CN109135400A - The application of red sorghum pigment, water stain and preparation method thereof and aqueous woodware paint - Google Patents
The application of red sorghum pigment, water stain and preparation method thereof and aqueous woodware paint Download PDFInfo
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- CN109135400A CN109135400A CN201810866198.XA CN201810866198A CN109135400A CN 109135400 A CN109135400 A CN 109135400A CN 201810866198 A CN201810866198 A CN 201810866198A CN 109135400 A CN109135400 A CN 109135400A
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- water stain
- water
- red sorghum
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- sorghum pigment
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/10—Transparent films; Clear coatings; Transparent materials
Abstract
The present invention relates to a kind of application of red sorghum pigment, water stain and preparation method thereof and aqueous woodware paints.Wherein, by weight, the water stain includes following raw material components: 10~45 parts of red sorghum pigment, 20~51 parts of water, 0.1~1 part of preservative, 0.5~1 part of form and aspect stabilizer, 0.1~2 part of viscosity stabiliser;The pH value of the water stain is 7~10.Not only color developing is good in water-base resin for the water stain, and the pH value range of the neutral meta-alkali of the most stable of coloring pH value range of form and aspect and water-base resin of red sorghum pigment matches, colorability is strong, paint film color is fresh, bright, saturating after being coloured with the colorant, it is fast light, heat-resisting, chemical resistance is good, it is nontoxic, the coloring effect of premetallized dye can be reached, and can environmental protection to avoid premetallized dye bring heavy metal ion and organic volatile, safety problem.
Description
Technical field
The present invention relates to technical field of aqueous paint, more particularly to the application of red sorghum pigment, water stain and its
Preparation method and aqueous woodware paint.
Background technique
Transparent woodcare paint is used to reveal the decoration of wood grain, required for further beautifying while holding timber original color
Color.Woodstain is a kind of colorant, a kind of solution of the coloring material of woodstain formed in color spreading agent
Or suspension, for revealing the decoration of wood grain, color required for further beautifying while holding timber original color.
The red transparent woodcare paint of series is the leading paint of medium-to-high grade wood furniture, and solvent type red premetallized dye is
The important illuminating colour and important component of red, transparent woodcare paint.Solvent type red, transparent woodcare paint passes through solvent type red metal
Complex dyestuff coloring, gained color is fresh, bright, saturating, imparts the dicoration that red wood furniture is penetrating, bright and beautiful, makes
The color most liked by user in wood furniture.But solvent type red premetallized dye is mainly by azo ligand
It is complexed with metallic atoms such as chromium (Cr), cobalt (Co), copper (Cu) and nickel (Ni), and solvent type red premetallized dye exists
It could be dissolved in organic solvent, heavy metal and a free huge sum of money can be brought using the solvent type woodcare paint containing the premetallized dye
Belong to the safe and environment-friendly hidden danger that ion is retained and organic volatile (VOC) is discharged.
With the execution of woodcare paint safety and environmental protection standard, woodcare paint has become woodenware by solvent type hydrotropism development and applies
Expect the only way which must be passed of industry.Since dissolubility of the premetallized dye in the aqueous woodware paint taken water as a solvent is bad, with water
Property resin poor compatibility, premetallized dye is easily precipitated, and coloring is difficult or even not colored, cannot play the dyeing effect of dyestuff;
Simultaneously because indissoluble or insoluble with water-base resin poor compatibility it is saturating to will lead to aqueous woodware paint to premetallized dye in water
Lightness reduces, gloss of film reduces, and influences paint film property.Moreover, the chemical dye of aqueous red, transparent coating can be used at present
Almost without therefore, developing a kind of new red colored dyestuff for being able to satisfy aqueous clear coating technical requirements, be aqueous red
Transparent woodcare paint develops the problem of urgent need to resolve.
Summary of the invention
Based on this, it is necessary to provide a kind of red sorghum pigment and be applied to prepare the colorant of aqueous woodware paint, coloring is saturating
Lightness is good, color just, it is tinting strength, tinting power, fast light heat-resist, can satisfy aqueous woodware paint to the technical requirements of colorant.
Phytochrome Nantural non-toxic, it is highly-safe, food, drug and cosmetics are applied to frequently as coloring additive
In.But phytochrome is many kinds of, property is complicated, for a kind of phytochrome, specificity is stronger when application, using model
Be with certain limitation, and most of phytochrome light, heat, oxygen, metal ion and pH value are changed it is sensitive, stability compared with
Difference, and have the shortcomings that tinting strength, tinting power is poor, it is bright to dye the floridity being not easy uniformly, without synthetic dyestuff, therefore, how a large amount of
Phytochrome in find a kind of phytochrome that can be suitable for aqueous woodware paint and become key.
A kind of application of red sorghum pigment, the red sorghum pigment are applied to prepare the colorant of aqueous woodware paint.
