube, said heating agent dispatch tube and water vapour source of the gas, flue hot gas source of the gas, cycling hot oil pump link.
3. a kind of dry type according to claim 1 is from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that said refrigerator, also can adopt cooling circulating water system, can also adopt refrigerant ice water circulation system and underground water to gather the recycle system.
4. a kind of dry type according to claim 1 is from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that said aromatics plant can for Rose, sweet osmanthus, Flower of Arabian Jasmine, lavender, peppermint, Thymus vulgaris, cape jasmine, Milan, flores anthemidis, Hyssopus officinalis, Rosmarinus officinalis, wild marjoram, Salvia japonica Thunb., sweet basil, peppermint, lemon, beeweed or fennel.
5. a kind of dry type according to claim 1 is characterized in that from the method for aromatics plant extract fragrance liquid and essential oil said aromatics plant can be bud, petal, leaf, stem, root, seed or the fruit of said plant.
6. a kind of dry type according to claim 1 is characterized in that from the method for aromatics plant extract fragrance liquid and essential oil said aromatics plant can be various leaf classes, root class, stem class, fruit type vegetables, fruit, wild fruit, berry, grain, oil crops, dry fruit, nut or herbal medicine medicinal material.
7. aromatic substance extraction element that uses the method for fragrance liquid and essential oil in formula from the aromatics plant extract, comprise casing (1), casing (1) internal fixing has heating chamber (4), evaporator room (1), extraction chamber (2) and blower fan (3), heating chamber (4) by pipeline and evaporator room (1), evaporator room (1) by pipeline and extraction chamber (2), extraction chamber (2) is by pipeline and blower fan (3), blower fan (3) is connected with heating chamber (4) by pipeline, forms airtight circulation line device
Be provided with electric heating tube (42) in the said heating chamber (4), electric heating tube (42) is connected with power supply,
Said evaporator room (1) is airtight container, and container inner wall is provided with some upper and lower stratified carriages (11), can put the pallet with holes (12) that can pass through air-flow on the said carriage (11),
Said extraction chamber (2) is airtight container, in be provided with refrigerator (9) by refrigerant pipeline (91,92) joining condensation combs (23) and fragrant liquid and essential oil vent pipe (24).
8. the aromatic substance extraction element that a kind of dry type according to claim 7 is used from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that in the said heating chamber (4) the heating agent dispatch tube being set, said heating agent dispatch tube links by pipeline and water vapour source of the gas, flue hot gas source of the gas or cycling hot oil pump.
9. the aromatic substance extraction element that a kind of dry type according to claim 7 is used from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that said refrigerator (9), also can adopt cooling circulating water system, can also adopt refrigerant ice water circulation system and underground water to gather the recycle system.
10. the aromatic substance extraction element that a kind of dry type according to claim 7 is used from the method for aromatics plant extract fragrance liquid and essential oil, it is characterized in that said aromatics plant can for Rose, sweet osmanthus, Flower of Arabian Jasmine, lavender, peppermint, Thymus vulgaris, cape jasmine, Milan, flores anthemidis, Hyssopus officinalis, Rosmarinus officinalis, wild marjoram, Salvia japonica Thunb., sweet basil, peppermint, lemon, beeweed or fennel.
11. the aromatic substance extraction element that a kind of dry type according to claim 7 is used from the method for aromatics plant extract fragrance liquid and essential oil is characterized in that said aromatics plant can be bud, petal, leaf, stem, root, seed or the fruit of said plant.
12. the aromatic substance extraction element that a kind of dry type according to claim 7 is used from the method for aromatics plant extract fragrance liquid and essential oil is characterized in that said aromatics plant can be various leaf classes, root class, stem class, fruit type vegetables, fruit, wild fruit, berry, grain, oil crops, dry fruit, nut or herbal medicine medicinal material.