Red sorghum pigment (Sorghum red pigment, SRP) is the phytochrome extracted from sorghum husk, belongs to Huang
Ketone compounds have very strong antioxidant activity containing multiple phenolic hydroxyl groups, are a kind of safe and nontoxic natural pigments, commonly use
Make foods and cosmetics additive;The main component of red sorghum pigment be 5,4 ' dihydroxy isoflavone -7-O- galactosides and 5,
4 ' dihydroxy isoflavone -6,8- dimethyl -7-O- galactosides, molecular structure are as follows:
Red sorghum pigment is dissolved in water, and tone changes with pH value and changed, in acid condition red sorghum pigment color
Pool is shallower, and transparency is good in neutral conditions, and bright-colored, color deepens under alkaline condition, and as pH increases, color is by shallowly becoming
To peony, and stable red is presented in the range of pH value 6~10;And the resin system of aqueous woodware paint is in neutrality or
Meta-alkalescence, pH value range are precisely the coloring pH value range that red color phase is the most stable in red sorghum pigment tone, therefore, are used
Red sorghum pigment makees the colorant of aqueous woodware paint, good with its resin miscible, film after strong coloring force, bright-colored, coloring
Transparency is good, color is penetrating after film curing, the coloring effect of solvent type premetallized dye can be reached, meet aqueous wooden ware
Paint the technical parameter requirement to colorant;And red sorghum pigment is fast light, heat-resist, stable chemical performance, nontoxic, safety,
Colorant as aqueous woodware paint is able to satisfy environmental requirement.
Another object of the present invention is to provide a kind of water stain, by weight, including following raw material components: sorghum
10~45 parts of haematochrome, 20~51 parts of water, 0.1~1 part of preservative, 0.5~1 part of form and aspect stabilizer and viscosity stabiliser 0.1~2
Part.
Above-mentioned water stain takes water as a solvent, natural plant dye red sorghum pigment is illuminating colour, in preservative, color
Under the collective effect of phase stabiliser and viscosity stabiliser, fast light, heat-resist, the good feature of chemical stability is made it have.It should
Water stain is not only good with water-base resin compatibility, and the color developing in water-base resin is good, and the form and aspect of red sorghum pigment
The pH value range of most stable of coloring pH value range and the neutral meta-alkali of water-base resin matches, and colorability is strong.With the coloring
Paint film color is fresh, bright, saturating after agent is coloured, fast light, heat-resisting, chemical resistance is good, nontoxic, can reach metal complex dye
The coloring effect of material, and can be asked to avoid the environmental protection of premetallized dye bring heavy metal ion and organic volatile, safety
Topic.
In one of the embodiments, the viscosity stabiliser be in hydroxyethyl cellulose and carboxymethyl cellulose at least
It is a kind of.
It is appreciated that viscosity stabiliser hydroxyethyl cellulose and hydroxymethyl cellulose not only can provide conjunction for water stain
Suitable viscosity, and their antibiont degradabilities are good, and the stability of product can be improved.
In one of the embodiments, the form and aspect stabilizer in sodium bicarbonate, sodium carbonate and sodium citrate extremely
Few one kind.In this way, stable, optimal coloring pH range can be provided for red sorghum pigment, and the stability of colorant is high.
In one of the embodiments, the preservative in sodium benzoate and methyl p-hydroxybenzoate at least one
Kind.
It is appreciated that sodium benzoate and methyl p-hydroxybenzoate are in the stable pH value range of the form and aspect of red sorghum pigment
Favorable anti-corrosion effect, in this way, water stain can be effectively prevent smelly, it is mouldy, go bad.
The red sorghum pigment is 20~30 parts in one of the embodiments, and the preservative is 0.2~0.6 part, institute
Stating form and aspect stabilizer is 0.5~0.8 part, and the viscosity stabiliser is 1~2 part.
The pH value of the water stain is 8.0~8.5 in one of the embodiments,.It is appreciated that in the pH value model
In enclosing, the form and aspect of water stain are red the most stable, and the color most liked by user in medium-to-high grade wood furniture.
Another object of the present invention is to provide a kind of preparation method of above-mentioned water stain, comprising the following steps:
The red sorghum pigment is dissolved in the water, the preservative, the form and aspect stabilizer and institute is then added
Viscosity stabiliser is stated, is uniformly mixed, obtains the water stain.
Above-mentioned preparation method simple process, it is easy to operate, it is suitable for industrialized production, is prepared by this method aqueous
- 4 glasss of viscosity of painting of colorant are 60 seconds~80 seconds, it is ensured that the uniform and stable property of water stain is prevented in transporting procedures
In there is micro red sorghum pigment to be precipitated to generate precipitating, to influence the colorability of water stain, gained water stain is equal
Even stabilization is free of organic solvent and heavy metal ion, and component used meets the safe and environment-friendly requirement of water paint, and fast light, resistance to
Heat, chemical resistance are good.
Based on above-mentioned water stain, another object of the present invention is to provide a kind of aqueous woodware paint, the aqueous wooden ware
The raw material of paint includes above-mentioned water stain.
Further, the aqueous woodware paint includes following raw material components:
It should be noted that water-base resin is the resin system using water instead of organic solvent as decentralized medium, admittedly contain
Amount generally 30%~50%.
Above-mentioned aqueous woodware paint using the red sorghum pigment good with water-base resin system compatibility as colorant, stablize by form and aspect,
The transparency of film is good after coloring, bright-colored, bright after film curing, and resistance to mild light resistance is good, can reach solvent type woodenware
The effect of paint, and have the characteristics that water paint is nontoxic, safe and environment-friendly.
Specific embodiment
To facilitate the understanding of the present invention, below will to invention is more fully described, and give it is of the invention compared with
Good embodiment.But the invention can be realized in many different forms, however it is not limited to embodiment described herein.Phase
Instead, purpose of providing these embodiments is makes the disclosure of the present invention more thorough and comprehensive.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein "and/or" includes one or more phases
Any and all combinations of the listed item of pass.
Red sorghum pigment used in the embodiment of the present invention is purchased from Keguang Natural Pigment Co., Ltd, Liaoning, other raw materials are general
Lead to commercially available.
Embodiment 1
A kind of formula of water stain: red sorghum pigment 10g, deionized water 50g, sodium benzoate 0.5g, sodium bicarbonate
0.5g, hydroxyethyl cellulose 0.5g.
The preparation method of water stain:
(1) each component is accurately weighed according to above-mentioned formula;
(2) red sorghum pigment is dissolved in 50 DEG C of deionized waters, stirs, after completely dissolution, sequentially adds sodium benzoate, carbon
Sour hydrogen sodium and hydroxyethyl cellulose, are sufficiently stirred, and mix.
It is 8.1 with the pH value that pH meter detects above-mentioned water stain, applying 4 glasss of measurement viscosity is 68 seconds.
Embodiment 2
A kind of formula of water stain: red sorghum pigment 40g, deionized water 50g, sodium benzoate 1g, sodium bicarbonate 1g,
Hydroxyethyl cellulose 2g.
The preparation method of water stain:
(1) each component is accurately weighed according to above-mentioned formula;
(2) red sorghum pigment is dissolved in 50 DEG C of deionized waters, stirs, after completely dissolution, sequentially adds sodium benzoate, carbon
Sour hydrogen sodium and hydroxyethyl cellulose, are sufficiently stirred, and mix.
It is 8.5 with the pH value that pH meter detects above-mentioned water stain, applying 4 glasss of measurement viscosity is 80 seconds.
Embodiment 3
A kind of formula of water stain: red sorghum pigment 25g, deionized water 45g, methyl p-hydroxybenzoate 0.5g,
Sodium citrate 0.7g, carboxymethyl cellulose 1.2g.
The preparation method of water stain:
(1) each component is accurately weighed according to above-mentioned formula;
(2) red sorghum pigment is dissolved in 50 DEG C of deionized waters, stirs, after completely dissolution, sequentially adds para hydroxybenzene first
Sour methyl esters, sodium citrate and carboxymethyl cellulose, are sufficiently stirred, and mix.
It is 8.3 with the pH value that pH meter detects above-mentioned water stain, applying 4 glasss of measurement viscosity is 75 seconds.
Embodiment 4
A kind of formula of water stain: red sorghum pigment 20g, deionized water 20g, methyl p-hydroxybenzoate 0.2g,
Sodium citrate 0.5g, carboxymethyl cellulose 1g.
The preparation method of water stain:
(1) each component is accurately weighed according to above-mentioned formula;
(2) red sorghum pigment is dissolved in 50 DEG C of deionized waters, stirs, after completely dissolution, sequentially adds para hydroxybenzene first
Sour methyl esters, sodium citrate and carboxymethyl cellulose, are sufficiently stirred, and mix.
It is 8.0 with the pH value that pH meter detects above-mentioned water stain, applying 4 glasss of measurement viscosity is 70 seconds.
Embodiment 5
By weight percentage, the formula of aqueous woodware paint is as follows:
The water stain that above-described embodiment 1~4 is respectively adopted is used as the colorant of aqueous red, transparent woodcare paint, accordingly
Obtain 4 kinds of aqueous woodware paints
Comparative example 1
Comparative example 1 is the aqueous transparent woodcare paint of bauhinia alcohol solube metallic complex dyestuff 698-41 preparation, specific formula
It is as follows:
Embodiment 6
It is red to the aqueous transparent of 4 kinds of woodcare paints and the preparation of 1 alcohol solube metallic complex dyestuff of comparative example in embodiment 5
Woodcare paint carries out tinting strength, tinting power, light resistance, heat resistance experiment, and is compared to tinting strength, tinting power, resistance to pass, heat resistance.