13. fragrant liquid and essential oil product from an aromatics plant extract is characterized in that it is to adopt the described dry type of claim 1 to make from the method for aromatics plant extract fragrance liquid and essential oil.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007101137228A CN101117614B (en) | 2007-08-30 | 2007-08-30 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2007101137228A CN101117614B (en) | 2007-08-30 | 2007-08-30 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101117614A true CN101117614A (en) | 2008-02-06 |
CN101117614B CN101117614B (en) | 2010-12-08 |
Family
ID=39053874
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2007101137228A Expired - Fee Related CN101117614B (en) | 2007-08-30 | 2007-08-30 | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN101117614B (en) |
Cited By (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102212419A (en) * | 2010-04-01 | 2011-10-12 | 宏芳香料(昆山)有限公司 | Perfume drying device and essential oil recycling method |
CN102295992A (en) * | 2010-06-23 | 2011-12-28 | 新疆天然芳香农业科技有限公司 | Plant essence gradient extraction device |
CN101747994B (en) * | 2010-01-06 | 2011-12-28 | 戴礼森 | Production method for drying and distilling rose buds and equipment thereof |
CN102690725A (en) * | 2011-03-25 | 2012-09-26 | 漳州弘烨机械制造有限公司 | Novel technology for fragrance recovery and device adopting the novel technology |
CN103031214A (en) * | 2012-08-02 | 2013-04-10 | 福建紫红苑本草科技有限公司 | Lemon verbena dehydration method capable of preparing lemon verbena essential oil incidentally |
CN103031204A (en) * | 2012-08-02 | 2013-04-10 | 福建紫红苑本草科技有限公司 | Ginger dehydration method capable of preparing ginger oil incidentally |
CN103045365A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Pogostemon cablin dehydrating method capable of simultaneously preparing pogostemon cablin essential oil |
CN103045358A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Thyme dehydrating method capable of simultaneously preparing thyme essential oil |
CN103045366A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Oregano dehydration method capable of preparing oregano essential oil |
CN103045367A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Lavender dehydration method capable of preparing lavender essential oil |
CN103947385A (en) * | 2014-05-05 | 2014-07-30 | 陈爱珍 | Method for realizing floral accelerated two-stage collection |
CN104004590A (en) * | 2014-05-07 | 2014-08-27 | 福建省闽神农业生物科技有限公司 | Osmanthus fragrans essential oil extraction method |
CN104017649A (en) * | 2013-03-29 | 2014-09-03 | 洛阳春魁农业开发有限公司 | Preparation method and device of peony and arabian jasmine flower mixed essential oil |
CN104017650A (en) * | 2013-03-29 | 2014-09-03 | 洛阳春魁农业开发有限公司 | Preparation method and device for peony-lavender blend essential oil |
CN104431942A (en) * | 2014-11-11 | 2015-03-25 | 青岛信和源生物科技有限公司 | Spice preparation system |
CN105154236A (en) * | 2015-09-23 | 2015-12-16 | 陈富强 | Full-automatic electric heating triple-effect plant essential oil extracting and purifying integrated device |
CN105779135A (en) * | 2016-05-28 | 2016-07-20 | 黄宇松 | Sweet osmanthus fragrance substance extracting method |
CN106635424A (en) * | 2016-12-29 | 2017-05-10 | 青岛玫瑰圣地农业综合开发有限公司 | Water-free vanilla hydrolat extraction method |
CN106635423A (en) * | 2016-12-29 | 2017-05-10 | 成都华西珐玛生物科技有限公司 | Method for preparing plant essential oil |
CN107047819A (en) * | 2017-02-27 | 2017-08-18 | 四川星麻哥食品有限公司 | It is a kind of that the equipment that flavour and fragrance substance produces flavored oils is extracted from spice |
CN107619720A (en) * | 2017-10-24 | 2018-01-23 | 金箍棒工业产品设计江阴有限公司 | A kind of sweet osmanthus aromatic liquid water extracting method |
CN107841380A (en) * | 2017-11-24 | 2018-03-27 | 尹大建 | A kind of extracting method of jasmine essential oil |
CN107897435A (en) * | 2017-11-24 | 2018-04-13 | 尹大建 | A kind of method of Jasmine drying tail gas recycle |
CN108441326A (en) * | 2018-05-15 | 2018-08-24 | 福建普民生物科技有限公司 | A kind of pure liquid distilled from honeysuckle flowers or lotus leaves extraction equipment of low temperature |
CN109161443A (en) * | 2017-11-13 | 2019-01-08 | 湖南诺泽生物科技有限公司 | A kind of fresh rosemary processing method |
CN109283268A (en) * | 2018-09-27 | 2019-01-29 | 甘肃出入境检验检疫局检验检疫综合技术中心 | The analysis method of fragrance component in a kind of brackish water rose water |
CN110419765A (en) * | 2019-08-12 | 2019-11-08 | 四川三联新材料有限公司 | A kind of preparation method and preparation facilities of electronic cigarette tobacco tar |
TWI679407B (en) * | 2018-04-13 | 2019-12-11 | 統一企業股份有限公司 | Analyzing Method for Aroma of Flower |
CN112760170A (en) * | 2021-01-19 | 2021-05-07 | 中华全国供销合作总社南京野生植物综合利用研究所 | Plant essential oil hot air circulation distillation technology |
CN113088399A (en) * | 2021-04-13 | 2021-07-09 | 康荍生物技术(上海)有限公司 | Method for extracting aroma substances from aromatic plants |
CN113214899A (en) * | 2021-03-31 | 2021-08-06 | 广西壮族自治区农业科学院 | Wao gan essential oil extraction element |
CN115068974A (en) * | 2022-05-16 | 2022-09-20 | 深圳昱朋科技有限公司 | Preparation method of plant spice |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1018524B (en) * | 1989-07-25 | 1992-10-07 | 中国石油化工总公司 | Catalytic distillation colum |
CN1108844C (en) * | 2000-03-22 | 2003-05-21 | 王玲 | Fractionating reaction column plate type catalytic distillating equipment |
CN1912082B (en) * | 2006-08-16 | 2010-12-08 | 戴礼森 | Drying, distillation device of aromatic plant and its method |
-
2007
- 2007-08-30 CN CN2007101137228A patent/CN101117614B/en not_active Expired - Fee Related
Cited By (38)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101747994B (en) * | 2010-01-06 | 2011-12-28 | 戴礼森 | Production method for drying and distilling rose buds and equipment thereof |
CN102212419A (en) * | 2010-04-01 | 2011-10-12 | 宏芳香料(昆山)有限公司 | Perfume drying device and essential oil recycling method |
CN102295992A (en) * | 2010-06-23 | 2011-12-28 | 新疆天然芳香农业科技有限公司 | Plant essence gradient extraction device |
CN102295992B (en) * | 2010-06-23 | 2012-11-07 | 新疆天然芳香农业科技有限公司 | Plant essence gradient extraction device |
CN102690725A (en) * | 2011-03-25 | 2012-09-26 | 漳州弘烨机械制造有限公司 | Novel technology for fragrance recovery and device adopting the novel technology |
CN103031214A (en) * | 2012-08-02 | 2013-04-10 | 福建紫红苑本草科技有限公司 | Lemon verbena dehydration method capable of preparing lemon verbena essential oil incidentally |
CN103031204A (en) * | 2012-08-02 | 2013-04-10 | 福建紫红苑本草科技有限公司 | Ginger dehydration method capable of preparing ginger oil incidentally |
CN103045365A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Pogostemon cablin dehydrating method capable of simultaneously preparing pogostemon cablin essential oil |
CN103045358A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Thyme dehydrating method capable of simultaneously preparing thyme essential oil |
CN103045366A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Oregano dehydration method capable of preparing oregano essential oil |
CN103045367A (en) * | 2012-08-02 | 2013-04-17 | 福建紫红苑本草科技有限公司 | Lavender dehydration method capable of preparing lavender essential oil |
CN104017650B (en) * | 2013-03-29 | 2016-03-02 | 洛阳春魁农业开发有限公司 | A kind of preparation method of Tree Peony flower lavandula angustifolia mediation essential oil and device |
CN104017649A (en) * | 2013-03-29 | 2014-09-03 | 洛阳春魁农业开发有限公司 | Preparation method and device of peony and arabian jasmine flower mixed essential oil |
CN104017650A (en) * | 2013-03-29 | 2014-09-03 | 洛阳春魁农业开发有限公司 | Preparation method and device for peony-lavender blend essential oil |
CN103947385B (en) * | 2014-05-05 | 2015-10-07 | 陈爱珍 | The fragrance of a flower accelerates the implementation method that secondary gathers |
CN103947385A (en) * | 2014-05-05 | 2014-07-30 | 陈爱珍 | Method for realizing floral accelerated two-stage collection |
CN104004590A (en) * | 2014-05-07 | 2014-08-27 | 福建省闽神农业生物科技有限公司 | Osmanthus fragrans essential oil extraction method |
CN104004590B (en) * | 2014-05-07 | 2016-05-11 | 福建省闽神农业生物科技有限公司 | DANGUIHUA method of extraction of essential oil |
CN104431942A (en) * | 2014-11-11 | 2015-03-25 | 青岛信和源生物科技有限公司 | Spice preparation system |
CN105154236A (en) * | 2015-09-23 | 2015-12-16 | 陈富强 | Full-automatic electric heating triple-effect plant essential oil extracting and purifying integrated device |
CN105779135A (en) * | 2016-05-28 | 2016-07-20 | 黄宇松 | Sweet osmanthus fragrance substance extracting method |
CN106635424A (en) * | 2016-12-29 | 2017-05-10 | 青岛玫瑰圣地农业综合开发有限公司 | Water-free vanilla hydrolat extraction method |
CN106635423A (en) * | 2016-12-29 | 2017-05-10 | 成都华西珐玛生物科技有限公司 | Method for preparing plant essential oil |
CN107047819A (en) * | 2017-02-27 | 2017-08-18 | 四川星麻哥食品有限公司 | It is a kind of that the equipment that flavour and fragrance substance produces flavored oils is extracted from spice |