1, tinting strength, tinting power is tested
Test method: by 4 kinds of aqueous transparent red woodcare paints of embodiment 5 and with the woodcare paint of comparative example 1 with 40 μm
Bar applies bar point or so and is coated in same art post paperboard, and the color and form and aspect of two films are observed after dried coating film.
As a result:
The results show that left and right film color depth is suitable in art post paperboard, form and aspect alcohol-soluble complex dyestuff has partially yellow for observation
Phase is basically unchanged using 4 kinds of woodcare paint film colors in the embodiment 5 of red sorghum pigment colorant, is shown using the present invention
4 kinds of woodcare paint tinting strength, tinting powers of the colorant of Examples 1 to 4 are good.
2, light fastness test
Test method:
Aqueous red, transparent woodenware prepared by 4 kinds of woodcare paints of embodiment 5 and 1 alcohol solube metallic complex dyestuff of comparative example
Coating is sprayed on the experiment plank of six block size 200mm × 150mm (every square metre of 90 grams of coating dosage) respectively.Room temperature
After (30 DEG C) dryings, is kept away at 1/2 with lighttight black paper jam envelope, be placed under sunlight after shining 30 days and open black paper jam, observation envelope is kept away
Part or expose portion color change situation, and color change size is evaluated.
As a result: 4 kinds of aqueous woodware paints in embodiment 5, by solar radiation 30 days, color was substantially unchanged, said
Bright light resistance is good.
3, heat-resistance test
Heat-resistant experiment experimental method: 4 kinds of embodiment 5 aqueous red, transparent woodwork coatings are sprayed on six block sizes
On the experiment plank of 200mm × 150mm (every square metre of 90 grams of coating dosage).After room temperature (30 DEG C) is done solid work, four pieces of plate are set
In the baking oven of temperature 50 C, takes out within every 5 days one piece and the template of non-entering to dry case compares, observe color change situation, observe feelings
Condition see the table below:
As a result: 4 kinds of woodcare paints of embodiment 5 were tested through 50 DEG C of baking oven, 20 days, and color is tested through 50 DEG C of heatproof, color
It is unchanged, meet heat resistant requirements.
Conclusion: carrying out film using 4 kinds of aqueous woodware paints in embodiment 5, and the color after paint film is dry takes on a red color, and
Transparency is good, and color is just, suitable with the effect of solvent type red, transparent woodcare paint of comparative example 1;By fast light and heat resistant test
It proves, 4 kinds of aqueous woodware paints of the embodiment of the present invention 5 are fast light and heat resistance reaches the technical requirements of woodcare paint, and explanation is adopted
The woodcare paint tinting strength, tinting power for using the water stain of the embodiment of the present invention 1~4 as colorant is good, and coloring effect can reach solvent type
The effect of red, transparent woodcare paint can satisfy the skill of aqueous red, transparent woodcare paint using red sorghum pigment as colorant dye
Art requirement.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (10)
1. a kind of application of red sorghum pigment, which is characterized in that the red sorghum pigment be applied to prepare aqueous woodware paint
Toner.
2. a kind of water stain, which is characterized in that by weight, including following raw material components:
3. water stain according to claim 2, which is characterized in that the viscosity stabiliser be hydroxyethyl cellulose and
At least one of carboxymethyl cellulose.
4. water stain according to claim 2, which is characterized in that the form and aspect stabilizer is selected from sodium bicarbonate, carbon
At least one of sour sodium and sodium citrate.
5. water stain according to claim 2, which is characterized in that the preservative is selected from sodium benzoate and to hydroxyl
At least one of methyl benzoate.
6. according to any water stain of claim 2~5, which is characterized in that the red sorghum pigment is 20~30
Part, the preservative is 0.2~0.6 part, and the form and aspect stabilizer is 0.5~0.8 part, and the viscosity stabiliser is 1~2 part.
7. water stain according to claim 6, which is characterized in that the pH value of the water stain be 8.0~
8.5。
8. a kind of preparation method of the water stain as described in claim 2~7 is any, which is characterized in that including following step
It is rapid:
The red sorghum pigment is dissolved in the water, the preservative, the form and aspect stabilizer and described viscous is then added
Stabilizer is spent, is uniformly mixed, obtains the water stain.
9. a kind of aqueous woodware paint, which is characterized in that the raw material of the aqueous woodware paint includes such as any institute of claim 3~8
The water stain stated.
10. aqueous woodware paint according to claim 9, which is characterized in that the aqueous woodware paint includes following raw material group
Point:
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Application publication date: 20190104 |