CN107619720A (en) * | 2017-10-24 | 2018-01-23 | 金箍棒工业产品设计江阴有限公司 | A kind of sweet osmanthus aromatic liquid water extracting method |
CN109161443A (en) * | 2017-11-13 | 2019-01-08 | 湖南诺泽生物科技有限公司 | A kind of fresh rosemary processing method |
CN107897435A (en) * | 2017-11-24 | 2018-04-13 | 尹大建 | A kind of method of Jasmine drying tail gas recycle |
CN107841380A (en) * | 2017-11-24 | 2018-03-27 | 尹大建 | A kind of extracting method of jasmine essential oil |
TWI679407B (en) * | 2018-04-13 | 2019-12-11 | 統一企業股份有限公司 | Analyzing Method for Aroma of Flower |
CN108441326A (en) * | 2018-05-15 | 2018-08-24 | 福建普民生物科技有限公司 | A kind of pure liquid distilled from honeysuckle flowers or lotus leaves extraction equipment of low temperature |
CN109283268A (en) * | 2018-09-27 | 2019-01-29 | 甘肃出入境检验检疫局检验检疫综合技术中心 | The analysis method of fragrance component in a kind of brackish water rose water |
CN110419765A (en) * | 2019-08-12 | 2019-11-08 | 四川三联新材料有限公司 | A kind of preparation method and preparation facilities of electronic cigarette tobacco tar |
CN112760170A (en) * | 2021-01-19 | 2021-05-07 | 中华全国供销合作总社南京野生植物综合利用研究所 | Plant essential oil hot air circulation distillation technology |
CN113214899A (en) * | 2021-03-31 | 2021-08-06 | 广西壮族自治区农业科学院 | Wao gan essential oil extraction element |
CN113214899B (en) * | 2021-03-31 | 2022-12-16 | 广西壮族自治区农业科学院 | Wa mandarin orange essential oil extraction device |
CN113088399A (en) * | 2021-04-13 | 2021-07-09 | 康荍生物技术(上海)有限公司 | Method for extracting aroma substances from aromatic plants |
CN115068974A (en) * | 2022-05-16 | 2022-09-20 | 深圳昱朋科技有限公司 | Preparation method of plant spice |
CN115068974B (en) * | 2022-05-16 | 2024-03-26 | 深圳昱朋科技有限公司 | Preparation method of plant spice |
Also Published As
Publication number | Publication date |
---|---|
CN101117614B (en) | 2010-12-08 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101117614B (en) | Method for extracting fragrant liquor and essential oil from aromatic plants by dry-process | |
CN202359093U (en) | Plant essential oil extraction device | |
CN103923748B (en) | A kind of volatile oil extracts collects separation equipment | |
CN204400945U (en) | A kind of essential oil extraction device | |
CN105001992A (en) | Small essential oil and hydrolat extraction equipment which can be assembled quickly with clamps | |
CN207685229U (en) | A kind of alembic and volatile oil extractor | |
CN106349015A (en) | Method for extracting high-purity natural borneol with multistage condensation and loop distillation | |
CN105126383B (en) | The integrated extraction concentration technique of the energy-efficient automation of Chinese medicine and technological equipment | |
CN209123397U (en) | A kind of ginger zingiberol circulation extracting apparatus | |
CN103585783B (en) | Honeysuckle extraction is steamed extraction element and method | |
CN204364938U (en) | The ultrasonic centrifugal extraction of a kind of Wave wheel type full automatic, concentrated and solvent reclaimer | |
CN108130187B (en) | Device and process for producing balsam by cyclic absorption | |
CN102260314A (en) | Betulin extraction method and device thereof | |
CN208500885U (en) | A kind of natural plant essential oils vacuum distillation apparatus | |
CN101508710A (en) | Dynamic counterflow extraction apparatus for soapberry saponin and producing process thereof | |
CN208485823U (en) | A kind of combination unit for realizing azeotropic rectifying continuous operation | |
CN204737937U (en) | Functional vegetable oil extraction element has | |
CN207726911U (en) | A kind of shale gas exploitation fracturing fluid cycle tubulation evaporation minimizing processing equipment | |
CN213506812U (en) | Integrated extraction element of high concentration essential oil | |
CN2643967Y (en) | Distilling device of flower essential oil | |
CN209974711U (en) | Spices draws enrichment facility | |
CN207537416U (en) | A kind of natural perfume material equipment for purifying | |
CN216786074U (en) | Fragrant smell gas collection system of spices | |
CN206814418U (en) | A kind of sludge protein liquid odor removal | |
CN204079946U (en) | Combined type solid-state water distilling apparatus |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20101208 Termination date: 20160830 |
|
CF01 | Termination of patent right due to non-payment of annual fee |